阅读说明：本技术 一种玫瑰香洗衣皂香精的制备方法 (Preparation method of rose-fragrance laundry soap essence ) 是由 林承岸 于 2021-07-23 设计创作，主要内容包括：本发明涉及洗衣皂香精技术领域,且公开了一种玫瑰香洗衣皂香精的制备方法,包括以下步骤：S1：原料配比,玫瑰花瓣20-50份、皂基10-29份、菊花精油2-6份、郁金香酯3-15份、去离子水12-24份、增稠剂3-6份、乳化剂2-6份、定香剂3-7份、修饰剂2-8份、苯甲醇3-5份；S2：原料处理；S3：搅拌混合；S4：静置过滤。本发明通过玫瑰花瓣的处理能够使得以玫瑰花瓣粉末融入洗衣皂中,使得洗衣皂融入玫瑰花精华,使其具有玫瑰花的香味,香味醇厚,适用性广,采用天然植物油皂基,内含椰子油、橄榄油等营养滋润元素,天然温和,遇水速溶释放更多有效成分。(The invention relates to the technical field of laundry soap essence, and discloses a preparation method of rose-fragrance laundry soap essence, which comprises the following steps: s1: the raw material ratio is that 20-50 parts of rose petal, 10-29 parts of soap base, 2-6 parts of chrysanthemum essential oil, 3-15 parts of tulip ester, 12-24 parts of deionized water, 3-6 parts of thickening agent, 2-6 parts of emulsifier, 3-7 parts of fixative, 2-8 parts of modifier and 3-5 parts of benzyl alcohol; s2: treating raw materials; s3: stirring and mixing; s4: standing and filtering. The rose petal powder can be blended into the laundry soap through the treatment of the rose petals, so that the laundry soap is blended with rose essence, has the fragrance of rose, is mellow in fragrance and wide in applicability, adopts natural vegetable oil soap base, contains nutrition and moistening elements such as coconut oil and olive oil, is natural and mild, and releases more effective components instantly dissolved in water.)

1. The preparation method of the rose-fragrance laundry soap essence is characterized by comprising the following steps of:

s1: the raw material ratio is that 20-50 parts of rose petal, 10-29 parts of soap base, 2-6 parts of chrysanthemum essential oil, 3-15 parts of tulip ester, 12-24 parts of deionized water, 3-6 parts of thickening agent, 2-6 parts of emulsifier, 3-7 parts of fixative, 2-8 parts of modifier and 3-5 parts of benzyl alcohol;

s2: processing raw materials, namely manually screening rose petals, then crushing, filtering by using a 600-mesh and 800-mesh sieve, removing impurities after filtering, collecting rose petal particles, then grinding to obtain rose petal powder;

s3: stirring and mixing, namely adding rose petal powder, soap base, chrysanthemum essential oil, tulip ester, deionized water, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 50-90 minutes before preparation;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fragrance fixing agent into a mixing tank, continuously stirring for 10-15 minutes, and heating while stirring to obtain a soap solution;

s6: demolding, namely pouring the prepared soap liquid into a prepared mold, cooling, and demolding to obtain a finished product;

s7: and (5) inspecting finished products, inspecting whether the obtained finished products are qualified or not, and calculating the qualified rate.

2. The method for preparing the rose-scented laundry soap essence according to claim 1, wherein the fragrance fixative in S1 is one or more of ambergris, musk, civet, castoreum, peru balsam, toluol, storax and oak moss extract.

3. The method for preparing the rose-scented laundry soap essence according to claim 1, wherein the thickener in S3 is one or more of pectin, gelatin, gum arabic, agar, starch, sodium alginate, sodium caseinate and sodium carboxymethylcellulose.

4. The method for preparing rose-scented laundry soap essence according to claim 1, wherein the soap base in the S1 is a mixture of coconut oil and olive oil, and the proportion of the mixture is 1: 0.6-2.

