阅读说明：本技术 一种抗蓝光隔离乳的配方和制备方法 (Formula and preparation method of anti-blue-light isolation emulsion ) 是由 夏胜成 于 2020-07-06 设计创作，主要内容包括：本发明公开了一种抗蓝光隔离乳的配方和制备方法,涉及护肤品技术领域。包含以下按质量份数计算的原料组分：丁二醇6.0％～10.0％、环五聚二甲基硅氧烷5.0％～10.0％、丁二醇二辛酸/二癸酸酯3.0％～6.0％、鲸蜡基PEG/PPG-10/1聚二甲基硅氧烷1.5％～3.5％、异十二烷2.0％～5.0％、PEG-10聚二甲基硅氧烷0.3％～1.5％、氯化钠0.6％～1.0％、无机紫外线吸收剂2.0％～10.0％、有机紫外线吸收剂3.0％～10.0％、二硬脂二甲铵锂蒙脱石0.1％～0.8％、氢化聚异丁烯1.0％～5.0％、植物提取修复精华液0.5％～2.0％、硬脂氧聚甲硅氧烷/聚二甲硅氧烷共聚物1.0％～2.0％、二甲基甲硅烷基化硅石0.3％～0.9％、生育酚乙酸酯0.05％～0.3％、乙醇1.0％～3.0％、苯氧乙醇&乙基己基甘油0.5％～0.6％、透明质酸钠0.01％～0.1％、聚二甲基硅氧烷1.0％～5.0％、抗蓝光植物提取成分0.35％～1.5％。(The invention discloses a formula and a preparation method of blue-light-resistant isolation milk, and relates to the technical field of skin care products. The material comprises the following raw material components in parts by weight: 6.0 to 10.0 percent of butanediol, 5.0 to 10.0 percent of cyclopentyldimethyl siloxane, 3.0 to 6.0 percent of butanediol dicaprylate/dicaprate, 1.5 to 3.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 2.0 to 5.0 percent of isododecane, 0.3 to 1.5 percent of PEG-10 polydimethylsiloxane, 0.6 to 1.0 percent of sodium chloride, 2.0 to 10.0 percent of inorganic ultraviolet absorbent, 3.0 to 10.0 percent of organic ultraviolet absorbent, 0.1 to 0.8 percent of disteardimonium hectorite, 1.0 to 5.0 percent of hydrogenated polyisobutene, 0.5 to 2.0 percent of plant extraction and repair essence, 1.0 to 2.0 percent of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.3 to 0.9 percent of dimethyl silylated silica, 0.05 to 0.3 percent of tocopherol acetate, 1.0 to 3.0 percent of ethanol, 0.5 to 0 percent of ethyl hexyl glycerol, and 0.6 to 0.6 percent of phenoxy glycerol, 0.01 to 0.1 percent of sodium hyaluronate, 1.0 to 5.0 percent of polydimethylsiloxane and 0.35 to 1.5 percent of blue light resistant plant extract component.)

1. The formula of the blue-light-resistant isolation milk is characterized by comprising the following raw material components in parts by mass: 6.0 to 10.0 percent of butanediol, 5.0 to 10.0 percent of cyclopentyldimethyl siloxane, 3.0 to 6.0 percent of butanediol dicaprylate/dicaprate, 1.5 to 3.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 2.0 to 5.0 percent of isododecane, 0.3 to 1.5 percent of PEG-10 polydimethylsiloxane, 0.6 to 1.0 percent of sodium chloride, 2.0 to 10.0 percent of inorganic ultraviolet absorbent, 3.0 to 10.0 percent of organic ultraviolet absorbent, 0.1 to 0.8 percent of disteardimonium hectorite, 1.0 to 5.0 percent of hydrogenated polyisobutene, 0.5 to 2.0 percent of plant extraction and repair essence, 1.0 to 2.0 percent of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.3 to 0.9 percent of dimethyl silylated silica, 0.05 to 0.3 percent of tocopherol acetate, 1.0 to 3.0 percent of ethanol, 0.5 to 0 percent of ethyl hexyl glycerol, and 0.6 to 0.6 percent of phenoxy glycerol, 0.01-0.1 percent of sodium hyaluronate, 1.0-5.0 percent of polydimethylsiloxane, 0.35-1.5 percent of blue light resistant plant extract component, 0.01-0.05 percent of essence, 0.05-0.30 percent of ferric oxide and the balance of deionized water being 100 percent.

