Laboratory research device of three useless base expanded materials of coal-electricity integration
阅读说明：本技术 一种煤电一体化三废基发泡材料的实验室研究装置 (Laboratory research device of three useless base expanded materials of coal-electricity integration ) 是由 万志军 王骏辉 熊路长 武兆鹏 程敬义 刘泗斐 王三伟 曹景轩 王子琦 张超 于 2019-09-30 设计创作，主要内容包括：一种煤电一体化三废基发泡材料的实验室研究装置,水液互驱单元的两个输入端分别与恒流恒压泵的输出端和补液泵的输出端连接,其输出端通过盘管和新型发泡器的液路通道连接；盘管和新型发泡器设置在循环水浴内部,高速摄像机用于采集新型发泡器的泡沫图像；高压储罐分别与气相色谱仪和气体混合罐连接；真空泵与气体混合罐连接；标定气瓶与气体混合罐贯通连接；气体混合罐依次通过电磁减压阀、逆止阀和涡旋式气体流量计与新型发泡器的气动接头连接；混合浆体搅拌器的两个输出支路分别与螺杆泵的进料口和称重器A连接；螺杆泵的出料口与新型发泡器的出料口与三废基发泡材料混合器的两个进料口连接。该装置能为三废基发泡材料的定性定量研究提供基础。(A laboratory research device for coal-electricity integrated three-waste-base foaming materials is characterized in that two input ends of a water-liquid mutual driving unit are respectively connected with an output end of a constant-current and constant-pressure pump and an output end of a liquid supplementing pump, and output ends of the water-liquid mutual driving unit are connected with a liquid channel of a novel foaming device through a coil pipe; the coil pipe and the novel foaming device are arranged in the circulating water bath, and the high-speed camera is used for collecting a foam image of the novel foaming device; the high-pressure storage tank is respectively connected with the gas chromatograph and the gas mixing tank; the vacuum pump is connected with the gas mixing tank; the calibration gas cylinder is communicated with the gas mixing tank; the gas mixing tank is connected with a pneumatic joint of the novel foam maker sequentially through an electromagnetic pressure reducing valve, a check valve and a vortex gas flowmeter; two output branches of the mixed slurry stirrer are respectively connected with a feed inlet of the screw pump and the weighing device A; the discharge port of the screw pump and the discharge port of the novel foaming device are connected with two feed ports of a three-waste-based foaming material mixer. The device can provide a basis for qualitative and quantitative research of the three-waste-based foaming material.)
1. A laboratory research device for a coal-electricity integrated three-waste-base foaming material comprises a coal-electricity integrated three-waste-base foaming material generation device, and is characterized by further comprising a constant-current device for a foaming agent mixed solution, a foam generation and observation device, a smoke component analysis and distribution device and a control console;
the constant flow device of the foaming agent mixed solution comprises a water liquid mutual driving unit, a constant flow and constant pressure pump (2) and a foaming agent solution mixing unit; the water mutual driving unit comprises a first bidirectional piston cylinder (6), a second bidirectional piston cylinder (7) and a plurality of switching valves; the structure of the first bidirectional piston cylinder (6) is the same as that of the second bidirectional piston cylinder (7), a piston which is in sliding sealing fit with the cylinder barrel is arranged in the cylinder barrel, the piston divides an inner cavity of the cylinder barrel into two rodless cavities which are independent from each other, the two rodless cavities are communicated with the outside through a working port A and a working port B which are arranged at two ends of the cylinder barrel respectively, and the first bidirectional piston cylinder (6) and the second bidirectional piston cylinder (7) are respectively provided with a first displacement sensor (3) and a second displacement sensor (5) which are used for detecting the positions of the respective pistons; the plurality of switching valves are a first switching valve (V1), a second switching valve (V2), a third switching valve (V3), a fourth switching valve (V4), a fifth switching valve (V5), a sixth switching valve (V6), a seventh switching valve (V7), and an eighth switching valve (V8), respectively, the switching valve is provided with a working port C and a working port D which are communicated or cut off and matched by control, the working port C of a fourth switching valve (V4) and the working port C of a first switching valve (V1) are communicated with each other and then are used as a water inlet of a water mutual driving unit, the working ports D of the fourth switching valve (V4) and the first switching valve (V1) are respectively connected with the working ports A of a first bidirectional piston cylinder (6) and a second bidirectional piston cylinder (7), the working ports D of a fifth switching valve (V5) and an eighth switching valve (V8) are communicated with each other and then are used as an outlet of the water mutual driving unit, and is connected with one end of an electromagnetic liquid flowmeter A (14) through a one-way valve (13); working ports C of a fifth switching valve (V5) and an eighth switching valve (V8) are respectively connected with working ports B of a first bidirectional piston cylinder (6) and a second bidirectional piston cylinder (7), the working ports C of the second switching valve (V2) and a third switching valve (V3) are both communicated with outside air, the working ports D of the second switching valve (V2) and the third switching valve (V3) are respectively connected with the working ports A of the first bidirectional piston cylinder (6) and the second bidirectional piston cylinder (7), the working ports C of a sixth switching valve (V6) and a seventh switching valve (V7) are respectively connected with the working ports B of the first bidirectional piston cylinder (6) and the second bidirectional piston cylinder (7), and the working ports D of the sixth switching valve (V6) and the seventh switching valve (V7) are communicated with each other and then serve as liquid inlets of a mutual driving unit; a liquid inlet of the constant-current and constant-pressure pump (2) is connected with the bottom of the cold water container (1) through a pipeline, and a liquid outlet of the constant-current and constant-pressure pump is connected with a water inlet of the water liquid mutual driving unit; the foaming agent solution mixing unit comprises a liquid supplementing pump (9), a foaming agent mixed solution storage barrel (10) and a safety valve (8), wherein a liquid inlet of the liquid supplementing pump (9) is connected with the bottom of the foaming agent mixed solution storage barrel (10) through a pipeline, and a liquid outlet of the liquid supplementing pump is connected with a liquid inlet of the water liquid mutual driving unit through the safety valve (8);
the foam generating and observing device comprises a circulating water bath (15), a novel foaming device (20) and a high-speed camera (21); the coil (16) is arranged on one side inside the circulating water bath (15), and one end of the coil (16) is connected with the other end of the electromagnetic liquid flowmeter A (14); the novel foaming device (20) is arranged inside the circulating water bath (15), the top of the novel foaming device (20) is provided with a gas-liquid mixing chamber (40) and a spraying hole (42) for communicating the gas-liquid mixing chamber (40) with the outside, and one side of the gas-liquid mixing chamber (40) is provided with a transparent vertical observation plane (4); the novel foam maker (20) is provided with a liquid path channel (23) positioned at the axis of the novel foam maker and a plurality of gas path channels (24) distributed around the liquid path channel (23) at the part below the gas-liquid mixing chamber (40), the upper end of the liquid path channel (23) is communicated with the gas-liquid mixing chamber (40), and the lower end of the liquid path channel is connected with the other end of the coil pipe (16); the inner end of the gas path channel (24) is communicated with the liquid path channel (23), and the outer end of the gas path channel is connected with the gas outlet end of a pneumatic joint (38) fixedly connected to the outer side of the novel foaming device (20); the ejection hole (42) is connected with the feed end of the heat-preservation pipeline (52); the high-speed camera (21) is erected on the outer side of the novel foaming device (20), and a lens is aligned to the vertical observation plane (4);
the smoke component analysis and gas distribution device comprises a high-pressure storage tank (46), a vacuum pump (48) and a plurality of calibration gas cylinders (45); the high-pressure storage tank (46) stores flue gas discharged by a power plant, and the high-pressure storage tank (46) is respectively connected with the gas chromatograph (44) and the gas mixing tank (47) through pipelines with control valves; the air inlet of the vacuum pump (48) is communicated with the gas mixing tank (47) through a pipeline; the calibration gas cylinder (45) is filled with laboratory standard gas and is communicated with the gas mixing tank (47) through a pipeline with an electromagnetic valve A (69); the gas mixing tank (47) is connected with a main gas transmission pipeline (75), the main gas transmission pipeline (75) is sequentially connected with an electromagnetic pressure reducing valve (50), a check valve (13) and a vortex gas flowmeter (51) in series, and the gas outlet end of the main gas transmission pipeline (75) is respectively connected with the gas inlet end of each pneumatic connector (38) through each gas transmission branch (76) connected with the gas outlet end of the main gas transmission pipeline;
the coal-electricity integrated three-waste-base foaming material generation device comprises a mixed slurry stirrer (55); one output branch of the mixed slurry stirrer (55) is connected with a feed inlet of the screw pump (70), and the other output branch is connected with a weigher A (65) through a quick switch electromagnetic valve A (62); a discharge hole of the screw pump (70) is connected with a feed inlet of a three-waste-based foaming material mixer (61) through an electromagnetic liquid flowmeter B (71); the other feed inlet of the three waste base foaming material mixer (61) is connected with the discharge end of the heat preservation pipeline (52), one output branch of the three waste base foaming material mixer (61) is connected with the weighing device B (63) through a quick switch electromagnetic valve B (72), and the other output branch is connected with the vibration viscometer (64) through an electromagnetic valve B (43);
the console is respectively connected with the constant-current and constant-pressure pump (2), the electromagnetic liquid flow meter A (14), the first switching valve (V1), the second switching valve (V2), the third switching valve (V3), the fourth switching valve (V4), the fifth switching valve (V5), the sixth switching valve (V6), the seventh switching valve (V7), the eighth switching valve (V8), the first displacement sensor (3), the second displacement sensor (5), the high-speed camera (21), the vacuum pump (48), the gas chromatograph (44), the electromagnetic valve A (69), the electromagnetic pressure reducing valve (50), the quick switch electromagnetic valve A (62), the quick switch electromagnetic valve B (72) and the vibration viscometer (64).
