Insecticide and preparation method thereof

文档序号:1383225 发布日期:2020-08-18 浏览:31次 中文

阅读说明:本技术 一种杀虫剂及其制备方法 (Insecticide and preparation method thereof ) 是由 张新 李智 钱露露 于 2020-05-12 设计创作,主要内容包括:本发明属于杀虫农药技术领域,具体的说是一种杀虫剂及其制备方法,该方法包括以下步骤:取净天南星,按大小分别用水浸泡,每日换水4次,如起白沫时,换水后加白矾,泡一日后,再进行换水,至切开口尝微有麻舌感时取出,接着将生姜片、白矾置锅内加适量水煮沸后,倒入天南星共煮至无干心时取出,除去姜片,晾至四至六成干,切薄片,干燥,然后取贯众用清水稍浸,取出,早晚各洒水一次,润软,切片,晒干,再将五加皮除去杂质,洗净,润透,切厚片,晒干;本发明主要用于提供一种杀虫剂及其制备方法,选用中药作为杀虫手段,能够麻醉害虫的神经系统,显著抑制害虫的呼吸,从而在以不伤害人体为基础上能够对害虫实现有效杀灭。(The invention belongs to the technical field of insecticidal pesticides, and particularly relates to an insecticide and a preparation method thereof, wherein the method comprises the following steps: soaking clean rhizoma arisaematis with water according to size, respectively, changing water 4 times a day, adding Alumen after changing water if foams appear, soaking for one day, changing water again, taking out when cut openings taste little tongue-and-groove feeling, then putting rhizoma Zingiberis recens slice and Alumen into a pot, adding appropriate amount of water, boiling, pouring rhizoma arisaematis, decocting until there is no dry center, taking out, removing rhizoma Zingiberis recens slice, air drying to four to six dry, slicing, drying, soaking rhizoma Osmundae in clear water, taking out, sprinkling water once in the morning and evening, moistening, slicing, sun drying, removing impurities from cortex Acanthopanacis, cleaning, moistening thoroughly, slicing into thick slices, and sun drying; the invention is mainly used for providing the pesticide and the preparation method thereof, the traditional Chinese medicine is selected as the pesticide means, the nervous system of pests can be anesthetized, the breathing of the pests is obviously inhibited, and the pests can be effectively killed on the basis of no harm to human bodies.)

1. An insecticide, characterized by: comprises the following components in parts by weight:

the traditional Chinese medicine composition comprises, by weight, 20 parts of quisqualis indica, 15 parts of datura flower, 10 parts of garden balsam stem, 10 parts of strychni ignatii semen, 5 parts of nicotine, 25 parts of areca nut, 26 parts of cortex acanthopanacis, 30 parts of radix euphorbiae lantu, 31 parts of cyrtomium rhizome, 20 parts of stone-like omphalia, 50 parts of rhizoma arisaematis, 20 parts of mint and 10 parts of lavender essence.

2. A preparation method of a pesticide is characterized by comprising the following steps: the preparation method is suitable for the pesticide as claimed in claim 1, and comprises the following steps:

s1, dicing a part of rhizoma arisaematis, putting the diced rhizoma arisaematis in clear water for full soaking, changing water every 12h in the soaking process, adding alum after changing water, soaking for one day, changing water again, requiring the soaking time to be 3 days, peeling and slicing the ginger, mixing the sliced ginger and the alum, placing the mixture in a boiler, slowly heating, slowly boiling, requiring the heating time to be 1h, adding the whole rhizoma arisaematis, keeping the water in a boiling state, continuously boiling for 30 minutes, taking out the rhizoma arisaematis, filtering out the water, drying the filtered ginger slices, taking the rhizoma Osmundae slightly soaked in clear water, taking out, sprinkling water once in the morning and evening, moistening, slicing, drying the cortex acanthopanacis, removing impurities, cleaning, moistening, cutting into thick slices, drying, removing impurities from the flos chrysanthae, cleaning, moistening, slicing, drying, and drying, Cutting herba Speranskiae Tuberculatae, air drying semen Ignatii, and grinding the air dried semen Ignatii into powder;

s2: adding the dried raw materials in the step S1 into a thermal pulverizer for pulverizing to obtain mixed coarse powder, then placing the mixed coarse powder into a ball mill for full ball milling to fully grind the mixed coarse powder to obtain mixed fine powder, then adding ethanol and nicotine into the mixed fine powder, fully stirring, and standing for 12 hours to obtain a clear solution;

s3: putting mint and lavender essence into a grinder, fully stirring and grinding to obtain paste, then putting the paste into a heating container, adding clear water for heating, controlling the heating temperature at 50 ℃, keeping the heating time for 15 minutes, fully filtering the cooked mixed solution, and standing for 12 hours to obtain fragrant liquid;

s4: mixing the clear solution and the fragrant solution obtained in S2, evaporating by an evaporator for standby, concentrating the filtrate by vacuum concentration, and drying the concentrate to obtain the pesticide.

