阅读说明：本技术 一种高效天然祛味剂及其制备方法 (Efficient natural deodorant and preparation method thereof ) 是由 余孟文 孙慧艳 黄伟 许锡招 鄢雪倩 于 2019-10-17 设计创作，主要内容包括：本发明公开了一种高效天然祛味剂,天然祛味剂由花椒、茶叶、甘蔗、绿巨人、发财树树根、混合花粉、常春藤以及柚皮混合加工而成,所述花椒、茶叶、甘蔗、绿巨人、发财树树根、混合花粉、常春藤以及柚皮配比为5～30：1～10：1～2：0.5～3：1～3：0.5～2：0.5～3：1～2。通过花椒粉、甘蔗粉、茶叶粉及柚皮之间协同增效,可将氨气与硫化氢气体直接分解和吸收,同时可有效抑制臭味源中细菌生长,阻止细菌分解有机物进一步产生臭味,从而大大提高了除臭效率和除臭作用时间。并且,本祛味剂还具有制备工艺简单、不会对环境造成二次污染、不会危害人和宠物健康、不受使用场所限制等优点。(The invention discloses a high-efficiency natural deodorant, which is prepared by mixing and processing pepper, tea, sugarcane, green giant, pachira macrocarpa tree root, mixed pollen, ivy and shaddock peel, wherein the proportion of the pepper, the tea, the sugarcane, the green giant, the pachira tree root, the mixed pollen, the ivy and the shaddock peel is 5-30: 1-10: 1-2: 0.5-3: 1-3: 0.5-2: 0.5-3: 1 to 2. Through synergy among the pepper powder, the sugarcane powder, the tea powder and the pomelo peel, ammonia and hydrogen sulfide gas can be directly decomposed and absorbed, and meanwhile, the growth of bacteria in an odor source can be effectively inhibited, so that the bacteria are prevented from decomposing organic matters to further generate odor, and the deodorization efficiency and the deodorization action time are greatly improved. In addition, the deodorant also has the advantages of simple preparation process, no secondary pollution to the environment, no harm to the health of people and pets, no limitation of use places and the like.)

1. A high-efficiency natural deodorant is characterized in that: the natural deodorant is prepared by mixing and processing pepper, tea, sugarcane, green giant, pachira macrocarpa tree root, mixed pollen, ivy and shaddock peel, wherein the proportion of the pepper, the tea, the sugarcane, the green giant, the pachira macrocarpa tree root, the mixed pollen, the ivy and the shaddock peel is 5-30: 1-10: 1-2: 0.5-3: 1-3: 0.5-2: 0.5-3: 1 to 2.

2. The preparation method of the high-efficiency natural odor-removing agent according to claim 1, characterized in that: the preparation method comprises the following steps:

s1, drying, crushing and screening pepper, tea, sugarcane, green giant, pachira macrocarpa tree root, ivy and shaddock peel in advance to obtain powder for later use;

s2, weighing 10 parts of pepper powder, 3 parts of tea powder, 1 part of sugarcane powder, 0.5 part of green giant powder, 0.5 part of pachira macrocarpa root powder, 1 part of ivy powder and 1 part of pomelo peel powder, placing the materials in a reactor, adding 82 parts of water as a solvent, stirring the materials in the reactor at 70 ℃ in a water bath for 3 hours, and then adding 1 part of mixed pollen into the reactor to be mixed with the solvent;

s3, after the reaction is finished, the feed liquid is sieved by a 200-mesh sieve in advance, the filtrate is taken and centrifuged for 10min at 2000r/min, and then the filtrate is filtered by slow-speed filter paper to obtain the deodorant.

3. The preparation method of the high-efficiency natural odor-removing agent according to claim 1, characterized in that: the mixed pollen is composed of phoenix-tail orchid, Chinese rose flower and morning glory, and the ratio of the phoenix-tail orchid to the Chinese rose flower to the morning glory is (0.25-1): 0.25-1: 0.5-1, drying and crushing the phoenix-tail fern, the Chinese rose and the morning glory, sieving to obtain powder, and stirring by a reactor to mix with the solvent to perform the step S3.

4. The preparation method of the high-efficiency natural odor-removing agent according to claim 3, characterized in that: the powder prepared from the phoenix-tail orchid and the Chinese rose flower is petal powder, and the phoenix-tail orchid and the Chinese rose flower are full-bloomed flowers.

Technical Field

The invention relates to the technical field of preparation of smell removing agents, and particularly relates to a high-efficiency natural smell removing agent and a preparation method thereof.

