阅读说明：本技术 一种厚朴爆珠精油及其制备方法 (Magnolia officinalis and pearl burst essential oil and preparation method thereof ) 是由 蹇顺华 吴成刚 张瑞萍 齐富友 刘吟 邵兴伟 于 2019-10-31 设计创作，主要内容包括：本发明公开的一种厚朴爆珠精油及其制备方法,包括1-5份绿茶精油、1-5份无花果精油、5-10份厚朴油树脂、0.1-1份吐温80、100-500份三辛酸甘油酯、0.1-0.5份脂溶性维生素、0.1-0.3份脂溶性抗氧化剂；其制备方法包括,研磨厚朴粒径至2-10mm；加入溶剂、纤维素酶,超声加热浸提5-10h,1000r/min离心3-5min至水油分离,取油相即得厚朴油树脂；将1-5份绿茶精油、1-5份无花果精油、5-10份厚朴油树脂、0.1-1份吐温80、0.1-0.5份脂溶性维生素、0.1-0.3份脂溶性辅酶Q10溶解于100-500份三辛酸甘油酯,过滤收集滤液；滤液于20-60℃下负压脱气0.5-2h,静置2-24h,即得厚朴爆珠精油,所制得爆珠精油厚朴提取物含量高,保存时间长,爆珠精油不与壁材发生反应,成型稳定,香气舒适纯正自然,香味持久稳定,香味强度可控。(The invention discloses a magnolia officinalis and exploded bead essential oil and a preparation method thereof, comprising 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 100-500 parts of tricaprylin, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble antioxidant; the preparation method comprises grinding cortex Magnolia officinalis to particle size of 2-10 mm; adding solvent and cellulase, ultrasonic heating and leaching for 5-10 hr, centrifuging at 1000r/min for 3-5min until water and oil are separated, and collecting oil phase to obtain Magnolia officinalis oleoresin; dissolving 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble coenzyme Q10 in 500 parts of tricaprylin 100, filtering and collecting filtrate; degassing the filtrate at 20-60 deg.C under negative pressure for 0.5-2 hr, standing for 2-24 hr to obtain cortex Magnolia officinalis and explode pearl essential oil, which has high content of cortex Magnolia officinalis extract, long storage time, no reaction of explode pearl essential oil with wall material, stable molding, comfortable, pure and natural fragrance, lasting and stable fragrance, and controllable fragrance intensity.)

1. The magnolia officinalis and bulbus fritilariae essential oil is characterized by comprising the following components: 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 100-500 parts of tricaprylin, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble antioxidant.

2. The essential oil of Magnolia officinalis what is claimed in claim 1, wherein the fat-soluble health vitamin comprises vitamin K and vitamin A.

3. The essential oil of Magnolia officinalis what is claimed in claim 1, wherein the fat-soluble antioxidant is fat-soluble coenzyme Q10.

4. The preparation method of the magnolia officinalis and bulbus fritilariae essential oil is characterized by comprising the following steps:

s1, grinding the particle size of the magnolia officinalis to 2-10 mm;

s2, adding a solvent and cellulase, ultrasonically heating and leaching for 5-10h, centrifuging at 1000r/min for 3-5min until water and oil are separated, and taking an oil phase to obtain magnolia officinalis oleoresin;

s3, dissolving 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble coenzyme Q10 in 500 parts of tricaprylin 100, filtering to remove insoluble substances, and collecting filtrate;

s4, degassing the filtrate at 20-60 ℃ under negative pressure for 0.5-2h, and standing for 2-24h to obtain the magnolia officinalis and bulbus fritilariae essential oil.

5. The method for preparing magnolia officinalis and bulbus fritilariae essential oil as claimed in claim 4, wherein the solvent S2 comprises 20% -40% ethanol water solution.

6. The method for preparing magnolia officinalis and bulbus fritilariae essential oil as claimed in claim 4, wherein the heating temperature of S2 is 30-45 ℃, and the ultrasonic leaching power is 10-20 kHz.

7. The application method of the magnolia officinalis and bulbus fritilariae essential oil is characterized by comprising the following steps: K1. dispersing 0.5-5 parts of Magnolia officinalis blasting pearl essential oil in polyethylene glycol, and adding adjuvant; K2. placing the mixture obtained by K1 in a tank of a natural condensation pill dripping machine, heating at 60-80 deg.C, mixing liquid flow rate of 40-50 particles/s, dripper size of 2.5mm, dripping distance of 3-5cm, and dripping pill cooling oil temperature of 10-15 deg.C; K3. removing oil stain on the surface of the dripping pill obtained by K2 with oil absorbing paper, and air drying.

8. The application method of essential oil of cortex magnoliae officinalis and blasting pearl as claimed in claim 7, wherein the molecular weight of the polyethylene glycol is 1000-2000.

9. The use method of essential oil of Magnolia bark and Polygala paniculata as claimed in claim 7, wherein the adjuvant comprises propylene glycol and sodium stearate.

Technical Field

The invention relates to the field of tobacco essence and flavor, and particularly relates to magnolia officinalis and pearl burst essential oil and a preparation method thereof.

Background

The bead blasting is a special process for perfuming auxiliary materials for cigarettes, is a great innovation in the tobacco industry, improves the safety of cigarette products in a bead blasting and perfuming mode, and greatly enriches the types of fragrant raw materials. In recent years, the investment of bead blasting of various large tobacco enterprises is increased, a large number of bead blasting cigarette products rich in self characteristics are provided, and the bead blasting of cigarettes is a brand new perfuming mode and is becoming an important direction of cigarette innovation in recent years. The essence for the bead blasting essential oil is basically a synthetic essence, plays an important role in the aspects of improving the aroma quality of bead blasting, enriching the tobacco aroma and the like, has thinner aroma and active chemical properties in the prior art, is very easy to react with base oil, wall materials and the like, and leads to an unstable state in the online bead blasting forming process, so that bead blasting forming is influenced, and the natural perfume is limited by the permission list of tobacco additives, so that the selectable aroma type is limited.

