阅读说明：本技术 一种胶原补水保湿面膜及其制备方法 (Collagen moisturizing mask and preparation method thereof ) 是由 石毛 林志隆 于 2021-07-08 设计创作，主要内容包括：本发明公开了一种胶原补水保湿面膜及其制备方法,该面膜中含有尿囊素、三乙醇胺、透明质酸钠、水解胶原、皱波角叉菜提取物、神经酰胺3、羟苯基丙酰胺苯甲酸、蜗牛分泌物滤液等多种有效活性成分,能够涵养皮肤水分,修复肌肤细胞,提高皮肤密度,减少肌肤皱纹的产生,使皮肤柔软丰满富有弹性,润滑角质层,刺激皮肤微循环,促进皮肤新陈代谢。而且制备工艺简单易行,具有极高的经济价值和实用价值。(The invention discloses a collagen moisturizing and moisture-preserving mask and a preparation method thereof, the mask contains a plurality of effective active ingredients such as allantoin, triethanolamine, sodium hyaluronate, hydrolyzed collagen, a carrageen crispus extract, ceramide 3, hydroxyphenyl propionamide benzoic acid, snail secretion filtrate and the like, and can nourish skin moisture, repair skin cells, improve skin density, reduce skin wrinkles, enable the skin to be soft, full and elastic, lubricate cuticle, stimulate skin microcirculation and promote skin metabolism. And the preparation process is simple and easy to implement, and has extremely high economic value and practical value.)

1. The collagen moisturizing mask is characterized by comprising the following components in parts by mass: 0.455-6.5 parts of skin conditioner, 0.01-0.2 part of antioxidant, 1.752-16.1 parts of humectant and 0.12-2 parts of collagen substance.

2. The collagen hydrating and moisturizing mask as claimed in claim 1, wherein the collagen hydrating and moisturizing mask comprises the following components by mass: 1.39-4.8 parts of skin conditioner, 0.02-0.1 part of antioxidant, 3.408-11.56 parts of humectant and 0.25-1.4 parts of collagen substance.

3. The collagen hydrating and moisturizing mask as claimed in claim 1 or 2, further comprising 0.25-2.1 parts by weight of emulsifier, 0.2-1 part by weight of thickener, 0.001-0.1 part by weight of essence, preferably 0.5-1.6 parts by weight of emulsifier, 0.24-0.8 part by weight of thickener, 0.002-0.01 part by weight of essence.

4. The collagen hydrating and moisturizing mask as claimed in any one of claims 1 to 3, wherein the skin conditioning agent is: at least one of dipotassium glycyrrhizinate, bisabolol, alpha-arbutin, extract of leaves/stems of Artocarpus millettii, extract of Coix lacryma-jobi, hydrolyzed red algae extract, caprylic/capric triglyceride, ethylhexyl palmitate, allantoin, sodium hyaluronate, hydroxyphenylpropionamide benzoic acid, or their combination.

5. The collagen hydrating and moisturizing mask as claimed in any one of claims 1 to 3, wherein the moisturizing agent is: at least one of sodium pyrrolidone carboxylate, dipropylene glycol, propylene glycol, glycerin, Chondrus crispus extract, ceramide 3, butylene glycol, 1, 2-hexanediol, or a combination thereof.

6. The collagen hydrating and moisturizing mask as claimed in any one of claims 1 to 3, wherein the collagen material is: at least one of hydrolyzed collagen, hydrolyzed elastin, snail secretion filtrate, or combinations thereof.

7. The collagen hydrating and moisturizing mask as claimed in any one of claims 1 to 3, wherein the antioxidant is: at least one of vitamin E, astaxanthin, canthaxanthin, lutein, olive pomace, tocopherol acetate or combinations thereof.

8. The collagen hydrating and moisturizing mask as claimed in claim 3, wherein said emulsifier is: at least one of PEG-20 methyl glucose sesquistearate, glyceryl stearate \ PEG-100 stearate, polyacrylamide/C13-14 isoalkane/laureth-7, or their combination;

the thickening agent is: at least one of xanthan gum, carbomer, triethanolamine or a combination thereof.

