阅读说明：本技术 一种粗、精双分子筛医用制氧装置 (Medical oxygen generating device with coarse and fine molecular sieves ) 是由 罗治雯 汤新 杨宣进 徐勇 章雪丰 宋卫海 殷雅兵 于 2020-08-14 设计创作，主要内容包括：本发明公开了一种粗、精双分子筛医用制氧装置,包括一组制氧机构、氧气贮罐和反向吹扫装置,所述制氧机构通过供气管与左侧的用于提供压缩空气的供气装置连通,且供气管上从左到右依次设有第一控制阀和第一放空阀,所述制氧机构通过氧气管与氧气贮罐连通,且氧气管上设有第二控制阀,所述氧气贮罐上设有氧气输送管路,所述制氧机构的右端通过吹扫管路与反向吹扫装置连通。本发明中,采用增加精筛工艺使制氧浓度更高,符我国所有医用氧制备要求,达到中国药典规定用氧纯度值,且在现有的单级沸石分子筛工艺基础上增加了一级碳分子筛,沿长了工艺线路,从而使本装置呈现出粗筛精筛异型双筛工艺。(The invention discloses a medical oxygen generating device with a coarse molecular sieve and a fine molecular sieve, which comprises a group of oxygen generating mechanisms, an oxygen storage tank and a reverse purging device, wherein the oxygen generating mechanisms are communicated with a left air supply device used for providing compressed air through an air supply pipe, a first control valve and a first emptying valve are sequentially arranged on the air supply pipe from left to right, the oxygen generating mechanisms are communicated with the oxygen storage tank through an oxygen pipe, a second control valve is arranged on the oxygen pipe, an oxygen conveying pipeline is arranged on the oxygen storage tank, and the right end of the oxygen generating mechanisms is communicated with the reverse purging device through a purging pipeline. In the invention, the concentration of oxygen generation is higher by adopting the fine screening process, the oxygen generation concentration meets all the requirements of medical oxygen preparation in China, the oxygen purity value specified in Chinese pharmacopoeia is reached, and the primary carbon molecular sieve is added on the basis of the existing single-stage zeolite molecular sieve process, and the process line is lengthened, so that the device presents a coarse-screening fine-screening special-shaped double-sieve process.)

1. The utility model provides a medical oxygenerator of thick, smart double molecular sieve, includes that a set of oxygenerator constructs (1), oxygen storage tank (2) and reverse purging device (3), its characterized in that: oxygen generation mechanism (1) is used for providing compressed air's air feeder intercommunication through air supply pipe (4) and left, and from left to right is equipped with first control valve (5) and first atmospheric valve (6) in proper order on air supply pipe (4), oxygen generation mechanism (1) is through oxygen accumulation pipe (7) and oxygen basin (2) intercommunication, and is equipped with second control valve (8) on oxygen pipe (7), be equipped with oxygen conveying pipeline (9) on oxygen basin (2), the right-hand member of oxygen generation mechanism (1) is through sweeping pipeline (10) and reverse device (3) intercommunication that sweeps.

2. The medical oxygen generation device with the coarse and fine molecular sieves as claimed in claim 1, wherein: the reverse blowing device (3) is a blower (31) or an overstock tank (32).

3. The medical oxygen generation device with the coarse and fine molecular sieves as claimed in claim 2, wherein: when the reverse purging device (3) is the blower (31), the purging pipeline (10) comprises a first purging pipe (1001), and a third control valve (1002) and a second emptying valve (1003) are arranged on the first purging pipe (1001).

4. The medical oxygen generation device with the coarse and fine molecular sieves as claimed in claim 2, wherein: when the reverse purging device (3) is an overstock tank (32), the purging pipeline (10) comprises a second purging pipe (1004), a fourth control valve (1005) is arranged on the second purging pipe (1004), an exhaust pipe (1006) is arranged on the other side of the overstock tank (32), and a pressure limiting valve (1007) is arranged on the exhaust pipe (1006).

5. The medical oxygen generation device with the coarse and fine molecular sieves as claimed in claim 1, wherein: oxygen mechanism (1) can set up two sets ofly side by side, and is equipped with equalizer tube (11) between air supply pipe (4) of two sets of oxygen mechanisms (1), be equipped with equalizer valve (12) on equalizer tube (11), and two sets of oxygen mechanisms (1) all communicate with oxygen storage tank (2) through oxygen hose (7).

