阅读说明：本技术 一种香水香精及其制备方法 (Perfume essence and preparation method thereof ) 是由 杨禄 邬奕 岑靓祎 胡永生 于 2019-10-24 设计创作，主要内容包括：本发明公开了一种香水香精,其原料由以下组分组成：降龙涎醚、麝香T、檀香803、甲位己基桂醛、二氢茉莉酮酸甲酯、檀香208、香茅醇、苯乙醇、芳樟醇、苯甲醇、对甲基苯甲醚、乙酸对甲酚酯、柳酸叶醇酯、α-紫罗兰酮、丙位十二内酯、灵猫香提取物、橙花醇、阿根廷柠檬油、一缩二丙二醇。本发明的香水香精不仅具有香水的吸引力,而且香气品质良好,具有优良的长效性和贮存稳定性,具有非常好的推广应用价值。(The invention discloses perfume essence which comprises the following raw materials: ambrox, musk T, sandalwood 803, methyl hexyl cinnamaldehyde, methyl dihydrojasmonate, sandalwood 208, citronellol, phenethyl alcohol, linalool, benzyl alcohol, p-methyl anisole, p-cresol acetate, folic alcohol salicylate, alpha-ionone, propyl dodecalactone, civet extract, nerol, argentine lemon oil and dipropylene glycol. The perfume essence disclosed by the invention not only has the attraction of perfume, but also has good fragrance quality, excellent long-acting property and storage stability, and very good popularization and application values.)

1. The perfume essence is characterized by comprising the following raw materials in parts by weight:

0.10-0.30 part of ambrox, 5.00-10.00 parts of musk T, 8030.10-0.25 part of sandalwood, 2.00-5.00 parts of methyl-hexyl cinnamaldehyde, 1.00-2.00 parts of methyl dihydrojasmonate, 2081.00-2.00 parts of sandalwood, 0.20-0.60 part of citronellol, 2.40-4.80 parts of phenethyl alcohol, 1.40-3.60 parts of linalool, 0.10-0.20 part of benzyl alcohol, 0.30-0.50 part of p-methyl anisole, 0.01-0.05 part of p-cresol acetate, 0.15-0.35 part of folic acid leaf alcohol ester, 0.20-1.20 part of alpha-irisone, 0.01-0.05 part of propyl dodecanol, 5.00-10.00 parts of civet extract, 0.01-0.05 part of nerol, 1.00-2.20 parts of Argentina lemon oil and 30.00-49.00 parts of dipropylene glycol.

2. The perfume essence according to claim 1, wherein the raw materials comprise the following components in parts by weight: 0.10 parts of ambrox, 5.00 parts of musk T, 8030.10 parts of sandalwood, 2.00 parts of methyl hexyl cinnamaldehyde, 1.00 parts of methyl dihydrojasmonate, 2081.00 parts of sandalwood, 0.20 part of citronellol, 2.40 parts of phenethyl alcohol, 1.40 parts of linalool, 0.10 part of benzyl alcohol, 0.30 part of p-methyl anisole, 0.01 part of p-cresol acetate, 0.15 part of folic acid salicylate, 0.20 part of alpha-ionone, 0.01 part of propyl dodecalactone, 5.00 parts of civet extract, 0.01 part of nerol, 1.00 part of Argentina lemon oil and 30.00 parts of dipropylene glycol.

3. The perfume essence according to claim 1, wherein the raw materials comprise the following components in parts by weight: 0.20 of ambrox, 8.00 of musk T, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of p-methyl anisole, 0.02 of p-cresol acetate, 0.25 of folic salicylate, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 8.00 of civet extract, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.

4. The perfume essence according to claim 1, wherein the raw materials comprise the following components in parts by weight: 0.30 parts of ambrox, 10.00 parts of musk T, 8030.25 parts of sandalwood, 5.00 parts of methyl hexyl cinnamaldehyde, 2.00 parts of methyl dihydrojasmonate, 2082.00 parts of sandalwood, 0.60 part of citronellol, 4.80 parts of phenethyl alcohol, 3.60 parts of linalool, 0.20 part of benzyl alcohol, 0.50 part of p-methyl anisole, 0.05 part of p-cresol acetate, 0.35 part of folic acid salicylate, 1.20 parts of alpha-ionone, 0.05 part of propyl dodecalactone, 10.00 parts of civet extract, 0.05 part of nerol, 2.20 parts of Argentina lemon oil and 49.00 parts of dipropylene glycol.

