阅读说明：本技术 一种除醛净味纳米蜡 (Formaldehyde-removing odor-removing nano wax ) 是由 侯勇军 于 2020-06-16 设计创作，主要内容包括：本发明提供一种除醛净味纳米蜡,涉及纳米蜡技术领域。该除醛净味纳米蜡,包括有如下步骤：S1、除醛净味纳米蜡与去离子水在高压反应釜中按照一定的比例投放,S2、将反应釜边升温边搅拌边加压,S3、高压输送方式加入乳化剂,纳米钛,纳米锌,纳米硅,S4、保持反应釜的压力、转速和温度恒定1小时,S5、排进釜内压力,搅拌速度降低,S6、釜内压力恒定,以此种状态保持1小时,S7、加入小分子肽,搅拌速度提升,搅拌出料。该除醛净味纳米蜡,蜡质细腻,采高温高压乳化至纳米尺寸,渗透深入滋养基材强,特殊工艺镶嵌纳米粒子,除醛净味更尺久并能长效释放人体所需的负离子。(The invention provides aldehyde-removing odor-removing nano wax, and relates to the technical field of nano wax. The aldehyde-removing odor-removing nano wax comprises the following steps: s1, putting the aldehyde-removing odor-removing nano wax and deionized water in a high-pressure reaction kettle according to a certain proportion, S2, heating the reaction kettle, stirring and pressurizing, S3, adding an emulsifier, nano titanium, nano zinc, nano silicon and S4 in a high-pressure conveying mode, keeping the pressure, the rotating speed and the temperature of the reaction kettle constant for 1 hour, S5, discharging the pressure in the reaction kettle, reducing the stirring speed, S6, keeping the pressure in the reaction kettle constant for 1 hour, S7, adding small molecular peptides, increasing the stirring speed, stirring and discharging. The aldehyde-removing odor-removing nano wax is fine and smooth in wax, emulsified to a nano size by adopting high temperature and high pressure, and deeply permeated into a nourishing base material, and embedded with nano particles by a special process, so that the aldehyde-removing odor-removing nano wax is more durable and can release negative ions required by a human body for a long time.)

1. The aldehyde-removing odor-removing nano wax is characterized by comprising the following steps:

s1, putting the aldehyde-removing odor-removing nano wax and deionized water in a high-pressure reaction kettle according to a certain proportion;

s2, heating the reaction kettle while stirring and pressurizing, so that the high-pressure reaction kettle is heated to a certain degree and the pressure is constant for 2 hours;

s3, adding the emulsifier, the nano titanium, the nano zinc and the nano silicon in a high-pressure conveying mode;

s4, keeping the pressure, the rotating speed and the temperature of the reaction kettle constant for 1 hour after the addition is finished;

s5, discharging the pressure in the kettle, starting a vacuum pump, reducing the stirring speed, and transferring the interlayer fluid of the reaction kettle to a coolant fluid to ensure that the reaction kettle is reduced to a long temperature at a highest speed;

s6, keeping the pressure in the kettle at negative 0.5 MPa for 1 hour;

and S7, adding the small molecular peptide, increasing the stirring speed, stirring for 30 minutes and discharging.

2. The aldehyde-removing odor-removing nano wax as claimed in claim 1, which comprises the following steps: according to the operation procedure in S1, imported toothed wooden root wax was used as the nano-wax, and the ratio of the nano-wax to the deionized water was: 40 to 60.

3. The aldehyde-removing odor-removing nano-wax as claimed in claim 2, comprising the steps of: the temperature was increased to 130 ℃ according to the procedure in S2, the stirring speed was 600 rpm and the pressure was kept constant at 5 MPa.

4. The aldehyde-removing odor-removing nano wax as claimed in claim 1, which comprises the following steps: according to the operation procedure in S3, the proportion of the emulsifier is 3 percent, the proportion of the nano titanium is 1.5 percent, the proportion of the nano zinc is 1 percent, and the proportion of the nano silicon is 1.5 percent.

5. The aldehyde-removing odor-removing nano wax as claimed in claim 1, which comprises the following steps: the pressure in the reactor according to the procedure in S4 was 6 MPa, the stirring speed was 1500 rpm, and the temperature was 135 ℃.

6. The aldehyde-removing odor-removing nano wax as claimed in claim 1, which comprises the following steps: the stirring speed was reduced to 100 rpm according to the procedure in S5, and the temperature was 20 ℃.

7. The aldehyde-removing odor-removing nano wax as claimed in claim 1, which comprises the following steps: the proportion of small peptides was 5 points, up to 500 rpm, according to the procedure in S7.

Technical Field

The invention relates to the technical field of nano wax, in particular to aldehyde-removing odor-removing nano wax.

