阅读说明：本技术 一种化妆品及其制备方法 (Cosmetic and preparation method thereof ) 是由 洪俊基 李昌炫 金利映 郝逸辰 郑越川 李娟� 赵振勋 于 2020-04-03 设计创作，主要内容包括：本申请实施例提供一种化妆品及其制备方法,涉及化妆品领域。化妆品包括填充于化妆品容器中的布,以及吸收到布中的化妆材料,化妆材料位于布的分离的线束之间的空间和/或布弯曲形成的空间中。化妆品的制备方法是在化妆品容器中填充布,且在填充布之前或之后在布中吸收化妆材料。本申请实施例是利用布吸收化妆材料,不拘于剂型使用容器,能够在任何容器中填充布之后吸收不同剂型的化妆材料,并通过布提高化妆材料的稳定性,以开发多种剂型和多种使用感的化妆材料,从而能够降低化妆品的容器费用。(The embodiment of the application provides a cosmetic and a preparation method thereof, and relates to the field of cosmetics. The cosmetic includes a cloth filled in a cosmetic container, and a cosmetic material absorbed into the cloth, the cosmetic material being located in a space between the separated strands of the cloth and/or a space formed by bending the cloth. The cosmetic is prepared by filling a cloth in a cosmetic container and absorbing the cosmetic material in the cloth before or after filling the cloth. The embodiment of the application utilizes the cloth to absorb the cosmetic materials, is not limited by a dosage form using container, can absorb the cosmetic materials of different dosage forms after the cloth is filled in any container, and improves the stability of the cosmetic materials through the cloth so as to develop the cosmetic materials of various dosage forms and various using feelings, thereby reducing the container cost of the cosmetic.)

1. A cosmetic characterized by comprising a cloth filled in a cosmetic container, and a cosmetic material absorbed into the cloth, the cosmetic material being located in a space between separated strands of the cloth and/or a space formed by bending the cloth.

2. The cosmetic according to claim 1, wherein the weight of the cosmetic material absorbed into the cloth is 10 to 100,000% by weight relative to the weight of the cloth.

3. The cosmetic as set forth in claim 1, wherein a net structure for blocking the cloth from flowing out of an extrusion port of the cosmetic container is provided in the cosmetic container; optionally, the mesh structure is disposed between the cloth and the extrusion opening, or disposed in the cloth, or wrapped outside the cloth.

4. The cosmetic according to any one of claims 1 to 3, wherein the cloth is selected from one or more of cotton cloth, cotton wool, linen, denim, ramie cloth, wool cloth, feather cloth, silk cloth, viscose fiber cloth, lyocell cloth, polylactic acid cloth, polyethylene terephthalate cloth, polyurethane cloth, polyethylene cloth, polypropylene cloth, polycaprolactam cloth, polyhexamethylene adipamide cloth, polytetrafluoroethylene cloth, polyvinyl chloride cloth, polyvinylidene chloride cloth, and polyvinyl alcohol cloth.

5. The cosmetic according to any one of claims 1 to 4, wherein the cosmetic material is in a form selected from one of an emulsion, a liquid, a solid and a dry powder.

6. The cosmetic according to any one of claims 1 to 5, wherein the cosmetic material is selected from one of skin lotion, skin milk, cream, essence, sunscreen, essential oil, makeup base, cream foundation, BB base, CC base, and concealer.

7. The cosmetic according to any one of claims 1 to 6, wherein the cosmetic container is selected from one of a hose, a vacuum bottle, a pump bottle, a press bottle, a stick shell, a pot body, a pan and a scale bottle.

8. A method for preparing a cosmetic as defined in claim 1, wherein a cloth is filled in the cosmetic container, and the cosmetic material is absorbed in the cloth before or after the cloth is filled.

9. The method for preparing a cosmetic according to claim 8, wherein the cosmetic container is refilled with the net structure provided inside the cloth or provided outside the cloth.

Technical Field

The application relates to the field of cosmetics, in particular to a cosmetic and a preparation method thereof.

Background

The cosmetic materials are generally dispensed, stored, sold and used in containers, and it is necessary to use a container suitable for the formulation or viscosity, and when other containers not suitable are used, problems such as reduction in stability or inconvenience in use occur. In general, skin lotion, skin cream, etc. are filled in a cosmetic water bottle, essence, foundation cream, etc. are filled in a pump bottle or a vacuum container, cream, BB cream, sunscreen cream, lip gloss, etc. are filled in a hose or a tank container, a mask is filled in a scale container, and an eye shadow, blush, foundation, two-purpose foundation, etc. are filled in a dish or foundation container. In recent years, with diversification of dosage forms and use feelings of cosmetics, it is urgently required to break through a fixed concept of using a conventional container, increase product stability, improve use feelings, and develop differentiated products.

