Self-cleaning mass spectrum device and mass spectrometer

文档序号:1447958 发布日期:2020-02-18 浏览:19次 中文

阅读说明:本技术 一种自清洗质谱装置和质谱仪 (Self-cleaning mass spectrum device and mass spectrometer ) 是由 肖鸿翔 于 2019-11-12 设计创作,主要内容包括:本发明公开了一种自清洗质谱装置和质谱仪,包括装置本体与清洗机构,所述清洗机构固定安装在装置本体的左侧,所述装置本体包括质谱仪本体、进料口、出料口、检测板、分隔板,所述质谱仪本体顶部的右侧设置有进料口,所述质谱仪本体右侧的底部设置有出料口,所述质谱仪本体的内壁上设置有检测用检测板,所述质谱仪本体的内壁上且位于检测板的左侧设置有分隔板。本发明通过装置本体与清洗机构之间的相互配合,实现了一种自清洗质谱装置和质谱仪,利用反冲洗功能对检测板上粘附的基质进行清理,不仅能够实现对器件的清理,为质谱仪的再次使用提供了良好的基础,而且不需要拆卸繁琐的部件,从而为工作人员提供了便利。(The invention discloses a self-cleaning mass spectrometry device and a mass spectrometer, which comprise a device body and a cleaning mechanism, wherein the cleaning mechanism is fixedly arranged on the left side of the device body, the device body comprises a mass spectrometer body, a feeding hole, a discharging hole, a detection plate and a partition plate, the feeding hole is formed in the right side of the top of the mass spectrometer body, the discharging hole is formed in the bottom of the right side of the mass spectrometer body, the detection plate for detection is arranged on the inner wall of the mass spectrometer body, and the partition plate is arranged on the inner wall of the mass spectrometer body and positioned on the. According to the self-cleaning mass spectrometer and the cleaning mechanism, the self-cleaning mass spectrometer and the cleaning mechanism are matched with each other, the matrix adhered to the detection plate is cleaned by utilizing the back washing function, so that not only can the cleaning of devices be realized, a good foundation is provided for the reuse of the mass spectrometer, but also the complex parts do not need to be disassembled, and therefore convenience is provided for workers.)

1. A self-cleaning mass spectrometer device and a mass spectrometer, comprising a device body (1) and a cleaning mechanism (2), characterized in that: the cleaning mechanism (2) is fixedly arranged on the left side of the device body (1);

the device body (1) comprises a mass spectrometer body (101), a feeding hole (102), a discharging hole (103), a detection plate (104) and a partition plate (105), wherein the feeding hole (102) is formed in the right side of the top of the mass spectrometer body (101), the discharging hole (103) is formed in the bottom of the right side of the mass spectrometer body (101), the detection plate (104) for detection is arranged on the inner wall of the mass spectrometer body (101), and the partition plate (105) is arranged on the inner wall of the mass spectrometer body (101) and located on the left side of the detection plate (104);

the cleaning mechanism (2) comprises a limiting fixing rod (201), a limiting sliding rod (202), a piston plate (203), a piston sealing gasket (204), a reset spring (205), a servo motor (206), an extrusion cam (207), an inlet pipe (208) and an outlet pipe (209), wherein the limiting fixing rod (201) is fixedly installed between the left side of the inner wall of the mass spectrometer body (101) and the partition plate (105), the limiting sliding rod (202) is arranged at the middle point of the bottom of the limiting fixing rod (201), the top of the limiting sliding rod (202) penetrates through the limiting fixing rod (201) and extends to the outside of the limiting fixing rod to be fixedly connected with the piston plate (203), the piston sealing gasket (204) is fixedly connected to the edge of the piston plate (203), the reset spring (205) is sleeved on the surface of the limiting sliding rod (202) and the position between the limiting fixing rod (201), the back fixed mounting of mass spectrograph body (101) has servo motor (206), the output of servo motor (206) runs through mass spectrograph body (101) and extends to the inside fixedly connected with extrusion cam (207) of mass spectrograph body (101), the left bottom of mass spectrograph body (101) is provided with into pipe (208), division board (105) left bottom is provided with exit tube (209).

2. A self-cleaning mass spectrometry apparatus and mass spectrometer according to claim 1 wherein: and one side of the piston sealing gasket (204) close to the mass spectrometer body (101) and one side of the separation plate (105) are in contact with each other.

3. A self-cleaning mass spectrometry apparatus and mass spectrometer according to claim 1 wherein: the top of the return spring (205) is fixedly connected with the bottom of the piston plate (203), and the bottom of the return spring (205) is fixedly connected with the top of the limiting fixing rod (201).