6. The crude and fine bimolecular sieve medical oxygen generation device according to claim 3 or 5, wherein: the blower (31) is respectively communicated with the oxygen generation mechanisms (1) of the corresponding group through first purging pipes (1001), and each first purging pipe (1001) is provided with a third control valve (1002) and a second emptying valve (1003).

7. The crude and fine bimolecular sieve medical oxygen generation device according to claim 4 or 5, wherein: the overstock tank (32) is communicated with the oxygen generation mechanism (1) of the corresponding group through a second purging pipe (1004), and a fourth control valve (1005) is arranged on the second purging pipe (1004).

8. The medical oxygen generation device with the coarse and fine molecular sieves as claimed in any one of claims 1 to 5, wherein: oxygen making mechanism (1) includes zeolite molecular sieve tower (101) and carbon molecular sieve tower (102), zeolite molecular sieve tower (101) and carbon molecular sieve tower (102) are through first pipeline (103) intercommunication, oxygen pipe (7) and the middle part intercommunication of first pipeline (103), and the both sides that lie in oxygen pipe (7) and first pipeline (103) junction on first pipeline (103) all are equipped with fifth control valve (104), air supply pipe (4) and zeolite molecular sieve tower (101) intercommunication, carbon molecular sieve tower (102) are through sweeping pipeline (10) and reverse device (3) intercommunication that sweeps.

9. The medical oxygen generation device with the coarse and fine molecular sieves as claimed in claim 8, wherein: the molecular sieve in the carbon molecular sieve tower (102) is a modified carbon molecular sieve, and the diameter range of micropores is 0.28nm-0.35 nm.

Technical Field

The invention relates to the field of oxygen generation devices, in particular to a medical oxygen generation device with a coarse molecular sieve and a fine molecular sieve.

Background

The medical oxygen generator uses zeolite molecular sieve as adsorbent and uses pressure-swing adsorption method (PSA method for short) to prepare medical oxygen, and said oxygen generator uses air as raw material to separate oxygen (about 21%) and nitrogen (about 78%) from air to obtain oxygen-enriched gas whose concentration is 90% -93% for medical use. However, the popularization and application are slow due to the fact that each region has a difference in understanding whether the oxygen concentration meets the medical oxygen and national regulations (the oxygen concentration is greater than 99.5% specified by Chinese pharmacopoeia).

Disclosure of Invention

The invention aims to provide a medical oxygen generating device with a coarse molecular sieve and a fine molecular sieve, which aims to solve the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme:

the utility model provides a medical oxygenerator of thick, smart double molecular sieve, includes that a set of oxygenerator constructs, oxygen stock tank and reverse purging device, oxygenerator constructs the air feeder intercommunication that is used for providing compressed air through air supply pipe and left, and from left to right is equipped with first control valve and first atmospheric valve in proper order on the air supply pipe, oxygenerator constructs through oxygen hose and oxygen stock tank intercommunication, and is equipped with the second control valve on the oxygen hose, be equipped with oxygen conveying pipeline on the oxygen stock tank, the right-hand member of oxygenerator constructs through purging pipeline and reverse purging device intercommunication.

Further, the reverse purging device is a blower or an accumulator tank.

Further, when the reverse purging device is an air blower, the purging pipeline comprises a first purging pipe, and a third control valve and a second emptying valve are arranged on the first purging pipe.

Furthermore, when the reverse purging device is an overstock tank, the purging pipeline comprises a second purging pipe, a fourth control valve is arranged on the second purging pipe, an exhaust pipe is arranged on the other side of the overstock tank, and a pressure limiting valve is arranged on the exhaust pipe.

Further, the system oxygen mechanism can set up two sets side by side, and is equipped with the equalizer tube between the air supply pipe of two sets of system oxygen mechanisms, be equipped with the equalizer valve on the equalizer tube, and two sets of system oxygen mechanisms all communicate with the oxygen storage tank through the oxygen hose.

Furthermore, the air blower is respectively communicated with the oxygen generation mechanisms of the corresponding groups through the first blowing pipes, and each first blowing pipe is provided with a third control valve and a second emptying valve.

