阅读说明：本技术 一种制备电解锰的酸性电解液设备及其方法 (Acid electrolyte equipment for preparing electrolytic manganese and method thereof ) 是由 梅泽锋 刘萍 俞国洪 章汉云 于 2021-08-10 设计创作，主要内容包括：本发明涉及电解设备技术领域,且公开了一种制备电解锰的酸性电解液设备及其方法,包括电解箱,所述电解箱的右侧外壁底侧设置有出液管,所述出液管与电解箱的侧壁连通设置,所述电解箱的顶部中轴处设置有转轴,所述转轴贯穿电解箱的顶部并延伸至内部。该制备电解锰的酸性电解液设备及其方法,当需要制备大量电解液时,反应物会产生大量的气体,气体会推动导流板发生上下的移动,进而可以使研磨板在横杆和辅助连接杆的作用下可以沿着支撑杆的外壁上下滑动,从而可以对筛选板上的固体反应物进行敲击挤压破碎处理,以此可以增强固体反应物和液体反应物的接触面积,进而提高反应效果。(The invention relates to the technical field of electrolytic equipment and discloses acid electrolyte equipment for preparing electrolytic manganese and a method thereof. This preparation electrolytic manganese's acid electrolyte equipment and method, when needs preparation a large amount of electrolyte, the reactant can produce a large amount of gases, and gas can promote the guide plate and take place the removal from top to bottom, and then can make the lapping plate can slide from top to bottom along the outer wall of bracing piece under the effect of horizontal pole and auxiliary connecting rod to can strike extrusion crushing treatment to the solid reactant on the screening board, with this area of contact that can strengthen solid reactant and liquid reactant, and then improve reaction effect.)

1. An acid electrolyte equipment for preparing electrolytic manganese and a method thereof, comprising an electrolytic tank (1), characterized in that: the utility model discloses an electrolytic cell, including electrolysis box (1), drain pipe (11) are provided with to the right side outer wall bottom side of electrolysis box (1), the lateral wall intercommunication setting of drain pipe (11) and electrolysis box (1), the top axis department of electrolysis box (1) is provided with pivot (12), pivot (12) run through the top of electrolysis box (1) and extend to inside, the extension surface fixed connection of pivot (12) has a plurality of rotary rod (14), the top fixedly connected with motor (2) of pivot (12), the top of electrolysis box (1) is provided with two pan feeding pipes (13), two pan feeding pipe (13) set up respectively in the both sides of pivot (12), two pan feeding pipe (13) all set up with the top intercommunication of electrolysis box (1).

2. The acid electrolyte equipment and the method for preparing electrolytic manganese according to claim 1, wherein: the inside of electrolysis box (1) is provided with screening board (3), the outer wall of screening board (3) and the inner wall fixed connection of electrolysis box (1), the extension of pivot (12) sets up with the top external surface contact of screening board (3), the fixed arc solid-liquid separation membrane (31) that is provided with of one end that pivot (12) were kept away from in screening board (3), the internal fixed surface of arc solid-liquid separation membrane (31) is connected with a plurality of straight-bar (32), a plurality of the one end that arc solid-liquid separation membrane (31) were kept away from in straight-bar (32) slides inside the sieve mesh that sets up on screening board (3), a plurality of the surface of rotary rod (14) sets up with the external surface contact of screening board (3).

3. The acid electrolyte equipment and the method for preparing electrolytic manganese according to claim 2, wherein: the top outer wall fixedly connected with a plurality of bracing piece (4) of screening board (3), a plurality of the surface of bracing piece (4) is equipped with sleeve (41), a plurality of the surface of sleeve (41) is fixedly connected with horizontal pole (42) respectively, a plurality of the axis department surface of horizontal pole (42) is fixedly connected with extension spring (43), a plurality of the one end that horizontal pole (42) were kept away from in extension spring (43) respectively with the top outer wall fixed connection of screening board (3).

4. The acid electrolyte equipment and the method for preparing electrolytic manganese according to claim 3, wherein: the outer surface of the cross rod (42) is fixedly connected with a connecting rod (5) respectively, and the connecting rod (5) is far away from one end of the cross rod (42) and is fixedly connected with a guide plate (51) in an inclined mode.