2. The laboratory research device of the coal-electricity integrated three waste base foaming material as claimed in claim 1, wherein the constant-current and constant-pressure pump (2) is a plunger type double-cylinder pump, and the output parameter of the constant-current and constant-pressure pump is constant-current liquid of 0-500 ml/min or constant-pressure liquid of 0-150 MPa; the model of the high-speed camera (21) is Phantom Miro LC series.
3. The laboratory research device for the coal-electricity integrated three-waste-base foaming material as claimed in claim 1 or 2, wherein the coil (16) is supported in the circulating water bath (15) longitudinally through a coil support frame (17).
4. The laboratory research device for the coal-electricity integrated three waste base foaming material according to claim 3, wherein the circulating water bath (15) comprises a temperature sensor (18), a heating rod (19), a thermostat (22) and a circulating pump, the temperature sensor (18) and the heating rod (19) are arranged inside the circulating water bath (15), the temperature sensor (18) is connected with the thermostat (22) arranged outside the circulating water bath (15) and used for feeding back the internal temperature of the circulating water bath (15), and the thermostat (22) is connected with the heating rod (19) and used for controlling the heating power of the heating rod (19) according to the fed-back internal temperature; the liquid inlet of the circulating pump is communicated with the bottom of the circulating water bath (15) through a pipeline, and the liquid outlet of the circulating pump is communicated with the upper part of the circulating water bath (15) through a pipeline.
5. The laboratory research device for the coal-electricity integrated three-waste-base foaming material according to claim 4, wherein a baffle (41) which is obliquely arranged is further fixedly connected to the gas-liquid mixing chamber (40), the baffle (41) is located right above the liquid path channel (23), and one end, close to the ejection hole (42), of the baffle (41) is lower than one end, far away from the ejection hole (42), of the baffle (41).
6. The laboratory research device for the coal-electricity integrated three waste base foaming material as claimed in claim 5, wherein two necking sections (39) are arranged at intervals on a section of the upper part of the liquid channel (23), the two necking sections (39) are respectively located above and below the inner end of the gas channel (24), and the necking sections (39) smoothly transition upwards and downwards.
7. The laboratory research device for the coal-electricity integrated three waste base foaming material as claimed in claim 6, wherein the novel foaming device (20) is composed of a mixing body (11), a jetting body A (27), a jetting body B (31) and a bottom supporting body which are sequentially distributed in the longitudinal direction;
the gas-liquid mixing chamber (40) is arranged inside the mixture (11), the vertical observation plane (4) is arranged on one side of the upper part of the mixture (11), and the ejection hole (42) is arranged on one side of the top of the mixture (11) and is positioned above the vertical observation plane (4);
the spraying body A (27) is of a step structure consisting of a large-diameter section (28) located at the upper end and a small-diameter section (67) located below the large-diameter section (28), the spraying body A (27) is provided with a first liquid path (73) which is axially communicated at the axis of the spraying body A, a plurality of first air paths (35) communicated with the first liquid path (73) are arranged on the outer side of the first liquid path (73), each first air path (35) is provided with an inclined section located on the inner side and a horizontal section located on the outer side, the outer side of each inclined section is obliquely arranged in a high-inner-low mode, and included angles between the inclined sections of the plurality of first air paths (35) and the axis of the spraying body A (27) are different; at least one positioning block (30) is arranged on the outer side of the upper part of the small-diameter section (67), and a connecting lug A (12) with external threads is arranged in the center of the lower end of the small-diameter section (67);
a bearing groove (32) matched with the small-diameter section (67) of the ejection body A (27) is formed in the axis of the upper part of the ejection body B (31), and a connecting groove (33) with internal threads is formed in the center of the bottom of the bearing groove (32); the outer side of the upper part of the bearing groove (32) of the ejection body B (31) is provided with a positioning ring groove (49) corresponding to the positioning block (30), a part above the positioning ring groove (49) is provided with a guide vertical groove (54) extending to the upper end surface of the ejection body B (31), the outer side of the upper part of the bearing groove (32) is radially provided with a plurality of second air channels (37) corresponding to the first air channels (35), and the second air channels (37) are communicated with the bearing groove (32) and the outer part of the ejection body B (31); the pneumatic joint (38) is fixedly connected to the outer surface of the ejection body B (31) and is communicated with the outer end of the corresponding second air path (37); the center of the lower end of the ejecting body B (31) is connected with a circular chuck (25) through a cylindrical extension part (66); the center of the bottom of the ejection body B (31) in the connecting groove (33) is provided with a second liquid path (29) extending to the lower end face of the extension part (66);
the bottom support body comprises a base (34) and two base sealing plates (74), the middle part of the base (34) is provided with an inverted T-shaped transverse sliding groove (68) for the circular chuck (25) and the extension part (66) to slide through, the center of the lower end of the base (34) is provided with a connecting convex block B (36) with external threads, and a third liquid path is arranged between the bottom of the transverse sliding groove (68) and the lower end face of the connecting convex block B (36) of the base (34);
the upper end face of the large-diameter section (28) is fixedly connected with the lower end face of the mixing body (11), and the upper end of the first liquid path (73) is communicated with the gas-liquid mixing chamber (40); the small-diameter section (67) is inserted into the bearing groove (32), the connecting lug A (12) is connected with the connecting groove (33) in a threaded fit manner, the large-diameter section (28) is connected with the upper end face of the ejection body B (31) in a bolt manner, a positioning block (30) longitudinally penetrating through the guide vertical groove (54) is in limit fit with the positioning ring groove (49), the outer end of the first air passage (35) is correspondingly connected with the inner end of the second air passage (37) in a penetrating manner, and the lower end of the first liquid passage (73) is correspondingly connected with the upper end of the second liquid passage (29) in a penetrating manner; the circular chuck (25) penetrates into the transverse sliding groove (68) in a sliding manner, and the upper end of the third air channel is communicated with the lower end of the second liquid channel (29); the two base sealing plates (74) are oppositely plugged at two ends of the transverse sliding chute (68) and are fixedly connected with the base (34) through bolts; the connecting lug B (36) is connected to the bottom of the circulating water bath (15) in a threaded fit manner;
the air channel (24) is formed by a first air channel (35) and a second air channel (37) which are communicated, and the liquid channel (23) is formed by a first liquid channel (73), a second liquid channel (29) and a third liquid channel which are communicated in sequence.
8. The laboratory research device of a coal-electric integrated three waste foamed material according to claim 7, characterized in that the screw pump (70) comprises a servo electric cylinder (56), an output end of the servo electric cylinder (56) is connected with one end of a screw shaft (59) through a connecting shaft (57) and a universal joint (58), and the screw shaft (59) is rotatably disposed in the bushing (60).
Technical Field
The invention belongs to the technical field of green mines, and particularly relates to a laboratory research device for a coal-electricity integrated three-waste-base foaming material.