There have been many publications that propose to put a foaming foam in the form of a sponge into a compact container and to fill a low-viscosity cosmetic material, breaking the concept of fixing a low-viscosity emulsion that requires the use of a cosmetic water bottle, and improving the problem that the use of an original cosmetic water bottle requires shaking due to the occurrence of phase separation due to the poor stability of the low-viscosity cosmetic material. However, the cosmetic material can exert the effect of improving the stability only by being impregnated into the pores of the porous foaming foam, the amount of the impregnated cosmetic material depends on the size or proportion of the pores of the foaming foam, the amount of impregnation is limited, and the effect of improving the stability cannot be obtained at all for the cosmetic material that has not entered the pores. Therefore, the foaming foam in the form of sponge requires an additional cutting process and, once cut into a desired shape, can be used only in a container of a corresponding shape, otherwise the cosmetic materials not impregnated in the pores of the foaming foam may still be phase-separated. Therefore, even if there are many containers, foamed foam in the form of sponge that can be used for each container is prepared separately.

Therefore, there is a need for a means for improving the stability of cosmetic materials regardless of the shape and formulation of the container.

Disclosure of Invention

An object of the present invention is to provide a cosmetic and a method for preparing the same, which can absorb a cosmetic material using a cloth, can absorb cosmetic materials of different formulations after filling the cloth in any container regardless of the formulation, and can improve the stability of the cosmetic material using the cloth, thereby developing cosmetic materials of various formulations and various feelings of use, and thus can reduce the container cost of the cosmetic.

In a first aspect, embodiments of the present application provide a cosmetic including a cloth filled in a cosmetic container, and a cosmetic material absorbed into the cloth, the cosmetic material being located in a space between separated strands of the cloth and/or a space formed by bending the cloth.

In the above technical solution, the present application fills the cloth in the cosmetic container, and the cloth can be deformed in the cosmetic container regardless of the shape of the cosmetic container, and thus can be commonly used in any container; furthermore, the cosmetic absorbed into the cloth is located in the space between the separated strands of the cloth and/or the space formed by bending the cloth, and the stability of the cosmetic can be improved by the support effect of the cloth, and the cosmetic can be stably protected regardless of the form of the cosmetic.

In one possible implementation, the weight of the cosmetic material absorbed into the cloth is 10 to 100,000% by weight relative to the weight of the cloth.

In the above-described aspect, when the cosmetic material is absorbed in an amount of 10 wt% to 100,000 wt% with respect to the weight of the cloth, since the cloth is woven by the strands and is not fixedly connected as a whole, the cloth can be self-expanded, and all the cosmetic material can be absorbed into the space between the separated strands of the cloth and/or the space formed by bending the cloth, without the cosmetic material being absorbed into the empty space between the strands of the cloth and the empty space formed by bending the cloth. If the weight of the cosmetic material absorbed into the cloth is less than 10 wt% with respect to the weight of the cloth, it is difficult to form a cosmetic that can be practically used, such as in the case of a liquid type cosmetic material, the cosmetic material can be squeezed out of the cosmetic container only if the weight ratio of the cosmetic material to the cloth is 10 wt% or more; in the case of solid and dry powder type cosmetic materials, if the weight of the cosmetic material absorbed into the cloth is less than 10% by weight with respect to the weight of the cloth, it is difficult to form into cosmetics. If the weight of the cosmetic material absorbed into the cloth is more than 100,000 wt% with respect to the weight of the cloth, the cloth hardly exerts its effect.

In one possible implementation, a net structure for blocking the cloth from flowing out of the extrusion opening of the cosmetic container is arranged in the cosmetic container; optionally, the mesh structure is disposed between the cloth and the extrusion opening, or disposed within the cloth, or wrapped disposed outside of the cloth.

In above-mentioned technical scheme, set up the network structure thing, not only can not influence the cosmetics material and flow out by the extrusion mouth of cosmetics container, but also can block cloth and flow out by the extrusion mouth, prevent to take out cloth and block the condition of extruding the mouth in order to hinder the cosmetics material and extrude when extruding the cosmetics material.

In one possible implementation, the cloth is selected from one or more of cotton cloth, absorbent cotton, linen, burlap, ramie cloth, wool cloth, feather cloth, silk cloth, viscose fiber woven cloth, lyocell woven cloth, polylactic acid cloth, polyethylene terephthalate cloth, polyurethane cloth, polyethylene cloth, polypropylene cloth, polycaprolactam cloth, polyhexamethylene adipamide cloth, polytetrafluoroethylene cloth, polyvinyl chloride cloth, polyvinylidene chloride cloth, and polyvinyl alcohol cloth.