4. A self-cleaning mass spectrometry apparatus and mass spectrometer according to claim 1 wherein: the side of the extrusion cam (207) close to the piston plate (203) is contacted with the piston plate.

5. A self-cleaning mass spectrometry apparatus and mass spectrometer according to claim 1 wherein: advance and be provided with first check valve (3) on pipe (208), first check valve (3) are for advancing right play from a left side, the left side of advancing pipe (208) is provided with flange.

6. A self-cleaning mass spectrometry apparatus and mass spectrometer according to claim 1 wherein: and a second one-way valve (4) is arranged on the outlet pipe (209), and the second one-way valve (4) is left-in and right-out.

Technical Field

The invention relates to the technical field of mass spectrometers, in particular to a self-cleaning mass spectrometer and a mass spectrometer.

Background

Mass spectrometers are also known as mass spectrometers. Apparatus for separating and detecting different isotopes. That is, based on the principle that charged particles can deflect in an electromagnetic field, the instrument separates and detects the composition of substances according to the mass difference of substance atoms, molecules or molecular fragments. Mass spectrometers are divided into isotope mass spectrometers, inorganic mass spectrometers and organic mass spectrometers in terms of the range of applications. Mass spectrometers with high resolution, medium resolution and low resolution according to resolution power; it is classified into a static instrument and a dynamic instrument according to the working principle. The mass spectrometer mainly detects a sample through a detection plate, and different matrixes are easily adsorbed on the detection plate after the mass spectrometer is used for a long time, so that the mass spectrometer needs to be cleaned and maintained. The current common cleaning method is to remove the polluted device and then use organic solvent to carry out flow cleaning, if necessary, the polluted device needs to be removed for ultrasonic cleaning, the cleaning and maintenance method needs organic solvent, and the removing process is complicated.

Disclosure of Invention

The invention provides a self-cleaning mass spectrometry device and a mass spectrometer for solving the problems.

In order to achieve the purpose, the invention provides the following technical scheme: a self-cleaning mass spectrum device and a mass spectrometer comprise a device body and a cleaning mechanism, wherein the cleaning mechanism is fixedly arranged on the left side of the device body;

the device body comprises a mass spectrometer body, a feeding hole, a discharging hole, a detection plate and a partition plate, wherein the feeding hole is formed in the right side of the top of the mass spectrometer body, the discharging hole is formed in the bottom of the right side of the mass spectrometer body, the detection plate for detection is arranged on the inner wall of the mass spectrometer body, and the partition plate is arranged on the inner wall of the mass spectrometer body and located on the left side of the detection plate;

the cleaning mechanism comprises a limiting fixed rod, a limiting slide rod, a piston plate, a piston sealing gasket, a reset spring, a servo motor, an extrusion cam, an inlet pipe and an outlet pipe, wherein the limiting fixed rod is fixedly arranged between the left side of the inner wall of the mass spectrometer body and the separation plate, the limiting slide rod is arranged at the middle point of the bottom of the limiting fixed rod, the top of the limiting slide rod penetrates through the limiting fixed rod and extends to the outside of the limiting fixed rod to be fixedly connected with the piston plate, the edge of the piston plate is fixedly connected with the piston sealing gasket, the reset spring is sleeved on the surface of the limiting slide rod and the position between the limiting fixed rod and the piston plate, the servo motor is fixedly arranged on the back of the mass spectrometer body, the output end of the servo motor penetrates through the mass spectrometer body and extends to, an outlet pipe is arranged at the bottom of the left side of the partition plate.

Preferably, the piston sealing gasket is contacted with the mass spectrometer body and one side of the separation plate close to the piston sealing gasket.

Preferably, the top of the return spring is fixedly connected with the bottom of the piston plate, and the bottom of the return spring is fixedly connected with the top of the limiting fixing rod.

Preferably, the pressing cam is in contact with the piston plate on a side thereof adjacent to the piston plate.

Preferably, advance to be provided with first check valve on the pipe, first check valve is for advancing right side and goes out from a left side, the left side of advancing the pipe is provided with flange.

Preferably, a second one-way valve is arranged on the outlet pipe, and the second one-way valve is left-in and right-out.

Compared with the prior art, the invention has the following beneficial effects:

according to the self-cleaning mass spectrometer and the cleaning mechanism, the self-cleaning mass spectrometer and the cleaning mechanism are matched with each other, the matrix adhered to the detection plate is cleaned by utilizing the back washing function, so that not only can the cleaning of devices be realized, a good foundation is provided for the reuse of the mass spectrometer, but also the complex parts do not need to be disassembled, and therefore convenience is provided for workers.