Background
The coal-electricity integration brings huge benefits, meanwhile, the burden of controlling and supervising the power generation cost of coal-electricity enterprises is inevitably increased, the coal-electricity integration integrates mine wastewater, mine high salt water, fly ash, flue gas and other wastes generated in the production of power plants in the production process of a coal mine, the volume is huge, and the local environment is greatly damaged.
The treatment and utilization problems of fly ash, flue gas and high-salt mine water (three wastes of solid, gas and liquid) generated by coal-electricity integration are difficult problems to be solved urgently, the comprehensive utilization degree of the coal-electricity integration waste by the conventional treatment device is low, the method is single and has poor feasibility, and the large-scale popularization and industrial application are not facilitated.
The three-waste-base foaming material is a foaming material produced by recycling ' fly ash-flue gas-high-salt mine water ' solid gas liquid three wastes ' in coal and electricity enterprises and by means of non-standard special equipment and related processes, has strong plastic deformation capacity, certain bearing capacity, strong fluidity and high accumulation, has the characteristics of rapid condensation (adjustable condensation time) and no water seepage, can be used for filling and plugging air leakage at the end of a mine working face and inhibiting coal oxidation fire-extinguishing operation in a mine goaf, and has good application in the aspects of waste mine flue gas and solid waste sealing, building heat-insulating materials, mine guniting materials and the like. However, in the prior art, no device suitable for laboratory research and preparation of three-waste-based foaming materials exists, so that the research on the flow state property of the three-waste-based foaming material under different variable conditions and the research on the physical and mechanical properties of the foaming material after solidification of different flow state properties are inconvenient.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a laboratory research device for a coal-electricity integrated three-waste-based foaming material, which can be used for quickly and efficiently preparing the three-waste-based foaming material by utilizing fly ash, flue gas and a high-salt mine water material, can intelligently monitor the production process of the three-waste-based foaming material, is convenient to obtain characteristic data of the three-waste-based foaming material, can provide a basis for qualitative research on the three-waste-based foaming material, is beneficial to researching the flow state property of the three-waste-based foaming material under different variable conditions and the physical and mechanical properties of the three-waste-based foaming material after the foaming material is solidified, and can guide the preparation and mine application of the three-waste-based foaming material.
The invention provides a laboratory research device for a coal-electricity integrated three-waste-base foaming material, which comprises a coal-electricity integrated three-waste-base foaming material generation device, a constant flow device for a foaming agent mixed solution, a foam generation and observation device, a smoke component analysis and gas distribution device and a control console, wherein the constant flow device is used for generating a foaming agent mixed solution;
the constant flow device of the foaming agent mixed solution comprises a water liquid mutual driving unit, a constant flow and constant pressure pump and a foaming agent solution mixing unit; the water mutual driving unit comprises a first bidirectional piston cylinder, a second bidirectional piston cylinder and a plurality of switching valves; the structure of the first bidirectional piston cylinder is the same as that of the second bidirectional piston cylinder, a piston which is in sliding seal fit with the cylinder barrel is arranged in the cylinder barrel, the piston divides an inner cavity of the cylinder barrel into two rodless cavities which are independent from each other, the two rodless cavities are communicated with the outside through a working port A and a working port B which are arranged at two ends of the cylinder barrel respectively, and the first bidirectional piston cylinder and the second bidirectional piston cylinder are respectively provided with a first displacement sensor and a second displacement sensor which are used for detecting the positions of the respective pistons; the multiple switching valves are respectively a first switching valve, a second switching valve, a third switching valve, a fourth switching valve, a fifth switching valve, a sixth switching valve, a seventh switching valve and an eighth switching valve, the switching valves are provided with a working port C and a working port D which are communicated or cut off and matched through control, the working ports C of the fourth switching valve and the first switching valve are communicated with each other and then used as water inlets of the water liquid mutual driving unit, the working ports D of the fourth switching valve and the first switching valve are respectively connected with the working ports A of the first bidirectional piston cylinder and the second bidirectional piston cylinder, and the working ports D of the fifth switching valve and the eighth switching valve are communicated with each other and then used as outlets of the water liquid mutual driving unit and are connected with one end of the electromagnetic liquid flow meter A through a one-way valve; working ports C of a fifth switching valve and an eighth switching valve are respectively connected with working ports B of a first bidirectional piston cylinder and a second bidirectional piston cylinder, the working ports C of the second switching valve and the third switching valve are both communicated with outside air, the working ports D of the second switching valve and the third switching valve are respectively connected with the working ports A of the first bidirectional piston cylinder and the second bidirectional piston cylinder, the working ports C of a sixth switching valve and a seventh switching valve are respectively connected with the working ports B of the first bidirectional piston cylinder and the second bidirectional piston cylinder, and the working ports D of the sixth switching valve and the seventh switching valve are communicated with each other and then serve as liquid inlets of a water-liquid mutual driving unit; the liquid inlet of the constant-current and constant-pressure pump is connected with the bottom of the cold water container through a pipeline, and the liquid outlet of the constant-current and constant-pressure pump is connected with the water inlet of the water liquid mutual driving unit; the foaming agent solution mixing unit comprises a liquid supplementing pump, a foaming agent mixed solution storage barrel and a safety valve, wherein a liquid inlet of the liquid supplementing pump is connected with the bottom of the foaming agent mixed solution storage barrel through a pipeline, and a liquid outlet of the liquid supplementing pump is connected with a liquid inlet of the water liquid mutual driving unit through the safety valve;
the foam generating and observing device comprises a circulating water bath, a novel foaming device and a high-speed camera; the coil is arranged on one side in the circulating water bath, and one end of the coil is connected with the other end of the electromagnetic liquid flowmeter A; the novel foaming device is arranged in the circulating water bath, a gas-liquid mixing chamber and an ejection hole for communicating the gas-liquid mixing chamber with the outside are arranged at the top of the novel foaming device, and a transparent vertical observation plane is arranged on one side of the gas-liquid mixing chamber; the novel foam maker is provided with a liquid path channel positioned at the axis of the novel foam maker and a plurality of gas path channels distributed around the liquid path channel at the part below the gas-liquid mixing chamber, the upper end of the liquid path channel is communicated with the gas-liquid mixing chamber, and the lower end of the liquid path channel is connected with the other end of the coil pipe; the inner end of the gas path channel is communicated with the liquid path channel, and the outer end of the gas path channel is connected with the gas outlet end of a pneumatic joint fixedly connected to the outer side of the novel foaming device; the ejection hole is connected with the feed end of the heat-insulation pipeline; the high-speed camera is erected outside the novel foaming device, and a lens is aligned to the vertical observation plane;
the smoke component analysis and gas distribution device comprises a high-pressure storage tank, a vacuum pump and a plurality of calibration gas cylinders; the high-pressure storage tank stores flue gas discharged by a power plant, and is respectively connected with the gas chromatograph and the gas mixing tank through pipelines with control valves; the air inlet of the vacuum pump is communicated with the gas mixing tank through a pipeline; the calibration gas cylinder is filled with laboratory standard gas and is communicated with the gas mixing tank through a pipeline with an electromagnetic valve A; the gas mixing tank is connected with a main gas transmission pipeline, an electromagnetic pressure reducing valve, a check valve and a vortex gas flowmeter are sequentially connected on the main gas transmission pipeline in series, and the gas outlet end of the main gas transmission pipeline is respectively connected with the gas inlet end of each pneumatic joint through each gas transmission branch connected with the main gas transmission pipeline;
the coal-electricity integrated three-waste-base foaming material generation device comprises a mixed slurry stirrer; one output branch of the mixed slurry stirrer is connected with a feed inlet of the screw pump, and the other output branch is connected with the weigher A through a quick switch electromagnetic valve A; a discharge port of the screw pump is connected with a feed port of a three-waste-based foaming material mixer through an electromagnetic liquid flowmeter B; the other feed inlet of the three waste base foaming material mixer is connected with the discharge end of the heat preservation pipeline, one output branch of the three waste base foaming material mixer is connected with the weighing device B through a quick switch electromagnetic valve B, and the other output branch is connected with the vibration type viscometer through an electromagnetic valve B;
the console is respectively connected with the constant-current and constant-pressure pump, the electromagnetic liquid flow meter A, the first switching valve, the second switching valve, the third switching valve, the fourth switching valve, the fifth switching valve, the sixth switching valve, the seventh switching valve, the eighth switching valve, the first displacement sensor, the second displacement sensor, the high-speed camera, the vacuum pump, the gas chromatograph, the electromagnetic valve A, the electromagnetic pressure reducing valve, the quick switch electromagnetic valve A, the quick switch electromagnetic valve B and the vibration viscometer.
