阅读说明：本技术 一种银耳多糖涂抹型面膜及其制备方法 (Tremella polysaccharide smearing type mask and preparation method thereof ) 是由 杨晓春 吴新春 卢卫红 马莺 张英春 王荣春 程翠林 丁忠庆 谢桂林 黎重阳 孙 于 2021-09-24 设计创作，主要内容包括：本发明公开了一种银耳多糖涂抹型面膜及其制备方法,以重量份计,银耳多糖涂抹型面膜包括以下组分：银耳提取液10～15份,甘油5～9份,丙二醇2～4份,低分子透明质酸钠2～4份,PEG-40氢化蓖麻油0.2～0.4份,三乙醇胺0.1～0.4份,尿囊素0.1～0.3份,卡卡波姆0.2～1.0份,汉生胶0.1～0.4份。本发明解决了现有涂抹型面膜的银耳多糖不易吸收的问题。(The invention discloses a tremella polysaccharide smearing type mask and a preparation method thereof, wherein the tremella polysaccharide smearing type mask comprises the following components in parts by weight: 10-15 parts of tremella extract, 5-9 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.4 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-1.0 part of carbomer and 0.1-0.4 part of xanthan gum. The invention solves the problem that the tremella polysaccharide of the existing smearing type mask is not easy to absorb.)

1. The smearing type tremella polysaccharide facial mask is characterized by comprising the following components in parts by weight:

10-15 parts of tremella extract, 5-9 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.4 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-1.0 part of carbomer and 0.1-0.4 part of xanthan gum.

2. The tremella polysaccharide smearing type mask as claimed in claim 1, which is characterized by comprising the following components in parts by weight:

10-15 parts of tremella extract, 5-9 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.4 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-1.0 part of carbomer, 0.1-0.4 part of xanthan gum and the balance of deionized water to 100 parts.

3. The tremella polysaccharide smearing type mask as claimed in claim 1, which is characterized by comprising the following components in parts by weight:

10-13 parts of tremella extract, 6-8 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.3 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-0.6 part of carbomer and 0.1-0.3 part of xanthan gum.

4. The tremella polysaccharide smearing type mask as claimed in claim 1, which is characterized by comprising the following components in parts by weight:

10-13 parts of tremella extract, 6-8 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.3 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-0.6 part of carbomer, 0.1-0.3 part of xanthan gum and the balance of deionized water to 100 parts.

5. The application-type tremella polysaccharide mask as claimed in any one of claims 1 to 4, wherein the tremella extract is prepared by the following steps:

putting the tremella into an oven for constant-temperature drying, crushing after fully drying, and sieving to obtain tremella powder; soaking the tremella powder in deionized water, placing the tremella powder in a water bath kettle for stirring and extracting, and finally centrifuging to collect supernatant.

6. The method for preparing the tremella polysaccharide smearing type mask as claimed in any one of claims 1 to 5, wherein the method comprises the following steps:

s1, extracting tremella polysaccharide:

s11, drying Tremella in oven at constant temperature, pulverizing after it is dried completely, and sieving to obtain Tremella powder;

s12, adding the tremella powder prepared in the step S11 into deionized water, placing the mixture into a water bath pot, stirring and extracting, centrifuging, and collecting supernatant to obtain tremella polysaccharide-containing tremella extract;

s2, preparing a mask paste:

heating deionized water, adding allantoin under stirring to dissolve completely, sequentially adding Tremella extractive solution prepared in step S1, glycerol, propylene glycol, low molecular sodium hyaluronate, PEG hydrogenated castor oil and triethanolamine, and stirring to dissolve completely to obtain phase A; and quickly adding carbomer and xanthan gum into the phase A, heating and stirring to obtain the tremella polysaccharide smearing type mask paste.

7. The preparation method of the tremella polysaccharide smearing type mask as claimed in claim 6, wherein in the step S11, the drying temperature is 60-80 ℃ at constant temperature, and the drying time is 2-4 hours; the screening mesh number of the tremella powder is 50-100 meshes.

8. The preparation method of the tremella polysaccharide smearing type mask as claimed in claim 6, wherein in the step S12, the mass ratio of tremella powder to deionized water is 1: 15-30.

9. The preparation method of the tremella polysaccharide smearing type mask as claimed in claim 6, wherein in the step S12, the water bath temperature is 85-95 ℃, and the leaching time is 45-90 min.

10. The preparation method of the tremella polysaccharide smearing type mask as claimed in claim 6, wherein in the step S2, the ionic water is heated to 70-80 ℃, and carbomer and xanthan gum are rapidly added into the phase A and then stirred for 20-40 min.

