阅读说明：本技术 活体生物诱生负氧离子的方法及应用、负氧离子涂料、远红外负氧离子粉、制备方法 (Method for inducing negative oxygen ions by living organisms and application thereof, negative oxygen ion coating, far infrared negative oxygen ion powder and preparation method ) 是由 王龙 于 2021-08-13 设计创作，主要内容包括：本发明公开了一种活体生物诱生负氧离子的方法及应用、负氧离子涂料、远红外负氧离子粉、制备方法,活体生物诱生负氧离子的方法,包括以下步骤：将以下重量份的组分混合得到叶面肥：独居石粉浸泡液45-55份、复合氨基酸1-4份、复合维生素5-8份、叶绿素提取物25-33份、古法中药煅烧炮制钍8-10份以及固氮剂0.4-1.2份；将叶面肥喷洒于桑树叶面上,叶面无明显水后摘取桑叶喂养蚕,收集蚕沙和蚕蛹；将蚕茧用盐水煮开成丝,将蚕丝分解萃取干燥得到蚕丝蛋白粉；能够降低所需蛋白粉中放射性元素的含量,得到的蚕丝蛋白粉、蚕沙以及蚕蛹还能释放负氧离子,增加了空气中负氧离子的浓度,有利于人体的健康。(The invention discloses a method for living organisms to induce negative oxygen ions and application thereof, a negative oxygen ion coating, far infrared negative oxygen ion powder and a preparation method thereof, and the method for living organisms to induce negative oxygen ions comprises the following steps: mixing the following components in parts by weight to obtain the foliar fertilizer: 45-55 parts of monazite powder soaking solution, 1-4 parts of compound amino acid, 5-8 parts of compound vitamin, 25-33 parts of chlorophyll extract, 8-10 parts of thorium prepared by calcining ancient Chinese medicines and 0.4-1.2 parts of nitrogen fixing agent; spraying a leaf fertilizer on the leaf surfaces of the mulberry trees, picking up the mulberry leaves after no obvious water exists on the leaf surfaces, feeding silkworms, and collecting silkworm excrement and silkworm pupas; boiling silkworm cocoons into silk by using saline water, and decomposing, extracting and drying the silk to obtain silk protein powder; the content of radioactive elements in the required protein powder can be reduced, the obtained silk protein powder, silkworm excrement and silkworm pupa can release negative oxygen ions, the concentration of the negative oxygen ions in the air is increased, and the health of a human body is facilitated.)

1. A method for inducing negative oxygen ions by living organisms is characterized by comprising the following steps:

extracting chlorophyll: mixing folium Mori, herba Taraxaci, folium Lactucae Sativae, oak leaf, caulis et folium Lactucae Sativae, folium Luffae, Lycii folium and leaf of Brassica Oleracea, and extracting chlorophyll to obtain chlorophyll extract;

preparing a mulberry planting foliar fertilizer: mixing the following components in parts by weight: 45-55 parts of monazite powder soaking solution, 1-4 parts of compound amino acid, 5-8 parts of compound vitamin, 25-33 parts of chlorophyll extract, 8-10 parts of thorium prepared by calcining ancient Chinese medicines and 0.4-1.2 parts of nitrogen fixing agent;

spraying a leaf fertilizer on the leaf surfaces of the mulberry trees, picking up the mulberry leaves after no obvious water exists on the leaf surfaces, feeding silkworms, and collecting silkworm excrement and silkworm pupas;

boiling silkworm cocoons into silk by using brine, and decomposing, extracting and drying the silk to obtain the silk protein powder.

2. The method as claimed in claim 1, wherein the foliar fertilizer is sprayed on the mulberry foliar surface in the morning.

3. The method as claimed in claim 1 or 2, wherein the mulberry leaves are extracted for 16:00 to 18: 00.

4. The method as claimed in claim 1, wherein preparing the mulberry planting foliar fertilizer: mixing the following components in parts by weight: 50 parts of monazite powder soaking solution, 3 parts of compound amino acid, 7 parts of compound vitamin, 30 parts of chlorophyll extract, 9.5 parts of thorium prepared by calcining ancient Chinese medicines and 0.5 part of nitrogen fixing agent.