In the technical scheme, the cloth has wide selection range and can absorb cosmetic materials.

In one possible implementation, the formulation of the cosmetic material is selected from one of an emulsion, a liquid, a solid, and a dry powder.

In the technical scheme, the cosmetic material has wide selection range of dosage forms, and can be applied to almost all dosage forms of cosmetic materials to form cosmetics.

In one possible implementation, the cosmetic material is selected from one of skin lotion, skin milk, cream, essence, sunscreen cream, essential oil, makeup cream, pre-makeup milk, foundation, BB cream, CC cream, and concealer.

In the technical scheme, the cosmetic material has wide selection range, and almost all cosmetics can be formed.

In one possible implementation, the cosmetic container is selected from one of a hose, a vacuum bottle, a pump bottle, a squeeze bottle, a stick shell, a can body, a cookie tray, and a scale bottle.

In the technical scheme, the cosmetic container has wide selection range and is not limited to the dosage form using container.

In a second aspect, the present embodiments provide a method for preparing a cosmetic product according to the first aspect, wherein a cloth is filled in a cosmetic container, and a cosmetic material is absorbed in the cloth before or after the cloth is filled.

In the technical scheme, the preparation method is simple and the preparation cost is low.

In one possible embodiment, the cosmetic container is refilled with the mesh structure inside the cloth or outside the cloth.

In the technical scheme, the net structure is arranged to limit the shape of the cloth, so that the process of filling the cloth into the cosmetic container is simpler and easier.

Drawings

In order to more clearly illustrate the technical solutions of the embodiments of the present application, the drawings that are required to be used in the embodiments of the present application will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present application and therefore should not be considered as limiting the scope, and that those skilled in the art can also obtain other related drawings based on the drawings without inventive efforts.

FIG. 1 is a photograph of No. 10 cosmetic material absorbed in polyethylene terephthalate cloth.

Detailed Description

In order to make the objects, technical solutions and advantages of the embodiments of the present application clearer, the technical solutions of the embodiments of the present application will be clearly and completely described below. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.

The following specifically describes the cosmetic and the method for producing the same according to the examples of the present application.

In a first aspect, embodiments of the present application provide a cosmetic including a cloth filled in a cosmetic container, and a cosmetic material absorbed into the cloth, the cosmetic material being located in a space between separated strands of the cloth and/or a space formed by bending the cloth.

In the art, "cosmetic material" means a content that cleans and beautifies the human body to enhance charm or appearance, or is used in a similar manner by painting, smearing, spraying, or the like in order to maintain or enhance the health of the skin or hair, exerts a cosmetic effect, and is expressed as a general composition; by "cosmetic product" is meant a cosmetic material contained in a container or an article of which the cosmetic material itself is capable of being used by a consumer. The "cosmetic product" of the present application means a cosmetic material contained in a container, and the cosmetic product of the present application can apply the discharged cosmetic material to the skin using the hand or a separate applicator.

In the art, "cloth" refers to a material woven from threads collected from plants, animals, or by-products thereof, or threads collected by post-processing or modification, or threads synthesized chemically, and used for producing clothes, quilts, and the like. In the present application, the cloth is woven from a bundle of wires, and has an advantage that it does not have a predetermined shape (i.e., an arbitrary shape), can be deformed to be adapted to any cosmetic container, and is easily filled. There is a space between the strands of the cloth itself (between the strands), and the cloth is curved (between the cloth surface and the cloth surface) to form a space according to the shape of the container after being filled in the cosmetic container. In the present application, even if not specifically described, "cosmetic material absorbed into the cloth" means that the cosmetic material is brought into contact with the cloth so that the cosmetic material is located in a vacant space between the strands constituting the cloth and the strands and/or a vacant space formed by bending the cloth. This application does not have the restriction to the length and the thickness of the pencil that constitute cloth, as long as there is the space between the pencil, and cloth can be crooked formation space can.

In actual use, the cloth with proper size can be cut out from the whole cloth or a plurality of cloth with same or different size, material and the like can be filled in the container for use.

It should be noted that the "porous material" in the prior art, such as a foam in the form of sponge, means a urethane foam having many small pores connected in a solid state, for example, on the surface or inside of a solid body. The pores do not mean solids completely separated from each other and empty spaces between the solids, and therefore, empty spaces between a body and a body of a porous substance composed of two or more bodies do not fall within the category of pores of the porous substance. Since the substances constituting the pores are fixed together, the size and impregnation amount of the pores are limited, and when the cosmetic material is filled in excess of the internal volume of the pores of the porous substance, an excessive amount of the cosmetic material exists outside the porous substance, and the effect of improving the stability of the cosmetic material cannot be achieved.