Preferably, the constant-current and constant-pressure pump is a plunger type double-cylinder pump, and the output parameter of the constant-current and constant-pressure pump is 0-500 ml/min constant-flow liquid or 0-150 MPa constant-pressure liquid; the model of the high-speed camera is Phantom Miro LC series.
Preferably, the coil is supported in the circulating water bath longitudinally through a coil support frame.
Preferably, the circulating water bath comprises a temperature sensor, a heating rod, a temperature controller and a circulating pump, the temperature sensor and the heating rod are arranged inside the circulating water bath, the temperature sensor is connected with the temperature controller arranged outside the circulating water bath and used for feeding back the internal temperature of the circulating water bath, and the temperature controller is connected with the heating rod and used for controlling the heating power of the heating rod according to the fed-back internal temperature; the liquid inlet of the circulating pump is communicated with the bottom of the circulating water bath through a pipeline, and the liquid outlet of the circulating pump is communicated with the upper part of the circulating water bath through a pipeline.
Further, in order to improve the foaming effect, a baffle plate which is obliquely arranged is fixedly connected in the gas-liquid mixing chamber, the baffle plate is positioned right above the liquid path channel, and one end, close to the spraying hole, of the baffle plate is lower than one end, far away from the spraying hole, of the baffle plate. The foam can be retained in the mixing chamber for a longer time through the arrangement of the baffle plate, so that the gas-liquid mixing can be further promoted, and the foaming effect can be improved.
Furthermore, a section of liquid way passageway upper portion is provided with two necking segments with the looks interval, and two necking segments are located the top and the below of gas way passageway inner end respectively, and the necking segment is the equal smooth transition of going up downwards. The arrangement of the two necking sections can ensure that gas and liquid are mixed more fully and complete turbulence can be realized, and the foaming efficiency can be effectively improved.
Further, in order to facilitate assembly and maintenance, the novel foam maker is composed of a mixing body, a spraying body A, a spraying body B and a bottom supporting body which are sequentially distributed in the longitudinal direction;
the gas-liquid mixing chamber is arranged in the mixture, the vertical observation plane is arranged on one side of the upper part of the mixture, and the ejection hole is arranged on one side of the top of the mixture and is positioned above the vertical observation plane;
the spraying body A is of a step structure consisting of a large-diameter section positioned at the upper end and a small-diameter section positioned below the large-diameter section, the spraying body A is provided with a first liquid path which is axially communicated at the axis center, a plurality of first gas paths communicated with the first liquid path are arranged on the outer side of the first liquid path, each first gas path is provided with an inclined section positioned on the inner side and a horizontal section positioned on the outer side, the inclined sections are obliquely arranged in a high-inside-low manner, and the inclined sections of the plurality of first gas paths have different included angles with the axis center line of the spraying body A; the outer side of the upper part of the small-diameter section is provided with at least one positioning block, and the center of the lower end of the small-diameter section is provided with a connecting lug A with external threads;
the axis of the upper part of the ejecting body B is provided with a bearing groove matched with the small-diameter section of the ejecting body A, and the center of the bottom of the bearing groove is provided with a connecting groove with internal threads; the outer side of the upper part of the bearing groove of the ejection body B is provided with a positioning ring groove corresponding to the positioning block, a guide vertical groove extending to the upper end surface of the ejection body B is arranged at the part above the positioning ring groove, the radial direction of the outer side of the upper part of the bearing groove is provided with a plurality of second air passages corresponding to the first air passages, and the second air passages are communicated with the bearing groove and the outer part of the ejection body B; the pneumatic joint is fixedly connected to the outer surface of the ejection body B and is communicated with the outer end of the corresponding second air path; the center of the lower end of the ejection body B is connected with a circular chuck through a cylindrical extension part; the center of the bottom of the connecting groove of the ejecting body B is provided with a second liquid path extending to the lower end face of the extension part;
the bottom support body comprises a base and two base sealing plates, the middle part of the base is provided with an inverted T-shaped transverse chute for the circular chuck and the extension part to pass through in a sliding manner, the center of the lower end of the base is provided with a connecting convex block B with external threads, and a third liquid path is arranged between the bottom of the transverse chute and the lower end face of the connecting convex block B; the setting of base can make things convenient for the change of novel foaming ware blowout hole position, simultaneously, can also make things convenient for the installation of this novel foaming ware on different positions.
The upper end surface of the large-diameter section is fixedly connected with the lower end surface of the mixture body, and the upper end of the first liquid path is communicated with the gas-liquid mixing chamber; the small-diameter section is inserted into the bearing groove, the connecting lug A is connected with the connecting groove in a threaded fit manner, the large-diameter section is connected with the upper end face of the ejecting body B in a bolt manner, the positioning block longitudinally penetrating through the guide vertical groove is in limit fit with the positioning ring groove, the outer end of the first gas path is correspondingly communicated with the inner end of the second gas path, and the lower end of the first liquid path is correspondingly communicated with the upper end of the second liquid path; the circular chuck penetrates into the transverse sliding chute in a sliding manner, and the upper end of the third air passage is communicated with the lower end of the second liquid passage; the two base sealing plates are oppositely plugged at two ends of the transverse sliding chute and are fixedly connected with the base through bolts; the connecting lug B is connected to the bottom of the circulating water bath in a threaded fit manner;
the gas path channel is formed by a first gas path and a second gas path which are communicated, and the liquid path channel is formed by a first liquid path, a second liquid path and a third liquid path which are sequentially communicated.
Preferably, the screw pump includes a servo electric cylinder, an output end of the servo electric cylinder is connected to one end of a screw shaft through a connecting shaft and a universal joint, and the screw shaft is rotatably disposed in the bushing.
The two bidirectional piston cylinders in the water liquid mutual driving unit can realize alternate liquid supplement and liquid discharge under the control of the console, and further can be matched with the constant-current constant-pressure pump and the liquid supplement pump to drive the continuous and stable output of the foaming agent mixed solution by using the liquid in the cold water container as power, thereby effectively ensuring the constant-current or constant-pressure supply of the foaming agent mixed solution and effectively avoiding the influence of pulse fluctuation on the solution output process. In addition, the water liquid mutual driving unit can effectively isolate the acidic foaming agent mixed solution from the constant-current and constant-pressure pump, can prevent the acidic foaming agent mixed solution from corroding the constant-current and constant-pressure pump, and is favorable for prolonging the service life of the constant-current and constant-pressure pump. The coil pipe setting is in the circulation water bath, and then the mixed solution of foamer can preheat fully in the coil pipe and can reach the settlement temperature before the liquid way passageway that gets into novel foaming ware, and novel foaming ware sets up in the circulation water bath equally, and its inside temperature is the settlement temperature, and like this, the foamer mixed solution after preheating can be with the quick foaming of optimum temperature after getting into novel foaming ware is inside, can effectually shorten the foaming time to can improve foaming efficiency. The high-speed camera can collect image data in the gas-liquid mixing chamber in real time and send the image data to the console, so that the console can obtain characteristic data reflecting the size and distribution of foam in real time through an image processing technology. The gas chromatograph in the flue gas component analysis and distribution device can quickly and effectively analyze the components of the flue gas and send the analyzed data to the console, the console can compare the received analysis data with the tested target components and volume quantities, so as to conveniently calculate the components and volume quantities of the gas to be supplemented in the gas mixing tank, and after the calculation is finished, the experimental gas in the corresponding calibration gas cylinder is controlled to be supplemented in the gas mixing tank by controlling the corresponding electromagnetic valve A, so that the quick supplement of the components and volume quantities of the flue gas is realized; gas well proportioned in the gas mixing tank sequentially passes through the electromagnetic pressure reducing valve, the check valve and the vortex gas flowmeter to be supplied to a gas path channel in the novel foaming device, and is finally mixed with foaming agent mixed solution reaching the set temperature in the liquid path channel. The electromagnetic pressure reducing valve can reduce the pressure of the mixed gas in the gas mixing tank and output the mixed gas at a constant flow rate, so that the mixed gas can stably and continuously impact the foaming agent mixed solution entering the liquid path channel, and the foaming efficiency can be further improved. The vortex gas flowmeter can calibrate the flow, so that the stable supply of mixed gas can be further ensured; the check valve can ensure mutual independence of the gas path and the liquid path and cannot influence each other. The screw pump stably outputs the mixed fly ash, cement and treated high-salt mine water to a three-waste-based foaming material mixer, so that the mixed fly ash, cement and treated high-salt mine water can be fully mixed with a foaming material output by a novel foaming device in the three-waste-based foaming material mixer, and the mixed material can be output to a using end for subsequent use. The weighing data can be fed back to the console by the weighing devices A and B, so that the console can calculate the sun gap degree of the foaming material quickly, the viscosity of the foaming material can be measured quickly and in real time by the vibration viscometer, and a foundation can be provided for the performance research of the subsequent foaming material. The invention can reasonably treat the coal-electricity integrated three-waste materials (coal-fired power plant fly ash, coal-fired power plant flue gas and coal mine high-salt mine water) and can effectively recycle the materials. The device can effectively monitor the foam property (size and distribution) and the property (porosity and viscosity) of the three-waste-based foaming material, and can play a guiding role in basic research and data accumulation on the industrial practice and application of the three-waste-based foaming material. Each part in the device can be conveniently disassembled, and the cleaning and the production are convenient.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic diagram of the novel foamer of the present invention;
FIG. 3 is a schematic view showing the assembly of the mixing body and the ejection body A according to the present invention;
FIG. 4 is a schematic view showing the structure of an ejection body B according to the present invention;
FIG. 5 is a schematic view of the structure of the base of the present invention;
FIG. 6 is a schematic view of the base closure plate of the present invention;
FIG. 7 is a flow chart of the preparation of the coal-electricity integrated three-waste-base foaming material.