5. The acid electrolyte equipment and the method for preparing electrolytic manganese according to claim 4, wherein: the guide plate is characterized in that the left end and the right end of the guide plate (51) are respectively fixedly connected with auxiliary rods (6), a sliding rod (61) is fixedly connected between the middle shafts of the two auxiliary rods (6), a sliding rod (62) is sleeved on the outer surface of the sliding rod (61), the two sliding rods (62) are fixedly connected through an elastic belt, and the two sliding rods (62) are respectively and fixedly connected with rubber rings (63) at the ends, far away from the sliding rod (61).

6. The acid electrolyte equipment and the method for preparing electrolytic manganese according to claim 5, wherein: the outer surface of the bottom of the middle shaft of the cross rods (42) is fixedly connected with auxiliary connecting rods (7) respectively, one ends, far away from the cross rods (42), of the auxiliary connecting rods (7) are provided with grinding plates (71) in a rotating mode respectively, and the side walls, close to one ends of the rotating shafts (12), of the grinding plates (71) are arranged in a contact mode with the outer walls of the rotating rods (14) respectively.

7. The acid electrolyte equipment and the method for preparing electrolytic manganese according to claim 6, wherein: the grinding plate (71) is internally hollowed, the grinding plate (71) is provided with grinding balls (72) in a rolling mode, wherein the grinding balls (72) are far away from one end of the auxiliary connecting rod (7), and the grinding balls (72) penetrate through the bottom wall of the grinding plate (71) and extend to the outside.

8. The acid electrolyte equipment and the method for preparing electrolytic manganese according to claim 7, wherein: the inside of abrasive disc (71) is provided with a plurality of vibrations ball (8), a plurality of the top outer wall of vibrations ball (8) passes through elastic plate (81) fixed connection with the top inner wall of abrasive disc (71), a plurality of the surface of the left and right sides of vibrations ball (8) articulates respectively has friction plate (82), a plurality of the surface of friction plate (82) sets up with the outer surface contact of a plurality of grinding ball (72) respectively, and is same through extrusion spring (83) fixed connection between two friction plates (82) on vibrations ball (8).

9. The acid electrolyte equipment and the method for preparing electrolytic manganese according to the claims 1 to 8, wherein the preparation method comprises the following steps;

s1: when a large amount of electrolyte need be prepared, the reactant can produce a large amount of gas, gas can promote guide plate (51) and take place the removal from top to bottom, and then can make lapping plate (71) can slide from top to bottom along the outer wall of bracing piece (4) under the effect of horizontal pole (42) and auxiliary connecting rod (7), thereby can strike extrusion crushing treatment to the solid reactant on screening plate (3), with this area of contact that can strengthen solid reactant and liquid reactant, and then improve reaction effect.

S2: the produced gas can be shunted to both sides under the action of the guide plate (51), and then the gas shunted to both sides can force the rubber ring (63) to deform outwards under the action of the sliding rod (62) and the sliding rod (61), and then the liquid reactant can be extruded and disturbed, so that the reaction effect of the solid reactant and the liquid reactant can be enhanced by utilizing the state.

S3: set up a plurality of pivot (12) through the surface at pivot (12), and then can realize the stirring to solid reactant and liquid reactant, and then strengthened the reaction effect, simultaneously under the state that lapping plate (72) reciprocated, the rotation of rotary rod (14) can be intermittent type nature and lapping plate (72) lateral wall rub, and then can promote lapping plate (72) under the effect of frictional resistance and transversely take place to rotate, thereby can realize that lapping plate (72) can also strengthen the grinding crushing effect to solid reactant when to liquid stirring.

S4: the grinding plate (72) moves up and down, so that the vibration balls (8) vibrate up and down in the grinding plate (71), the friction plate (82) can be forced to move along the outer surface of the grinding balls (72), the grinding balls (72) can rotate under the action of friction resistance, and therefore the grinding plate (71) can be matched with transverse rotation to provide a lateral grinding force for the solid reactant on the basis, and the grinding and crushing effects of the device on the solid reactant are enhanced.

S5: along with the reaction, the solid reactant is simultaneously ground and crushed, so that the volume of the solid reactant is smaller and smaller, the solid reactant with small volume can fall into the arc-shaped solid-liquid separation membrane (31) through the screening plate (3), the arc-shaped solid-liquid separation membrane (31) can vibrate up and down under the action of gravity, the straight rod (32) can be forced to move up and down along the inside of a sieve pore on the screening plate (3), due to the rotation of the grinding plate (71) and the rotating rod (14), the straight rod (32) can intermittently collide the grinding plate (71) and the rotating rod (14) in the up-and-down moving process, the crushing effect on the intermediate solid reactant can be enhanced under the action of the collision force, and when the straight rod (32) does not collide the grinding plate (71) and the rotating rod (14), the up-and-down moving of the straight rod (32) can provide a driving force for the solid reactant, the solid reactant can be overturned under the action of the pushing force, so that the contact area of the solid reactant and the liquid reactant is increased, and the reaction effect is enhanced.