In some embodiments of the present application, the weight of the cosmetic material absorbed into the cloth is 10 wt% to 100,000 wt% relative to the weight of the cloth, i.e., the absorption rate of the cosmetic material in the cloth is 10 wt% to 100,000 wt%, such as 10 wt%, 100 wt%, 1,000 wt%, 10,000 wt%, 100,000 wt%, and the absorption rate is calculated according to the following formula:

absorption (% by weight) x 100 (weight of cosmetic material ÷ weight of cloth).

In the cosmetic filled with the cloth absorbing the cosmetic material of the present invention, in order to prevent the cloth from flowing out through the extrusion port, a net structure for blocking the cloth from flowing out through the extrusion port of the cosmetic container is provided in the cosmetic container; optionally, the mesh structure is disposed between the cloth and the extrusion opening, or disposed within the cloth, or wrapped disposed outside of the cloth.

In some embodiments of the present application, the thread material of the cloth for absorbing the cosmetic material may be selected from burlap, ramie cloth, flax cloth, canvas, oxford, slub oxford (slub oxford), jacquard cloth, tertian cloth, twill, plain cloth, sub-silk cloth, flannel, burlap (chambray), denim, corduroy, wool, damask, tweed, knot (bougler), heronsmen (herringbone), silk, satin, soft, chiffon, satin, polyester, blended fabric, jacquard (jacquard), Velvet (Velvet), acrylic, spandex, microfiber, oilfelt, knitting, rib cloth (shibori), rib yarn, sheepskin (reed), and lamb fabric.

The cloth in the application is selected from one or more than two of cotton figured cloth, absorbent cotton, linen, bur cloth, wool cloth, feather cloth, silk cloth, viscose fiber woven cloth, Richcel fiber woven cloth, Lyocell woven cloth, polylactic acid cloth, polyethylene terephthalate cloth, polyurethane cloth, polyethylene cloth, polypropylene cloth, polycaprolactam cloth, polyhexamethylene adipamide cloth, polytetrafluoroethylene cloth, polyvinyl chloride cloth, polyvinylidene chloride cloth and polyvinyl alcohol cloth.

The formulation of the cosmetic material received in the cloth is not particularly limited, and the formulation of the cosmetic material is selected from one of emulsion, liquid, solid and dry powder types. The emulsion may be one of oil-in-water, water-in-oil-in-water, and oil-in-water-in-oil type, the liquid may be one of water dispersion, gel, and oil dispersion type, the solid may be one of press bar and press cake type, and the dry powder may be one of powder and compressed powder type, but is not limited thereto.

The present application is not particularly limited in kind of cosmetic material, and may be combined with any existing cosmetic material for functional use or possible cosmetic material, and specifically, the cosmetic material is selected from one of skin care water skin, skin care lotion (lotion), face cream, essence (stress), sunscreen cream, essential oil (oil), makeup base cream (makeup base), makeup pre-lotion (primer), foundation (foundation), BB cream, CC cream, and concealer, but is not limited thereto.

The kind of the cosmetic container is not particularly limited in the present application, and may be any container, such as one selected from a hose, a vacuum bottle, a pump bottle, a dip bottle, a stick shell, a jar body (jar), a cookie tray, and a scale bottle, but is not limited thereto. The cosmetic of the present application is not limited to the dosage form container, and for example, the skin lotion and the skin milk may be filled into not only a cosmetic water bottle but also a tube; essence, makeup base liquid and the like are filled into a pump bottle or a vacuum container, and can be filled into a tank body and the like, so long as the makeup materials can flow out.

In a second aspect, embodiments of the present application provide a method of preparing a cosmetic as described above, filling a cloth in a cosmetic container, and absorbing a cosmetic material in the cloth before or after filling the cloth. The method specifically comprises the following steps: filling a cloth in the cosmetic container and absorbing the cosmetic material in the filled cloth; or filling a cosmetic container with a cosmetic material and filling a cloth to absorb the cosmetic material; or after the cosmetic material is absorbed in the cloth, the cosmetic container is filled with the cloth having the cosmetic material absorbed therein.

In the cosmetic filled with the cloth absorbing the cosmetic material, in order to facilitate the process of filling the cloth before absorbing the cosmetic material or the cloth absorbing the cosmetic material into the cosmetic container, the cosmetic container may further include a net structure disposed inside the cloth or a net structure disposed outside the cloth (disposed between the outside of the cloth and the extrusion port, or wrapped outside the cloth) to define the shape of the cloth, so that the process of filling the cloth before absorbing the cosmetic material or the cloth absorbing the cosmetic material into the cosmetic container may be simpler and easier, and blocking of the outflow of the cloth may be avoided.

The features and properties of the present application are described in further detail below with reference to examples.