5. The negative oxygen ion coating is characterized by comprising the following components in parts by weight: 7-15 parts of sterol, 0.1-0.5 part of yeast, 1-3 parts of pine needle extracting solution, 5-10 parts of radix puerariae powder, 50-60 parts of silver ion-containing powder, 1-3 parts of silk protein powder prepared according to claim 1, 2-5 parts of titanium dioxide powder and 0.8-2 parts of shell powder.

6. The method for preparing the negative oxygen ion coating according to claim 5, comprising the steps of:

mixing sterol, yeast, folium Pini extractive solution, radix Puerariae powder, silver ion-containing powder and fibroin powder, and fermenting for 18-25 hr to obtain fermentation broth;

adding titanium dioxide powder into the fermentation liquor, uniformly stirring, drying to obtain powder, and then adding shell powder and grinding.

7. The method according to claim 6, wherein the particle size of the negative oxygen ion coating material is 2000 mesh.

8. The far infrared negative oxygen ion powder is characterized by comprising the following components in parts by weight: 5-10 parts of silkworm excrement prepared by the method of claim 1, 3-5 parts of silkworm chrysalis prepared by the method of claim 1, 1-5 parts of liquorice, 3-8 parts of dried ginger, 5-9 parts of cinnamon, 1-3 parts of anise, 2-5 parts of bay leaves, 6-9 parts of fennel, 3-7 parts of clove, 60-70 parts of far infrared ceramic powder, 0.5-2 parts of bamboo salt and 0.01-0.03 part of sulfur.

9. The method for preparing far infrared negative oxygen ion powder according to claim 8, comprising the steps of:

mixing faeces Bombycis, pupa Bombycis, Glycyrrhrizae radix, Zingiberis rhizoma, cortex Cinnamomi, fructus Anisi Stellati, folium Neocinnamomi Delavayi, fructus Foeniculi, flos Caryophylli and Sulfur, calcining into powder to obtain base powder;

mixing the base powder, bamboo salt and far infrared ceramic powder, and grinding into powder.

10. An application of the silk protein powder prepared by the method of claim 1 in the textile field.

Technical Field

The invention belongs to the technical field of negative oxygen ions, and particularly relates to a method for inducing negative oxygen ions by living organisms, application of the method, a negative oxygen ion coating, far infrared negative oxygen ion powder and a preparation method.

Background

The negative ion is a gas ion with negative charge in the air. In a natural ecosystem, forests and wetlands are important places for generating negative ions.

The negative ions are called as 'air vitamins', and are considered to have important functions on human bodies like vitamins.

At present, the health care pillow mainly has two main functions, namely recuperation and health care, and air optimization.

The negative ions can actively attack and capture small-particle dust particles, so that the small-particle dust particles are condensed and precipitated, and the harm of PM2.5 to human health can be effectively reduced. Research shows that the concentration of negative oxygen ions is in positive correlation with human health, and the product has health care effect on human body. According to related researches, the negative ions have the effects of calming, inhibiting, relieving and assisting in treating more than 30 diseases of 7 systems of human bodies, and particularly have more obvious health-care effect on the human bodies.

Improving the function of natural killer cells which can destroy cancer cells, and inhibiting the occurrence and progression of cancer;

can improve and increase lung function, and increase lung capacity; obviously dilate blood vessels, relieve arterial vasospasm, effectively improve angina and restore normal blood pressure; the blood is slowed down, the blood coagulation time is prolonged, the oxygen content in the blood is increased, and the blood oxygen transportation, absorption and utilization are facilitated; effectively improving the function of cerebral cortex, revivifying, eliminating fatigue, improving sleep and increasing appetite; can inhibit serum cholesterol, activate macrophage for blood purification, and prevent fat deposition on blood vessel wall; inhibiting leukotrienes that cause allergic or inflammatory symptoms; inhibiting adrenalin, dilating peripheral blood vessel, improving blood circulation, and stabilizing blood pressure; preventing arterialization or liver disorders; promoting metabolism, enhancing immunity, improving body muscle energy, and regulating body function balance.