3. A pesticide according to claim 1, wherein: the areca nut is a complete unpeeled fruit; the rhizoma Osmundae is one or more of rhizoma Osmundae, rhizoma Dryopteridis Crassirhizomatis, rhizoma Dryopteris Crassirhizomatis, rhizoma Osmundae, rhizoma Dryopteridis Crassirhizomatis, rhizoma Cyrtomii Falcati, and rhizoma Cibotii rhizoma Cyrtomii Falcati.

4. The process for preparing an insecticide according to claim 1, wherein: in the preparation step S1, 20kg of ginger and alum are added into every 120kg of rhizoma arisaematis; the vegetable oil should be applied on gloves, mask or hands during the processing operation, so as to prevent skin from itching and swelling.

5. The process for preparing an insecticide according to claim 2, wherein: the evaporator comprises a main frame body (1), a liquid inlet groove (2), a liquid inlet pipe (3), an evaporation cavity (4), a rotating wheel (5) and a poking plate (6); a liquid inlet groove (2) is formed in the upper end wall of the main frame body (1); a liquid inlet pipe (3) is fixedly embedded at the lower end of the middle part of the liquid inlet tank (2); the lower end of the liquid inlet pipe (3) is communicated with the evaporation cavity (4), and evaporation plates (31) are fixedly arranged on two sides of the lower end of the liquid inlet pipe (3); the evaporation cavity (4) is formed in the wall of the main frame body (1), and a heat preservation ring (41) is fixedly arranged on the outer side of the evaporation cavity (4); the evaporation plate (31) is arc-shaped, the evaporation plate (31) is arranged above the evaporation cavity (4), the temperature of the evaporation plate (31) is higher than that of the heat preservation ring (41), and the evaporation plate (31) is in a filter plate shape; the rotating wheel (5) is rotatably arranged in the evaporation cavity (4) in the main frame body (1) through a motor, and the outer surface of the rotating wheel (5) is uniformly and fixedly provided with a poking plate (6); the poking plate (6) is arc-shaped, the outer end of the poking plate (6) is fixedly provided with a collecting plate (7), and the outer side of the poking plate (6) is provided with a hair filter (61); the filter bristles (61) are uniformly and fixedly arranged on the inner wall of the lower end of the evaporation cavity (4).

6. The process for preparing an insecticide as claimed in claim 5, wherein: the outer end of the poking plate (6) is fixedly connected with a filter screen (62); the filter screen (62) is made of flexible stainless steel metal materials, and the inner end part of the filter screen (62) is fixedly connected with packing rubber (63); an installation groove (64) is formed in the packaging rubber (63); the mounting groove (64) is filled with non-Newtonian fluid.

Technical Field

The invention belongs to the technical field of insecticidal pesticides, and particularly relates to an insecticide and a preparation method thereof.

Background

The pesticides can be used for killing insects, fungi and other organisms harmful to the growth of crops, and the first pesticides used are DDT, Liuliu, and the like, which can largely kill pests. But they are good in stability, can exist in the environment for a long time, and are continuously accumulated in animals, plants and human bodies, so that they are eliminated. Later, organophosphorus pesticides, such as dichlorvos, were substituted for the original pesticides. Because of the great toxicity and great harm to human and livestock, in recent years, a batch of high-efficiency and low-toxicity pesticides appear, and have specificity, namely hormone pesticides, which are good for plants and cause potential safety hazards when being eaten by mistake.