The emulsion in the experiment was prepared using an emulsifying machine (t.k. robo miscs, SN 957015B, Tokushu Kika Kogyo co., japan); stirring with a stirrer (Heidon mixer, Model BL 1,200, new eastern science co., japan); appearance photographs were taken with a digital camera (Model DSC T-30, Sony co., japan); the photomicrographs were taken using a phase contrast microscope (Model BXF4, Olympus co., japan) and a digital image analyzer (Model TK-C138 1380U, Olympus co., japan).

To confirm the effect of the present application, an experiment was conducted to prepare a cosmetic material having poor stability in a formulation having relatively poor stability, and to compare whether the stability is improved by absorbing the same cosmetic material into a cloth.

One, ordinary cosmetic materials

No. 1: skin care lotion

TABLE 1 skin lotion formulation

Numbering	Name of raw materials	Content (wt%)
			1	Butanediol	10
2	Ethanol	10
			3	Glycerol	5
4	Perfume	5
			5	PEG-60 hydrogenated Castor oil	1
6	Purified water	to 100

The preparation method comprises the following steps: and weighing 1-6 raw materials, uniformly mixing the raw materials for 10 minutes at the normal temperature by using a stirrer at 400rpm, and sealing and storing the raw materials.

No. 2: skin care cream

TABLE 2 skin cream formulations

The preparation method comprises the following steps: weighing 1-2 raw materials simultaneously, adding 3 raw materials to prepare a water phase while stirring with a stirrer at normal temperature, adding 4-5 (oil phase) raw materials which are weighed separately and uniformly mixed while stirring the water phase with an emulsifying machine, emulsifying at 2,000rpm for 10 minutes, adding 6 raw materials, thickening, and sealing for storage.

No. 3: face cream

Table 3 formula of cream

Numbering	Name of raw materials	Content (wt%)
			1	Glycerol	10.00
2	Purified water	to 100
			3	Carbomer	0.10
4	Dimethicone	20.00
			5	Shea butter	2.00
6	Polysorbate 20	0.50
			7	Triethylamine	0.10

The preparation method comprises the following steps: simultaneously weighing 1-2 raw materials, adding 3 raw materials while stirring by a stirrer at 60 ℃ to prepare a water phase, adding 4-6 (oil phase) raw materials which are weighed separately and uniformly mixed and heated to 60 ℃ while stirring the water phase by an emulsifying machine, emulsifying for 10 minutes at 2,000rpm, adding 7 raw materials, thickening, and sealing for storage.

No. 4: essence liquid

Table 4 formula of essence

The preparation method comprises the following steps: weighing 1-3 raw materials simultaneously, adding 4 raw materials to prepare a water phase while stirring with a stirrer at normal temperature, adding 5-6 (oil phase) raw materials which are weighed separately and uniformly mixed while stirring the water phase with an emulsifying machine, emulsifying at 2,000rpm for 10 minutes, adding 7 raw materials, thickening, and sealing for storage.

No. 5: sunscreen cream

TABLE 5 formula of sunscreen cream

Numbering	Name of raw materials	Content (wt%)
			1	Purified water	to 100
2	Carbomer	0.15
			3	Cyclopentasiloxane	10.00
4	Ethyl hexyl methoxy cinnamate	5.00
			5	Ethyl hexyl salicylate	2.00
6	Bis-ethylhexyloxyphenol methoxyphenyl triazine	1.00
			7	Polysorbate 20	0.30
8	Triethylamine	0.15

The preparation method comprises the following steps: stirring the raw material 1 by a stirrer at normal temperature, adding the raw material 2 to prepare a water phase, stirring the water phase by an emulsifying machine, adding 3-7 (oil phase) of the raw materials which are weighed and uniformly mixed independently, emulsifying at 2,000rpm for 10 minutes, adding 8 of the raw materials, thickening, and sealing for storage.

No. 6: essential oil

TABLE 6 formulation of essential oils

The preparation method comprises the following steps: simultaneously weighing 1-2 raw materials, stirring the raw materials by a stirrer at normal temperature to prepare an oil phase, adding 3-5 (water phase) of the separately weighed and uniformly mixed raw materials while stirring the oil phase by an emulsifying machine, emulsifying the mixture at 2,000rpm for 10 minutes, and sealing and storing the mixture.

No. 7: make-up cream

TABLE 7 formula for sun screen

Numbering	Name of raw materials	Content (wt%)
			1	Dimethicone	40.00
2	PEG-10 dimethicone	1.00
			3	Titanium dioxide	3.00
4	Chromium oxide green	0.10
			5	Butanediol	10.00
6	Sodium chloride	0.50
			7	Purified water	to 100

The preparation method comprises the following steps: weighing 1-2 raw materials at the same time, stirring the raw materials by a stirrer at normal temperature, adding 3-4 raw materials to prepare an oil phase, stirring the oil phase by an emulsifying machine, adding 5-7 (water phase) raw materials which are weighed and uniformly mixed independently, emulsifying the mixture at 2,000rpm for 10 minutes, and sealing and storing the mixture.