9. The collagen hydrating and moisturizing mask as claimed in claim 3, wherein the collagen hydrating and moisturizing mask comprises the following components by mass: 0.05-0.5 part of PEG-20 methyl glucose sesquistearate, 0.05-0.5 part of methyl glucose sesquistearate, 0.1-2 parts of ethylhexyl palmitate, 0.01-0.2 part of tocopherol acetate, 0.05-0.3 part of allantoin, 0.1-0.5 part of carbomer, 1-8 parts of glycerol, 0.1-0.5 part of triethanolamine, 0.005-0.2 part of sodium hyaluronate, 0.1-1.5 part of hydrolyzed collagen, 0.15-2 parts of Chondrus crispus extract, 0.002-0.1 part of ceramide 3, 0.1-2 parts of hydroxyphenylpropionamide benzoic acid, 0.5-4 parts of butanediol, 0.1-2 parts of 1, 2-hexanediol, 0.1-1 part of p-hydroxyacetophenone, 0.02-0.5 part of snail secretion, 0.1-0.8 part of glyceryl stearate, PEG-100 parts of glyceryl stearate, 0.2-2 parts of caprylic/capric acid triester, 0.05-0.3 part of polyacrylamide/C13-14 isoalkane/laureth-7 and 0.001-0.1 part of rose essence.

10. The method for preparing the collagen hydrating and moisturizing mask as claimed in claim 3, comprising the steps of:

mixing skin conditioner, antioxidant, humectant, collagen substance, emulsifier, thickener and water, and adding essence to obtain the final product.

Technical Field

The invention belongs to the field of cosmetics, and particularly relates to a collagen moisturizing mask and a preparation method thereof.

Background

In the modern society, along with the improvement of the living standard of people, people pay more and more attention to the living quality and consume more and more in the aspect of beautifying and protecting skin. As is known, the basis of skin care is water supplement, water shortage is the root cause of all skin problems, and the skin becomes rough, tight, even peeled and sensitive due to water shortage and dryness, and can easily form expression lines, accelerate aging, and form more skin problems such as pigmentation, wrinkles, spots and the like. The immunity of the skin which is lack of water for a long time is reduced, and the self-repairing ability is gradually lost. Therefore, it is very important to protect the skin even if the skin is moisturized so that it is continuously repaired by itself.

For most customers who use cosmetics, facial masks are necessary skin care products in addition to daily skin care lotions or essences. The facial mask is a cosmetic skin care product applied on the face, a film which is tightly stretched on the face can be formed on the face, and the effect is higher or lower than the transdermal absorption rate of nutrient components in the facial mask. The problems of unobvious moisturizing effect, poor moisturizing effect and the like generally exist in common skin care products or masks.

Aiming at the problems, the safe and effective moisturizing mask which can help skin to quickly moisturize and improve self-repairing capability has extremely high market value and customer favor.

Disclosure of Invention

The present invention is directed to solving at least one of the problems of the prior art described above. Therefore, the collagen moisturizing mask provided by the invention contains various moisturizing components, can preserve the moisture of the skin and enables the skin to have good affinity. Meanwhile, the collagen skin cream is rich in a large amount of collagen substances, can repair skin cells, improve skin density, reduce skin wrinkles, enable the skin to be soft, full and elastic, lubricate cuticle, stimulate skin microcirculation, promote skin metabolism, and enable the skin to be fine, smooth and bright.

According to the first aspect of the invention, the collagen hydrating and moisturizing mask comprises the following components in parts by mass: 0.455-6.5 parts of skin conditioner, 0.01-0.2 part of antioxidant, 1.752-16.1 parts of humectant and 0.12-2 parts of collagen substance.

According to a first aspect of the present invention, in some embodiments of the present invention, the collagen hydrating moisture mask comprises the following components by mass: 1.39-4.8 parts of skin conditioner, 0.02-0.1 part of antioxidant, 3.408-11.56 parts of humectant and 0.25-1.4 parts of collagen substance.

In some preferred embodiments of the present invention, the collagen hydrating and moisturizing mask further comprises 0.25 to 2.1 parts by weight of an emulsifier, 0.2 to 1 part by weight of a thickener, and 0.001 to 0.1 part by weight of an essence.

In some more preferred embodiments of the present invention, the collagen hydrating and moisturizing mask further comprises 0.5 to 1.6 parts by mass of an emulsifier, 0.24 to 0.8 parts by mass of a thickener, and 0.002 to 0.01 parts by mass of an essence.

In some preferred embodiments of the invention, the skin conditioning agent is: at least one of dipotassium glycyrrhizinate, bisabolol, alpha-arbutin, extract of leaves/stems of Artocarpus millettii, extract of Coix lacryma-jobi, hydrolyzed red algae extract, caprylic/capric triglyceride, ethylhexyl palmitate, allantoin, sodium hyaluronate, hydroxyphenylpropionamide benzoic acid, or their combination.

In some more preferred embodiments of the invention, the skin conditioning agent is: caprylic/capric triglyceride, ethylhexyl palmitate, allantoin, sodium hyaluronate and hydroxyphenylpropionamide benzoic acid.