In the application number of CN110477046A, a Chinese traditional medicine insecticide and its preparation method, the materials of rangooncreeper fruit, radix euphorbiae lantu and areca seed are used, the rangooncreeper fruit contains potassium rangooncreeper fruit, betulinic acid and oleic acid, etc., and has paralysis effect on pests; the radix euphorbiae lantu contains flavonoid compounds, and can obviously inhibit the respiration of pests; the areca nut contains rich arecoline, can anaesthetize the nervous system of pests, is safe, efficient and environment-friendly, is not easy to produce drug resistance, provides a material guarantee for developing green agriculture and organic agriculture, but has the following defects in the scheme:

1. the pesticide has poor systemic property of plant roots, low mammalian toxicity, high efficiency, broad spectrum, poor environmental compatibility and the like, and especially has no good control effect on homoptera aphids and hemiptera planthoppers.

2. The toxicity of the current pesticide is generally high, and modern agriculture production green products and pollution-free products are not allowed to be used, but the toxicity is light, and the effect is little for some insects with high drug resistance.

3. Subjective standards are more on the one hand in the manufacturing process, large-batch production is difficult to realize during production, and meanwhile, raw materials are not effectively cut before cooking, so that the cooking time is longer, the efficiency is lower, and finally, the crushed particles are larger, so that effective components are difficult to effectively release.

4. Meanwhile, various plant raw materials are mixed, the smell is heavy, and some people can reject the pungent taste and even have adverse reactions and other problems.

Aiming at the technical scheme, the method is remarkably optimized and improved on the basis of the process steps of the scheme, adopts special raw materials, can improve the production efficiency, shorten the production time, reduce the process conditions and the cost and enhance the insecticidal effect.

Therefore, the company designs and develops an insecticide and a preparation method thereof, and solves the technical problems.

Disclosure of Invention

In order to make up for the defects of the prior art, the invention provides an insecticide and a preparation method thereof. The invention is mainly used for providing the pesticide and the preparation method thereof, the traditional Chinese medicine is selected as the pesticide means, the nervous system of pests can be anesthetized, the breathing of the pests is obviously inhibited, and the pests can be effectively killed on the basis of no harm to human bodies.

The technical scheme adopted by the invention for solving the technical problems is as follows: the pesticide provided by the invention comprises the following components in parts by weight:

20 parts of rangooncreeper fruit, 15 parts of datura flower, 10 parts of garden balsam stem, 10 parts of strychnine, 5 parts of nicotine, 25 parts of areca nut, 26 parts of cortex acanthopanacis, 30 parts of radix euphorbiae lantu, 31 parts of cyrtomium rhizome, 20 parts of Omphalia and 50 parts of rhizoma arisaematis.

A process for the preparation of a pesticide, the process comprising the steps of:

s1, dicing a part of rhizoma arisaematis, putting the diced rhizoma arisaematis in clear water for full soaking, changing water every 12h in the soaking process, adding alum after changing water, soaking for one day, changing water again, requiring the soaking time to be 3 days, peeling and slicing the ginger, mixing the sliced ginger and the alum, placing the mixture in a boiler, slowly heating, slowly boiling, requiring the heating time to be 1h, adding the whole rhizoma arisaematis, keeping the water in a boiling state, continuously boiling for 30 minutes, taking out the rhizoma arisaematis, filtering out the water, drying the filtered ginger slices, taking the rhizoma Osmundae slightly soaked in clear water, taking out, sprinkling water once in the morning and evening, moistening, slicing, drying the cortex acanthopanacis, removing impurities, cleaning, moistening, cutting into thick slices, drying, removing impurities from the flos chrysanthae, cleaning, moistening, slicing, drying, and drying, Cutting herba Speranskiae Tuberculatae, air drying semen Ignatii, and grinding the air dried semen Ignatii into powder; the flos Daturae Metelis and herba speranskiae tuberculatae are cut off and the semen Ignatii is ground, so that the raw materials are mixed and crushed together, and the raw material space is reduced.

S2: adding the dried raw materials in the step S1 into a thermal pulverizer for pulverizing to obtain mixed coarse powder, then placing the mixed coarse powder into a ball mill for full ball milling to fully grind the mixed coarse powder to obtain mixed fine powder, then adding ethanol and nicotine into the mixed fine powder, fully stirring, and standing for 12 hours to obtain a clear solution; the prepared nicotine pesticide has the characteristics of unique and novel action mode, good root systemic property, low mammalian toxicity, high efficiency, broad spectrum, good environmental compatibility and the like, particularly has a very good control effect on homoptera aphids and hemiptera planthoppers, and meanwhile, large particle powder can be finely ground by a ball mill to obtain mixed fine powder, so that the effective components of the mixed fine powder can be fully and quickly released.