2. The preparation method of the formula of the blue-light resistant isolation milk is characterized by comprising the following steps:

s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring the mixture, and finely grinding the mixture for 30min by using a colloid mill to obtain a required raw material I for later use;

s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxymethylsiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopheryl acetate and polydimethylsiloxane according to the percentage, putting the materials into an emulsifying pot, heating to dissolve the materials, and uniformly stirring the materials to obtain a required raw material II for later use;

s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again to obtain a required mixture;

s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating for dissolving, and uniformly stirring to obtain a required raw material III for later use;

s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 800-1200rpm, and slowly pumping the dissolved solution in the step S4 into the emulsifying pot until no water is accumulated on the liquid surface of the complete package for later use;

s6, secondary treatment of the mixture: weighing the plant extraction repair essence and the blue-light resisting plant extraction components in percentage in sequence, putting into the emulsifying pot in the step S5, stirring uniformly, and stirring at high speed for 3min for later use;

s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step (S6) and starting the first homogenization treatment, cooling, sequentially adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot, starting the second homogenization treatment, and continuously stirring for 10min to finish the preparation, thereby obtaining the required blue-light resistant isolation milk.

3. The method for preparing the formulation of blue light resistant barrier milk according to claim 2, wherein the inorganic ultraviolet absorbent in step S1 is preferably one or a combination of nano titanium dioxide, nano zinc oxide, triethoxyoctylsilane and nano cerium oxide.

4. The method for preparing the formulation of blue light resistant barrier milk according to claim 2, wherein the organic UV absorber in step S2 is preferably one or a combination of ethylhexyl methoxycinnamate, hexyl diethylamino hydroxybenzoyl benzoate, ethylhexyl salicylate, methylene bis-benzotriazolyl tetramethylbutyl phenol, bis-ethylhexyloxyphenol methoxyphenyl triazine, and ethylhexyl triazone.

5. The method for preparing the formulation of blue light resistant barrier milk according to claim 2, wherein the dissolution temperature in step S2 is 80-85 ℃, the stirring homogenization speed in step S3 is 3000rpm, and the stirring time is 20-30 min.

6. The method for preparing the formula of the blue-light resistant barrier milk according to claim 2, wherein the plant extraction and repair essence in step S6 is a combination of dendrobium nobile lindl extract, sophora flavescens ait root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbadensis extract.

7. The method of claim 2, wherein the blue-light resistant plant extract component of step S6 is a combination of wild soybean oil, rice germ extract, and rice extract.

8. The method for preparing the formula of the blue-light resistant barrier milk according to claim 2, wherein the heating temperature of the water phase pot in the step S4 is 75-80 ℃.

9. The method for preparing the formulation of blue-light resistant barrier milk according to claim 2, wherein the rotation speed of the first homogenization treatment in step S7 is 3000rpm for 5min, the temperature after the temperature reduction treatment in step S7 is 40-50 ℃, and the rotation speed of the second homogenization treatment in step S7 is 3000rpm for 5 min.

Technical Field

The invention relates to the technical field of skin care products, in particular to a formula and a preparation method of blue light resistant isolation milk.