5. The perfume essence of claim 1, wherein the civet extract is prepared by the following steps:

(1) mixing civet and ethanol water solution according to the weight ratio of 1: (4-5) uniformly mixing, then performing primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃ respectively, and collecting to obtain a primary molecular distillation distillate, a secondary molecular distillation distillate and a tertiary molecular distillation distillate;

(2) mixing the first-stage molecular distillation distillate, the second-stage molecular distillation distillate and the third-stage molecular distillation distillate according to the weight ratio of 1: (2-4): (5-7) mixing uniformly to obtain the civet extract.

6. The perfume essence according to claim 5, wherein in the step (1), the first molecular distillation, the second molecular distillation and the third molecular distillation are carried out in a wiped film type molecular distillation device, wherein the feeding speed is 4-5ml/min, the operating pressure is 5-10Pa, and the wiped film speed is 80-120 r/min.

7. The perfume essence according to claim 5, wherein the volume concentration of the ethanol aqueous solution is 80-90%.

8. A process for the preparation of a perfume fragrance according to any of claims 1 to 7, comprising the steps of:

(1) mixing ambrox, Moschus T, lignum Santali albi 803, radix Clematidis Finetianae extract and dipropylene glycol, dissolving, and stirring;

(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering to obtain perfume essence.

Technical Field

The invention relates to the technical field of perfume, in particular to perfume essence and a preparation method thereof.

Background

The perfume is one of important cosmetics, has volatility, can be sensed by smell or taste of people, can emit pleasant fragrance when being sprayed on parts such as lappets, handkerchiefs, hairlines and the like, and achieves the purposes of being loved and spiritual pleasure. For a long time, how to prepare the perfume essence with good fragrance and long-acting property has important significance.

Disclosure of Invention

The invention aims to make up for the defects of the prior art and provides the perfume essence which has the advantages of good fragrance and long-lasting effect.

The invention is realized by the following technical scheme:

the perfume essence comprises the following raw materials in parts by weight:

0.10-0.30 part of ambrox, 5.00-10.00 parts of musk T, 8030.10-0.25 part of sandalwood, 2.00-5.00 parts of methyl-hexyl cinnamaldehyde, 1.00-2.00 parts of methyl dihydrojasmonate, 2081.00-2.00 parts of sandalwood, 0.20-0.60 part of citronellol, 2.40-4.80 parts of phenethyl alcohol, 1.40-3.60 parts of linalool, 0.10-0.20 part of benzyl alcohol, 0.30-0.50 part of p-methyl anisole, 0.01-0.05 part of p-cresol acetate, 0.15-0.35 part of folic acid leaf alcohol ester, 0.20-1.20 part of alpha-irisone, 0.01-0.05 part of propyl dodecanol, 5.00-10.00 parts of civet extract, 0.01-0.05 part of nerol, 1.00-2.20 parts of Argentina lemon oil and 30.00-49.00 parts of dipropylene glycol.

Preferably, the perfume essence comprises the following raw materials in parts by weight: 0.10 parts of ambrox, 5.00 parts of musk T, 8030.10 parts of sandalwood, 2.00 parts of methyl hexyl cinnamaldehyde, 1.00 parts of methyl dihydrojasmonate, 2081.00 parts of sandalwood, 0.20 part of citronellol, 2.40 parts of phenethyl alcohol, 1.40 parts of linalool, 0.10 part of benzyl alcohol, 0.30 part of p-methyl anisole, 0.01 part of p-cresol acetate, 0.15 part of folic acid salicylate, 0.20 part of alpha-ionone, 0.01 part of propyl dodecalactone, 5.00 parts of civet extract, 0.01 part of nerol, 1.00 part of Argentina lemon oil and 30.00 parts of dipropylene glycol.