S3: putting mint and lavender essence into a grinder, fully stirring and grinding to obtain paste, then putting the paste into a heating container, adding clear water for heating, controlling the heating temperature at 50 ℃, keeping the heating time for 15 minutes, fully filtering the cooked mixed solution, and standing for 12 hours to obtain fragrant liquid; the perfume liquid processed by the mint and lavender essence can be added into the pesticide to neutralize the taste of the pesticide, so that the pesticide can emit special fragrance, and the rejection reaction of workers and users is reduced.

S4: mixing the clear solution obtained in S2 with the fragrant solution, evaporating by an evaporator for later use, concentrating the filtrate by adopting a vacuum concentration mode, and drying the concentrate to obtain the pesticide; through using this evaporimeter, the clarification solution that can make is more quick is evaporated, improves production efficiency by a wide margin, avoids direct open-type evaporation simultaneously, makes the ambient air of nicotine evaporation easily, produces the pollution to the surrounding environment on the one hand, and on the other hand staff inhales the nicotine of evaporation, produces serious harm to can the human body.

The areca nut is a complete unpeeled fruit; the rhizoma Osmundae is one or more of rhizoma Osmundae, rhizoma Dryopteridis Crassirhizomatis, rhizoma Dryopteris Crassirhizomatis, rhizoma Osmundae, rhizoma Dryopteridis Crassirhizomatis, rhizoma Cyrtomii Falcati, and rhizoma Cibotii rhizoma Cyrtomii Falcati.

In the preparation step S1, 20kg of ginger and alum are added into every 120kg of rhizoma arisaematis; the vegetable oil should be applied on gloves, mask or hands during the processing operation, so as to prevent skin from itching and swelling.

The evaporator comprises a main frame body, a liquid inlet groove, a liquid inlet pipe, an evaporation cavity, a rotating wheel and a stirring plate; a liquid inlet groove is formed in the upper end wall of the main frame body; a liquid inlet pipe is fixedly embedded at the lower end of the middle part of the liquid inlet tank; the lower end of the liquid inlet pipe is communicated with the evaporation cavity, and evaporation plates are fixedly arranged on two sides of the lower end of the liquid inlet pipe; the evaporation cavity is formed in the wall of the main frame body, and a heat preservation ring is fixedly arranged on the outer side of the evaporation cavity; the evaporation plate is arc-shaped, is arranged above the evaporation cavity, has a higher temperature than the heat preservation ring and is in a filter plate shape; the rotating wheel is rotatably arranged in an evaporation cavity in the main frame body through a motor, and the outer surface of the rotating wheel is uniformly and fixedly provided with a poking plate; the poking plate is arc-shaped, the outer end of the poking plate is fixedly provided with a collecting plate, and the outer side of the poking plate is provided with filter bristles; the filter bristles are uniformly and fixedly arranged on the inner wall of the lower end of the evaporation cavity; when the clarified solution needs to be evaporated, the heat-insulating ring can be heated to enable the temperature in the evaporation cavity to be higher than that of the outer side of the evaporator, the clarified solution is slowly poured into the liquid inlet groove and then enters the evaporation cavity through the liquid inlet pipe, at the moment, the motor is started to drive the rotating wheel to rotate, the rotating wheel starts to drive the stirring plate to stir the clarified solution, the clarified solution is stirred up to the evaporation plate through the collecting plate at the outer end of the rotating wheel, at the moment, the temperature of the evaporation plate is higher than that of the heat-insulating ring, namely, the evaporation plate can heat and evaporate the clarified solution on the lower surface of the evaporation plate, the clarified solution enters the cavity above the evaporation plate through the evaporation plate and is led out through the pores in the right side wall of the main frame body, and in the process, the evaporation plate can also heat the air in the cavity above the evaporation cavity so as to assist the clarified solution on the lower surface of the evaporation plate, and the heat preservation ring can preheat the clear solution, and the cooperation is rotated the wheel and is controlled its temperature at the easy critical point that evaporates under its not by the condition of evaporation to make clear solution more quick by the evaporation, improve production efficiency by a wide margin.