In some preferred embodiments of the present invention, the humectant is: at least one of sodium pyrrolidone carboxylate, dipropylene glycol, propylene glycol, glycerin, Chondrus crispus extract, ceramide 3, butylene glycol, 1, 2-hexanediol, or a combination thereof.

In some more preferred embodiments of the present invention, the humectant is: glycerol, Chondrus crispus extract, ceramide 3, butanediol and 1, 2-hexanediol.

Chondrus Crispus Extract (Chondrus Crispus (Carrageenan) Extract) is a water-locking and moisture-keeping material extracted from natural seaweed, and its main active ingredient is Carrageenan, which is an important polysaccharide ingredient in carrageen and is a hydrophilic colloid. In cosmetics, the surface activity and water absorption of carrageenan can be used as emulsifier and stabilizer, and can prevent separation of suspended substances and make skin absorb well. In addition, the aqueous solution of Chondrus crispus extract has good consistency and can be used as thickener for cosmetic.

Ceramide (Ceramide) is a major part of the intercellular matrix and plays an important role in maintaining the water balance of the stratum corneum. Ceramides have a strong ability to associate with water molecules, and they maintain skin moisture by forming a network in the stratum corneum. Therefore, ceramide has the effect of retaining skin moisture.

In some preferred embodiments of the invention, the collagen material is: at least one of hydrolyzed collagen, hydrolyzed elastin, snail secretion filtrate, or combinations thereof.

In some more preferred embodiments of the invention, the collagen material is: hydrolyzed collagen and snail secretion filtrate.

The hydrolyzed collagen contains hydrophilic natural moisturizing factors and has a triple-helix structure, moisture can be locked strongly, the skin is protected to maintain a moist and tender state, protein molecules of the hydrolyzed collagen are small and are very easy to be absorbed by the skin, the absorbed hydrolyzed collagen is filled between the dermis of the skin, the tightness of the skin is increased, the skin tension is generated, pores of the skin are reduced, the skin becomes tight and elastic, and therefore the effects of fading fine wrinkles and stretching coarse wrinkles can be achieved. In addition, after the active hydrolyzed collagen is absorbed by the skin, the normal growth of cells in the skin can be effectively promoted, and the effect of skin repair is achieved.

The snail mucus contains collagen, elastin, urodermin, protein, vitamins, and glycolic acid. The glycolic acid in the snail mucus slightly peels the skin and promotes the metabolism of the skin; meanwhile, some nutrient substances have the function of nourishing the skin. After the snail mucus is simply treated, snail secretion filtrate can be obtained, and the snail secretion filtrate has the effects of efficiently replenishing water and locking water, removing old cutin, accelerating cell regeneration, and reducing skin wrinkles and scars.

In some preferred embodiments of the invention, the antioxidant is: at least one of vitamin E, astaxanthin, canthaxanthin, lutein, olive pomace, tocopherol acetate or combinations thereof.

In some more preferred embodiments of the invention, the antioxidant is: tocopheryl acetate and p-hydroxyacetophenone.

In some preferred embodiments of the invention, the emulsifier is: PEG-20 methyl glucose sesquistearate, glyceryl stearate \ PEG-100 stearate, polyacrylamide/C13-14 isoalkane/laureth-7, or their combination.

In some more preferred embodiments of the invention, the emulsifier is: PEG-20 methyl glucose sesquistearate, glyceryl stearate \ PEG-100 stearate and polyacrylamide/C13-14 isoalkane/laureth-7.

In some preferred embodiments of the present invention, the thickener is: at least one of xanthan gum, carbomer, triethanolamine or a combination thereof.

In some more preferred embodiments of the invention, the thickener is: carbomer and triethanolamine.

In some preferred embodiments of the invention, the collagen hydrating and moisturizing mask comprises the following components in parts by mass: 0.05-0.5 part of PEG-20 methyl glucose sesquistearate, 0.05-0.5 part of methyl glucose sesquistearate, 0.1-2 parts of ethylhexyl palmitate, 0.01-0.2 part of tocopherol acetate, 0.05-0.3 part of allantoin, 0.1-0.5 part of carbomer, 1-8 parts of glycerol, 0.1-0.5 part of triethanolamine, 0.005-0.2 part of sodium hyaluronate, 0.1-1.5 part of hydrolyzed collagen, 0.15-2 parts of Chondrus crispus extract, 0.002-0.1 part of ceramide 3, 0.1-2 parts of hydroxyphenylpropionamide benzoic acid, 0.5-4 parts of butanediol, 0.1-2 parts of 1, 2-hexanediol, 0.1-1 part of p-hydroxyacetophenone, 0.02-0.5 part of snail secretion, 0.1-0.8 part of glyceryl stearate, PEG-100 parts of glyceryl stearate, 0.2-2 parts of caprylic/capric acid triester, 0.05-0.3 part of polyacrylamide/C13-14 isoalkane/laureth-7 and 0.001-0.1 part of rose essence.