No. 8: makeup cream

TABLE 8 formula of pre-makeup emulsion

Numbering	Name of raw materials	Content (wt%)
			1	Cyclopentasiloxane	to 100
2	Dimethicone	30.00
			3	Vinyl dimethicone polymer	10.00

The preparation method comprises the following steps: and weighing 1-2 raw materials, adding 3 raw materials while stirring by a stirrer at normal temperature, uniformly stirring at 2,000rpm for 10 minutes, and sealing for storage.

Number 9: foundation make-up liquid

TABLE 9 formulation of liquid foundation

Numbering	Name of raw materials	Content (wt%)
			1	Dimethicone	40.00
2	PEG-10 dimethicone	1.00
			3	Titanium dioxide	10.00
4	Yellow iron oxide	0.80
			5	Red iron oxide	0.50
6	Black iron oxide	0.20
			7	Butanediol	10.00
8	Sodium chloride	0.50
			9	Purified water	to 100

The preparation method comprises the following steps: weighing 1-2 raw materials at the same time, stirring the raw materials by a stirrer at normal temperature, adding 3-6 raw materials to prepare an oil phase, stirring the oil phase by an emulsifying machine, adding 7-9 (water phase) raw materials which are weighed and uniformly mixed independently, emulsifying the mixture at 2,000rpm for 10 minutes, and sealing and storing the mixture.

No. 10: BB cream

TABLE 10 formulation of BB cream

The preparation method comprises the following steps: weighing 1-3 raw materials at the same time, stirring the raw materials by a stirrer at 60 ℃, adding 4-7 raw materials to prepare an oil phase, stirring the oil phase by an emulsifying machine, adding 8-10 (water phase) raw materials which are weighed independently, heated to 60 ℃ and uniformly mixed, emulsifying the mixture at 2,000rpm for 10 minutes, cooling and sealing for storage.

Number 11: CC cream

TABLE 11 formulation of CC cream

Numbering	Name of raw materials	Content (wt%)
			1	Purified water	to 100
2	Butanediol	10.00
			3	Polyacrylamide sodium salt	0.30
4	Dimethicone	10.00
			5	Polysorbate 20	1.00
6	Titanium dioxide	5.00
			7	Yellow iron oxide	0.50
8	Red iron oxide	0.20
			9	Black iron oxide	0.10

The preparation method comprises the following steps: weighing 1-2 raw materials simultaneously, stirring by a stirrer at normal temperature, adding 3 raw materials to prepare a water phase, continuously stirring 4-5 raw materials which are weighed independently and uniformly mixed at normal temperature, adding 6-9 raw materials to prepare an oil phase, adding the oil phase while stirring the water phase by an emulsifying machine, emulsifying for 10 minutes at 2,000rpm, and sealing and storing.

Number 12: concealer

Watch 12 concealer formulation

Numbering	Name of raw materials	Content (wt%)
			1	Dimethicone	40.00
2	Microcrystalline wax	2.00
			3	PEG-10 dimethicone	1.00
4	Titanium dioxide	10.00
			5	Yellow iron oxide	0.80
6	Red iron oxide	0.50
			7	Black iron oxide	0.20
8	Butanediol	10.00
			9	Sodium chloride	0.50
10	Purified water	to 100

The preparation method comprises the following steps: weighing 1-3 raw materials simultaneously, adding 4-7 raw materials while stirring with a stirrer at 80 ℃ to prepare an oil phase, adding 8-10 (water phase) raw materials which are weighed separately and heated to 80 ℃ and mixed uniformly while stirring the oil phase with an emulsifying machine, emulsifying at 2,000rpm for 10 minutes, cooling, sealing and storing.

Second, stability improvement comparative experiment

(1) Absorption of cosmetic Material into cloth

The implementation mode is as follows: a No. 10 cosmetic material was added to a transparent container with a lid, and a polyethylene terephthalate cloth was filled, and the state of the cloth absorbing the cosmetic material was observed with a microscope.

FIG. 1 is a photomicrograph of a cloth-absorbed cosmetic material observed with a microscope, wherein a) is a photomicrograph of a polyethylene terephthalate cloth (X40); b) is a photomicrograph of polyethylene terephthalate cloth. As can be seen from fig. 1, the cosmetic material is stably located in the vacant spaces between the separated strands of the cloth and the strands and the vacant space formed by bending the cloth.