The existing methods for generating negative oxygen ions include the following types: the first type: tourmaline ore, such as hexacyclic stone, has the advantages of generating negative ions, improving air quality, generating 1000 negative ions per cubic centimeter generally, and generating more negative ions.

The second type: negative ion electromagnetic generator products, namely, negative ion air purifiers or negative ion generators commonly on the market, are generally powered. The principle is that the low voltage is increased to the direct current negative high voltage, a large amount of electrons are released into the air, and the electrons (which cannot exist stably in the air) can be captured by oxygen molecules to form negative oxygen ions; the disadvantages are as follows: the negative ions are generated and ozone is generated at the same time, so that the human organs can be injured by breathing.

In the third category: the outer layer electrons of gas or atoms in the air escape to form positively charged positive ions, and the escaped electrons combine with neutral molecules to form negative ions in the air, and combine with oxygen to form negative oxygen ions, which are only present in theory and not actually used.

Disclosure of Invention

The invention aims at the problems of the existing negative ion generation mode, and provides a method for biologically inducing negative oxygen ions in a living body.

The invention adopts the following technical scheme: a method for in vivo biological induction of negative oxygen ions, comprising the steps of: extracting chlorophyll: mixing folium Mori, herba Taraxaci, folium Lactucae Sativae, oak leaf, caulis et folium Lactucae Sativae, folium Luffae, Lycii folium and leaf of Brassica Oleracea, and extracting chlorophyll to obtain chlorophyll extract;

preparing a mulberry planting foliar fertilizer: mixing the following components in parts by weight: 45-55 parts of monazite powder soaking solution, 1-4 parts of compound amino acid, 5-8 parts of compound vitamin, 25-33 parts of chlorophyll extract, 8-10 parts of thorium prepared by calcining ancient Chinese medicines and 0.4-1.2 parts of nitrogen fixing agent;

spraying a leaf fertilizer on the leaf surfaces of the mulberry trees, picking up the mulberry leaves after no obvious water exists on the leaf surfaces, feeding silkworms, and collecting silkworm excrement and silkworm pupas;

boiling silkworm cocoons into silk by using brine, and decomposing, extracting and drying the silk to obtain the silk protein powder.

The preparation method of thorium processed by calcining ancient traditional Chinese medicines comprises the following steps:

s1: parching thorium material into tabasheer, sieving to remove slag salt and sand, placing into a pot, heating, spraying water, instantly generating transpiration gas, oxygen stewing for 15 min, opening the pot, adding fermented oxalic acid water soaked by traditional Chinese medicine in advance, to obtain mixture; the preparation method of the fermented oxalic acid water comprises the following steps: 100g of each of liquorice, dried ginger, angelica dahurica and wormwood, 1g of sodium bicarbonate, 20g of beer yeast powder and 2.5kg of water are added to ferment into acid water, and then 250ml of vinegar is added;

s2: grinding the mixture, pouring the suspension on the upper part, then continuously grinding the coarse powder deposited on the lower part, repeating the operation until the fine powder is residue-free, and obtaining the processed thorium;

s3: 1000g of soaked soybeans and the processed thorium are ground into soybean milk, gypsum is added into the soybean milk to be dried in the sun, and the soybean milk is ground into white powder for later use, wherein the white powder is prepared by calcining the thorium by an ancient method.

Further limiting, the foliar fertilizer is sprayed on the leaf surfaces of the mulberry trees in the morning.

Further limiting, the mulberry leaf picking time is 16:00-18: 00.

Further limiting, preparing the mulberry planting foliar fertilizer: mixing the following components in parts by weight: 50 parts of monazite powder soaking solution, 3 parts of compound amino acid, 7 parts of compound vitamin, 30 parts of chlorophyll extract, 9.5 parts of thorium prepared by calcining ancient Chinese medicines and 0.5 part of nitrogen fixing agent.