5. The method for preparing rose-scented laundry soap essence according to claim 1, wherein the rotation speed of the pulverization in S2 is 1200r/min, and the filtered impurities are poured in next pulverization.

6. The method for preparing the rose-scented laundry soap essence according to claim 3, wherein the emulsifier in S3 is one or more of glyceryl monostearate, soybean lecithin, sorbitan fatty acid ester and polyoxyethylene xylitol anhydride stearate.

7. The method of claim 1, wherein the modifier in S4 is one or more of apple essential oil, orange essential oil, lemon essential oil, and strawberry essential oil.

8. The method for preparing rose-scented laundry soap essence according to claim 1, wherein a layer of oil film is brushed into the mold during the process of reverse molding in S6, and trimming is performed after demolding.

9. The method as claimed in claim 1, wherein the detection contents in S7 include size, color, flavor and smoothness, and the qualified rate is less than 98%, so that full-line detection is performed.

Technical Field

The invention relates to the technical field of laundry soap essence, in particular to a preparation method of rose-fragrance laundry soap essence.

Background

The essence is a raw material for endowing cosmetics with certain fragrance, and is one of key raw materials in the manufacturing process. The essence is properly selected, is not only loved by consumers, but also can cover certain unpleasant odor in the product medium. The essence is prepared by blending and mixing a plurality of spices and has certain type of fragrance, namely aroma type, and when the cosmetics are perfumed, the proper aroma type is selected, and the selected essence has no influence on the product quality and the using effect.

The laundry soap is a washing article with the longest use history for human, and is durable and convenient to use; the raw materials are salt generated by animal and vegetable oil, fatty acid and alkali, and are easy to biodegrade and have small water pollution, so the laundry soap is one of the main products in the domestic washing market at present, the prior laundry soap essence has little fragrance types during preparation and is not soft enough, and the fragrance is not lasting after use, so the laundry soap cannot meet the requirements of people.

Disclosure of Invention

Technical problem to be solved

Aiming at the defects of the prior art, the invention provides a preparation method of a rose-fragrance laundry soap essence, and solves the problems that the conventional laundry soap essence has too few fragrance types and is not soft enough during preparation, and the fragrance is not lasting enough after use, so that the requirements of people cannot be met.

(II) technical scheme

In order to achieve the purpose, the invention provides the following technical scheme:

a preparation method of rose-fragrance laundry soap essence comprises the following steps:

s1: the raw material ratio is that 20-50 parts of rose petal, 10-29 parts of soap base, 2-6 parts of chrysanthemum essential oil, 3-15 parts of tulip ester, 12-24 parts of deionized water, 3-6 parts of thickening agent, 2-6 parts of emulsifier, 3-7 parts of fixative, 2-8 parts of modifier and 3-5 parts of benzyl alcohol;

s2: processing raw materials, namely manually screening rose petals, then crushing, filtering by using a 600-mesh and 800-mesh sieve, removing impurities after filtering, collecting rose petal particles, then grinding to obtain rose petal powder;

s3: stirring and mixing, namely adding rose petal powder, soap base, chrysanthemum essential oil, tulip ester, deionized water, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 50-90 minutes before preparation;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fragrance fixing agent into a mixing tank, continuously stirring for 10-15 minutes, and heating while stirring to obtain a soap solution;

s6: demolding, namely pouring the prepared soap liquid into a prepared mold, cooling, and demolding to obtain a finished product;

s7: and (5) inspecting finished products, inspecting whether the obtained finished products are qualified or not, and calculating the qualified rate.

As a further scheme of the invention, the fixative in S1 is one or more of ambergris, musk, civet, castoreum, peru balsam, Tulu balsam, benzoin resin, storax resin and oak moss extract.

Further, the thickener in S3 is one or more of pectin, gelatin, gum arabic, agar, starch, sodium alginate, sodium caseinate, and sodium carboxymethylcellulose.