Preferably, the perfume essence comprises the following raw materials in parts by weight: 0.20 of ambrox, 8.00 of musk T, 8030.15 of sandalwood, 3.00 of methyl hexyl cinnamaldehyde, 1.50 of methyl dihydrojasmonate, 2081.50 of sandalwood, 0.40 of citronellol, 3.50 of phenethyl alcohol, 1.80 of linalool, 0.15 of benzyl alcohol, 0.40 of p-methyl anisole, 0.02 of p-cresol acetate, 0.25 of folic salicylate, 0.60 of alpha-ionone, 0.04 of propyl dodecalactone, 8.00 of civet extract, 0.04 of nerol, 1.6 of Argentina lemon oil and 40.00 of dipropylene glycol.

Preferably, the perfume essence comprises the following raw materials in parts by weight: 0.30 parts of ambrox, 10.00 parts of musk T, 8030.25 parts of sandalwood, 5.00 parts of methyl hexyl cinnamaldehyde, 2.00 parts of methyl dihydrojasmonate, 2082.00 parts of sandalwood, 0.60 part of citronellol, 4.80 parts of phenethyl alcohol, 3.60 parts of linalool, 0.20 part of benzyl alcohol, 0.50 part of p-methyl anisole, 0.05 part of p-cresol acetate, 0.35 part of folic acid salicylate, 1.20 parts of alpha-ionone, 0.05 part of propyl dodecalactone, 10.00 parts of civet extract, 0.05 part of nerol, 2.20 parts of Argentina lemon oil and 49.00 parts of dipropylene glycol.

Preferably, the preparation method of the civet extract comprises the following steps:

(1) mixing civet and ethanol water solution according to the weight ratio of 1: (4-5) uniformly mixing, then performing primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃ respectively, and collecting to obtain a primary molecular distillation distillate, a secondary molecular distillation distillate and a tertiary molecular distillation distillate;

(2) mixing the first-stage molecular distillation distillate, the second-stage molecular distillation distillate and the third-stage molecular distillation distillate according to the weight ratio of 1: (2-4): (5-7) mixing uniformly to obtain the civet extract.

Preferably, in the step (1), the first-stage molecular distillation, the second-stage molecular distillation and the third-stage molecular distillation are carried out in a wiped film type molecular distillation device, wherein the feeding speed is 4-5ml/min, the operating pressure is 5-10Pa, and the wiped film speed is 80-120 r/min.

Preferably, the volume concentration of the ethanol water solution is 80-90%.

A preparation method of perfume essence comprises the following steps:

(1) mixing ambrox, Moschus T, lignum Santali albi 803, radix Clematidis Finetianae extract and dipropylene glycol, dissolving, and stirring;

(2) adding the rest raw materials, stirring, homogenizing under high pressure, standing, and filtering to obtain perfume essence.

The invention has the beneficial effects that:

the ambrox, the musk T, the sandalwood 803, the methyl dihydrojasmonate and the dipropylene glycol are compounded to play a role in fixing fragrance, reduce the loss of effective fragrance components, prolong the long-acting property of the fragrance and improve the storage stability of the essence; the ambrox, the musk T, the sandalwood 803, the sandalwood 208 and the argentine lemon oil are compounded, so that the fragrance of the civet extract can be gained, and the excellent fragrance quality of the perfume essence can be improved. In the preparation process of the civet extract, the molecular distillation method is adopted, the civet extract is obtained by respectively carrying out primary molecular distillation, secondary molecular distillation and tertiary molecular distillation at 50 ℃, 60 ℃ and 80 ℃, and compounding the collected primary molecular distillation distillate, the secondary molecular distillation distillate and the tertiary molecular distillation distillate according to a certain proportion, so that the proportion of high-boiling-point and low-boiling-point aroma substances in the civet extract and the proportion of the aroma substances which have synergistic and gain effects with other components in the essence can be adjusted, the optimal proportion is obtained, the civet extract can be matched with components with a fixed aroma effect in the essence, the long-lasting property of the essence is further improved, and the excellent aroma quality of the perfume essence is better improved. The perfume essence disclosed by the invention not only has the attraction of perfume, but also has good fragrance quality, excellent long-acting property and storage stability, and very good popularization and application values.

Detailed Description