The invention has the beneficial effects that: the chlorophyll extract is obtained by extracting chlorophyll of a plant, and is mixed with monazite powder soaking solution, compound amino acid, compound vitamin, the chlorophyll extract, thorium calcined and processed by an ancient method traditional Chinese medicine and a nitrogen fixing agent to be used as a leaf fertilizer of mulberry leaves, the obtained mulberry leaves are fed to silkworms, and the compound amino acid, the compound vitamin and the chlorophyll extract can reduce the side effect of the monazite powder soaking solution and the thorium calcined and processed by the ancient method traditional Chinese medicine on the silkworms; the prepared silkworm excrement, silkworm chrysalis and silk protein powder can be used as negative ion generation raw materials and used for improving the concentration of negative oxygen ions in air; and the content of radioactive sources in the silk protein powder meets the national standard (GB6566-2010, or 0.5) through biological chain conversion, and the prepared silk protein powder also has the functions of bacteriostasis and sterilization and is used for manufacturing melt-blown cloth.

The invention also discloses a negative oxygen ion coating which comprises the following components in parts by weight: 7-15 parts of sterol, 0.1-0.5 part of yeast, 1-3 parts of pine needle extracting solution, 5-10 parts of radix puerariae powder, 50-60 parts of silver ion-containing powder, 1-3 parts of silk protein powder prepared by the above steps, 2-5 parts of titanium dioxide powder and 0.8-2 parts of shell powder.

The silk protein powder is used as a radioactive source, chloroplast photo-energy storage, the titanium dioxide powder and the shell powder are synthesized into an electric conductor, the pine needle extracting solution provides biological enzyme and air catalytic carrier change, the dispersion and concentrated radiation is realized, the sterol radioactive tip radiation ionization conductor generates negative oxygen ions under the action of oxygen atoms in the air.

The invention also discloses a preparation method of the negative oxygen ion coating, which comprises the following steps:

mixing sterol, yeast, folium Pini extractive solution, radix Puerariae powder, silver ion-containing powder and fibroin powder, and fermenting for 18-25 hr to obtain fermentation broth;

adding titanium dioxide powder into the fermentation liquor, uniformly stirring, drying to obtain powder, and then adding shell powder and grinding.

Further defined, the particle size of the negative oxygen ion coating is 2000 meshes.

The invention has the beneficial effects that: according to the invention, the silk protein powder is added, and is mixed with sterol, yeast, pine needle extract, radix puerariae powder and silver ion-containing powder for fermentation to release negative oxygen ions, 1260 per cubic centimeter are still detected at a detection distance of 14 meters, and more than 8 ten thousand are close to the surface; the titanium dioxide powder has the effect of assisting in degrading air formaldehyde; the enzyme action in the negative oxygen ion coating is to utilize enzyme catalysis to realize the change between the light energy storage carrier and the air, disperse the light energy storage carrier to the concentrated radiation ionization, dry in nature in the way that the resin absorbs a large amount of positive ions under the irradiation of sunlight, the trees can be evacuated to the tips of the leaves through veins to be radiated and ionized, and the trees can be easily burned to cause fire due to strong insolation and drying.

The invention also discloses far infrared negative oxygen ion powder which comprises the following components in parts by weight: 5-10 parts of silkworm excrement, 3-5 parts of silkworm chrysalis, 1-5 parts of liquorice, 3-8 parts of dried ginger, 5-9 parts of cinnamon, 1-3 parts of star anise, 2-5 parts of bay leaves, 6-9 parts of fennel, 3-7 parts of clove, 60-70 parts of far infrared ceramic powder, 0.5-2 parts of bamboo salt and 0.01-0.03 part of sulfur.

The invention also discloses a preparation method of the far infrared negative oxygen ion powder, which comprises the following steps:

mixing faeces Bombycis, pupa Bombycis, Glycyrrhrizae radix, Zingiberis rhizoma, cortex Cinnamomi, fructus Anisi Stellati, folium Neocinnamomi Delavayi, fructus Foeniculi, flos Caryophylli and Sulfur, calcining into powder to obtain base powder;

mixing the base powder, bamboo salt and far infrared ceramic powder, and grinding into powder.