In the figure: 1. a cold water container, 2, a constant-current and constant-pressure pump, 3, a first displacement sensor, 4, a vertical observation plane, 5, a second displacement sensor, 6, a first bidirectional piston cylinder, 7, a second bidirectional piston cylinder, 8, a safety valve, 9, a liquid supplementing pump, 10, a foaming agent mixed solution storage barrel, 11, a mixture, 12, a connecting lug A, 13, a one-way valve, 14, an electromagnetic liquid flowmeter A, 15, a circulating water bath, 16, a coil, 17, a coil supporting frame, 18, a temperature sensor, 19, a heating rod, 20, a novel foaming device, 21, a high-speed camera, 22, a temperature controller, 23, a liquid channel, 24, an air channel, 25, a circular chuck, 26, a ball, 27, an ejection body A, 28, a large-diameter section, 29, a second liquid channel, 30, a positioning block, 31, an ejection body B, 32, a bearing groove, 33, a connecting groove, 34, A base, 35, a first gas circuit, 36, connecting convex blocks B, 37, a second gas circuit, 38, a pneumatic connector, 39, a necking section, 40, a gas-liquid mixing chamber, 41, a baffle, 42, an ejection hole, 43, a solenoid valve B, 44, a gas chromatograph, 45, a calibration gas cylinder, 46, a high-pressure storage tank, 47, a gas mixing tank, 48, a vacuum pump, 49, a positioning ring groove, 50, an electromagnetic pressure reducing valve, 51, a vortex gas flowmeter, 52, a heat preservation pipeline, 53, a chromatograph calibration bottle, 54, a guide vertical groove, 55, a mixed slurry stirrer, 56, a servo electric cylinder, 57, a connecting shaft, 58, a universal joint, 59, a screw shaft, 60, a bush, 61, a three-waste-based foaming material mixer, 62, a quick-switching solenoid valve A, 63, a weighing device B, 64, a vibratile viscometer, 65, a weighing device A, 66, an extension part, 67, a small-diameter section, 68 and, 69. the system comprises electromagnetic valves A, 70, screw pumps, 71, electromagnetic liquid flow meters B, 72, fast switching electromagnetic valves B, 73, a first liquid path, 74, a base sealing plate, 75, a main gas transmission pipeline, 76 and a gas transmission branch;
v1, a first switching valve, V2, a second switching valve, V3, a third switching valve, V4, a fourth switching valve, V5, a fifth switching valve, V6, a sixth switching valve, V7, a seventh switching valve, V8, and an eighth switching valve.
Detailed Description
The invention will be further explained with reference to the drawings.
As shown in fig. 1, a laboratory research device for a coal-electricity integrated three-waste-base foaming material comprises a coal-electricity integrated three-waste-base foaming material generation device, a constant flow device for a foaming agent mixed solution, a foam generation and observation device, a smoke component analysis and distribution device and a console; preferably, the console is an industrial computer;
the constant flow device of the foaming agent mixed solution comprises a water liquid mutual driving unit, a constant flow and constant pressure pump 2 and a foaming agent solution mixed unit; the water mutual driving unit comprises a first bidirectional piston cylinder 6, a second bidirectional piston cylinder 7 and a plurality of switching valves; the first bidirectional piston cylinder 6 and the second bidirectional piston cylinder 7 have the same structure, a piston which is in sliding seal fit with the cylinder is arranged in the cylinder, the piston divides the inner cavity of the cylinder into two independent rodless cavities which are respectively communicated with the outside through a working port A and a working port B which are arranged at two ends of the cylinder, the first bidirectional piston cylinder 6 and the second bidirectional piston cylinder 7 are respectively provided with a first displacement sensor 3 and a second displacement sensor 5 which are used for detecting the positions of the respective pistons, the displacement sensors are used for collecting position signals in the pistons in the bidirectional piston cylinders, the position of the piston is judged by the console according to the received position signal, and then whether the liquid supplementing state and the liquid injection state are finished or not is judged, so that the console can control the foaming agent mixed solution to be stably output in a constant-current or constant-pressure state; the plurality of switching valves are respectively a first switching valve V1, a second switching valve V2, a third switching valve V3, a fourth switching valve V4, a fifth switching valve V5, a sixth switching valve V6, a seventh switching valve V7 and an eighth switching valve V8, the switching valves are provided with a working port C and a working port D which are communicated or cut off and matched through control, the working ports C of the fourth switching valve V4 and the first switching valve V1 are communicated with each other to be used as water inlets of the water mutual driving unit, the working ports D of the fourth switching valve V4 and the first switching valve V1 are respectively connected with the working ports A of the first bidirectional piston cylinder 6 and the second bidirectional piston cylinder 7, the working ports D of the fifth switching valve V5 and the eighth switching valve V8 are communicated with each other to be used as outlets of the water mutual driving unit, and are connected with one end of an electromagnetic liquid flow meter A14 through a check valve 13; working ports C of the fifth and eighth switching valves V5 and V8 are connected to working ports B of the first and second bidirectional piston cylinders 6 and 7, respectively, working ports C of the second and third switching valves V2 and V3 are communicated with the outside air, working ports D of the second and third switching valves V2 and V3 are connected to working ports a of the first and second bidirectional piston cylinders 6 and 7, respectively, working ports C of the sixth and seventh switching valves V6 and V7 are connected to working ports B of the first and second bidirectional piston cylinders 6 and 7, respectively, and working ports D of the sixth and seventh switching valves V6 and V7 are communicated with each other to serve as liquid inlets of the water hydraulic interdriving unit; the water liquid mutual driving unit can isolate the acidic foaming agent mixed solution from the constant-current and constant-pressure pump 2, can prevent the acidic foaming agent mixed solution from corroding the constant-current and constant-pressure pump 2, and can output the foaming agent mixed solution at constant current or constant pressure by matching with the constant-current and constant-pressure pump 2 and the fluid infusion pump 9; the liquid inlet of the constant-current and constant-pressure pump 2 is connected with the bottom of the cold water container 1 through a pipeline, the liquid outlet of the constant-current and constant-pressure pump is connected with the water inlet of the water liquid mutual driving unit, and the constant-current and constant-pressure pump 2 is used for driving the cold water container to flow; the foaming agent solution mixing unit comprises a liquid supplementing pump 9, a foaming agent mixed solution storage barrel 10 and a safety valve 8, wherein a liquid inlet of the liquid supplementing pump 9 is connected with the bottom of the foaming agent mixed solution storage barrel 10 through a pipeline, and a liquid outlet of the liquid supplementing pump is connected with a liquid inlet of the water liquid mutual driving unit through the safety valve 8; the safety valve 8 can protect the foaming agent solution mixing unit by setting a maximum release pressure. The foaming agent mixed solution storage barrel 10 is used for uniformly mixing the added foaming agent and the treated high-salt mine water according to a certain proportion to form a foaming agent mixed solution, and the foaming agent solution mixing unit is used for supplying the foaming agent mixed solution to a liquid inlet of the water liquid mutual driving unit.