Background

Aqueous waxes are widely used in aqueous coatings: printing ink, glazing oil, wood coloring, adhesives, leather textiles, polishing products, special paper coatings and the like, and the water-based wax is an aqueous emulsion prepared from natural wax and/or synthetic wax and the like. The low melting point wax can give the leather surface a waxy feel, appropriately seal grain surface damage, improve leather stacking property, and prevent sticking during ironing or embossing. The wax emulsion with higher melting point can endow high gloss, can be polished, has excellent transparency, and can be used for coating aniline.

However, the water wax in the current market has single performance, only can perform nursing and brightening, is difficult to deeply permeate into a base material due to large wax particles, and has no aldehyde removal and odor purification functions.

Disclosure of Invention

The invention aims to provide an aldehyde-removing odor-removing nano wax, which solves the problems in the prior art.

In order to achieve the purpose, the invention is realized by the following technical scheme: an aldehyde-removing odor-removing nano wax comprises the following steps:

s1, adding the aldehyde-removing odor-removing nano wax and deionized water in a high-pressure reaction kettle according to a certain proportion.

S2, heating the reaction kettle while stirring and pressurizing, so that the temperature of the high-pressure reaction kettle is raised to a certain degree, and the pressure is constant for 2 hours.

S3, adding the emulsifier, the nano titanium, the nano zinc and the nano silicon in a high-pressure conveying mode.

And S4, keeping the pressure, the rotating speed and the temperature of the reaction kettle constant for 1 hour after the addition is finished.

And S5, discharging the pressure in the kettle, starting a vacuum pump, reducing the stirring speed, and transferring the interlayer fluid of the reaction kettle to the coolant fluid to ensure that the reaction kettle is extremely quickly cooled to the long temperature.

S6, keeping the pressure in the kettle at negative 0.5 MPa for 1 hour.

And S7, adding the small molecular peptide, increasing the stirring speed, stirring for 30 minutes and discharging.

Further, according to the operation in S1, the nano-wax was imported toothed wooden: 40 to 60.

Further, according to the operation procedure in S3, the proportion of the emulsifier is 3 percent, the proportion of the nano titanium is 1.5 percent, the proportion of the nano zinc is 1 percent, and the proportion of the nano silicon is 1.5 percent.

Further, according to the operation in S4, the pressure in the reaction vessel was set at 6 MPa, the stirring speed was set at 1500 rpm, and the temperature was set at 135 ℃.

Further, according to the operation in S5, the stirring speed was decreased to 100 rpm, and the temperature was 20 ℃.

Further, the ratio of the small molecule peptide was 5 points and increased to 500 rpm according to the procedure in S7.

The invention provides an aldehyde-removing odor-removing nano wax. The method has the following beneficial effects:

1. the wax is fine and smooth, emulsified to nanometer size by adopting high temperature and high pressure, and deeply permeated into a nourishing base material.

2. The nano particles are embedded in the special process, so that the formaldehyde is removed, the odor is removed for a longer time, and the negative ions required by a human body can be released for a long time.

Detailed Description

The invention provides a technical scheme that: an aldehyde-removing odor-removing nano wax comprises the following specific implementation steps:

s1, putting the aldehyde-removing odor-removing nano wax and deionized water in a high-pressure reaction kettle according to a certain proportion, wherein the nano wax is imported toothed wooden wax, and the proportion of the nano wax to the deionized water is as follows: 40 to 60.

S2, heating the reaction kettle while stirring and pressurizing, heating the high-pressure reaction kettle to a certain degree, heating to 130 ℃, stirring at a speed of 600 revolutions per minute, keeping the pressure at 5 MPa, and keeping the pressure constant for 2 hours.

S3, adding an emulsifier, nano titanium, nano zinc and nano silicon in a high-pressure conveying manner, wherein the proportion of the emulsifier is 3 percent, the proportion of the nano titanium is 1.5 percent, the proportion of the nano zinc is 1 percent, and the proportion of the nano silicon is 1.5 percent.

And S4, keeping the pressure, the rotating speed and the temperature of the reaction kettle constant for 1 hour after the addition is finished, wherein the pressure of the reaction kettle is 6 MPa, the stirring speed is 1500 rpm, and the temperature is 135 ℃.

And S5, discharging the pressure in the kettle, starting a vacuum pump, reducing the stirring speed, transferring the interlayer fluid of the reaction kettle to the coolant fluid to reduce the extreme speed of the reaction kettle to the long temperature, and reducing the stirring speed to 100 revolutions per minute at the temperature of 20 ℃.

S6, keeping the pressure in the kettle at negative 0.5 MPa for 1 hour.

And S7, adding small molecular peptides, wherein the proportion of the small molecular peptides is 5 points, increasing the stirring speed to 500 revolutions per minute, stirring for 30 minutes, and discharging.