(2) Results of difference experiment according to filling method

The implementation mode is as follows: for the experiments, depending on whether there is stability or other differences that can occur with the filling method, the following methods were carried out: a. filling a container with cloth, and absorbing No. 10 cosmetic material in the filled cloth; b. filling a No. 10 cosmetic material in the container, and filling a cloth to absorb the cosmetic material; c. after absorbing the No. 10 cosmetic material in the cloth, the container was filled.

The experimental results are as follows: the results of experiments on whether or not there is a difference in stability or other characteristics that can be produced depending on the filling method show that no particular difference is found in the feeling of use including filling stability. Therefore, the order of filling the cloth and the cosmetic material or the cosmetic material after filling is absorbed and the cosmetic material is filled in the cloth, and the stability, the feeling of use, and the like are not affected.

(3) Stability improvement test according to dosage form

TABLE 13 cosmetic materials corresponding to various examples and comparative examples

The implementation mode is as follows: in a transparent container with a cover for stability inspection filled with 1g of cotton cloth, 50g of cosmetic materials No. 1 to No. 12 were absorbed to prepare cosmetics of examples 1 to 12; in the same container, 50g of cosmetic materials No. 1 to No. 12 were filled without cloth to prepare cosmetics of comparative examples 1 to 12; the resulting mixture was stored in a thermostatic bath at 45 ℃ and the separation stability was compared.

The experimental results are as follows: the results of comparing the separation stability of the examples in which the emulsion and the liquid type cosmetic material were absorbed in the cloth with that of the comparative examples in which the emulsion and the liquid type cosmetic material were not absorbed in the cloth in the constant temperature bath at 45 ℃ showed that the stability time of the comparative examples was only 3 or 4 days on average, and on the contrary, the examples were stable for three or more months, but the feeling of use after the filling of the examples was not different, and the specific results are shown in table 14.

TABLE 14 stabilization times for the different examples and comparative examples

(4) Stability improvement test according to the type of cloth

The implementation mode is as follows: in a transparent container with a cover for stability inspection filled with 1g of various cloths, 50g of cosmetic material No. 10 was absorbed to prepare the cosmetics of examples 13 to 33, and stored in a constant temperature bath at 45 ℃ to compare the separation stability.

TABLE 15 cloths for the different examples

The experimental results are as follows: the results of comparing the separation stability of the examples in which the cosmetic material No. 10 was absorbed in various cloths in a constant temperature bath at 45 ℃ showed that the stability time of the comparative examples without cloth filling was only 2 days, whereas the examples were stable for three months or more, but the feeling of use after filling was not different, and the specific results are shown in Table 16.

TABLE 16 stabilization time for various examples

Examples

Example 13

Example 14

Example 15

Example 16

Example 17

Example 18

Example 19

Time of settling

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

Examples

Example 20

Example 21

Example 22

Example 23

Example 24

Examples25

Example 26

Time of settling

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

Examples

Example 27

Example 28

Example 29

Example 30

Example 31

Example 32

Example 33

Time of settling

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

For more than 3 months

(5) Stability improvement test according to kinds of containers

The implementation mode is as follows: in various cosmetic containers filled with 1g of cotton figured cloth, 50g of cosmetic material No. 10 was absorbed to prepare cosmetics of examples 34 to 42, and together with cosmetics of comparative examples 34 to 42 prepared by filling 50g of cosmetic material No. 10 in the same container without cloth, the cosmetics were kept in a constant temperature bath at 45 ℃ and the separation stability was compared.

TABLE 17 Container for various examples and comparative examples

The experimental results are as follows: comparing the results of the separation stability in the 45 c constant temperature bath between the example of the present application using the cosmetic material No. 10 in various cosmetic containers and the comparative example of filling the cosmetic material in the same container without cloth, the stability time of the comparative example was only 2 days, and on the contrary, the examples were stable for three months or more, but the feeling of use after filling was not different, and the specific results are shown in table 18. Therefore, all cloths can be filled regardless of the type of container, depending on the container, without any inconvenience.

TABLE 18 stability of the various examples and comparative examples

Comparative example	Comparative example 34	Comparative example 35	Comparative example 36	Comparative example 37	Comparative example 38
						Time of settling	2 days	2 days	2 days	2 days	2 days
Comparative example	Comparative example 39	Comparative example 40	Comparative example 41	Comparative example 42	-
						Time of settling	2 days	2 days	2 days	2 days	-
Examples	Example 34	Example 35	Example 36	Example 37	Example 38
						Time of settling	For more than 3 months	For more than 3 months	For more than 3 months	For more than 3 months	For more than 3 months
Examples	Example 39	Example 40	EXAMPLE 41	Example 42	-
						Time of settling	For more than 3 months	For more than 3 months	For more than 3 months	For more than 3 months	-

(6) Examination of minimum absorbable amount

The implementation mode is as follows: a hose container of known weight was filled with 5g of various cloths, and 50g of No. 10 cosmetic material was absorbed to prepare cosmetics of examples 43 to 64; the amount of the remaining cosmetic material was measured by squeezing the whole cosmetic material out of the container for 30 women of 20 to 40 years old, and the remaining rate was calculated as follows:

the remaining ratio (% by weight) is (weight of remaining cosmetic material ÷ weight of cloth) × 100.