Background

Various sun-proof isolation products on the market are various, and mainly claim a sun-proof function, namely ultraviolet rays for preventing solar radiation in the daytime, and in addition, the sun-proof isolation products also have additional functions with skin care and maintenance effects of moisturizing, whitening, oil control and the like, and have sun protection of UVA and UVB wave bands, namely wave band protection of 275-400 nm wavelength. The products are subdivided with different SPF and PA values, and distinguished on top of the additional function of skin care. The frequency of use of electronic products with display screens in modern work and life is increasing, and besides natural sunlight radiating ultraviolet rays, people are also exposed to blue light radiated by the electronic products at a higher frequency.

Because blue light radiated by an electronic product display screen is very harmful to a human body, at present, fewer protective cosmetics specially applied to blue light radiation have good market prospects by combining multiple effects of sun protection in broad spectrum, radiation pollution isolation, skin repair, blemish hiding, skin color brightening and the like, and a design and development of an isolation emulsion for applying on the skin are needed to reduce or block the damage of the blue light radiated by the electronic display product to the human body and simultaneously provide more repair and maintenance effects for the skin.

Disclosure of Invention

Aiming at the defects of the prior art, the invention provides a formula and a preparation method of an anti-blue-light isolation milk, which aim to solve the problems in the background art.

In order to achieve the purpose, the invention provides the following technical scheme: the formula of the blue-light-resistant isolation milk comprises the following raw material components in parts by mass: 6.0 to 10.0 percent of butanediol, 5.0 to 10.0 percent of cyclopentyldimethyl siloxane, 3.0 to 6.0 percent of butanediol dicaprylate/dicaprate, 1.5 to 3.5 percent of cetyl PEG/PPG-10/1 polydimethylsiloxane, 2.0 to 5.0 percent of isododecane, 0.3 to 1.5 percent of PEG-10 polydimethylsiloxane, 0.6 to 1.0 percent of sodium chloride, 2.0 to 10.0 percent of inorganic ultraviolet absorbent, 3.0 to 10.0 percent of organic ultraviolet absorbent, 0.1 to 0.8 percent of disteardimonium hectorite, 1.0 to 5.0 percent of hydrogenated polyisobutene, 0.5 to 2.0 percent of plant extraction and repair essence, 1.0 to 2.0 percent of stearyloxypolysiloxane/polydimethylsiloxane copolymer, 0.3 to 0.9 percent of dimethyl silylated silica, 0.05 to 0.3 percent of tocopherol acetate, 1.0 to 3.0 percent of ethanol, 0.5 to 0 percent of ethyl hexyl glycerol, and 0.6 to 0.6 percent of phenoxy glycerol, 0.01-0.1 percent of sodium hyaluronate, 1.0-5.0 percent of polydimethylsiloxane, 0.35-1.5 percent of blue light resistant plant extract component, 0.01-0.05 percent of essence, 0.05-0.30 percent of ferric oxide and the balance of deionized water being 100 percent.

A preparation method of a formula of blue light resistant isolation milk comprises the following steps:

s1, grinding of the raw material I: weighing butanediol dicaprylate/dicaprate, PEG-10 polydimethylsiloxane, an inorganic ultraviolet absorbent, hydrogenated polyisobutene and ferric oxide in sequence according to the percentage, putting the mixture into a tank, uniformly stirring the mixture, and finely grinding the mixture for 30min by using a colloid mill to obtain a required raw material I for later use;

s2, dissolving a second raw material: sequentially weighing cyclopentadimethylsiloxane, cetyl PEG/PPG-10/1 polydimethylsiloxane, isododecane, organic ultraviolet absorbent, disteardimonium hectorite, stearyloxymethylsiloxane/polydimethylsiloxane copolymer, silica dimethyl silylate, tocopheryl acetate and polydimethylsiloxane according to the percentage, putting the materials into an emulsifying pot, heating to dissolve the materials, and uniformly stirring the materials to obtain a required raw material II for later use;

s3, preparing a mixture: putting the ground raw material I in the step S1 into the emulsifying pot in the step S2, and stirring and homogenizing again to obtain a required mixture;

