阅读说明：本技术 一种宠物香波制备方法 (Preparation method of pet shampoo ) 是由 占慧 王乾 于 2019-10-29 设计创作，主要内容包括：本发明公开了一种宠物香波制备方法,包括以下步骤：1)按质量配比称取各原料：聚季铵盐、阴离子表面活性剂、赋酯剂、两性表面活性剂、氨基酸表面活性剂、珠光剂、发用调理剂、保湿剂、柠檬酸、香精、防腐剂、去屑剂、植物提取液和色素；2)将去离子水加入反应釜中,搅拌中加入聚季铵盐、阴离子表面活性剂,再升温至70-85℃,然后加入的赋酯剂,搅拌溶化；3)降温至50-60℃,加入两性表面活性剂、氨基酸表面活性剂、珠光剂、发用调理剂、保湿剂,搅拌均匀；4)降温至40-45℃,加入柠檬酸,通过柠檬酸调节PH值,再加入色素、香精、防腐剂、去屑剂、植物提取液,搅拌均匀；5)使用氯化钠调节粘度；6)制成微胶囊乳状。(The invention discloses a preparation method of pet shampoo, which comprises the following steps: 1) weighing the following raw materials in parts by mass: polyquaternium, anionic surfactant, ester forming agent, amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, humectant, citric acid, essence, antiseptic, dandruff removing agent, plant extract and pigment; 2) adding deionized water into a reaction kettle, adding polyquaternary ammonium salt and anionic surfactant while stirring, heating to 70-85 ℃, adding an ester-forming agent, and stirring to dissolve; 3) cooling to 50-60 deg.C, adding amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring; 4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extract, and stirring; 5) adjusting the viscosity using sodium chloride; 6) making into microcapsule emulsion.)

1. A preparation method of pet shampoo is characterized in that: the method comprises the following steps:

1) weighing the following raw materials in parts by mass: 0.1-1% of polyquaternium, 8.0-20.0% of anionic surfactant, 0.3-2.0% of ester excipient, 3.0-15.0% of amphoteric surfactant, 0.1-5.0% of amino acid surfactant, 0.1-4.0% of pearling agent, 1.0-5.0% of hair conditioner, 1.0-5.0% of humectant, 0.1-1.0% of citric acid, 0.1-2.0% of essence, 0.05-0.3% of preservative, 0.1-1.0% of anti-dandruff agent, 0.1-3.0% of plant extract, 0.01-0.1% of pigment and 33-87% of deionized water, wherein the total mass percentage of the components is 100%;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

2. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the total cooling time from the step 2) to the step 4) is 25-35 minutes.

3. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the pH value range of the citric acid regulated in the step 4 is 6.2-6.8.

4. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the pet shampoo is microcapsule emulsion.

5. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the mass percentages of the raw materials in the steps 2) to 5) are as follows: 0.1% of polyquaternium, 8% of anionic surfactant, 0.3% of ester-forming agent, 3% of amphoteric surfactant, 0.1% of amino acid surfactant, 0.1% of pearling agent, 1% of hair conditioner, 1% of humectant, 0.1% of citric acid, 0.1% of essence, 0.05% of preservative, 0.1% of anti-dandruff agent, 0.1% of plant extract, 0.01% of pigment and 87% of deionized water.

6. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the mass percentages of the raw materials in the steps 2) to 5) are as follows: 0.55% of polyquaternium, 14% of anionic surfactant, 1.15% of ester-forming agent, 8% of amphoteric surfactant, 2.5% of amino acid surfactant, 2% of pearling agent, 3% of hair conditioner, 3% of humectant, 0.5% of citric acid, 1% of essence, 1.05% of preservative, 0.5% of anti-dandruff agent, 1.5% of plant extract, 0.05% of pigment and 60% of deionized water.

7. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the mass ratio of the raw materials in the steps 2) to 5) is as follows: 1% of polyquaternium, 20% of anionic surfactant, 2% of ester forming agent, 15% of amphoteric surfactant, 5% of amino acid surfactant, 4% of pearling agent, 5% of hair conditioner, 5% of humectant, 1% of citric acid, 2% of essence, 0.3% of preservative, 1% of anti-dandruff agent, 3% of plant extract, 0.1% of pigment and 33% of deionized water.

8. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the mass ratio of the raw materials in the steps 2) to 5) is as follows: 0.8% of polyquaternium, 15% of anionic surfactant, 1.5% of ester-forming agent, 10% of amphoteric surfactant, 3% of amino acid surfactant, 1% of pearling agent, 3% of hair conditioner, 2% of humectant, 0.3% of citric acid, 1.5% of essence, 0.1% of preservative, 0.3% of anti-dandruff agent, 2% of plant extract, 0.08% of pigment and 60% of deionized water.

9. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the mass ratio of the raw materials in the steps 2) to 5) is as follows: 0.3% of polyquaternium, 10% of anionic surfactant, 0.6% of ester-forming agent, 7% of amphoteric surfactant, 1.2% of amino acid surfactant, 1% of pearling agent, 4% of hair conditioner, 1.5% of humectant, 0.8% of citric acid, 2% of essence, 0.3% of preservative, 0.5% of anti-dandruff agent, 2% of plant extract, 0.1% of pigment and 69% of deionized water.

10. A method of producing a pet shampoo as defined in claim 1, wherein the method comprises the steps of: the mass ratio of the raw materials in the steps 2) to 5) is as follows: 0.8% of polyquaternium, 17% of anionic surfactant, 1.5% of ester-forming agent, 12% of amphoteric surfactant, 4% of amino acid surfactant, 3% of pearling agent, 4% of hair conditioner, 0.8% of humectant, 1.5% of citric acid, 1.5% of essence, 0.2% of preservative, 0.8% of anti-dandruff agent, 2.5% of plant extract, 0.08% of pigment and 47% of deionized water.

Technical Field

The invention relates to a preparation method of pet shampoo.

Background

The pet shampoo is a product such as soap and shower gel for bathing pets, the traditional shampoo can only play a basic cleaning role on pet hair, deep care is not carried out on the hair, and the hair fragrance of the pet cannot be reserved and can be smelly again after bathing for a period of time, so that a novel pet shampoo is urgently needed to be developed to solve the problem that the smelly again appears after the hair is cleaned in a short time at present.

Disclosure of Invention

The invention aims to solve the technical problem of providing a preparation method of pet shampoo, which is convenient to use, can be suitable for most special pet hair, can deeply repair the pet hair, condition, moisten and restore the original hair color of the pet, increase the shining luster, eliminate the odor generated on the pet body, improve the surrounding environment of the pet, keep the fragrance of the pet hair for a long time, and has practicability and wide application.

In order to solve the problems, the invention adopts the following technical scheme:

a preparation method of pet shampoo comprises the following steps:

1) weighing the following raw materials in parts by mass: 0.1-1% of polyquaternium, 8.0-20.0% of anionic surfactant, 0.3-2.0% of ester excipient, 3.0-15.0% of amphoteric surfactant, 0.1-5.0% of amino acid surfactant, 0.1-4.0% of pearling agent, 1.0-5.0% of hair conditioner, 1.0-5.0% of humectant, 0.1-1.0% of citric acid, 0.1-2.0% of essence, 0.05-0.3% of preservative, 0.1-1.0% of anti-dandruff agent, 0.1-3.0% of plant extract, 0.01-0.1% of pigment and 33-87% of deionized water, wherein the total mass percentage of the components is 100%;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

As a preferable technical scheme, the total temperature reduction time from the step 2) to the step 4) is 25-35 minutes.

Preferably, the pH value after citric acid adjustment in the step 4 is 6.2-6.8.

As a preferred technical scheme, the pet shampoo is microcapsule emulsion.

As a preferred technical scheme, the mass percentages of the raw materials in the steps 2) to 5) are as follows: 0.1% of polyquaternium, 8% of anionic surfactant, 0.3% of ester-forming agent, 3% of amphoteric surfactant, 0.1% of amino acid surfactant, 0.1% of pearling agent, 1% of hair conditioner, 1% of humectant, 0.1% of citric acid, 0.1% of essence, 0.05% of preservative, 0.1% of anti-dandruff agent, 0.1% of plant extract, 0.01% of pigment and 87% of deionized water.