Technical Field

The invention relates to the technical field of electrolytic equipment, in particular to acid electrolyte equipment for preparing electrolytic manganese and a method thereof.

Background

The electrolytic manganese metal is elemental metal which is obtained by acid leaching manganese ore to obtain manganese salt and then is sent to an electrolytic bath for electrolysis to be separated out, the electrolytic manganese metal has the appearance similar to iron, is irregular flaky, hard and brittle, has one bright surface and one rough surface, is silvery white to brown, and is silvery gray after being processed into powder; it is easy to oxidize in air, and when it meets with diluted acid, it can be dissolved and replaced by hydrogen, and when it is slightly higher than room temp., it can decompose water and release hydrogen.

When the electrolytic manganese is prepared, a manganese mixture which does not react with the acid electrolyte is generated when the manganese reacts with the acid electrolyte and is attached to the outer surface of the solid reactant, so that the reaction of the solid reactant and the acid electrolyte is hindered, and the reaction of the solid reactant and the acid electrolyte is not thorough.

Disclosure of Invention

The invention aims to provide acid electrolyte equipment for preparing electrolytic manganese and a method thereof, so as to solve the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme: the device comprises an electrolytic tank, wherein a liquid outlet pipe is arranged on the bottom side of the outer wall of the right side of the electrolytic tank, the liquid outlet pipe is communicated with the side wall of the electrolytic tank, a rotating shaft is arranged at the middle shaft of the top of the electrolytic tank, the rotating shaft penetrates through the top of the electrolytic tank and extends to the inside of the electrolytic tank, a plurality of rotating rods are fixedly connected to the outer surface of the extending part of the rotating shaft, a motor is fixedly connected to the top of the rotating shaft, two feeding pipes are arranged at the top of the electrolytic tank, the two feeding pipes are respectively arranged on two sides of the rotating shaft, and the two feeding pipes are communicated with the top of the electrolytic tank.

Preferably, the inside of electrolysis box is provided with the screening board, the outer wall of screening board and the inner wall fixed connection of electrolysis box, the extension of pivot sets up with the top surface contact of screening board, the fixed arc solid-liquid separation membrane that is provided with of one end that the pivot was kept away from to the screening board, the internal surface fixed connection of arc solid-liquid separation membrane has a plurality of straight-bar, a plurality of the one end that the arc solid-liquid separation membrane was kept away from to the straight-bar slides inside the sieve mesh of setting on the screening board, a plurality of the surface of rotary bar sets up with the surface contact of screening board.

Preferably, the top outer wall of the screening plate is fixedly connected with a plurality of supporting rods, the outer surfaces of the plurality of supporting rods are respectively sleeved with a sleeve, the outer surfaces of the plurality of sleeves are respectively and fixedly connected with a cross rod, the outer surfaces of the center shafts of the plurality of cross rods are respectively and fixedly connected with extension springs, and one ends, far away from the cross rod, of the extension springs are respectively and fixedly connected with the top outer wall of the screening plate.

Preferably, the outer surfaces of the cross rods are fixedly connected with connecting rods respectively, and the ends, far away from the cross rods, of the connecting rods are fixedly connected with guide plates in an inclined mode.

Preferably, the left end and the right end of the guide plate are respectively fixedly connected with an auxiliary rod, a sliding rod is fixedly connected between the middle shafts of the two auxiliary rods, sliding rods are sleeved on the outer surfaces of the two sliding rods and fixedly connected with each other through elastic belts, and rubber rings are respectively fixedly connected to the ends, far away from the sliding rods, of the two sliding rods.

Preferably, the outer surface of the bottom of the middle shaft of the plurality of cross rods is fixedly connected with an auxiliary connecting rod respectively, one ends, far away from the cross rods, of the plurality of auxiliary connecting rods are provided with grinding plates in a rotating mode respectively, and the side walls, close to one end of the rotating shaft, of the grinding plates are arranged in a contact mode with the outer walls of the rotating rods respectively.