Technical Field

The invention relates to the technical field of cosmetic processing, in particular to a tremella polysaccharide smearing type mask and a preparation method thereof.

Background

Tremella is a traditional medicine and food dual-purpose product, and belongs to a rare tonic in ancient times. With the success of the artificial cultivation technology of tremella, tremella is developed to every family. People can taste the tea. The traditional Chinese medicine theory considers that the tremella has the effects of nourishing yin, moistening lung, nourishing stomach, promoting the production of body fluid, tonifying qi and lubricating intestines, and is an inexorable beauty tonic for moistening skin, resisting aging and beautifying. Tremella is rich in natural plant colloid, has effects of nourishing yin, and can be used as skin caring food for long-term administration. According to records of Taiping Shenghui Fang and Yu Yao Ji Fang, etc., white fungus has the efficacy of nourishing yin and beautifying, and Yang noble concubine which says one of four ancient Chinese beauty women prefers to use white fungus to beautify and beautify.

The tremella polysaccharide is an active ingredient of tremella and has excellent moisture-preserving and water-locking capabilities. Tremella polysaccharides can absorb a large amount of water, and have the same high moisture retention property under low humidity or high humidity conditions. The tremella polysaccharide is applied to skin care cosmetics, has the functions of repairing epidermis, increasing the water content of the epidermis, improving the moisture content of stratum corneum and providing soft feeling to the skin; the skin conductivity integral value is improved, and the water retention capacity of the skin is improved; the water release constant was reduced, indicating that the product was able to improve the barrier function of the skin and prevent evaporation of water from the skin. The tremella polysaccharide has certain ability of eliminating hydroxyl free radicals. The tremella polysaccharide can be used as an anti-aging component to be applied to cosmetics. The skin aging is prevented, the growth of elastic cells is promoted, the damage of UV to the skin is reduced, epidermal cells are activated, and the photodamaged skin is repaired by inhibiting the peroxidation of cell lipid; accelerating skin regeneration, eliminating wrinkle and wrinkle. The tremella polysaccharide has the same moisturizing capability of hyaluronic acid, does not have sticky feeling, does not feel tight after being dried, gives moist and smooth feeling to skin, can resist partial free radicals, and is particularly suitable for skin care products. The tremella polysaccharide is a revolutionary plant-derived high-efficiency humectant, is the only one million-grade molecular weight natural moisturizing raw material at present, can not only moisturize efficiently, but also has the functions of resisting aging and oxidation, and is often used in high-grade cosmetics.

In recent years, the consumption of masks is increasing, especially, various masks added with natural functional ingredients are popular with consumers, tremella is also used for preparing masks, tremella superfine powder is usually adopted for the existing mask for applying the mask, tremella polysaccharide cannot be well absorbed, the effect of the prepared mask is reduced, and the ingredients of the existing tremella mask are complex.

Disclosure of Invention

The invention aims to provide a tremella polysaccharide smearing type mask and a preparation method thereof, and solves the problem that tremella polysaccharide of an existing smearing type mask is not easy to absorb.

The invention is realized by the following technical scheme:

the tremella polysaccharide smearing type mask comprises the following components in parts by weight:

10-15 parts of tremella extract, 5-9 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.4 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-1.0 part of carbomer and 0.1-0.4 part of xanthan gum.

The smearing type facial mask disclosed by the invention adopts the tremella extract as a main active ingredient, has a moisturizing effect, can promote growth of cytokines and beautify skin, and is suitable for all people. The facial mask liquid has the characteristics of being natural and non-irritant, and integrating multiple effects of moisturizing, color fading and color precipitation, brightness and luster, compactness and softness.

Compared with the existing tremella superfine powder, the tremella extracting solution used in the invention is easier to be absorbed by skin, shows the efficacy of tremella polysaccharide, and solves the problem that tremella polysaccharide of the existing smearing type mask is not easy to be absorbed.

Meanwhile, the invention has simple components, does not add essence and preservative, adopts pure natural components, and is safe and non-irritant.

Further, the coating comprises the following components in parts by weight:

10-15 parts of tremella extract, 5-9 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.4 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-1.0 part of carbomer, 0.1-0.4 part of xanthan gum and the balance of deionized water to 100 parts.

Further, the coating comprises the following components in parts by weight:

10-13 parts of tremella extract, 6-8 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.3 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-0.6 part of carbomer and 0.1-0.3 part of xanthan gum.

Further, the coating comprises the following components in parts by weight:

10-13 parts of tremella extract, 6-8 parts of glycerol, 2-4 parts of propylene glycol, 2-4 parts of low-molecular sodium hyaluronate, 0.2-0.4 part of PEG-40 hydrogenated castor oil, 0.1-0.3 part of triethanolamine, 0.1-0.3 part of allantoin, 0.2-0.6 part of carbomer, 0.1-0.3 part of xanthan gum and the balance of deionized water to 100 parts.