In some more preferred embodiments of the present invention, the collagen hydrating and moisturizing mask comprises the following components by mass: 0.1-0.4 part of PEG-20 methyl glucose sesquistearate, 0.1-0.4 part of methyl glucose sesquistearate, 0.5-1.5 parts of ethylhexyl palmitate, 0.02-0.1 part of tocopherol acetate, 0.08-0.2 part of allantoin, 0.12-0.4 part of carbomer, 2-6 parts of glycerol, 0.12-0.4 part of triethanolamine, 0.01-0.1 part of sodium hyaluronate, 0.2-1 part of hydrolyzed collagen, 0.2-1 part of carrageen crispus extract, 0.008-0.06 part of ceramide 3, 0.3-1.5 part of hydroxyphenylpropionamide benzoic acid, 1-3 parts of butanediol, 0.2-1.5 part of 1, 2-hexanediol, 0.2-0.8 part of p-hydroxy-phenyl ethyl ketone, 0.05-0.4 part of snail secretion filtrate, 0.2-0.6 part of stearic triglyceride stearate, 0.5-100 parts of PEG-caprylic acid/capric acid, 0.1-0.2 part of polyacrylamide/C13-14 isoalkane/laureth-7 and 0.002-0.01 part of rose essence.

In a second aspect of the present invention, there is provided a method for preparing a collagen hydrating and moisturizing mask according to the first aspect of the present invention, comprising the steps of:

mixing skin conditioner, antioxidant, humectant, collagen substance, emulsifier, thickener and water, and adding essence to obtain the final product.

According to a second aspect of the present invention, in some embodiments of the present invention, the method for preparing the collagen hydrating and moisturizing mask according to the first aspect of the present invention specifically comprises:

dissolving PEG-20 methyl glucose sesquistearate, ethylhexyl palmitate, tocopheryl acetate, allantoin, carbomer, glycerol, triethanolamine, sodium hyaluronate, hydrolyzed collagen, Chondrus crispus extract, ceramide 3, hydroxyphenyl propionamide benzoic acid, butanediol, 1, 2-hexanediol, p-hydroxyacetophenone and snail secretion filtrate in water, adding premixed glyceryl stearate \ PEG-100 stearate, caprylic/capric triglyceride, polyacrylamide/C13-14 isoalkane/laureth-7 and essence, and stirring.

The invention has the beneficial effects that:

1. the collagen hydrating and moisturizing mask contains various hydrating and moisturizing components, can nourish the skin moisture, and enables the skin to have good affinity. Meanwhile, the collagen skin cream is rich in a large amount of collagen substances, can repair skin cells, improve skin density, reduce skin wrinkles, enable the skin to be soft, full and elastic, lubricate cuticle, stimulate skin microcirculation, promote skin metabolism, and enable the skin to be fine, smooth and bright.

2. The preparation method of the collagen hydrating and moisturizing mask is simple and easy to implement, has an obvious effect, can meet the preparation requirements of large-scale production, and has extremely high economic value.

Detailed Description

In order to make the objects, technical solutions and technical effects of the present invention more clear, the present invention will be described in further detail with reference to specific embodiments. It should be understood that the detailed description and specific examples, while indicating the preferred embodiment of the invention, are intended for purposes of illustration only and are not intended to limit the scope of the invention.

The raw materials used, unless otherwise specified, are all consumables and reagents which are conventionally available commercially.

Example 1

A collagen hydrating and moisturizing mask is prepared by the following steps:

dissolving PEG-20 methyl glucose sesquistearate, ethylhexyl palmitate, tocopheryl acetate, allantoin, carbomer, glycerol, triethanolamine, sodium hyaluronate (from Cinfruida), hydrolyzed collagen (from BioStine HP), Chondrus crispus extract (from Cimick France), ceramide 3, hydroxyphenylpropionamide benzoic acid, butanediol, 1, 2-hexanediol, p-hydroxyacetophenone, and snail secretion filtrate (from Guangzhou Peng Rui) in water, then adding pre-mixed glyceryl stearate \ PEG-100 stearate (from Heda), caprylic/capric triglyceride (from COGNIS), polyacrylamide/C13-14 isoalkane/laureth-7 (from SEPPIC), and essence, and stirring.

The specific amounts of each component added are shown in table 1.