Preferably, a plurality of the inside of abrasive disc is drawn empty and is set up, a plurality of the one end that auxiliary connecting rod was kept away from to the abrasive disc rolls and is provided with the grinding ball, a plurality of the grinding ball runs through the diapire of abrasive disc and extends to the outside.

Preferably, a plurality of vibration balls are arranged in the grinding plate, the top outer walls of the plurality of vibration balls are fixedly connected with the top inner wall of the grinding plate through elastic plates, the outer surfaces of the left side and the right side of each vibration ball are respectively hinged with a friction plate, the outer surfaces of the friction plates are respectively in contact with the outer surfaces of the plurality of grinding balls, and the two friction plates on the same vibration ball are fixedly connected through an extrusion spring.

The acid electrolyte equipment for preparing electrolytic manganese and the method thereof according to any one of the claims, comprising the steps of,

s1: when a large amount of electrolyte is prepared to needs, the reactant can produce a large amount of gas, and gas can promote the guide plate and take place removal from top to bottom, and then can make the lapping plate slide from top to bottom along the outer wall of bracing piece under the effect of horizontal pole and supplementary connecting rod to can strike extrusion broken handle to the solid reactant on the screening board, with this area of contact that can strengthen solid reactant and liquid reactant, and then improve reaction effect.

S2: the gas that produces can shunt to both sides under the effect of guide plate, and then can force the rubber circle to take place to outside deformation under the effect of slide bar and slide bar to the gas of both sides reposition of redundant personnel, and then can extrude the disturbance to liquid reactant to utilize this state can strengthen the reaction effect of solid reactant and liquid reactant.

S3: set up a plurality of pivot through the surface in the pivot, and then can realize the stirring to solid reactant and liquid reactant, and then strengthened the reaction effect, reciprocate simultaneously at the lapping plate under the state, the rotation of rotary rod can intermittent type nature and the lapping plate lateral wall rubs, and then can promote the lapping plate and transversely take place to rotate under the effect of frictional resistance to can realize that the lapping plate can also strengthen the grinding crushing effect to solid reactant when liquid stirring.

S4: the reciprocating of lapping plate can make vibrations ball about lapping plate is inside takes place, and then can force the friction plate to take place to remove along the surface of lapping ball, can make the lapping ball take place to rotate under the effect of frictional resistance to can cooperate the horizontal rotation of lapping plate to have a lateral grinding power for solid reactant on this basis, with this grinding crushing effect that has strengthened the device to solid reactant.

S5: the solid reactant is ground and crushed while being matched with the reaction, so that the volume of the solid reactant is smaller and smaller, the solid reactant with small volume can fall into the arc-shaped solid-liquid separation membrane through the screening plate, the arc-shaped solid-liquid separation membrane can vibrate up and down under the action of gravity, the straight rod can be forced to move up and down along the inside of the sieve pores on the screening plate, the straight rod can intermittently collide the grinding plate and the rotating rod in the up-and-down moving process due to the rotation of the grinding plate and the rotating rod, the crushing effect on the intermediate solid reactant can be enhanced under the action of the collision force, meanwhile, when the straight rod does not collide the grinding plate and the rotating rod, the up-and-down moving of the straight rod can provide a driving force for the solid reactant, the solid reactant can be overturned under the action of the driving force, and the contact area of the solid reactant and the liquid reactant is increased, the reaction effect is enhanced.

Compared with the prior art, the invention has the beneficial effects that:

(1) this preparation electrolytic manganese's acid electrolyte equipment and method, when needs preparation a large amount of electrolyte, the reactant can produce a large amount of gases, and gas can promote the guide plate and take place the removal from top to bottom, and then can make the lapping plate can slide from top to bottom along the outer wall of bracing piece under the effect of horizontal pole and auxiliary connecting rod to can strike extrusion crushing treatment to the solid reactant on the screening plate, with this area of contact that can strengthen solid reactant and liquid reactant, and then improve reaction effect.

(2) The generated gas can be shunted to two sides under the action of the guide plate, and then the gas shunted to the two sides can force the rubber ring to deform outwards under the action of the sliding rod and the sliding rod, so that the liquid reactant can be extruded and disturbed, and the reaction effect of the solid reactant and the liquid reactant can be enhanced by utilizing the state.