As a preferred technical scheme, the mass percentages of the raw materials in the steps 2) to 5) are as follows: 0.55% of polyquaternium, 14% of anionic surfactant, 1.15% of ester-forming agent, 8% of amphoteric surfactant, 2.5% of amino acid surfactant, 2% of pearling agent, 3% of hair conditioner, 3% of humectant, 0.5% of citric acid, 1% of essence, 1.05% of preservative, 0.5% of anti-dandruff agent, 1.5% of plant extract, 0.05% of pigment and 60% of deionized water.

As a preferable technical scheme, the mass ratio of the raw materials in the steps 2) to 5) is as follows: 1% of polyquaternium, 20% of anionic surfactant, 2% of ester forming agent, 15% of amphoteric surfactant, 5% of amino acid surfactant, 4% of pearling agent, 5% of hair conditioner, 5% of humectant, 1% of citric acid, 2% of essence, 0.3% of preservative, 1% of anti-dandruff agent, 3% of plant extract, 0.1% of pigment and 33% of deionized water.

As a preferable technical scheme, the mass ratio of the raw materials in the steps 2) to 5) is as follows: 0.8% of polyquaternium, 15% of anionic surfactant, 1.5% of ester-forming agent, 10% of amphoteric surfactant, 3% of amino acid surfactant, 1% of pearling agent, 3% of hair conditioner, 2% of humectant, 0.3% of citric acid, 1.5% of essence, 0.1% of preservative, 0.3% of anti-dandruff agent, 2% of plant extract, 0.08% of pigment and 60% of deionized water.

As a preferable technical scheme, the mass ratio of the raw materials in the steps 2) to 5) is as follows: 0.3% of polyquaternium, 10% of anionic surfactant, 0.6% of ester-forming agent, 7% of amphoteric surfactant, 1.2% of amino acid surfactant, 1% of pearling agent, 4% of hair conditioner, 1.5% of humectant, 0.8% of citric acid, 2% of essence, 0.3% of preservative, 0.5% of anti-dandruff agent, 2% of plant extract, 0.1% of pigment and 69% of deionized water.

As a preferable technical scheme, the mass ratio of the raw materials in the steps 2) to 5) is as follows: 0.8% of polyquaternium, 17% of anionic surfactant, 1.5% of ester-forming agent, 12% of amphoteric surfactant, 4% of amino acid surfactant, 3% of pearling agent, 4% of hair conditioner, 0.8% of humectant, 1.5% of citric acid, 1.5% of essence, 0.2% of preservative, 0.8% of anti-dandruff agent, 2.5% of plant extract, 0.08% of pigment and 47% of deionized water.

The invention has the beneficial effects that:

1. is convenient to use, can be suitable for most special pet hair, can repair the deep layer of the pet hair, condition and moisten the pet hair to restore the original hair color of the pet and increase the shining luster,

2. can eliminate the odor generated on the pet body, improve the surrounding environment of the pet, and simultaneously, the hair of the pet can keep the faint scent for a long time.

3. When the pet and the owner knead the hair, the fragrance can burst instantly and maintain the hair for a long time, thereby greatly improving the competitiveness of the product.

Detailed Description

A preparation method of pet shampoo comprises the following steps:

1) weighing the following raw materials in parts by mass: 0.1-1% of polyquaternium, 8.0-20.0% of anionic surfactant, 0.3-2.0% of ester excipient, 3.0-15.0% of amphoteric surfactant, 0.1-5.0% of amino acid surfactant, 0.1-4.0% of pearling agent, 1.0-5.0% of hair conditioner, 1.0-5.0% of humectant, 0.1-1.0% of citric acid, 0.1-2.0% of essence, 0.05-0.3% of preservative, 0.1-1.0% of anti-dandruff agent, 0.1-3.0% of plant extract, 0.01-0.1% of pigment and 33-87% of deionized water, wherein the total mass percentage of the components is 100%;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, the viscosity is adjusted by using a proper percentage of sodium chloride.

6) Making into microcapsule emulsion, sealing and packaging.

The total cooling time from the step 2) to the step 4) is 25-35 minutes.

The pH value range of the citric acid regulated in the step 4 is 6.2-6.8.

The pet shampoo is microcapsule emulsion.