Drawings

FIG. 1 is a structural cross-sectional view in elevation of the present invention;

FIG. 2 is a schematic left side view of the present invention.

In the figure: the device comprises a device body 1, a cleaning mechanism 2, a mass spectrometer body 101, a feed inlet 102, a discharge outlet 103, a detection plate 104, a separation plate 105, a limit fixing rod 201, a limit sliding rod 202, a piston plate 203, a piston sealing gasket 204, a return spring 205, a servo motor 206, an extrusion cam 207, a pipe 208, a pipe 209, a first check valve 3 and a second check valve 4.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1-2, a self-cleaning mass spectrometer and a mass spectrometer includes a device body 1 and a cleaning mechanism 2, wherein the cleaning mechanism 2 is fixedly installed at the left side of the device body 1.

Referring to fig. 1-2, the device body 1 includes a mass spectrometer body 101, a feeding hole 102, a discharging hole 103, a detecting plate 104, and a separating plate 105, the feeding hole 102 is disposed on the right side of the top of the mass spectrometer body 101, the discharging hole 103 is disposed at the bottom of the right side of the mass spectrometer body 101, the detecting plate 104 for detection is disposed on the inner wall of the mass spectrometer body 101, and the separating plate 105 is disposed on the inner wall of the mass spectrometer body 101 and on the left side of the detecting plate.

Referring to fig. 1-2, the cleaning mechanism 2 includes a limit fixing rod 201, a limit sliding rod 202, a piston plate 203, a piston gasket 204, a return spring 205, a servo motor 206, an extrusion cam 207, an inlet pipe 208 and an outlet pipe 209, the limit fixing rod 201 is fixedly installed between the left side of the inner wall of the mass spectrometer body 101 and the separating plate 105, the limit sliding rod 202 is disposed at the midpoint of the bottom of the limit fixing rod 201, the top of the limit sliding rod 202 penetrates through the limit fixing rod 201 and extends to the outside of the limit fixing rod 201 and is fixedly connected with the piston plate 203, the edge of the piston plate 203 is fixedly connected with the piston gasket 204, the piston gasket 204 is close to one side of the mass spectrometer body 101 and the separating plate 105 and is contacted with the same, the return spring 205 is sleeved on the surface of the limit sliding rod 202 and is located between the limit fixing, the bottom of a reset spring 205 is fixedly connected with the top of a limiting fixed rod 201, a servo motor 206 is fixedly installed on the back of a mass spectrometer body 101, the output end of the servo motor 206 penetrates through the mass spectrometer body 101 and extends to the inside of the mass spectrometer body 101 to be fixedly connected with an extrusion cam 207, one side, close to a piston plate 203, of the extrusion cam 207 is in contact with the extrusion cam, an inlet pipe 208 is arranged at the bottom of the left side of the mass spectrometer body 101, a first one-way valve 3 is arranged on the inlet pipe 208, the first one-way valve 3 is in left-in and right-out, a connecting flange is arranged on the left side of the inlet pipe 208, an outlet pipe 209 is arranged at the bottom of the left side of a partition plate 105, a second one-way valve 4 is arranged on the outlet pipe 209, the second one-way valve 4 is in left-in and right-out, through the mutual matching between a device, not only can realize the clearance to the device, provide good basis for the reuse of mass spectrograph, need not dismantle loaded down with trivial details part moreover to provide convenience for the staff.

When the cleaning device is used, when the detection plate 104 needs to be cleaned, the cleaning device is connected with an external cleaning medium only through a connecting flange on the inlet pipe 208, then the servo motor 206 is started to drive the extrusion cam 207 to extrude the piston plate 203 at different radiuses, and under the action of the elastic force of the return spring 205, the piston plate 203 can reciprocate up and down, when the piston plate 203 moves upwards, the cleaning medium can be sucked into the left side of the partition plate 105 through the inlet pipe 208, when the piston plate 203 moves downwards, the cleaning medium on the left side of the partition plate 105 can be discharged to the right side of the partition plate 105 through the outlet pipe 209 and can permeate the cleaning medium into the detection plate 104 through reciprocating discharge, so that the cleaning of the detection plate 104 is achieved, and the cleaned waste liquid is discharged through the discharge hole 103.

In summary, the following steps: the self-cleaning mass spectrum device and the mass spectrometer solve the problems mentioned in the background technology by arranging the device body 1 and the cleaning mechanism 2.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

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