Example 2

A collagen hydrating and moisturizing mask is prepared by the following steps:

dissolving PEG-20 methyl glucose sesquistearate, ethylhexyl palmitate, tocopheryl acetate, allantoin, carbomer, glycerol, triethanolamine, sodium hyaluronate, hydrolyzed collagen, Chondrus crispus extract, ceramide 3, hydroxyphenyl propionamide benzoic acid, butanediol, 1, 2-hexanediol, p-hydroxyacetophenone and snail secretion filtrate in water, adding premixed glyceryl stearate \ PEG-100 stearate, caprylic/capric triglyceride, polyacrylamide/C13-14 isoalkane/laureth-7 and essence, and stirring.

The specific amounts of each component added are shown in table 1.

Example 3

A collagen hydrating and moisturizing mask is prepared by the following steps:

dissolving PEG-20 methyl glucose sesquistearate, ethylhexyl palmitate, tocopheryl acetate, allantoin, carbomer, glycerol, triethanolamine, sodium hyaluronate, hydrolyzed collagen, Chondrus crispus extract, ceramide 3, hydroxyphenyl propionamide benzoic acid, butanediol, 1, 2-hexanediol, p-hydroxyacetophenone and snail secretion filtrate in water, adding premixed glyceryl stearate \ PEG-100 stearate, caprylic/capric triglyceride, polyacrylamide/C13-14 isoalkane/laureth-7 and essence, and stirring.

The specific amounts of each component added are shown in table 1.

Example 4

A collagen hydrating and moisturizing mask is prepared by the following steps:

dissolving PEG-20 methyl glucose sesquistearate, ethylhexyl palmitate, tocopheryl acetate, allantoin, carbomer, glycerol, triethanolamine, sodium hyaluronate, hydrolyzed collagen, Chondrus crispus extract, ceramide 3, hydroxyphenyl propionamide benzoic acid, butanediol, 1, 2-hexanediol, p-hydroxyacetophenone and snail secretion filtrate in water, adding premixed glyceryl stearate \ PEG-100 stearate, caprylic/capric triglyceride, polyacrylamide/C13-14 isoalkane/laureth-7 and essence, and stirring.

The specific amounts of each component added are shown in table 1.

Comparative example 1

The method of preparing the moisturizing mask of comparative example 1 was identical to that of the collagen moisturizing mask of example 1 except that hydrolyzed collagen was not added.

The specific amounts of other components added are shown in table 1.

Comparative example 2

The method of preparing the moisturizing mask of comparative example 2 was identical to that of the collagen moisturizing mask of example 1 except that the carrageen crispus extract was not added.

The specific amounts of other components added are shown in table 1.

Comparative example 3

The method of preparing the moisturizing mask of comparative example 3 was identical to that of the collagen moisturizing mask of example 1 except that no hydroxyphenylpropionamide benzoic acid was added.

The specific amounts of other components added are shown in table 1.

Comparative example 4

The preparation method of the moisturizing mask of comparative example 4 was identical to that of the collagen moisturizing mask of example 1 except that the snail secretion filtrate was not added.

The specific amounts of other components added are shown in table 1.

TABLE 1 tables of formulations of examples and comparative examples

Effect testing experiment

And (4) testing the moisturizing effect:

selecting 80 volunteers aged 18-35 years and having skin complexion L values close to each other, uniformly dividing into 8 groups, measuring the initial skin hydration degree (averaging) of each group of volunteers, respectively using the moisturizing facial masks in the examples 1-4 and the comparative examples 1-4, keeping for 4 weeks once a day, testing the skin hydration degree (averaging) of each group of volunteers, and evaluating the moisturizing effect of the facial mask, wherein the test results are shown in Table 2.

TABLE 2 moisturizing effect of masks in examples and comparative examples

Duration of test	Example 1	Example 2	Example 3	Example 4	Comparative example 1	Comparative example 2	Comparative example 3	Comparative example 4
									0 week	45.0	46.5	45.8	46.1	45.5	46.3	45.7	46.2
4 weeks	76.1	71.6	79.8	78.2	65.1	66.4	66.1	65.5

From the results, it can be found that, in the case of consistent initial skin hydration degrees, after 4 weeks of tests, the skin hydration degrees of users using the facial masks of examples 1 to 4 are all above 70 and up to above 78, while the skin hydration degrees of users using the facial masks of comparative examples 1 to 4 with the ingredients deleted are only 65 to 67, which is significantly different from the test results of examples 1 to 4, and therefore, it can be fully demonstrated that the facial masks of examples 1 to 4 have excellent moisturizing effects, and significant moisturizing and reinforcing effects exist among the components, and have significant irreplaceability.

The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.