Preferably, the cylinders of the first bidirectional piston cylinder 6 and the second bidirectional piston cylinder 7 are made of 403 stainless steel cylinders.
Preferably, the control process of the first to second switching valves V1 to V8 is: a fluid infusion stage: the console controls the liquid supplementing pump 9 to work to reversely push the foaming agent mixed solution to the two bidirectional piston cylinders of the first bidirectional piston cylinder 6 and the second bidirectional piston cylinder 7, at the moment, the console controls the switching valve to act, and the specific switching valve is in the state as follows: the sixth switching valve V6, the seventh switching valve V7, the second switching valve V2 and the third switching valve V3 are opened, other switching valves are closed, pistons in two piston cylinders reach the upper end, the first displacement sensor 3 and the second displacement sensor 5 send a liquid supplementing completion signal to the console after sensing that the pistons reach the upper end, the console controls the liquid supplementing pump 9 to stop working and the constant-current and constant-pressure pump 2 to work after receiving the liquid supplementing completion signal, and meanwhile, the switching valves are controlled to act, and the states of the specific switching valves are as follows: when the fourth switching valve V4 and the eighth switching valve V8 are opened and the third switching valve V3 and the seventh switching valve V7 are closed, the liquid in the cold water container 1 pumped by the constant-current and constant-pressure pump 2 is supplied to the rodless cavity at one end of the first bidirectional piston cylinder 6, and then the foaming agent mixed solution in the other rodless cavity of the first bidirectional piston cylinder 6 is pushed to the coil pipe 16, and the second bidirectional piston cylinder 7 is in a waiting state in the process. After the first bidirectional piston cylinder 6 finishes injecting liquid, the piston thereof arrives at the lower end, and after the piston arrives the lower end, the first displacement sensor 3 perception sends and annotates liquid and finishes the signal and give the control cabinet, and the control cabinet receives the liquid injection that first displacement sensor 3 sent and finishes the signal and then control the change-over valve action, and the state of specific change-over valve is: the fourth switching valve V4, the eighth switching valve V8, the second switching valve V2 and the sixth switching valve V6 are closed, the third switching valve V3, the seventh switching valve V7, the first switching valve V1 and the fifth switching valve V5 are controlled to work, meanwhile, the fluid infusion pump 9 is controlled to work to infuse fluid into the first bidirectional piston cylinder 6, and the second bidirectional piston cylinder 7 continues to inject fluid into the second bidirectional piston cylinder, in the process, the control console controls the fluid infusion speed of the fluid infusion pump 9 to be higher than the fluid infusion speed of the constant-current constant-pressure pump 2, and the fluid infusion process of the first bidirectional piston cylinder 6 is completed before the fluid infusion process of the second bidirectional piston cylinder 7. And the first bidirectional piston cylinder 6 finishes fluid infusion and is in a standby state, and the first bidirectional piston cylinder 6 and the second bidirectional piston cylinder 7 are alternately injected to ensure stable output of constant current or constant voltage on the same principle.
The foam generating and observing device comprises a circulating water bath 15, a novel foaming device 20 and a high-speed camera 21; the coil pipe 16 is arranged at one side inside the circulating water bath 15, and preferably, the coil pipe 16 is made of 304 stainless steel materials and has the diameter of 6 mm; one end of the coil 16 is connected with the other end of the electromagnetic liquid flowmeter A14; as shown in fig. 2, the novel foaming device 20 is arranged inside the circulating water bath 15, the top of the novel foaming device 20 is provided with a gas-liquid mixing chamber 40 and a spouting hole 42 communicating the gas-liquid mixing chamber 40 with the outside, and one side of the gas-liquid mixing chamber 40 is provided with a transparent vertical observation plane 4; the novel foam maker 20 is provided with a liquid path channel 23 positioned at the axis of the novel foam maker and a plurality of gas path channels 24 distributed around the liquid path channel 23 at the part below the gas-liquid mixing chamber 40, the upper end of the liquid path channel 23 is communicated with the gas-liquid mixing chamber 40, and the lower end of the liquid path channel 23 is connected with the other end of the coil pipe 16; the inner end of the gas path channel 24 is communicated with the liquid path channel 23, and the outer end of the gas path channel is connected with the gas outlet end of a pneumatic joint 38 fixedly connected to the outer side of the novel foaming device 20; the ejection hole 42 is connected with the feeding end of the heat-insulating pipeline 52; the high-speed camera 21 is supported at the outer side of the novel foaming device 20, the lens of the high-speed camera is aligned to the vertical observation plane 4, and the high-speed camera 31 is used for acquiring image data in the gas-liquid mixing chamber 40 in real time and sending the image data to the console in real time; the console processes the received image data to obtain the size and distribution characteristic parameters of the foam generated in the gas-liquid mixing chamber 40; preferably, the outer side of the pipe wall of the thermal insulation pipeline 52 is sequentially coated with an inner tin foil paper layer, a thermal insulation asbestos layer and an outer tin foil paper layer.
The foaming agent mixed solution is injected into the novel foaming device 20 through the coil pipe 16 under the action of the water liquid mutual driving unit, the coil pipe 16 is placed into the circulating water bath 15, the temperature of the foaming agent mixed solution injected into the novel foaming device 20 can be guaranteed to be within a set range, so that the foaming efficiency can be effectively improved, and the foaming time can be effectively shortened.
The flue gas component analyzing and distributing device comprises a high-pressure storage tank 46, a vacuum pump 48 and a plurality of calibration gas cylinders 45, wherein the plurality of calibration gas cylinders 45 are respectively filled with CO2、SO2、N2And NOXAnd the like; the high pressure storage tank 46 stores flue gas discharged by a power plant, specifically, the flue gas is stored in the high pressure storage tank 46 at a pressure of 10MPa, the high pressure storage tank 46 is respectively connected with the gas chromatograph 44 and the gas mixing tank 47 through pipelines with control valves, and as a preferred option, the gas chromatograph 44 is connected with a chromatograph calibration bottle 53. The gas chromatograph 44 is used for analyzing the components of the flue gas and sending the analysis data to the console; the console calculates the components and the volume of the gas to be supplemented in the gas mixing tank 47 according to the analysis data, and controls the corresponding electromagnetic valve A to be opened for a set time according to the calculation result so as to correspondingly calibrate the experiment in the gas cylinder 45The gas is supplemented into the gas mixing tank 47; an air inlet of the vacuum pump 48 is communicated with the gas mixing tank 47 through a pipeline, and the vacuum pump 48 is used for vacuumizing the gas mixing tank 47 so as to conveniently supplement the flue gas component and the volume of the standard laboratory gas in the calibration gas cylinder 45 according to a target value; the calibration gas cylinder 45 is filled with laboratory standard gas with the purity of 99.99 percent and is communicated with the gas mixing tank 47 through a pipeline with an electromagnetic valve A69; the gas mixing tank 47 is connected with a main gas pipeline 75, the main gas pipeline 75 is sequentially connected with an electromagnetic pressure reducing valve 50, a check valve 13 and a vortex gas flowmeter 51 in series, and the gas outlet end of the main gas pipeline 75 is respectively connected with the gas inlet end of each pneumatic connector 38 through each gas transmission branch 76 connected with the main gas pipeline; the electromagnetic pressure reducing valve 50 is used for reducing the pressure of the mixed gas in the gas mixing tank 47 and outputting the mixed gas at a constant flow rate, and the vortex gas flowmeter 51 is used for calibrating the flow rate; the check valve 13 is used for ensuring that the gas path and the liquid path are independent from each other and cannot influence each other.
The flue gas component analysis and distribution device enables the proportioned flue gas of the power plant with pressure to enter the gas channel 24 through the main gas transmission pipeline 75 and the gas transmission branch 76, and then enter the liquid channel 23 to be fully impacted and mixed with the foaming agent mixed solution.