TABLE 19 cloths for the different examples

Examples	Example 43	Example 44	Example 45
				Cloth	Cotton	Absorbent cotton	Flax
Examples	Example 46	Example 47	Example 48
				Cloth	Coarse hemp	Ramie (Chinese Ramie)	Wool
Examples	Example 49	Example 50	Example 51
				Cloth	Feather	Silk cloth	viscose rayon
Examples	Example 52	Example 53	Example 54
				Cloth	polynosic rayon	lyocell	Polylactic acid
Examples	Example 55	Example 56	Example 57
				Cloth	Polyethylene terephthalate	Polyurethane	Polyethylene
Examples	Example 58	Example 59	Example 60
				Cloth	Polypropylene fiber	Polycaprolactam	Polyhexamethylene adipamide
Examples	Example 61	Example 62	Example 63
				Cloth	Polytetrafluoroethylene	Polyvinyl chloride	Polyvinylidene chloride
Examples	Example 64	-	-
				Cloth	Polyvinyl alcohol	-	-

The experimental results are as follows: when the present application was carried out using a cosmetic material and a plurality of cloths in a flexible tube container, and the amount of the remaining cosmetic material was measured for 30 women aged 20 to 40 by squeezing the entire cosmetic material out of the container, the remaining rate was not more than 10% by weight (average 8.7% by weight) based on the weight of the cloth filled, and the specific results are shown in table 20. Therefore, when the content is less than 10% by weight based on the weight of the cloth, it is not valuable as a cosmetic.

TABLE 20 survival rates of the different examples

(7) Examination of maximum absorbable amount

The implementation mode is as follows: in a transparent container with a cover for stability inspection filled with 0.05g of various cloths, 50g (an amount corresponding to 100,000 wt% of the weight of the cloths) of cosmetic material No. 10 was absorbed to prepare cosmetics of examples 65 to 86, which were stored in a constant temperature bath at 45 ℃ to compare separation stability.

TABLE 21 cloth for different examples

The experimental results are as follows: the stability results were compared by absorbing at an absorption rate of 100,000 wt% with respect to the weight of various cloths and storing in a constant temperature bath at 45 ℃ together with comparative examples, and the stabilization time of comparative examples was only 2 days, whereas examples were all stable for more than one month. This is because, when the cosmetic material is filled at 100,000% by weight, the cloth swells by itself, and bulk which is not absorbed by the cloth and exists outside cannot be seen, whereas when the absorption exceeds 100,000% by weight, a case similar to that in which the cloth is not used is also found, and therefore the effect which can be obtained when the cosmetic material is absorbed in the cloth may not be obtained.

(8) Panel test experiment

The implementation mode is as follows: absorbing a cosmetic material in cotton cloth to prepare the cosmetics of examples 87 to 98, and filling the same container with the same cosmetics to prepare comparative examples 87 to 98 in a cloth-free manner; 30 women of 20-40 years old were used as subjects and comparative tests of feeling of use, usability and the like were conducted.

TABLE 22 cosmetic materials for various examples and comparative examples

The experimental results are as follows: the results of comparative tests on the feeling of use, usability and the like of 30-position women aged 20 to 40 years for the examples of the present application and the comparative examples filled with the same material without cloth were similar to the results of the overall feeling of use of the comparative examples and examples, but the results of the examples were more excellent in usability, and particularly, the fluidity problem of the comparative examples was very serious for the types of emulsions and liquids, and the feeling of squeezing out of the containers was not good, but the examples were able to squeeze out an appropriate amount stably.

As described above, according to the cosmetics and the preparation method thereof of the embodiment of the present application, the cosmetic materials are absorbed by the cloth, and regardless of the form of the cosmetic container, the cosmetic materials of different forms can be absorbed after the cloth is filled in any container, and the stability of the cosmetic materials can be improved by the cloth, so that the cosmetics of various forms and various use feelings can be developed, and thus the cost of the cosmetic container can be reduced.

The above description is only an example of the present application and is not intended to limit the scope of the present application, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, improvement and the like made within the spirit and principle of the present application shall be included in the protection scope of the present application.