Furthermore, the overstock tank is communicated with the oxygen generation mechanism corresponding to the group through a second purging pipe, and a fourth control valve is arranged on the second purging pipe.

Further, system oxygen mechanism includes zeolite molecular sieve tower and carbon molecular sieve tower, zeolite molecular sieve tower and carbon molecular sieve tower are through first pipeline intercommunication, the middle part intercommunication of oxygen hose and first pipeline, and the both sides that lie in oxygen hose and first pipeline junction on the first pipeline all are equipped with the fifth control valve, air supply pipe and zeolite molecular sieve tower intercommunication, the carbon molecular sieve tower is through sweeping pipeline and reverse device intercommunication that sweeps.

Furthermore, the molecular sieve in the carbon molecular sieve tower is a modified carbon molecular sieve, and the diameter range of the micropores is 0.28nm-0.35 nm.

Compared with the prior art, the invention has the beneficial effects that:

in the invention, the concentration of oxygen generation is higher by adopting the fine screening process, meets the requirements of all medical oxygen preparation standards in China and exceeds the oxygen purity standard specified in Chinese pharmacopoeia.

The carbon molecular sieve is added on the basis of the existing single-stage zeolite molecular sieve process, and the process line is lengthened, so that the device presents a coarse-sieve fine-sieve special-shaped double-sieve process.

The reverse purging device at the tail end of the process line can adopt a blower or an overstocking tank, so that the reverse purging is performed on the two-stage molecular sieve during pressure reduction and desorption, and the regeneration of the molecular sieve is facilitated.

Two groups of oxygen generation mechanisms are used in parallel and alternately, so that continuous oxygen generation is realized, and the oxygen generation capacity is improved.

Drawings

FIG. 1 is a flow chart of a medical oxygen generation device with a coarse and fine molecular sieve;

FIG. 2 is a flow chart of a crude and fine molecular sieve medical oxygen generator in which oxygen generation mechanisms are arranged in parallel and a reverse purging device is a blower;

FIG. 3 is a flow chart of oxygen generation mechanisms in parallel arrangement and a back purging device which is a pressure tank in a coarse and fine double molecular sieve medical oxygen generation device.

In the figure: 1. an oxygen generation mechanism; 101. a zeolite molecular sieve column; 102. a carbon molecular sieve column; 103. a first conduit; 104. a fifth control valve; 2. an oxygen storage tank; 3. a reverse purging device; 31. a blower; 32. accumulating the tank; 4. a gas supply pipe; 5. a first control valve; 6. a first vent valve; 7. an oxygen tube; 8. a second control valve; 9. an oxygen delivery line; 10. purging the pipeline; 1001. a first purge tube; 1002. a third control valve; 1003. a second vent valve; 1004. a second purge tube; 1005. a fourth control valve; 1006. an exhaust pipe; 1007. a pressure limiting valve; 11. a pressure equalizing pipe; 12. and a pressure equalizing valve.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1, the present invention provides a technical solution:

the utility model provides a thick, medical oxygenerator of smart double molecular sieve, including a set of oxygenerator 1, oxygen stock tank 2 and reverse purging device 3, oxygenerator 1 communicates through air supply pipe 4 and left air feeder that is used for providing compressed air, and from left to right be equipped with first control valve 5 and first atmospheric valve 6 in proper order on the air supply pipe 4, oxygenerator 1 passes through oxygen hose 7 and 2 intercommunications of oxygen stock tank, and be equipped with second control valve 8 on the oxygen hose 7, be equipped with oxygen conveying pipeline 9 on the oxygen stock tank 2, the right-hand member of oxygenerator 1 is through purging pipeline 10 and reverse purging device 3 intercommunication.

The reverse purging device 3 is a blower 31 or an overstock tank 32 and is used for performing reverse purging on the two-stage molecular sieve during pressure reduction and desorption so as to facilitate the regeneration of the molecular sieve.

When the reverse purging device 3 is the blower 31, the purging pipeline 10 includes a first purging pipe 1001, and a third control valve 1002 and a second venting valve 1003 are disposed on the first purging pipe 1001.