The coal-electricity integrated three-waste-base foaming material generation device comprises a mixed slurry stirrer 55, wherein the mixed slurry stirrer 55 is used for uniformly mixing coal-fired power plant fly ash, ordinary portland cement and treated high-salt mine water to form three-waste-base foaming materials, and stably pumping out the three-waste-base foaming materials; one output branch of the mixed slurry stirrer 55 is connected with a feed inlet of the screw pump 70, and the other output branch is connected with a weigher A65 through a quick switching electromagnetic valve A62; the discharge port of the screw pump 70 is connected with one feed port of the three-waste-based foaming material mixer 61 through an electromagnetic liquid flowmeter B71; the other feed inlet of the three waste base foaming material mixer 61 is connected with the discharge end of the heat preservation pipeline 52, one output branch of the three waste base foaming material mixer 61 is connected with the weighing device B63 through a quick switch electromagnetic valve B72, the other output branch is connected with the vibrating viscometer 64 through an electromagnetic valve B43, and meanwhile, the output branch is used as the using end of the three waste base foaming material; the vibrative viscometer 64 can measure the viscosity data of the three-waste-based foaming material and feed the viscosity data back to the console, the measurement principle is to measure the amplitude change of the vibrative sensor in the liquid, calculate the resistance of the liquid, calculate the viscosity of the liquid and feed the viscosity data back to the console, which belongs to dynamic measurement, and the influence of the mutual offset of two sensor discs makes it possible to measure the viscosity of the flowing sample, which is an advantage compared with the traditional viscometer.
When in work, the console controls the quick switch electromagnetic valve A62 to be opened t2Second at t2The mixed slurry material with the volume V is injected into the weighing device A65 within seconds, and the weighing device A65 measures the weight w of the mixed slurry material2And weighing and feeding back to the console. The console controls the quick switch electromagnetic valve B72 to be opened t1Second at t1Three-waste-based foaming material with the volume of V is injected into the weighing device B63 within seconds, and the weighing device B63 is used for weighing the weight w of the three-waste-based foaming material1Weigh and give to console. Since the degree of tertiary porosity is ((true relative density-apparent relative density)/true phase density) —, and the density is weight/volume, the degree of tertiary porosity is (1-P)%, where,thus, the console averages the weighing data of the weighing machine A65 and the weighing machine B63 according to the weighing data in a plurality of periods of time, and the ratio of the weighing data to the weighing data
The console is respectively connected with the constant-current and constant-pressure pump 2, the electromagnetic liquid flow meter a14, the first switching valve V1, the second switching valve V2, the third switching valve V3, the fourth switching valve V4, the fifth switching valve V5, the sixth switching valve V6, the seventh switching valve V7, the eighth switching valve V8, the first displacement sensor 3, the second displacement sensor 5, the high-speed camera 21, the vacuum pump 48, the gas chromatograph 44, the electromagnetic valve a69, the electromagnetic pressure reducing valve 50, the fast switching electromagnetic valve a62, the fast switching electromagnetic valve B72, and the vibration viscometer 64.
The constant-current and constant-pressure pump 2 is a plunger type double-cylinder pump, and the output parameter of the constant-current and constant-pressure pump is constant-current liquid of 0-500 ml/min or constant-pressure liquid of 0-150 MPa; the high-speed camera 21 is of a Phantom Miro LC series, has the functions of image pickup and photographing, and has a resolution ratio of 1920 x [email protected] frames/second. The high-speed camera 21 is used for shooting the whole process of foam generation in the gas-liquid mixing chamber 40 in the novel foaming device 20, image data shot by the high-speed camera 21 is transmitted to the console in real time, the console can research the size and distribution characteristics of foam under different conditions through image recognition and analysis software after receiving the image data, and analysis results and data can be displayed in real time through a display module connected with the console.
The coil 16 is supported longitudinally inside the circulating water bath 15 by a coil support 17.
The circulating water bath 15 comprises a temperature sensor 18, a heating rod 19, a temperature controller 22 and a circulating pump, the temperature sensor 18 and the heating rod 19 are arranged inside the circulating water bath 15, the temperature sensor 18 is connected with the temperature controller 22 arranged outside the circulating water bath 15 and used for feeding back the internal temperature of the circulating water bath 15, preferably, the temperature sensor 18 adopts a temperature thermocouple PT100, and the temperature controller 22 is connected with the heating rod 19 and used for controlling the heating power of the heating rod 19 according to the fed back internal temperature; the liquid inlet of the circulating pump is communicated with the bottom of the circulating water bath 15 through a pipeline, and the liquid outlet of the circulating pump is communicated with the upper part of the circulating water bath 15 through a pipeline.
The gas-liquid mixing chamber 40 is also fixedly connected with a baffle 41 which is obliquely arranged, the baffle 41 is positioned right above the liquid channel 23, and one end of the baffle 41 close to the ejection hole 42 is lower than one end far away from the ejection hole 42.
One section of liquid way passageway 23 upper portion is provided with two necking segments 39 with looks interval, and two necking segments 39 are located the top and the below of gas way passageway 24 inner end respectively, and necking segment 39 is the equal smooth transition of downward and upward, and the contained angle of necking segment 39 transition and liquid way flow direction is between 90 degrees to 150 degrees to can guarantee that high-pressure flue gas efflux gets into in liquid passageway 23 and impact in the foamer mixed solution completely, thereby realize the intensive mixing of gas-liquid.
The necked-down sections 39 are arranged according to the venturi effect, and the gas outlet end of the gas path channel 24 is located between the two necked-down sections 39, and the angle is in the form of shearing the liquid downwards, so that the gas and the liquid in the liquid path channel 23 can be fully mixed and complete turbulence can be realized.
As shown in fig. 3 to 6, for the convenience of assembly and maintenance, the novel foamer 20 is composed of a mixing body 11, a jetting body a27, a jetting body B31 and a bottom support body which are longitudinally distributed in sequence; like this, if faults such as jam appear can dismantle fast and pertinence is changed a certain part, do not need the whole change, practiced thrift the cost, simultaneously, also made things convenient for the washing to the blowout part, and each part can process alone, reduced the difficulty of monolithic fabrication, this novel foaming ware 20 has overcome shortcomings such as difficult clearance of traditional foaming ware.
The gas-liquid mixing chamber 40 is arranged inside the mixture body 11, the vertical observation plane 4 is arranged on one side of the upper part of the mixture body 11, and the ejection hole 42 is arranged on one side of the top of the mixture body 11 and is positioned above the vertical observation plane 4;
the ejector A27 is a ladder structure composed of a large-diameter section 28 at the upper end and a small-diameter section 67 below the large-diameter section 28, the ejector A27 is provided with a first liquid path 73 which is axially through at the axis, a plurality of first air paths 35 which are communicated with the first liquid path 73 are arranged at the outer side of the first liquid path 73, each first air path 35 is provided with an inclined section which is arranged at the inner side and a horizontal section which is arranged at the outer side, the outer part of the inclined section is arranged in a high-inner-low inclined manner, and the inclined sections of the plurality of first air paths 35 and the axial line of the ejector A27 are different in included angle; at least one positioning block 30 is arranged on the outer side of the upper part of the small-diameter section 67, and a connecting bump A12 with an external thread is arranged in the center of the lower end of the small-diameter section 67;
the axial center of the upper part of the ejecting body B31 is provided with a bearing groove 32 matched with the small-diameter section 67 of the ejecting body A27, and the center of the bottom of the bearing groove 32 is provided with a connecting groove 33 with internal threads; the ejection body B31 is provided with a positioning ring groove 49 corresponding to the positioning block 30 on the outer side of the upper part of the bearing groove 32, a guide vertical groove 54 extending to the upper end surface of the ejection body B31 is arranged on the part above the positioning ring groove 49, a plurality of second air passages 37 corresponding to the first air passages 35 are arranged on the outer side of the upper part of the bearing groove 32 in the radial direction, and the second air passages 37 are communicated with the bearing groove 32 and the outer part of the ejection body B31; the pneumatic joint 38 is fixedly connected to the outer surface of the ejection body B31 and is communicated with the outer end of the corresponding second air path 37; the center of the lower end of the ejecting body B31 is connected with the circular chuck 25 through the cylindrical extension part 66, in order to effectively reduce the friction force, the edge of the circular chuck 25 is provided with the ball 26, the ball 26 can reduce the friction force between the circular chuck 25 and the base 34, so that the adjusting process is smoother, the angle of the speed-adjusting ejecting body B31 relative to the base 34 can be conveniently adjusted, and the ejecting direction of the speed-adjusting ejecting hole 42 can be further adjusted.