(3) This preparation electrolytic manganese's acid electrolyte equipment and method, surface through at the pivot sets up a plurality of pivot, and then can realize the stirring to solid reactant and liquid reactant, and then strengthened the reaction effect, simultaneously under the state that the lapping plate reciprocated, the rotation of rotary rod can intermittent type nature and rub with the lapping plate lateral wall, and then can promote the lapping plate under the effect of frictional resistance and transversely take place to rotate, thereby can realize that the lapping plate can also strengthen the grinding crushing effect to solid reactant when stirring to liquid.

(4) The up-and-down movement of the grinding plate can enable the vibration ball to vibrate up and down in the grinding plate, so that the friction plate can be forced to move along the outer surface of the grinding ball, the grinding ball can be rotated under the action of friction resistance, and therefore lateral grinding force can be provided for the solid reactant by matching with the transverse rotation of the grinding plate on the basis, and the grinding and crushing effects of the device on the solid reactant are enhanced.

(5) The acid electrolyte equipment and the method for preparing electrolytic manganese are characterized in that the equipment and the method are matched with the grinding and crushing treatment of the solid reactant along with the reaction, so that the volume of the solid reactant is smaller and smaller, the small-volume solid reactant can fall into the arc-shaped solid-liquid separation membrane through the screening plate, the arc-shaped solid-liquid separation membrane can vibrate up and down under the action of gravity, the straight rod can be forced to move up and down along the inside of a sieve pore on the screening plate, the straight rod can intermittently collide the grinding plate and the rotating rod in the up-and-down moving process due to the rotation of the grinding plate and the rotating rod, the crushing effect of the middle solid reactant can be enhanced under the action of the collision force, meanwhile, when the straight rod does not collide the grinding plate and the rotating rod, the up-and-down moving of the straight rod can provide a driving force for the solid reactant, and the solid reactant can be overturned under the action of the driving force, thereby increasing the contact area of the solid reactant and the liquid reactant and enhancing the reaction effect.

Drawings

FIG. 1 is a schematic view of the overall structure of the present invention;

FIG. 2 is a half sectional view of the overall structure of the present invention;

FIG. 3 is a schematic view of the internal structure of the electrolytic tank of the present invention;

FIG. 4 is a schematic view of the overall structure of the polishing plate according to the present invention;

FIG. 5 is an enlarged view of A of FIG. 2 according to the present invention;

FIG. 6 is an enlarged view of B of FIG. 4 according to the present invention;

FIG. 7 is a flow chart of the preparation method of the present invention.

In the figure: 1. an electrolytic tank; 11. a liquid outlet pipe; 12. a rotating shaft; 13. a feeding pipe; 14. rotating the rod; 2. a motor; 3. screening the plate; 31. an arc-shaped solid-liquid separation membrane; 32. a straight rod; 4. a support bar; 41. a sleeve; 42. a cross bar; 43. an extension spring; 5. a connecting rod; 51. a baffle; 6. an auxiliary lever; 61. a slide bar; 62. a slide bar; 63. a rubber ring; 7. an auxiliary connecting rod; 71. a grinding plate; 72. grinding balls; 8. a vibration ball; 81. an elastic plate; 82. a friction plate; 83. compressing the spring.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1-7, the present invention provides a technical solution: an acid electrolyte device for preparing electrolytic manganese and a method thereof, comprising an electrolytic tank 1, the purpose of the arrangement is to contain electrolyte, a liquid outlet pipe 11 is arranged at the bottom side of the outer wall of the right side of the electrolytic tank 1, the purpose of the arrangement is to facilitate liquid outlet, the liquid outlet pipe 11 is communicated with the side wall of the electrolytic tank 1, the purpose of the arrangement is to facilitate liquid discharge, a rotating shaft 12 is arranged at the middle shaft of the top of the electrolytic tank 1, the purpose of the arrangement is to facilitate the arrangement of the rotating shaft 12, the rotating shaft 12 penetrates through the top of the electrolytic tank 1 and extends to the inside, the purpose of the arrangement is to facilitate the rotation of the rotating shaft 12, a plurality of rotating rods 14 are fixedly connected to the outer surface of the extending part of the rotating shaft 12, the purpose of the arrangement is to facilitate the arrangement of the rotating rods 14, a motor 2 is fixedly connected to the top of the rotating shaft 12, and the purpose of the arrangement is to facilitate power supply, the top of electrolysis box 1 is provided with two pan feeding pipes 13, and the purpose that sets up like this is for the ease of the pan feeding, and two pan feeding pipes 13 set up the both sides at pivot 12 respectively, and the purpose that sets up like this is for the ease of the pan feeding, and two pan feeding pipes 13 all set up with the top intercommunication of electrolysis box 1, and the purpose that sets up like this is for the ease of the pan feeding.