The outer end of the poking plate is fixedly connected with a filter screen; the filter screen is made of flexible stainless steel metal material, and the inner end part of the filter screen is fixedly connected with packing rubber; an installation groove is formed in the packaging rubber; the mounting groove is filled with non-Newtonian fluid; when the stirring plate is used for stirring up the clarified solution to the lower surface of the evaporating plate, the outer end of the stirring plate is fixedly connected with a filter screen which is made of a flexible stainless steel metal material, so that the clarified solution can be filtered by the filter screen and then sprayed to the lower surface of the evaporating plate when being stirred, further filtration of the clarified solution is realized in the process of stirring and promoting fusion, impurities such as dust and the like are prevented from being adsorbed in the gas evaporated when the clarified solution is transferred and poured into a liquid inlet groove, and accordingly, the pesticide blocks a spray opening of a bottle opening after being packaged, and the use is inconvenient, meanwhile, because the inner end part of the filter screen is fixedly connected with packaging rubber, an installation groove is formed in the packaging rubber, and non-Newtonian fluid is filled in the installation groove, so that the non-Newtonian fluid is subjected to great throwing power and is solidified when the rotating wheel rotates at, thereby improved its centrifugal gravity greatly when the rotation wheel rotates, impurity such as the dust that makes to be filtered is by the compaction to make impurity be difficult for droing, further ensure that the clarification solution of evaporating plate lower surface is in the no impurity state.

The invention has the following beneficial effects:

1. according to the technical scheme provided by the invention, the pesticide and the preparation method thereof adopt the materials of rangooncreeper fruit, radix euphorbiae lantu, semen arecae and the like, and the rangooncreeper fruit contains potassium rangooncreeper fruit, betulinic acid, oleic acid and the like, and has a paralysis effect on pests; the radix euphorbiae lantu contains flavonoid compounds, and can obviously inhibit the respiration of pests; the areca nut contains rich arecoline, can anaesthetize the nervous system of pests, is safe, efficient and environment-friendly, is not easy to produce drug resistance, provides a material guarantee for developing green agriculture and organic agriculture, meanwhile, the nicotine pesticide prepared by adding nicotine has the characteristics of unique and novel action mode, good systemic property in roots, low mammalian toxicity, high efficiency, broad spectrum, good environmental compatibility and the like, and particularly has very good control effect on homoptera aphids and hemiptera planthoppers, the essence obtained by processing the peppermint essence and the lavender essence can be added into the pesticide, the smell of the pesticide is neutralized, and the pesticide can emit special fragrance, reduce the rejection reaction of workers and users, meanwhile, the large-particle powder can be finely ground through the ball mill to obtain mixed fine powder, so that the effective components of the mixed fine powder can be fully and quickly released.

2. Through the technical scheme provided by the invention, when the clarified solution needs to be evaporated, the heat-insulating ring can be heated to ensure that the temperature in the evaporation cavity is higher than that of the outer side of the evaporator, the clarified solution is slowly poured into the liquid inlet groove and then enters the evaporation cavity through the liquid inlet pipe, the motor is started to drive the rotating wheel to rotate, the rotating wheel starts to drive the stirring plate to stir the clarified solution, the clarified solution is stirred up to the evaporation plate through the collecting plate at the outer end of the rotating wheel, at the moment, because the temperature of the evaporation plate is higher than that of the heat-insulating ring, the evaporation plate can heat and evaporate the clarified solution on the lower surface of the evaporation plate, the clarified solution enters the cavity above the evaporation plate through the evaporation plate and is led out through the pores in the right side wall of the main frame body, and in the process, the evaporation plate can heat the air in the cavity above the evaporation cavity when evaporating the clarified solution on the lower surface of the evaporation plate, thereby the clarification solution to evaporating plate lower surface is assisted, and the heat preservation ring can preheat clarification solution, cooperates the rotation wheel with its temperature control at the critical point of easy evaporation under its not by the circumstances of evaporation to make clarification solution more quick by the evaporation, improve production efficiency by a wide margin.