Further, the preparation process of the tremella extract is as follows:

putting the tremella into an oven for constant-temperature drying, crushing after fully drying, and sieving to obtain tremella powder; soaking the tremella powder in deionized water, placing the tremella powder in a water bath kettle for stirring and extracting, and finally centrifuging to collect supernatant.

A preparation method of a tremella polysaccharide smearing type mask comprises the following steps:

s1, extracting tremella polysaccharide:

s11, drying Tremella in oven at constant temperature, pulverizing after it is dried completely, and sieving to obtain Tremella powder;

s12, adding the tremella powder prepared in the step S11 into deionized water, placing the mixture into a water bath pot, stirring and extracting, centrifuging, and collecting supernatant to obtain tremella polysaccharide-containing tremella extract;

s2, preparing a mask paste:

heating deionized water, adding allantoin under stirring to dissolve completely, sequentially adding Tremella extractive solution prepared in step S1, glycerol, propylene glycol, low molecular sodium hyaluronate, PEG hydrogenated castor oil and triethanolamine, and stirring to dissolve completely to obtain phase A; and quickly adding carbomer and xanthan gum into the phase A, heating and stirring to obtain the tremella polysaccharide smearing type mask paste.

Further, in the step S11, the constant-temperature drying temperature is 60-80 ℃, and the time is 2-4 hours; the screening mesh number of the tremella powder is 50-100 meshes.

Further, in the step S12, the mass ratio of the tremella powder to the deionized water is 1: 15-30.

Further, in the step S12, the water bath temperature is 85-95 ℃, and the leaching time is 45-90 min.

Further, in step S2, the ionized water is heated to 70-80 ℃, carbomer and xanthan gum are rapidly added into the phase A, and then the stirring time is 20-40 min.

Compared with the prior art, the invention has the following advantages and beneficial effects:

1. the tremella polysaccharide smearing type mask obtained by the invention is not added with essence and preservative, adopts pure natural components, and is safe and non-irritant.

2. The invention has the effect of moisturizing, can promote the growth of cytokines and beautify the skin, and is suitable for all people. The facial mask liquid has the characteristics of being natural and non-irritant, and integrating multiple effects of moisturizing, color fading and color precipitation, brightness and luster, compactness and softness.

3. The tremella polysaccharide smearing type mask has important practical significance for accelerating transformation and upgrading of tremella from traditional processed food to health food, prolonging the tremella processing industry chain and promoting development of tremella industry.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail below with reference to examples, and the exemplary embodiments and descriptions thereof are only used for explaining the present invention and are not used as limitations of the present invention.

Example 1:

1000g of a tremella polysaccharide smearing type mask comprises the following raw materials in parts by mass: 120g of tremella extract, 60g of glycerol, 30g of propylene glycol, 30g of low-molecular-weight sodium hyaluronate, 3g of PEG-40 hydrogenated castor oil, 2g of triethanolamine, 2g of allantoin, 5g of carbomer, 2g of xanthan gum and deionized water, wherein the amount of deionized water is up to 1000 g.

The preparation method of the tremella polysaccharide smearing type mask comprises the following steps:

s1, extracting tremella polysaccharide:

s11, placing the tremella in an oven for constant-temperature drying at 75 ℃ for 4 hours; pulverizing after fully drying, and sieving with 80 mesh sieve to obtain Tremella powder;

s12, adding the tremella powder prepared in the step S11 into deionized water (the material-liquid ratio is 1:15), placing the tremella powder into a water bath kettle, stirring and extracting, wherein the water bath temperature is 92 ℃, the leaching time is 60min, centrifuging to collect supernatant, the centrifuging parameter is 3000r/min, the centrifuging time is 20min, adding deionized water into precipitates, and performing secondary extraction; mixing the two centrifugated supernatants to obtain Tremella extractive solution containing Tremella polysaccharide;

s2, preparing a mask paste:

heating deionized water to 75 ℃, adding allantoin to be completely dissolved under stirring, then sequentially adding the tremella extract prepared in the step S1, glycerol, propylene glycol, low-molecular-weight sodium hyaluronate, PEG hydrogenated castor oil and triethanolamine, and stirring to be completely dissolved to obtain phase A; and quickly adding carbomer and xanthan gum into the phase A, and stirring at 75 ℃ for 35min to obtain the tremella polysaccharide smearing type mask paste.