Preferably, in this embodiment, in order to facilitate separation of solid and liquid, the inside of the electrolytic tank 1 is provided with the screening plate 3, the purpose of such setting is to facilitate setting of the screening plate 3, the outer wall of the screening plate 3 is fixedly connected with the inner wall of the electrolytic tank 1, the purpose of such setting is to facilitate fixing of the screening plate 3, the extending portion of the rotating shaft 12 is arranged in contact with the outer surface of the top of the screening plate 3, the purpose of such setting is to facilitate stirring and overturning of the solid, one end of the screening plate 3, which is far away from the rotating shaft 12, is fixedly provided with the arc-shaped solid-liquid separation membrane 31, the purpose of such setting is to facilitate solid-liquid separation, the inner surface of the arc-shaped solid-liquid separation membrane 31 is fixedly connected with a plurality of straight rods 32, the purpose of such setting is to facilitate setting of the straight rods 32, one end of the plurality of the straight rods 32, which is far away from the arc-shaped solid-liquid separation membrane 31, is slidably arranged inside the sieve holes on the screening plate 3, the purpose of this is to facilitate the pressing of the solid, and the outer surface of the plurality of rotating rods 14 is in contact with the outer surface of the sieving plate 3, and this is to facilitate the stirring and inverting of the solid.

Preferably, in this embodiment, in order to facilitate carrying out the extrusion breakage to the solid, a plurality of bracing piece 4 of top outer wall fixedly connected with of screening plate 3, the purpose that sets up like this is for facilitating setting up bracing piece 4, the surface of a plurality of bracing piece 4 is equipped with sleeve 41 respectively, the purpose that sets up like this is for facilitating setting up sleeve 41, the surface difference fixedly connected with horizontal pole 42 of a plurality of sleeve 41, the purpose that sets up like this is for facilitating setting up horizontal pole 42, the axis department surface difference fixedly connected with extension spring 43 of a plurality of horizontal pole 42, the purpose that sets up like this is for facilitating setting up extension spring 43, the one end that horizontal pole 42 was kept away from to a plurality of extension spring 43 is respectively with the top outer wall fixed connection of screening plate 3, the purpose that sets up like this is for facilitating fixing extension spring 43.

Preferably, in this embodiment, in order to facilitate the up-and-down movement using the sleeve 41, the outer surfaces of the plurality of cross bars 42 are respectively and fixedly connected with the connecting rods 5, and the purpose of the arrangement is to facilitate the fixing of the connecting rods 5, and one end of the plurality of connecting rods 5 far away from the cross bars 42 is obliquely and fixedly connected with the guide plate 51, and the purpose of the arrangement is to facilitate the arrangement of the guide plate 51.

Preferably, in this embodiment, in order to facilitate the utilization of the shunting effect of the guide plate 51 and further disturb the liquid, the auxiliary rods 6 are fixedly connected to the left and right ends of the guide plate 51 respectively, the purpose of setting up is to facilitate the setting up of the auxiliary rods 6, the slide rods 61 are fixedly connected between the middle axes of the two auxiliary rods 6, the purpose of setting up is to facilitate the setting up of the slide rods 61, the outer surface sleeves of the two slide rods 61 are provided with the slide rods 62, the purpose of setting up is to facilitate the setting up of the slide rods 62, the purpose of setting up is to facilitate the resetting of the slide rods 62 through the elastic band fixed connection between the two slide rods 62, one end of each slide rod 62 away from the slide rod 61 is fixedly connected with the rubber ring 63, and the purpose of setting up is to facilitate the setting up of the rubber ring 63.

Preferably, in this embodiment, in order to facilitate the extrusion grinding of the solid, the outer surface of the bottom of the central axis of the plurality of cross rods 42 is fixedly connected with the auxiliary connecting rods 7 respectively, the purpose of the setting is to facilitate the setting of the auxiliary connecting rods 7, one ends of the plurality of auxiliary connecting rods 7, which are far away from the cross rods 42, are rotatably provided with the grinding plates 71 respectively, the purpose of the setting is to facilitate the setting of the grinding plates 71, the side walls of the plurality of grinding plates 71, which are near one end of the rotating shaft 12, are in contact with the outer walls of the rotating rods 14 respectively, and the purpose of the setting is to facilitate the rotation of the grinding plates 71.