On the basis of the scheme, the soap base in the S1 is a mixture of coconut oil and olive oil, and the proportion of the coconut oil to the olive oil is 1: 0.6-2.

Further, the rotation speed at the time of pulverization in the step S2 was 1200r/min, and the filtered impurities were poured in next pulverization.

On the basis of the scheme, the emulsifier in the S3 is one or more of glyceryl monostearate, soybean lecithin, sorbitan fatty acid ester and polyoxyethylene xylitol anhydride stearate.

In a still further aspect of the present invention, the modifying agent in S4 is one or more of apple essential oil, orange essential oil, lemon essential oil, and strawberry essential oil.

Further, in the step S6, a layer of oil film is applied to the mold during the reverse molding, and trimming is performed after demolding.

On the basis of the above scheme, the detected content in S7 includes size, color, flavor and smoothness, and if the qualified rate is lower than 98%, full-line detection is performed.

(III) advantageous effects

Compared with the prior art, the invention provides a preparation method of rose-fragrance laundry soap essence, which has the following beneficial effects:

1. the compatible substances in the formula are green and healthy, and the rose petal powder can be blended into the laundry soap through the treatment of the rose petals, so that the laundry soap is blended with rose essence, and has the fragrance of rose, mellow fragrance and wide applicability.

2. According to the invention, the natural vegetable oil soap base is adopted, contains nutrition and moistening elements such as coconut oil and olive oil, is natural and mild, releases more effective components instantly dissolved in water, and comprehensively exerts the washing and protecting effects.

3. According to the invention, the filtered impurities are poured in next crushing for recycling, the secondary crushing is performed, the cost is saved, the emulsifying and stabilizing effect can be achieved by adding the emulsifying agent, the thickening agent is matched to adjust the viscosity property of the essence, the main fragrance style can be adjusted according to different requirements by adding the modifying agent, the diversity is improved, and thus the requirements of different people are met.

4. According to the invention, the oil film is arranged, so that the prepared product can be prevented from being adhered during demoulding and influencing the finished product rate, and the finished product can be improved by finishing after demoulding.

Drawings

Fig. 1 is a schematic flow structure diagram of a preparation method of the rose-scented laundry soap essence provided by the invention.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1

Referring to fig. 1, a method for preparing a rose-scented laundry soap essence comprises the following steps:

s1: the raw materials comprise 32 parts of rose petals, 15 parts of soap base, 3 parts of chrysanthemum essential oil, 6 parts of tulip ester, 15 parts of deionized water, 3 parts of thickening agent, 2 parts of emulsifier, 5 parts of fixative, 7 parts of modifier and 3 parts of benzyl alcohol;

s2: the method comprises the following steps of (1) raw material treatment, namely, manually screening rose petals, then crushing, filtering by using a 600-mesh sieve, removing impurities after filtering, collecting rose petal particles, then grinding to obtain rose petal powder, and blending the rose petal powder into laundry soap through the treatment of the rose petals, so that the laundry soap is blended with rose essence and has rose fragrance, mellow fragrance and wide applicability;

s3: stirring and mixing, namely adding rose petal powder, soap base, chrysanthemum essential oil, tulip ester, deionized water, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 55 minutes before preparation;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fragrance fixing agent into a mixing tank, continuously stirring for 12 minutes, and heating while stirring to obtain a soap solution;

s6: demolding, namely pouring the prepared soap liquid into a prepared mold, cooling, and demolding to obtain a finished product;

s7: and (5) inspecting finished products, inspecting whether the obtained finished products are qualified or not, and calculating the qualified rate.

The fragrance fixative in S1 is an oak moss extract, is not easy to volatilize by itself and can inhibit the volatilization rate of other volatile spices by adding the fragrance fixative, so that the volatilization rate of the whole essence is reduced, the fragrance characteristics or fragrance types of the essence can be kept consistent all the time to keep the essence with lasting fragrance, the thickening agent in S3 is agar and starch, the soap base in S1 is a mixture of coconut oil and olive oil, and the proportion is 1: 2, the soap base is made of natural vegetable oil, contains nutrient and moistening elements such as coconut oil and olive oil, is natural and mild, releases more effective components instantly dissolved in water, and gives full play to the washing and protecting effects.