The ejector B31 is provided with a second liquid path 29 extending to the lower end face of the extension part 66 at the center of the bottom of the connecting groove 33;
the bottom support comprises a base 34 and two base closing plates 74, wherein the middle part of the base 34 is provided with an inverted T-shaped transverse sliding groove 68 for the circular chuck 25 and the extension part 66 to slide through, the center of the lower end of the base 34 is provided with a connecting lug B36 with external threads, and the part of the base 34 between the bottom of the transverse sliding groove 68 and the lower end surface of the connecting lug B36 is provided with a third liquid path; the setting of base can make things convenient for the change of novel foaming ware blowout hole position, simultaneously, can also make things convenient for the installation of this novel foaming ware on different positions.
The circular chuck 25 is matched with the base 34 in a clamping way, so that the novel foaming device 20 can be conveniently and fixedly installed;
the upper end surface of the large-diameter section 28 is fixedly connected with the lower end surface of the mixture body 11, and the upper end of the first liquid path 73 is communicated with the gas-liquid mixing chamber 40; the small-diameter section 67 is inserted into the bearing groove 32, the connecting bump A12 is connected with the connecting groove 33 in a threaded fit manner, the large-diameter section 28 is connected with the upper end face of the ejection body B31 in a bolt manner, the positioning block 30 longitudinally penetrating through the guide vertical groove 54 is in limit fit with the positioning ring groove 49, the outer end of the first air passage 35 is correspondingly connected with the inner end of the second air passage 37 in a penetrating manner, and the lower end of the first liquid passage 73 is correspondingly connected with the upper end of the second liquid passage 29 in a penetrating manner; the circular chuck 25 penetrates into the transverse sliding groove 68 in a sliding manner, and the upper end of the third air passage is communicated with the lower end of the second liquid passage 29; the two base sealing plates 74 are oppositely plugged at two ends of the transverse sliding groove 68 and fixedly connected with the base 34 through bolts; the connection projection B36 is connected to the bottom of the circulating water bath 15 by screw-fitting so that the novel bubbler 20 is vertically supported inside the circulating water bath 15.
When the sprayer is installed, the positioning blocks 30 are respectively aligned with the guide vertical grooves 54, the positioning blocks 30 enter the positioning ring grooves 49 along the guide vertical grooves 54 so that the spraying bodies A27 are matched and seated in the bearing grooves 32 along the central axis direction of the spraying bodies B31, and then the spraying bodies A27 are rotated so that the positioning blocks 30 move in the positioning ring grooves 49 so that the spraying bodies A27 and the spraying bodies B31 are connected and fixed together.
In order to ensure good sealing performance between the ejection body A27 and the ejection body B31, sealing gaskets are arranged between the lower end face of the large-diameter end 28 and the upper end face of the ejection body B31 and between the connecting bump A12 and the connecting groove 33; because the sealing washer has certain thickness, can provide the pretightning force after fastening and guarantee that gas or liquid can not leak the junction between blowout body A and blowout body B.
The air passage channel 24 is formed by a first air passage 35 and a second air passage 37 which are communicated with each other, and the liquid passage channel 23 is formed by a first liquid passage 73, a second liquid passage 29 and a third liquid passage which are communicated with each other in sequence.
The novel foam maker 20 is composed of a plurality of split parts, so that the assembly and the maintenance are convenient, if faults such as blockage occur, the novel foam maker can be quickly disassembled and a certain part can be replaced in a targeted manner, the integral replacement is not needed, and the cost is saved; the cleaning of each part is convenient; and each part can be processed alone, has reduced the degree of difficulty of whole manufacturing, and this novel foaming ware 20 has overcome shortcomings such as difficult clearance of traditional foaming ware.
The screw pump 70 includes a servo motor cylinder 56, and an output end of the servo motor cylinder 56 is connected to one end of a screw shaft 59 through a connecting shaft 57 and a universal joint 58, the screw shaft 59 being rotatably provided in a bushing 60. In operation of the screw pump 70, the screw 59 rotates on one hand about its axis and on the other hand rolls along the inner surface of the liner 60, thus forming a sealed chamber of the pump. With each revolution of the screw 59, the liquid in the seal cavities of the bushing 60 advances one pitch, and as the screw 59 continues to rotate, the liquid is pressed in a spiral fashion from one seal cavity to the other, eventually extruding the pump body. The screw pump 70 outputs the mixed slurry material at a constant flow, controls the rotating speed through the servo electric cylinder 56, measures the outlet flow through the electromagnetic liquid flow meter B71 to calibrate the flow speed, and simultaneously feeds the flow back to the console through the electromagnetic liquid flow meter B71.
The laboratory preparation and research process of the three-waste-based foaming material by the laboratory research device of the coal-electricity integrated three-waste-based foaming material is as follows, and the main flow is shown in figure 7:
1. three-waste material collection and pretreatment for power plant
Collecting the fly ash of a power plant, carrying out XRF, XRD, SEM and other necessary analyses on the fly ash, knowing the basic physicochemical properties of the fly ash, and screening out the fly ash with the particle size of less than 0.4mm for later use. The high-salinity mine water collected from the mine shaft bottom sump is treated to meet the test standard. Collecting and storing the flue gas of the power plant to an experimental high-pressure storage tank, wherein the pressure is 10 MPa.
2. Flue gas composition analysis and distribution
① the composition and volume of the flue gas from the power plant is analyzed by the gas chromatograph 44 and the data is transmitted to the console to calculate the volumetric amount of the standard gas required to make up to the target value (e.g., CO2: S02: N2: NOX 1:0.5:0.5: 1).
② the vacuum pump 48 vacuumizes the gas mixing tank 47, then the flue gas in the high pressure storage tank 46 is injected into the gas mixing tank 47, and then the flue gas is proportioned by the standard gas in the standard gas bottle 45.
3. Ratio of foaming agent mixed solution
The foaming agent and the treated high-salinity mine water are proportioned, uniformly mixed and then placed into a foaming agent mixed solution storage barrel 10 for standby.
4. Foam generation
① the temperature controller 22 is used to set the temperature of the circulating water bath 15 at 60 deg.C, when the temperature reaches the target value, the foaming agent mixed solution is injected into the new foaming device 20 with a constant flow rate of a ml/min under the control of the console.
② the air channel 24 with 150 degree angle is selected to inject the flue gas into the new type foam maker 20 with the flow rate of b ml/min.
③ the flue gas and the foaming agent mixed solution are fully mixed in the liquid path channel 23, and foam is formed through the two necking sections 39 and the baffle 41, at this time, the foam generation process is recorded by the high-speed camera 21 in the whole process, the image in the process for a certain time is fed back to the console, and the console gives comprehensive evaluation to the size and the characteristics of the foam through the image recognition and analysis technology.
5. Laboratory generation of three waste based foamed materials
Uniformly mixing fly ash, cement, treated high-salt mine water and the like, setting the output rotating speed (corresponding to the flow rate c ml/min) of a servo electric cylinder 56, fully mixing the mixed slurry and foam in a mixed slurry stirrer 55, outputting the mixture through a screw pump 70, fully mixing the mixture with the foam material output by the novel foaming device 20 in a three-waste-based foam material mixer 61, and finally outputting the mixture to a using end of the foam material for use, wherein the output foam material can be used for performing operations such as goaf air leakage blocking, fire prevention, fire extinguishing, filling and sealing.
6. Evaluation of porosity and viscosity of three-waste-base foamed Material
After the three-waste-base foaming material stably flows out from the use end of the foaming material, the console controls the quick switch electromagnetic valve B72 to be opened and closed, and the operations are repeated for a plurality of times to obtain the average weight of the mixed slurry material
The vibratory viscometer 64 can measure the viscosity of the three waste based foaming material and feed back to the console in real time.
7. The image recognition, analysis and evaluation of the foam, the porosity equivalent value P and the viscosity reflect the properties of the three-waste-based foaming material under the test working condition, and the influence of different variables on the foaming material can be researched by changing the test conditions.
8.① types and pH values (acidity, neutrality and alkalinity) of different foaming agents, ② flow rates of different foaming agent solutions when entering a foaming device, ③ temperature (namely environment temperature) of different foaming agent solutions when entering the foaming device, ④ types and volume amounts of belt-pressure flue gas when entering the foaming device, ⑤ pressure and flow rate of belt-pressure flue gas when entering the foaming device, ⑥ angle between an air passage and a liquid passage in the foaming device (namely angle of gas impact liquid), ⑦ proportions of different foaming agent solutions (proportions of foaming agent and water), different slurry proportions (proportions of treated high-salt well water, cement, fly ash and an additive) and ⑧ flow rates of different mixed slurry.
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