3. Through the technical scheme provided by the invention, when the poking plate swings the clarified solution to the lower surface of the evaporation plate, the outer end of the poking plate is fixedly connected with the filter screen which is made of flexible stainless steel metal material, so that the clarified solution can be filtered by the filter screen and then sprayed to the lower surface of the evaporation plate when being swung, further filtration of the clarified solution is realized in the process of stirring and fusion promotion, impurities in evaporated gas caused by adsorption of impurities such as dust and the like when the clarified solution is transferred and poured into the liquid inlet groove are prevented from being carried in the gas, so that the pesticide blocks a spray opening of a bottle opening after packaging is finished, and the use is inconvenient, meanwhile, because the inner end part of the filter screen is fixedly connected with packaging rubber, the packaging rubber is internally provided with a mounting groove which is filled with non-Newtonian fluid, the non-Newtonian fluid can be solidified by large swinging force when the rotating wheel rotates at high speed, thereby improved its centrifugal gravity greatly when the rotation wheel rotates, impurity such as the dust that makes to be filtered is by the compaction to make impurity be difficult for droing, further ensure that the clarification solution of evaporating plate lower surface is in the no impurity state.

Drawings

FIG. 1 is a diagram of the method steps of the present invention;

FIG. 2 is a schematic view of the evaporator of the present invention;

FIG. 3 is an enlarged view of a portion of the invention at A in FIG. 2;

in the figure: the device comprises a main frame body 1, a liquid inlet groove 2, a liquid inlet pipe 3, an evaporation plate 31, an evaporation cavity 4, a heat preservation ring 41, a rotating wheel 5, a poking plate 6, filter bristles 61, a filter screen 62, packing rubber 63, a mounting groove 64 and a collecting plate 7.

Detailed Description

An insecticide and a method for producing the same according to an embodiment of the present invention will be described below with reference to fig. 1 to 3.

As shown in fig. 1-3, the pesticide of the present invention comprises the following components by weight:

20 parts of rangooncreeper fruit, 15 parts of datura flower, 10 parts of garden balsam stem, 10 parts of strychnine, 5 parts of nicotine, 25 parts of areca nut, 26 parts of cortex acanthopanacis, 30 parts of radix euphorbiae lantu, 31 parts of cyrtomium rhizome, 20 parts of Omphalia and 50 parts of rhizoma arisaematis.

A process for the preparation of a pesticide, the process comprising the steps of:

s1, dicing a part of rhizoma arisaematis, putting the diced rhizoma arisaematis in clear water for full soaking, changing water every 12h in the soaking process, adding alum after changing water, soaking for one day, changing water again, requiring the soaking time to be 3 days, peeling and slicing the ginger, mixing the sliced ginger and the alum, placing the mixture in a boiler, slowly heating, slowly boiling, requiring the heating time to be 1h, adding the whole rhizoma arisaematis, keeping the water in a boiling state, continuously boiling for 30 minutes, taking out the rhizoma arisaematis, filtering out the water, drying the filtered ginger slices, taking the rhizoma Osmundae slightly soaked in clear water, taking out, sprinkling water once in the morning and evening, moistening, slicing, drying the cortex acanthopanacis, removing impurities, cleaning, moistening, cutting into thick slices, drying, removing impurities from the flos chrysanthae, cleaning, moistening, slicing, drying, and drying, Cutting herba Speranskiae Tuberculatae, air drying semen Ignatii, and grinding the air dried semen Ignatii into powder; the flos Daturae Metelis and herba speranskiae tuberculatae are cut off and the semen Ignatii is ground, so that the raw materials are mixed and crushed together, and the raw material space is reduced.

S2: adding the dried raw materials in the step S1 into a thermal pulverizer for pulverizing to obtain mixed coarse powder, then placing the mixed coarse powder into a ball mill for full ball milling to fully grind the mixed coarse powder to obtain mixed fine powder, then adding ethanol and nicotine into the mixed fine powder, fully stirring, and standing for 12 hours to obtain a clear solution; the prepared nicotine pesticide has the characteristics of unique and novel action mode, good root systemic property, low mammalian toxicity, high efficiency, broad spectrum, good environmental compatibility and the like, particularly has a very good control effect on homoptera aphids and hemiptera planthoppers, and meanwhile, large particle powder can be finely ground by a ball mill to obtain mixed fine powder, so that the effective components of the mixed fine powder can be fully and quickly released.

S3: putting mint and lavender essence into a grinder, fully stirring and grinding to obtain paste, then putting the paste into a heating container, adding clear water for heating, controlling the heating temperature at 50 ℃, keeping the heating time for 15 minutes, fully filtering the cooked mixed solution, and standing for 12 hours to obtain fragrant liquid; the perfume liquid processed by the mint and lavender essence can be added into the pesticide to neutralize the taste of the pesticide, so that the pesticide can emit special fragrance, and the rejection reaction of workers and users is reduced.