Background

Along with the improvement of living standard of people, the requirements of people on the comfort, cleanness and sanitation of living environment are improved, and the tolerance to odor is greatly reduced. In daily life, the odor becomes audible everywhere. Such as refuse ponds, toilets, sewers, areas of active pet discharge, and carcasses not promptly cleaned by sanitary pests, etc. There is an increasing demand for deodorants, and various deodorants such as refrigerator deodorants, air fresheners, etc. are coming up.

The existing smell removing agents mainly comprise physical adsorption type, aroma masking type, chemical reagent type and plant type smell removing agents. The physical adsorption type odor removing agent achieves the adsorption effect of odor by utilizing the special structure of an adsorbent material, but the adsorption efficiency is low; the aroma masking type smell remover utilizes aroma concentration to mask off odor and eliminates the odor from human olfactory illusion, but the smell cannot be effectively eliminated, but the secondary pollution of aroma components to air is increased and the harm is caused to human bodies and pet bodies; the chemical agent type smell remover eliminates smell by utilizing the reaction of effective components and odor molecules, has high efficiency, but can cause a large amount of chemical agents to remain in the air and cannot eliminate the chemical agents, thereby causing health hidden troubles.

However, with the deepening of the concept of 'green development', the plant-type smell removing agent has the advantages of environmental friendliness, no toxicity, no harm and the like which are not possessed by the smell removing agent, and is more and more favored by people. Compared with foreign countries, the research of plant-type odor removing agents in China is late, and most of the plant-type odor removing agents have the defects of single use place, complex preparation process, unsatisfactory deodorization efficiency, short deodorization time, no sterilization and bacteriostasis effect and the like.

Disclosure of Invention

Aiming at the defects of the existing smell removing agent, the invention provides an efficient natural smell removing agent and a preparation method thereof, and solves the problems of low smell removing efficiency and incomplete smell removing.

In order to achieve the purpose, the invention provides the following technical scheme: the efficient natural deodorant is prepared by mixing and processing pepper, tea, sugarcane, green giant, pachysandra macrocarpa root, mixed pollen, ivy and shaddock peel, wherein the proportion of the pepper, the tea, the sugarcane, the green giant, the pachysandra macrocarpa root, the mixed pollen, the ivy and the shaddock peel is 5-30: 1-10: 1-2: 0.5-3: 1-3: 0.5-2: 0.5-3: 1 to 2.

Preferably, the preparation method comprises the following steps:

s1, drying, crushing and screening pepper, tea, sugarcane, green giant, pachira macrocarpa tree root, ivy and shaddock peel in advance to obtain powder for later use;

s2, weighing 10 parts of pepper powder, 3 parts of tea powder, 1 part of sugarcane powder, 0.5 part of green giant powder, 0.5 part of pachira macrocarpa root powder, 1 part of ivy powder and 1 part of pomelo peel powder, placing the materials in a reactor, adding 82 parts of water as a solvent, stirring the materials in the reactor at 70 ℃ in a water bath for 3 hours, and then adding 1 part of mixed pollen into the reactor to be mixed with the solvent;

s3, after the reaction is finished, the feed liquid is sieved by a 200-mesh sieve in advance, the filtrate is taken and centrifuged for 10min at 2000r/min, and then the filtrate is filtered by slow-speed filter paper to obtain the deodorant.

Preferably, the mixed pollen consists of phoenix-tail orchid, Chinese rose and morning glory, and the ratio of the phoenix-tail orchid to the Chinese rose to the morning glory is 0.25-1: 0.25-1: 0.5-1, drying and crushing the phoenix-tail fern, the Chinese rose and the morning glory, sieving to obtain powder, and stirring by a reactor to mix with the solvent to perform the step S3.

Preferably, the powder prepared from the phoenix-tail orchid and the Chinese rose flower is petal powder, and the phoenix-tail orchid and the Chinese rose flower are full-bloom flowers.

The beneficial effects are as follows:

according to the efficient natural deodorant and the preparation method, through synergistic interaction among the pepper powder, the sugarcane powder, the tea powder and the pomelo peel, ammonia gas and hydrogen sulfide gas can be directly decomposed and absorbed, meanwhile, the growth of bacteria in an odor source can be effectively inhibited, and the bacteria are prevented from decomposing organic matters to further generate odor, so that the deodorization efficiency and the deodorization action time are greatly improved. In addition, the deodorant also has the advantages of simple preparation process, no secondary pollution to the environment, no harm to the health of people and pets, no limitation of use places and the like.