It is specially noted that the rotation speed is 1200r/min when the S2 is pulverized, the filtered impurities are poured in when the next pulverization is performed, the impurities are recycled, the secondary pulverization is performed, the cost is saved, the emulsifier in the S3 is polyoxyethylene xylitol anhydride stearate, the emulsifying stabilization effect can be realized through the addition of the emulsifier, the emulsifier is matched with the thickener to adjust the viscosity property of the essence, the modifier in the S4 is apple essential oil, the style of the main fragrance can be adjusted according to different requirements through the addition of the modifier to improve the diversity so as to meet the requirements of different crowds, a layer of oil film is brushed in the mold when the mold is inverted in the S6, the trimming is performed after the mold is removed, the prepared product can be prevented from being adhered when the mold is removed, the yield of the product is influenced, the trimming is performed after the mold is removed, the phase of the finished product can be improved, and the detection contents in the S7 comprise the size, the color and the color, And (4) performing full-line detection if the flavor degree and the smoothness are lower than 98 percent.

Example 2

Referring to fig. 1, a method for preparing a rose-scented laundry soap essence comprises the following steps:

s1: the raw materials comprise 35 parts of rose petals, 13 parts of soap base, 3 parts of chrysanthemum essential oil, 5 parts of tulip ester, 15 parts of deionized water, 3 parts of thickening agent, 2 parts of emulsifier, 5 parts of fixative, 7 parts of modifier and 3 parts of benzyl alcohol;

s2: the method comprises the following steps of (1) raw material treatment, namely, manually screening rose petals, then crushing, filtering by using a 600-mesh sieve, removing impurities after filtering, collecting rose petal particles, then grinding to obtain rose petal powder, and blending the rose petal powder into laundry soap through the treatment of the rose petals, so that the laundry soap is blended with rose essence and has rose fragrance, mellow fragrance and wide applicability;

s3: stirring and mixing, namely adding rose petal powder, soap base, chrysanthemum essential oil, tulip ester, deionized water, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 75 minutes before preparation;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fragrance fixing agent into a mixing tank, continuously stirring for 12 minutes, and heating while stirring to obtain a soap solution;

s6: demolding, namely pouring the prepared soap liquid into a prepared mold, cooling, and demolding to obtain a finished product;

s7: and (5) inspecting finished products, inspecting whether the obtained finished products are qualified or not, and calculating the qualified rate.

The fixative in S1 of the invention is ambergris, musk, civet, through the addition of the fixative, it is not easy to volatilize, can inhibit the volatilization rate of other volatile spices, make the volatilization rate of the whole essence slow down, can make the aroma characteristic or odor type of the essence keep unanimous all the time at the same time, in order to keep the lasting essence of aroma, the thickening agent in S3 is gum arabic, agar, starch, the soap base in S1 is the mixture of coconut oil, olive oil, its proportion is 1: 1, the soap base is natural vegetable oil soap base, contains nutrition and moistening elements such as coconut oil and olive oil, is natural and mild, releases more effective components instantly dissolved in water, and gives full play to the washing and protecting effects.

It should be specially noted that the rotation speed is 1200r/min when the grinding is carried out in S2, the filtered impurities are poured in next grinding and recycled, the secondary grinding is carried out, the cost is saved, the emulsifier in S3 is soybean lecithin, the emulsifying stabilization effect can be achieved through the addition of the emulsifier, the thickening performance of the essence is adjusted through the matching of the emulsifier and the thickener, the modifier in S4 is strawberry essential oil, the style of the main fragrance can be adjusted according to different requirements through the addition of the modifier, the diversity is improved, the requirements of different crowds are met, a layer of oil film is brushed into a mold when the mold is reversed in S6, the trimming is carried out after the mold is removed, the adhesion of the prepared product during the mold removal can be prevented through the arrangement of the oil film, the product yield is influenced, the trimming is carried out after the mold removal, the product phase can be improved, the detection contents in S7 comprise the size, the color, the fragrance degree and the smoothness, and if the qualified rate is lower than 98%, carrying out full-line detection.