S4: mixing the clear solution obtained in S2 with the fragrant solution, evaporating by an evaporator for later use, concentrating the filtrate by adopting a vacuum concentration mode, and drying the concentrate to obtain the pesticide; through using this evaporimeter, the clarification solution that can make is more quick is evaporated, improves production efficiency by a wide margin, avoids direct open-type evaporation simultaneously, makes the ambient air of nicotine evaporation easily, produces the pollution to the surrounding environment on the one hand, and on the other hand staff inhales the nicotine of evaporation, produces serious harm to can the human body.

The areca nut is a complete unpeeled fruit; the rhizoma Osmundae is one or more of rhizoma Osmundae, rhizoma Dryopteridis Crassirhizomatis, rhizoma Dryopteris Crassirhizomatis, rhizoma Osmundae, rhizoma Dryopteridis Crassirhizomatis, rhizoma Cyrtomii Falcati, and rhizoma Cibotii rhizoma Cyrtomii Falcati.

In the preparation step S1, 20kg of ginger and alum are added into every 120kg of rhizoma arisaematis; the vegetable oil should be applied on gloves, mask or hands during the processing operation, so as to prevent skin from itching and swelling.

The evaporator comprises a main frame body 1, a liquid inlet groove 2, a liquid inlet pipe 3, an evaporation cavity 4, a rotating wheel 5 and a stirring plate 6; a liquid inlet groove 2 is formed in the upper end wall of the main frame body 1; a liquid inlet pipe 3 is fixedly embedded at the lower end of the middle part of the liquid inlet tank 2; the lower end of the liquid inlet pipe 3 is communicated with the evaporation cavity 4, and evaporation plates 31 are fixedly arranged on two sides of the lower end of the liquid inlet pipe 3; the evaporation cavity 4 is arranged in the wall of the main frame body 1, and a heat preservation ring 41 is fixedly arranged on the outer side of the evaporation cavity 4; the evaporation plate 31 is arc-shaped, the evaporation plate 31 is arranged above the evaporation cavity 4, the temperature of the evaporation plate 31 is higher than that of the heat preservation ring 41, and the evaporation plate 31 is in a filter plate shape; the rotating wheel 5 is rotatably arranged in the evaporation cavity 4 in the main frame body 1 through a motor, and the poking plate 6 is uniformly and fixedly arranged on the outer surface of the rotating wheel 5; the poking plate 6 is arc-shaped, the outer end of the poking plate 6 is fixedly provided with the collecting plate 7, and the outer side of the poking plate 6 is provided with the filter bristles 61; the filter bristles 61 are uniformly and fixedly arranged on the inner wall of the lower end of the evaporation cavity 4; when the clarified solution needs to be evaporated, the heat-insulating ring 41 can be heated to enable the temperature in the evaporation cavity 4 to be higher than the outer side of the evaporator, and the clarified solution is slowly poured into the liquid inlet groove 2 and then enters the evaporation cavity 4 through the liquid inlet pipe 3, at the moment, the motor is started to drive the rotating wheel 5 to rotate, namely, the rotating wheel 5 starts to drive the stirring plate 6 to stir the clarified solution, and the clarified solution is stirred up to the evaporation plate 31 through the collecting plate 7 at the outer end of the rotating wheel, at the moment, because the temperature of the evaporation plate 31 is higher than that of the heat-insulating ring 41, the evaporation plate 31 can heat and evaporate the clarified solution on the lower surface of the evaporation plate, and finally the clarified solution enters the cavity above the evaporation plate 31 through the evaporation plate 31 and is led out through the pores in the right side wall of the main frame body 1, in the process, when the evaporation plate 31 evaporates the clarified solution on the lower surface of the evaporation plate, the cavity above the evaporation cavity 4 can, thereby the clarification solution to evaporating plate 31 lower surface is assisted, and heat preservation ring 41 can preheat the clarification solution, cooperates rotation wheel 5 under its not the circumstances of evaporating and is at the critical point of easy evaporation with its temperature control to make clarification solution faster by the evaporation, improve production efficiency by a wide margin.