Detailed Description

All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention provides a technical scheme that: the efficient natural deodorant is prepared by mixing and processing pepper, tea, sugarcane, green giant, pachysandra macrocarpa root, mixed pollen, ivy and shaddock peel, wherein the proportion of the pepper, the tea, the sugarcane, the green giant, the pachysandra macrocarpa root, the mixed pollen, the ivy and the shaddock peel is 5-30: 1-10: 1-2: 0.5-3: 1-3: 0.5-2: 0.5-3: 1 to 2.

The preparation method comprises the following steps:

s1, drying, crushing and screening pepper, tea, sugarcane, green giant, pachira macrocarpa tree root, ivy and shaddock peel in advance to obtain powder for later use;

s2, weighing 10 parts of pepper powder, 3 parts of tea powder, 1 part of sugarcane powder, 0.5 part of green giant powder, 0.5 part of pachira macrocarpa root powder, 1 part of ivy powder and 1 part of pomelo peel powder, placing the materials in a reactor, adding 82 parts of water as a solvent, stirring the materials in the reactor at 70 ℃ in a water bath for 3 hours, and then adding 1 part of mixed pollen into the reactor to be mixed with the solvent;

s3, after the reaction is finished, the feed liquid is sieved by a 200-mesh sieve in advance, the filtrate is taken and centrifuged for 10min at 2000r/min, and then the filtrate is filtered by slow-speed filter paper to obtain the deodorant.

The mixed pollen comprises the phoenix-tail orchid, the Chinese rose and the morning glory, wherein the ratio of the phoenix-tail orchid to the Chinese rose to the morning glory is 0.25-1: 0.25-1: 0.5-1, drying, crushing and sieving the phoenix-tail fern, the Chinese rose and the morning glory (the morning glory can be made of branches and leaves) to obtain powder, stirring the powder by a reactor, and mixing the powder with a solvent to perform the step S3, wherein the plant characteristics of the phoenix-tail fern, the Chinese rose and the morning glory are utilized to dissolve plant molecules into a smell removing agent, so that the speed of the smell removing agent for removing odor is increased.

Wherein, the powder prepared from the phoenix-tail orchid and the Chinese rose flower is petal powder, and the phoenix-tail orchid and the Chinese rose flower are full-bloomed flowers.

Deodorization test method:

1. placing a spray bottle containing a certain amount of sample to be detected (deodorant), a detection instrument (JEK 500-Y-M3) in a started state, a container containing an on-site odor removal source (odor source-ammonia preparation: 50g of ammonia water solution prepared from 0.25g of strong ammonia water, 0.5g of the prepared ammonia water solution in a small centrifugal tube for standby, odor source-hydrogen sulfide preparation: 0.5g of saturated hydrogen sulfide solution in the small centrifugal tube for standby), a culture dish and other articles in a glove test box (length 50cm, width 40cm, height 20cm, small hole in the center of a top cover and electric fan attached inside), and tightly locking and sealing the top cover;

2. placing the culture dish at the middle position of the test box, pouring the odor removal source in the container out of the center of the culture dish, turning on the electric fan for 10 minutes, turning off the electric fan, controlling the ammonia gas concentration in the test box to be about 25mg/m (the hydrogen sulfide concentration is about 4 mg/m) for cultivating after the data measured by the instrument is stable, if the ammonia gas or the hydrogen sulfide concentration measured in the test box is higher than the value, opening an exhaust hole in the top cover of the test box, and injecting air and externally absorbing ammonia gas or hydrogen sulfide gas into the test box by using a 300cc capacity injector so that the ammonia gas concentration in the test box is stable to be about 25mg/m (the hydrogen sulfide concentration is about 4mg/m for full-year);

3. after the reading is stable, spraying 3 times of deodorant on the culture dish and 3 times of deodorant on the specified position of the test box, wherein the spraying is carried out for 6 times, and after 120 minutes of action, cleaning the test box;

4. and (3) calculating the deodorization rate:

。

the bacteriostasis test method comprises the following steps:

1. preparation of bacterial suspension: the test bacteria 24h slant culture was washed with PBS to prepare a bacterial suspension (the number of recovered bacteria was 1X 10)⁴～9×10⁴cfu/mL）

2. Adding 1mL of the bacterial suspension into 9mL of test sample solution (sample to be tested) and PBS (control sample), starting timing, properly diluting 2 ~ 3 dilutions after 20min, sucking 0.5mL of the diluted bacterial suspension respectively, placing the diluted bacterial suspension in a plate, pouring 15mL of soytone agar medium, mixing uniformly, performing turnover culture after agar solidification, performing turnover culture at 35 ℃ for 48h, and counting after the culture is finished.

3. Calculation of the bacteriostatic Rate

X-bacteriostasis rate; a-average colony number of control samples; b-average colony number of test sample.

Detection reference basis: GB/T15979-2002