s4, preparation of a raw material III: weighing butanediol, sodium chloride, sodium hyaluronate and deionized water in percentage in turn, putting into a water phase pot, heating for dissolving, and uniformly stirring to obtain a required raw material III for later use;

s5, first treatment of the mixture: stirring the emulsifying pot in the step S3 at a high speed of 800-1200rpm, and slowly pumping the dissolved solution in the step S4 into the emulsifying pot until no water is accumulated on the liquid surface of the complete package for later use;

s6, secondary treatment of the mixture: weighing the plant extraction repair essence and the blue-light resisting plant extraction components in percentage in sequence, putting into the emulsifying pot in the step S5, stirring uniformly, and stirring at high speed for 3min for later use;

s7, obtaining blue-light resistant isolation milk: and (5) stirring the emulsifying pot in the step (S6) and starting the first homogenization treatment, cooling, sequentially adding ethanol, phenoxyethanol & ethylhexyl glycerin and essence into the emulsifying pot, starting the second homogenization treatment, and continuously stirring for 10min to finish the preparation, thereby obtaining the required blue-light resistant isolation milk.

In order to further optimize the technical solution, the inorganic ultraviolet absorbent in step S1 is preferably one or a combination of nano titanium dioxide, nano zinc oxide, triethoxy octyl silane and nano cerium oxide.

In order to further optimize the technical solution, the organic ultraviolet absorbent in step S2 is preferably one or a combination of ethylhexyl methoxycinnamate, hexyl diethylamino-benzoylbenzoate, ethylhexyl salicylate, methylene bis-benzotriazolyl tetramethylbutylphenol, bis-ethylhexyloxyphenol methoxyphenyl triazine, and ethylhexyl triazone.

Further optimizing the technical scheme, the dissolving temperature in the step S2 is 80-85 ℃, the stirring homogenizing rotation speed in the step S3 is 3000rpm, and the stirring time is 20-30 min.

Further optimizing the technical scheme, the plant extraction and repair essence in the step S6 is a composition of dendrobium nobile extract, sophora flavescens root extract, echinacea purpurea extract, lycium barbarum fruit extract and aloe barbadensis extract.

Further optimizing the technical solution, the anti-blue-light plant extract component in step S6 is a combination of wild soybean oil, rice germ extract and rice extract.

Further optimizing the technical scheme, wherein the heating temperature of the water phase pot in the step S4 is 75-80 ℃.

Further optimizing the technical scheme, the rotation speed of the first homogenization treatment in the step S7 is 3000rpm, the time is 5min, the temperature after the temperature reduction treatment in the step S7 is 40-50 ℃, the rotation speed of the second homogenization treatment in the step S7 is 3000rpm, and the time is 5 min.

Compared with the prior art, the invention provides a formula and a preparation method of blue-light resistant isolation milk, and the blue-light resistant isolation milk has the following beneficial effects:

1. according to the formula and the preparation method of the anti-blue-light isolation emulsion, the organic ultraviolet absorbent, the inorganic absorbent and the anti-blue-light component extracted from plants are used in a matching manner, the synergistic effect is promoted, the damage of an ultraviolet blue-light waveband to skin is blocked, the stable and efficient absorbent with the UVA wavelength of 320 nm and 400nm and the nano cerium oxide are particularly screened and used in an accurate ratio, the comprehensive absorption capacity is provided for the blue-light waveband, and the blue-light resistance and the cell damage caused by the blue-light resistance are repaired.

2. The blue light resistant isolation milk is scientific in proportioning, good in light stability, efficient in absorption, low in dosage, low in irritation and high in safety coefficient, excellent blue light resistant application of the plant rice embryo extract component brings safer and milder guarantee for the product, and meanwhile, the preparation method is easy to realize and can realize large-scale mass production.

Drawings

FIG. 1 is a flow chart of a formula and a preparation method of the blue light resistant isolation milk provided by the invention.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.