The outer end of the poking plate 6 is fixedly connected with a filter screen 62; the filter screen 62 is made of flexible stainless steel metal material, and the inner end part of the filter screen 62 is fixedly connected with packing rubber 63; an installation groove 64 is formed in the packaging rubber 63; the mounting groove 64 is filled with non-Newtonian fluid; when the poking plate 6 is used for swinging up the clarified solution to the lower surface of the evaporating plate 31, the outer end of the poking plate 6 is fixedly connected with the filter screen 62, the filter screen 62 is made of flexible stainless steel metal material, so that the clarified solution can be filtered by the filter screen 62 and sprayed to the lower surface of the evaporating plate 31 when being swung up, further filtration of the clarified solution is realized in the process of promoting fusion by stirring, impurities such as dust and the like are prevented from being adsorbed when the clarified solution is transferred and poured into the liquid inlet groove 2 to cause evaporation, so that the pesticide blocks a spray opening of a bottle mouth after packaging is completed, inconvenience in use is caused, meanwhile, the inner end part of the filter screen 62 is fixedly connected with packaging rubber 63, an installation groove 64 is formed in the packaging rubber 63, and non-Newtonian fluid is filled in the installation groove 64, so that the non-Newtonian fluid is solidified due to large swinging force when the rotating wheel 5 rotates at, thereby improved its centrifugal gravity greatly when the running wheel 5 rotates, that is to say that impurity such as the dust that gets filtered is by the compaction to make impurity be difficult for droing, further ensure that the clarification solution of evaporating plate 31 lower surface is in the no impurity state.

The specific working process is as follows:

when the clarified solution needs to be evaporated, the heat-insulating ring 41 can be heated to enable the temperature in the evaporation cavity 4 to be higher than the outer side of the evaporator, and the clarified solution is slowly poured into the liquid inlet groove 2 and then enters the evaporation cavity 4 through the liquid inlet pipe 3, at the moment, the motor is started to drive the rotating wheel 5 to rotate, namely, the rotating wheel 5 starts to drive the stirring plate 6 to stir the clarified solution, and the clarified solution is stirred up to the evaporation plate 31 through the collecting plate 7 at the outer end of the rotating wheel, at the moment, because the temperature of the evaporation plate 31 is higher than that of the heat-insulating ring 41, the evaporation plate 31 can heat and evaporate the clarified solution on the lower surface of the evaporation plate, and finally the clarified solution enters the cavity above the evaporation plate 31 through the evaporation plate 31 and is led out through the pores in the right side wall of the main frame body 1, in the process, when the evaporation plate 31 evaporates the clarified solution on the lower surface of the evaporation plate, the cavity above the evaporation cavity 4 can, thereby assisting the clarified solution on the lower surface of the evaporating plate 31, the heat preservation ring 41 can preheat the clarified solution, the temperature of the clarified solution is controlled at the critical point of easy evaporation by matching with the rotating wheel 5 under the condition that the clarified solution is not evaporated, thereby the clarified solution is evaporated more rapidly, the production efficiency is greatly improved, when the poking plate 6 swings the clarified solution to the lower surface of the evaporating plate 31, because the outer end of the poking plate 6 is fixedly connected with the filter screen 62, the filter screen 62 is made of flexible stainless steel metal material, the clarified solution can be filtered by the filter screen 62 and then sprayed to the lower surface of the evaporating plate 31 when being swung, further filtering the clarified solution in the process of promoting fusion by stirring is realized, the clarified solution is prevented from adsorbing impurities such as dust and the like to cause the evaporated gas to carry impurities when being transferred and poured into the liquid inlet tank 2, thereby causing the injection port of the blockage of the insecticide after the packaging is completed, cause the use inconvenient, end fixedly connected with packing rubber 63 because of filter screen 62 simultaneously, mounting groove 64 has been seted up to packing rubber 63's inside, the mounting groove 64 intussuseption is filled with non-newton fluid, so can make non-newton fluid receive great power of getting rid of and take place the solidification when rotating wheel 5 high-speed rotation, thereby improved its centrifugal gravity greatly when rotating wheel 5 and rotating, even if impurity such as filtered dust is compacted, thereby make impurity be difficult for droing, further ensure that the clarification solution of evaporating plate 31 lower surface is in the no impurity state.

While the present invention has been described with reference to the embodiments shown in the drawings, the present invention is not limited to the embodiments, which are illustrative and not restrictive, and it will be apparent to those skilled in the art that various changes and modifications can be made therein without departing from the spirit and scope of the invention as defined in the appended claims.

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