Sensory evaluation of the tremella polysaccharide spread-type mask prepared in this example:

with reference to the standards of QB/T1857-. A certain amount of sample to be tested is smeared on the skin of a test, and the smearing is rotated in one direction at the speed of 1 revolution per second until resistance is felt. The test result shows that the product is milky white in appearance and has less bubbles. The smearing force is moderate and uniform. Has good skin moistening effect, and can be applied for 10min with good water retention. Has good refreshing feeling and moderate viscosity.

The performance test of the tremella polysaccharide smearing type mask prepared in this example:

the test method comprises the following steps: measuring the pH value of the sample according to a method of QB/T13531.1-2008 'determination of pH value in cosmetic general detection method'; respectively placing the mask cream at 40 deg.C to-6 deg.C for 24 hr, and performing heat resistance test and cold resistance test; placing the facial mask cream at 40 deg.C for 24h, taking out, standing at room temperature for 12h, then standing at-6 deg.C for 24h, and performing cold and hot alternation test; centrifuging at 20 deg.C and 3000r/min for 15min, and performing centrifugal test; weighing a certain amount of sample, uniformly coating the sample on the surface of a culture dish, standing at the room temperature of 20 ℃, and recording the drying time until the sample is not sticky.

And (3) testing results: the pH value of the sample is 5.65, the sample is weakly acidic, and the sample accords with the pH value of normal skin and the regulation of QB/T2872-2017 facial mask cosmetics; the stability result shows that the mask cream has good heat resistance, cold and hot alternating stability and centrifugal stability, no oil and water stratification is caused under various conditions set by the test, and the overall appearance is not changed; the average drying time of the facial mask is (1210 + -15) s, and the drying time is proper.

Example 2:

this example is based on example 1, and differs from example 1 in that:

the facial mask has different formulas and different preparation parameters, and specifically comprises the following components:

1000g of a tremella polysaccharide smearing type mask comprises the following raw materials in parts by mass: 130g of tremella extract, 80g of glycerol, 40g of propylene glycol, 40g of low-molecular-weight sodium hyaluronate, 3g of PEG-40 hydrogenated castor oil, 3g of triethanolamine, 3g of allantoin, 8g of carbomer, 3g of xanthan gum and deionized water which are supplemented to 1000 g.

In the step S11, the constant temperature drying is carried out at 80 ℃ for 3 h; the tremella powder is sieved by a sieve with 100 meshes.

In step S12, the ratio of material to liquid (mass ratio) is 1: 30; the water bath temperature is 95 deg.C, and the extraction time is 50 min.

In step S2, the ionized water is heated to 80 deg.C, carbomer and xanthan gum are rapidly added into phase A, and the stirring time is 40 min.

Sensory evaluation of the tremella polysaccharide spread-type mask prepared in this example:

with reference to the standards of QB/T1857-. A certain amount of sample to be tested is smeared on the skin of a test, and the smearing is rotated in one direction at the speed of 1 revolution per second until resistance is felt. The test result shows that the product is milky white in appearance and has less bubbles. The smearing force is moderate and uniform. Has good skin moistening effect, and can be applied for 10min with good water retention. Has good refreshing feeling and moderate viscosity.

The performance test of the tremella polysaccharide smearing type mask prepared in this example:

the test method comprises the following steps: measuring the pH value of the sample according to a method of QB/T13531.1-2008 'determination of pH value in cosmetic general detection method'; respectively placing the mask cream at 40 deg.C to-6 deg.C for 24 hr, and performing heat resistance test and cold resistance test; placing the facial mask cream at 40 deg.C for 24h, taking out, standing at room temperature for 12h, then standing at-6 deg.C for 24h, and performing cold and hot alternation test; centrifuging at 20 deg.C and 3000r/min for 15min, and performing centrifugal test; weighing a certain amount of sample, uniformly coating the sample on the surface of a culture dish, standing at the room temperature of 20 ℃, and recording the drying time until the sample is not sticky.

And (3) testing results: the pH value of the sample is 5.68, the sample is weakly acidic, and the sample accords with the pH value of normal skin and the regulation of QB/T2872-2017 facial mask cosmetics; the stability result shows that the mask cream has good heat resistance, cold and hot alternating stability and centrifugal stability, no oil and water stratification is caused under various conditions set by the test, and the overall appearance is not changed; the average drying time of the facial mask is (1210 + -15) s, and the drying time is proper.

From the data of example 1 and example 2, it can be seen that:

when the amount ratio of each component in the mask is within the range of the present invention, the prepared mask has substantially uniform effects. The whole effect is good.

The above-mentioned embodiments are intended to illustrate the objects, technical solutions and advantages of the present invention in further detail, and it should be understood that the above-mentioned embodiments are merely exemplary embodiments of the present invention, and are not intended to limit the scope of the present invention, and any modifications, equivalent substitutions, improvements and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.