Example 3

Referring to fig. 1, a method for preparing a rose-scented laundry soap essence comprises the following steps:

s1: the raw materials comprise 25 parts of rose petals, 19 parts of soap base, 3 parts of chrysanthemum essential oil, 6 parts of tulip ester, 23 parts of deionized water, 3 parts of thickening agent, 2 parts of emulsifier, 7 parts of fixative, 7 parts of modifier and 3 parts of benzyl alcohol;

s2: the method comprises the following steps of (1) raw material treatment, namely, manually screening rose petals, then crushing, filtering by using a 600-mesh sieve, removing impurities after filtering, collecting rose petal particles, then grinding to obtain rose petal powder, and blending the rose petal powder into laundry soap through the treatment of the rose petals, so that the laundry soap is blended with rose essence and has rose fragrance, mellow fragrance and wide applicability;

s3: stirring and mixing, namely adding rose petal powder, soap base, chrysanthemum essential oil, tulip ester, deionized water, a thickening agent and an emulsifying agent into a mixing tank for preliminary preparation by stirring, and checking and mixing the raw materials for 75 minutes before preparation;

s4: standing and filtering, namely adding the modifier and benzyl alcohol into a mixing tank together for continuous stirring, then heating, standing and filtering after heating;

s5: mixing, namely adding the fragrance fixing agent into a mixing tank, continuously stirring for 12 minutes, and heating while stirring to obtain a soap solution;

s6: demolding, namely pouring the prepared soap liquid into a prepared mold, cooling, and demolding to obtain a finished product;

s7: and (5) inspecting finished products, inspecting whether the obtained finished products are qualified or not, and calculating the qualified rate.

The fragrance fixative in S1 is ambergris, styrax resin and oak moss extract, is not easy to volatilize by adding the fragrance fixative, can inhibit the volatilization rate of other volatile spices, can slow down the volatilization rate of the whole essence, can keep the fragrance characteristics or fragrance types of the essence consistent all the time so as to keep the essence with lasting fragrance, the thickening agent in S3 is pectin, agar, sodium caseinate and sodium carboxymethylcellulose, the soap base in S1 is a mixture of coconut oil and olive oil, and the proportion is 1: 1.5, the soap base is natural vegetable oil soap base which contains coconut oil, olive oil and other nutrition and moistening elements, is natural and mild, releases more effective components instantly dissolved in water and gives full play to the washing and protecting effects.

It should be particularly noted that the rotation speed is 1200r/min when the S2 is pulverized, filtered impurities are poured in when the S3 is pulverized next time and are recycled, the cost is saved, the emulsifier is glyceryl monostearate in the S3, the emulsifier can play a role in emulsification and stabilization by adding the emulsifier, the thickener is matched with the emulsifier to adjust the viscosity property of essence, the modifier is apple essential oil in the S4, the style of the main fragrance can be adjusted according to different requirements by adding the modifier to improve the diversity so as to meet the requirements of different crowds, an oil film is brushed into a mold when the S6 is inverted, the trimming is carried out after the demolding, the prepared product can be prevented from being adhered when the demolding is carried out by setting the oil film to influence the yield of the product, the trimming is carried out after the demolding, the grade of the finished product can be improved, and the detection contents in the S7 comprise the size, the color, the fragrance degree and the degree of the color, And 4, performing full-line detection if the smoothness and the qualified rate are lower than 98%.

In the description herein, it is noted that relational terms such as first and second, and the like, are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.