Further limit, the particle size of the far infrared bioelectricity carbon negative oxygen ion powder is 2000 meshes.

The invention has the beneficial effects that: the silkworm excrement, the silkworm chrysalis, the liquorice, the dried ginger, the cinnamon, the aniseed, the bay leaves, the fennel, the clove and the sulfur are mixed and calcined to obtain the base material powder, the base material powder is mainly carbon and is mixed with the bamboo salt and the far infrared ceramic powder, so that the base material powder can sterilize and inhibit bacteria, purify the air environment, absorb moisture and prevent corrosion, has a lasting sterilization effect, and can generate 5 ten thousand negative ions per cubic centimeter when being detected.

Detailed Description

The compound amino acid and the compound vitamin are purchased from the market, and the nitrogen-fixing microbial inoculum is a microbial inoculum commonly used in the existing plant cultivation process;

sterol, specification: 800 meshes, food grade, various plant fibers as extraction raw materials, and is produced in the Hubei Danao pharmaceutical industry;

the yeast is prepared by fermenting edible fungus spores and Angel brand yeast;

the pine needle extract is extracted from pine needle plants;

pueraria powder is purchased from Zhongxiang city simple and child food Co Ltd; the silver ion-containing powder can be purchased from products circulated in the existing market, and has the sterilization effect.

Titanium dioxide powder and far infrared ceramic powder are bought by Taobao on a net, and the specification is as follows: 2000 mesh, purity 95%;

grinding shell powder purchased from North Daihe into powder with 2000 meshes, and integrating the functions of carriers;

example 1

A method for in vivo biological induction of negative oxygen ions, comprising the steps of:

extracting chlorophyll: mixing folium Mori 500g, herba Taraxaci 300g, folium Brassicae campestris 200g, folium Oak 700g, caulis et folium Lactucae Sativae 800g, folium Luffae 500g, Lycii folium 300g and caulis et folium Brassicae campestris 1000g, and extracting chlorophyll to obtain chlorophyll extract;

preparing a mulberry planting foliar fertilizer: mixing the following components by mass: 45kg of monazite powder soaking solution, 1kg of compound amino acid, 5kg of compound vitamin, 25kg of chlorophyll extract, 8kg of thorium calcined by an ancient method traditional Chinese medicine and 0.4kg of nitrogen fixing agent;

spraying a leaf fertilizer on the leaf surfaces of the mulberry trees in the morning, picking up mulberry leaves at a speed of 16:00-18:00 to feed silkworms, and collecting silkworm excrement and silkworm pupas;

boiling silkworm cocoons into silk by using brine, and decomposing, extracting and drying the silk to obtain the silk protein powder.

In the embodiment, the silkworms in the east and north of China are silkworm eggs with large heads and hard silkworms.

Example 2

A preparation method of a negative oxygen ion coating comprises the following steps:

s1: weighing the following raw materials by mass: 1000g of sterol, 30g of microzyme, 200g of pine needle extract, 800g of radix puerariae powder, 5500g of silver ion-containing powder, 100g of silver ion-containing powder and 200g of silk protein powder;

s2: mixing sterol, yeast, pine needle extracting solution, radix puerariae powder, silver ion-containing powder and the silk protein powder prepared in the embodiment 1, and fermenting for 18-25 hours to obtain fermentation liquor;

s3: adding titanium dioxide powder into the fermentation liquor, uniformly stirring, drying to obtain powder, then adding shell powder, and grinding to obtain 2000-mesh powder.

Example 3

A preparation method of far infrared negative oxygen ion powder comprises the following steps:

s1: weighing the following raw materials by mass: 500g of silkworm excrement and 300g of silkworm chrysalis prepared in example 1, 300g of liquorice, 500g of dried ginger, 800g of cinnamon, 200g of anise, 400g of bay leaf, 800g of fennel, 500g of clove, 150g of bamboo salt, 6000g of far infrared ceramic powder and 2g of sulfur;

s2: mixing silkworm excrement and silkworm chrysalis obtained in example 1, liquorice, dried ginger, cinnamon, anise, bay leaves, fennel, clove and sulfur, and calcining to obtain base powder;

s3: mixing the base material powder, bamboo salt and far infrared ceramic powder, and grinding into 2000 mesh powder.