When the reverse purging device 3 is the surge tank 32, the purging pipeline 10 comprises a second purging pipe 1004, a fourth control valve 1005 is arranged on the second purging pipe 1004, an exhaust pipe 1006 is arranged on the other side of the surge tank 32, a pressure limiting valve 1007 is arranged on the exhaust pipe 1006, and when the pressure of the surge tank 32 exceeds the pressure limiting value of the pressure limiting valve 1007, the excessive part can be discharged.

In the adsorption stage, the oxygen generation mechanism 1 stores nitrogen and oxygen, other gases pass through the molecular sieve and are discharged, and pressure equalization and oxygen collection are carried out after adsorption is completed.

Pressure equalizing and oxygen collecting:

when only one group of oxygen generating mechanism 1 is provided and the reverse purging device 3 is the blower 31, the gas supply pipe 4 stops supplying gas, the first control valve 5 is closed, the adsorption pressurization is stopped at the moment, the higher pressure is accumulated in the oxygen generating mechanism 1, the first emptying valve 6 is opened at the moment, the second control valve 8 is opened, the interior of the oxygen generating mechanism 1 is disconnected, oxygen is adsorbed in the micropores of the carbon molecular sieve under the action of pressure, and gases such as argon and the like can pass through the molecular sieve and are discharged through the second emptying valve 1003, so that the oxygen is separated out after the pressure is reduced and is sent to the oxygen storage tank 2 through the oxygen pipe 7; after waiting pressure balance, close second control valve 8 to make the inside intercommunication of oxygenerator 1, start air-blower 31 and carry out reverse purge, adsorb in the inert gas such as nitrogen gas, argon in oxygenerator 1 through first atmospheric valve 6 after the discharge, can carry out the preparation of oxygen once more.

When only one group of oxygen generating mechanism 1 is arranged and the reverse purging device 3 is the pressure accumulation tank 32, the air supply pipe 4 stops supplying air, the first control valve 5 is closed, the adsorption pressurization is stopped at the moment, the higher pressure is accumulated in the oxygen generating mechanism 1 at the moment, the first emptying valve 6 is opened, the second control valve 8 is opened, the inside of the oxygen generating mechanism 1 is disconnected, oxygen is separated out along with the pressure reduction, and the oxygen is sent into the oxygen storage tank 2 through the oxygen pipe 7 to finish the collection of the oxygen; after waiting pressure balance, close second control valve 8, open fourth control valve 1005 to make the inside intercommunication of oxygenerator 1, because the existence of pressure limiting valve 1007, so there is higher atmospheric pressure inside the overstock jar 32, after fourth control valve 1005 opened, inside air current flows to oxygenerator 1 from the overstock jar 32, reverse purging carries out, nitrogen gas that adsorbs in oxygenerator 1 discharges through first atmospheric valve 6, oxygen passes through the oxygen pipe flow and enters the oxygen storage tank, accomplish the preparation of oxygen promptly and wait for next cycle.

Referring to fig. 2-3, in another embodiment, two oxygen generation mechanisms 1 can be arranged in parallel, and a pressure equalizing pipe 11 is arranged between the air supply pipes 4 of the two oxygen generation mechanisms 1, a pressure equalizing valve 12 is arranged on the pressure equalizing pipe 11, and the two oxygen generation mechanisms 1 are both communicated with the oxygen storage tank 2 through the oxygen pipe 7.

The pressure equalizing and oxygen receiving steps at this time are as follows:

when two groups of oxygen generating mechanisms 1 are arranged in parallel and the reverse blowing device 3 is a blower 31, the air supply pipe 4 stops supplying air, the first control valve 5 which is arranged on the upper group is closed firstly, at the moment, the adsorption pressurization stops, higher pressure is accumulated in the oxygen generating mechanism 1, the pressure equalizing valve 12 and the second control valve 8 are opened, the pressure inside the oxygen generating mechanism 1 which is arranged in parallel up and down is balanced, oxygen is led into the oxygen storage tank 2, the pressure balance is realized, after the pressure equalization is finished, the second control valve 8 is closed, the first emptying valve 6 is opened, air is blown through the blower 31, the oxygen generating mechanism 1 which is arranged on the upper group is reversely pressurized, the reverse blowing is realized, and therefore inert gases such as nitrogen, argon and the like which are adsorbed on molecular sieves in the zeolite molecular sieve tower 101 and the carbon molecular sieve tower 102 on the upper group are discharged through the first emptying valve 6, and the mechanism 1 which is arranged on the lower group continuously supplies air, after the oxygen generation mechanism 1 of the upper group completes the reverse purging, the air supply pipe 4 of the oxygen generation mechanism 1 of the lower group stops supplying air, and the steps are repeated.