The first embodiment of the invention:

1) weighing the following raw materials in parts by mass: 0.1% of polyquaternium, 8% of anionic surfactant, 0.3% of ester-forming agent, 3% of amphoteric surfactant, 0.1% of amino acid surfactant, 0.1% of pearling agent, 1% of hair conditioner, 1% of humectant, 0.1% of citric acid, 0.1% of essence, 0.05% of preservative, 0.1% of anti-dandruff agent, 0.1% of plant extract, 0.01% of pigment and 87% of deionized water;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

Embodiment two of the present invention:

1) weighing the following raw materials in parts by mass: 0.3% of polyquaternium, 10% of anionic surfactant, 0.6% of ester-forming agent, 7% of amphoteric surfactant, 1.2% of amino acid surfactant, 1% of pearling agent, 4% of hair conditioner, 1.5% of humectant, 0.8% of citric acid, 2% of essence, 0.3% of preservative, 0.5% of anti-dandruff agent, 2% of plant extract, 0.1% of pigment and 69% of deionized water;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

The third embodiment of the invention:

1) weighing the following raw materials in parts by mass: 0.55% of polyquaternium, 14% of anionic surfactant, 1.15% of ester-forming agent, 8% of amphoteric surfactant, 2.5% of amino acid surfactant, 2% of pearling agent, 3% of hair conditioner, 3% of humectant, 0.5% of citric acid, 1% of essence, 0.05% of preservative, 0.5% of anti-dandruff agent, 1.5% of plant extract, 0.05% of pigment and 60% of deionized water;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

The fourth embodiment of the invention:

1) weighing the following raw materials in parts by mass: 0.8% of polyquaternium, 15% of anionic surfactant, 1.5% of ester-forming agent, 10% of amphoteric surfactant, 3% of amino acid surfactant, 1% of pearling agent, 3% of hair conditioner, 2% of humectant, 0.3% of citric acid, 1.5% of essence, 0.1% of preservative, 0.3% of anti-dandruff agent, 2% of plant extract, 0.08% of pigment and 60% of deionized water;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

Example five of the present invention:

1) weighing the following raw materials in parts by mass: 0.8% of polyquaternium, 17% of anionic surfactant, 1.5% of ester-forming agent, 12% of amphoteric surfactant, 4% of amino acid surfactant, 3% of pearling agent, 4% of hair conditioner, 0.8% of humectant, 1.5% of citric acid, 1.5% of essence, 0.2% of preservative, 0.8% of anti-dandruff agent, 2.5% of plant extract, 0.08% of pigment and 47% of deionized water;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

Example six of the present invention:

1) weighing the following raw materials in parts by mass: 1% of polyquaternium, 20% of anionic surfactant, 2% of ester forming agent, 15% of amphoteric surfactant, 5% of amino acid surfactant, 4% of pearling agent, 5% of hair conditioner, 5% of humectant, 1% of citric acid, 2% of essence, 0.3% of preservative, 1% of anti-dandruff agent, 3% of plant extract, 0.1% of pigment and 33% of deionized water;

2) adding a proper amount of deionized water into a reaction kettle, starting stirring, adding a proper amount of polyquaternium and anionic surfactant in percentage while stirring, heating to 70-85 ℃, then adding a proper amount of ester-forming agent in percentage, and stirring for dissolving;

3) cooling to 50-60 deg.C, adding appropriate amount of amphoteric surfactant, amino acid surfactant, pearling agent, hair conditioner, and humectant, and stirring;

4) cooling to 40-45 deg.C, adding citric acid, regulating pH with citric acid, adding pigment, essence, antiseptic, dandruff remover, and plant extractive solution, and stirring;

5) finally, adjusting the viscosity by using a proper amount of sodium chloride;

6) making into microcapsule emulsion, sealing and packaging.

When the invention is manufactured, the following matters are noted:

firstly, the production workshop is kept clean and tidy, and pollution is prevented when the product is manufactured;

weighing the raw materials according to the raw material ratio catalog and the mass ratio;

thirdly, controlling the stirring time and the stirring speed according to the raw material ratio;

fourthly, controlling the temperature and paying attention to the raw materials added at different temperature sections;

and fifthly, the product is stored in a sealed manner, so that the fragrance loss is prevented.

In the production process of the product, the stirring speed is generally 20-40 revolutions per minute, the time is 10-30 minutes, the rotating speed is strictly controlled, and a large amount of bubbles are prevented from being generated in the stirring process.

After trial and detection, the pet hair cleaned by the cleaning agent can keep the fragrance for 5-10 days.

The above is only a specific embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that are not thought of through the inventive work should be included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope defined by the claims.