Now, the silk protein powder prepared in example 1 is detected, the content of a radiation source in the silk protein powder is 0.3 wt%, and the silk protein powder conforms to the GB6566-2010 standard, which shows that the content of radioactive elements in the needed protein powder can be reduced by means of a biological chain, the obtained silk protein powder can release negative oxygen ions, the concentration of the negative oxygen ions in the air is increased, and the health of a human body is facilitated.

The results of testing the oxygen anion-generating coating prepared in example 2 are shown in table 1.

TABLE 1

Note undetected description: a volatile organic compound content (VOC) < 2 g/L; the total amount of benzene, toluene, ethylbenzene and xylene is less than 50mg/kg, the free formaldehyde is less than 5mg/kg, the cadmium Cd is less than 0.5mg/kg, and the mercury Hg is less than 0.1 mg/kg.

The negative oxygen ion coating prepared in example 2 was applied to a test chamber, the concentration of negative oxygen ions in the air in the test chamber was measured after 2 days, and the test chamber without the negative oxygen ion coating was a blank control, and the results are shown in table 2.

TABLE 2

As can be seen from tables 1 and 2, the content of each substance in the negative oxygen ion coating prepared in example 2 meets the corresponding national standard, and the amount of the negative oxygen ions induced in the air can reach 1.22 × 10¹⁰(ions/(s﹒m²) Detection basis: GB/T28628-2012 ensures that the quantity of negative oxygen ions in the air is kept at a high level, which is beneficial to the health of human bodies.

The results of radionuclide detection of the oxygen anion-generating coating prepared in example 2 are shown in Table 3.

TABLE 3

Radionuclides	Specific activity of radionuclide (Bq/kg)
		226Ra	14.60
232Th	75.44
		40K	156.17

The oxygen anion-generating coating prepared in example 2 was examined and the results are shown in Table 4.

TABLE 4

As can be seen from tables 3 and 4, the activity of the radionuclide is low, and the internal and external radiation indices are much smaller than the standard, so that it can be safely and safely used.

The far infrared negative oxygen ion powder prepared in example 3 was examined and the results are shown in tables 5 and 6.

TABLE 5 far infrared Performance test results

TABLE 6 measurement results of negative oxygen ions

As can be seen from tables 5 and 6, the far infrared emissivity and the far infrared radiation temperature rise of the far infrared negative oxygen ion powder prepared in example 3 both meet the standard requirements, and the negative oxygen ions in the air are significantly improved, which is beneficial to the health of human body.

Example 4

The silk protein powder prepared in example 1 is added into the raw material for preparing the melt-blown fabric, the preparation method and the process are the same as those of the existing melt-blown fabric preparation, and the detailed description is omitted in this example.

The results of the bacteriostatic tests on the common bacteria using the meltblown fabric prepared in this example and the commercially available meltblown fabric (used as a control group) are shown in table 7.

TABLE 7

According to the provisions of GB15979-2002 hygienic Standard for Disposable sanitary articles, appendix C4: the bacteriostatic rate is more than or equal to 50-90%, the product has bacteriostatic effect, the bacteriostatic rate is more than or equal to 50-90%, and the product has bacteriostatic action; the bacteriostasis rate is more than or equal to 50-90%, and the product has stronger bacteriostasis.

As can be seen from Table 7, the fibroin powder obtained by biological induction of negative oxygen ions in vivo has good bacteriostatic effect, and especially has strong bacteriostatic action on Escherichia coli and Staphylococcus aureus; has great application prospect in the textile field, in particular to melt-blown cloth.

Finally, it should be noted that: the above description is only a preferred embodiment of the present invention, and is not intended to limit the scope of the present invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.