Similarly, when two sets of oxygen generating mechanisms 1 are arranged in parallel, and the reverse purging device 3 is the pressure accumulation tank 32, the internal pressure balance mode of the oxygen generating mechanisms 1 is the same, only when the reverse purging is performed, the corresponding fourth control valve 1005 and the first emptying valve 6 are opened, due to the existence of the pressure limiting valve 1007, the internal pressure of the pressure accumulation tank 32 is larger, after the fourth control valve 1005 is opened, the corresponding oxygen generating mechanisms 1 can be reversely pressurized, the reverse purging is realized, and therefore inert gases such as nitrogen and argon adsorbed on the molecular sieves in the zeolite molecular sieve tower 101 and the carbon molecular sieve tower 102 above are discharged through the first emptying valve 6, and oxygen is collected in the oxygen storage tank. Meanwhile, the other group of oxygen generating mechanisms 1 continuously supply air, the molecular sieve is used for carrying out the adsorption process of nitrogen, oxygen and argon, after the last group of oxygen generating mechanisms 1 finishes reverse purging, the air supply pipe 4 of the group stops supplying air, and the steps of pressure equalizing and reverse purging are repeated.

In addition, two sets of oxygen generating mechanisms 1 are arranged in parallel, the reverse purging device 3 is a blower 31 or an overstock tank 32, and the specific structure of the purging pipeline 10 is correspondingly changed so as to meet different use requirements.

When the blower 31 is respectively communicated with the oxygen making mechanism 1 of the corresponding group through the first purge pipe 1001, and each first purge pipe 1001 is provided with a third control valve 1002 and a second vent valve 1003, the third control valve 1002 is used for controlling the on-off of the first purge pipe 1001, so that the third control valve is opened only during reverse purge, and the second vent valve 1003 is used for arranging redundant gas during oxygen extraction, so that the third control valve is opened during oxygen extraction, and the second control valve is closed during reverse purge.

Similarly, the pressure accumulation tanks 32 are all communicated with the oxygen generation mechanisms 1 of the corresponding group through the second purging pipes 1004, the second purging pipes 1004 are provided with fourth control valves 1005, the pressure limiting valves 1007 are used for stabilizing the pressure inside the pressure accumulation tanks 32, when the oxygen generation mechanisms 1 balance the internal air pressure, the fourth control valves 1005 are closed, and when the oxygen generation mechanisms perform reverse purging, the fourth control valves 1005 are opened.

The oxygen generation mechanism 1 in the above embodiment is preferably configured as follows: including zeolite molecular sieve tower 101 and carbon molecular sieve tower 102, zeolite molecular sieve tower 101 and carbon molecular sieve tower 102 are through first pipeline 103 intercommunication, and oxygen hose 7 communicates with the middle part of first pipeline 103, and the both sides that lie in oxygen hose 7 and first pipeline 103 junction on first pipeline 103 all are equipped with fifth control valve 104, and air supply pipe 4 communicates with zeolite molecular sieve tower 101, and carbon molecular sieve tower 102 communicates with reverse purging device 3 through purging pipeline 10.

Wherein, the nitrogen adsorption molecule is adsorbed by the zeolite molecular sieve in the zeolite molecular sieve tower 101, and the oxygen is adsorbed in the carbon molecular sieve micropores in the carbon molecular sieve tower 102 under the pressure, so that after the pressure is reduced, the oxygen is separated out, and when the pressure is balanced, the fifth control valve 104 positioned at the left side of the first pipeline 103 is closed, and the fifth control valve 104 and the second control valve 8 positioned at the right side are opened, so that the oxygen in the carbon molecular sieve tower 102 is sent into the oxygen storage tank 2.

The molecular sieve in the carbon molecular sieve tower 102 is a modified carbon molecular sieve, and the diameter range of the micropores is 0.28nm-0.35nm, so that oxygen can be better adsorbed.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.