Preferably, in this embodiment, in order to enhance the grinding effect of the grinding plate 71 on the solid, the grinding plates 71 are hollowed out, so as to facilitate the arrangement of the grinding balls 72, and one end of each grinding plate 71, which is away from the auxiliary connecting rod 7, is provided with the grinding balls 72 in a rolling manner, so as to facilitate the rotation of the grinding balls 72, and the grinding balls 72 penetrate through the bottom wall of the grinding plate 71 and extend to the outside, so as to facilitate the grinding of the grinding balls 72 on the solid.

Preferably, in this embodiment, in order to realize the rotation of the grinding balls 72, a plurality of vibration balls 8 are provided inside the grinding plate 71, the purpose of this arrangement is to facilitate the arrangement of the vibration balls 8, the top outer walls of a plurality of vibration balls 8 are fixedly connected with the top inner wall of the grinding plate 71 through the elastic plate 81, the purpose of this arrangement is to facilitate the resetting of the vibration balls 8, the outer surfaces of the left and right sides of the plurality of vibration balls 8 are respectively hinged with friction plates 82, this is for the purpose of facilitating the arrangement of the friction plates 82, the outer surfaces of the plurality of friction plates 82 are respectively arranged in contact with the outer surfaces of the plurality of grinding balls 72, this is provided in order to facilitate the friction of the friction plates 82 with the grinding balls 72, and the two friction plates 82 on the same vibration ball 8 are fixedly connected by the pressing spring 83, and this is provided in order to facilitate the quick return rotation of the friction plates 82.

An acid electrolyte equipment for preparing electrolytic manganese and a method thereof, the preparation method is as follows;

when a large amount of electrolyte is prepared to needs, the reactant can produce a large amount of gas, and gas can promote guide plate 51 and take place the removal from top to bottom, and then can make lapping plate 71 can slide from top to bottom along the outer wall of bracing piece 4 under the effect of horizontal pole 42 and supplementary connecting rod 7 to can strike extrusion broken handle to the solid reactant on the screening plate 3, with this area of contact that can strengthen solid reactant and liquid reactant, and then improve reaction effect.

The gas that produces can shunt to both sides under the effect of guide plate 51, and then the gas of shunting to both sides can force rubber circle 63 to take place to outside deformation under the effect of slide bar 62 and slide bar 61, and then can extrude the disturbance to the liquid reactant to utilize this state can strengthen the reaction effect of solid reactant and liquid reactant.

Set up a plurality of pivot 12 through the surface at pivot 12, and then can realize the stirring to solid reactant and liquid reactant, and then strengthened the reaction effect, simultaneously under the state that lapping plate 72 reciprocated, the rotation of rotary rod 14 can be intermittent type nature and the rubbing board 72 lateral wall rubs, and then can promote lapping plate 72 under the effect of frictional resistance and transversely take place the rotation, thereby can realize that lapping plate 72 can also strengthen the grinding crushing effect to solid reactant when stirring to liquid.

The up-and-down movement of the grinding plate 72 can cause the vibration balls 8 to vibrate up and down in the grinding plate 71, further force the friction plate 82 to move along the outer surface of the grinding balls 72, and enable the grinding balls 72 to rotate under the action of friction resistance, so that the lateral grinding force can be provided for the solid reactant on the basis of the lateral rotation of the grinding plate 71, and the grinding and crushing effects of the device on the solid reactant are enhanced.

Along with the reaction, the solid reactant is simultaneously ground and crushed, so that the volume of the solid reactant is smaller and smaller, the solid reactant with small volume can fall into the arc-shaped solid-liquid separation membrane 31 through the screening plate 3, the arc-shaped solid-liquid separation membrane 31 can vibrate up and down under the action of gravity, the straight rod 32 can be forced to move up and down along the inside of the sieve holes on the screening plate 3, due to the rotation of the grinding plate 71 and the rotating rod 14, the straight rod 32 can intermittently collide the grinding plate 71 and the rotating rod 14 in the up-and-down moving process, the crushing effect on the intermediate solid reactant can be enhanced under the action of the collision force, meanwhile, when the straight rod 32 does not collide the grinding plate 71 and the rotating rod 14, the up-and-down moving of the straight rod 32 can provide a driving force for the solid reactant, and the solid reactant can turn over under the action of the driving force, thereby increasing the contact area of the solid reactant and the liquid reactant and enhancing the reaction effect.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.