The magnolia bark-magnolia bark extract is a common traditional Chinese medicine and clinically has the effects of relieving cough and eliminating phlegm, helping digestion and guiding qi downward, and resolving dampness and harmonizing stomach, and the pharmacological test proves that the magnolia bark-magnolia bark extract has the obvious effects of reducing blood pressure and inhibiting pathogenic microorganisms, the smell of the magnolia bark is spicy, the chemical components are volatile oil, alkaloid, saponin, tannin, trace nicotinic acid and the like, and the magnolia bark-magnolia bark extract mainly contains magnolol and magnolol, eugenol-4' -O- β -D-glucopyranoside, magnolia bark lignan A, magnolia bark lignan B, magnolia bark lignan C, magnolia bark lignan D, magnolia bark lignan E, magnolia bark lignan F, magnolia bark lignan G, magnolia bark lignan H, magnolia bark lignan I, borneol magnolol and the like, and various magnolia bark extracts have a fresh and sweet taste in tobacco, are coordinated with smoke, and can obviously reduce the throat irritation in smoking, and are good natural tobacco flavors, and related magnolia bark-magnolia bark extracts are not reported at present.

Disclosure of Invention

In order to solve the problems, the invention provides the magnolia officinalis exploder essential oil and the preparation method thereof, the prepared magnolia officinalis exploder essential oil has high magnolia officinalis extract content and long storage time, the exploder essential oil does not react with wall materials, the forming is stable, the fragrance is comfortable, pure and natural, the fragrance is lasting and stable, and the fragrance intensity is controllable.

The technical scheme of the invention is that the magnolia officinalis and bulbus fritilariae essential oil is provided, and comprises the following components: 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 100-500 parts of tricaprylin, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of antioxidant.

Preferably, the fat-soluble sanitary vitamin comprises vitamin K and vitamin A.

Preferably, the antioxidant is fat-soluble coenzyme Q10.

Further, a preparation method of the magnolia officinalis and bulbus fritilariae essential oil is also provided, and comprises the following steps:

s1, grinding the particle size of the magnolia officinalis to 2-10 mm;

s2, adding a solvent and cellulase, ultrasonically heating and leaching for 5-10h, removing the organic solvent by rotary evaporation, centrifuging at 1000r/min for 3-5min until water and oil are separated, and taking an oil phase to obtain magnolia officinalis oleoresin;

s3, dissolving 1-5 parts of green tea essential oil, 1-5 parts of fig essential oil, 5-10 parts of magnolia officinalis oleoresin, 0.1-1 part of tween 80, 0.1-0.5 part of fat-soluble vitamin and 0.1-0.3 part of fat-soluble coenzyme Q10 in 500 parts of tricaprylin 100, filtering to remove insoluble substances, and collecting filtrate;

s4, degassing the filtrate at 20-60 ℃ under negative pressure for 0.5-2h, and standing for 2-24h to obtain the magnolia officinalis and bulbus fritilariae essential oil.

Preferably, the solvent of S2 includes 20% to 40% aqueous ethanol.

Preferably, the heating temperature of S2 is 30-45 ℃, and the ultrasonic leaching power is 10-20 kHz.

Further, a use method of the magnolia officinalis and bulbus fritilariae essential oil is also provided, and the use method comprises the following steps: K1. 0.5-5 parts of the essential oil of the magnolia officinalis blasting pearls is scattered in polyethylene glycol, and an auxiliary agent is added; K2. placing the mixture obtained by K1 in a tank of a natural condensation pill dripping machine, heating at 60-80 deg.C, mixing liquid flow rate of 40-50 particles/s, dripper size of 2.5mm, dripping distance of 3-5cm, and dripping pill cooling oil temperature of 10-15 deg.C; K3. removing oil stain on the surface of the dripping pill obtained by K2 with oil absorbing paper, and air drying.

Further, the molecular weight of the polyethylene glycol is 1000-.

Further, the auxiliary agent comprises propylene glycol and sodium stearate.

The invention has the beneficial effects that:

1. when the magnolia officinalis is applied to cigarette flavoring, a remarkable fresh, spicy and sweet flavor can be brought by a small using amount, the fragrance is strong, the fragrance is comfortable and natural, and the stimulation during smoking can be obviously reduced;

2. the tricaprylin has better anti-corrosion effect and stable property, and cannot react with wall materials;

3. adding fat-soluble antioxidant into essential oil to prevent the rancidity of tricaprylin or essential oil, and prolong the storage time of essential oil;

4. the mangnolia officinalis oleoresin is released more thoroughly by using enzymolysis, the extraction rate is higher, on one hand, the use activity of enzyme is ensured by extracting with 20-40% ethanol water, on the other hand, the extraction efficiency is improved, nonpolar substances are removed as much as possible, and the essential oil is purer;

5.1000-2000 molecular weight polyethylene glycol is in gel state at normal temperature, and melts into liquid when heated, and can well lock fragrance when in gel state, the porosity is uniform and fine, the external fragrance is not penetrated, the fragrance is kept for a long time, and no obvious negative effect is caused, if the fragrance intensity is required to be enhanced, the polyethylene glycol can be broken by pinching or the part of a filter tip wrapping the polyethylene glycol is contacted with a mouth for continuous low-temperature heating, so that the polyethylene glycol melts, the magnolia officinalis essential oil is released, and the fragrance intensity is enhanced;

6. the green tea essential oil has effects of refreshing brain, treating common cold, cough, rhinitis and asthma, recovering activity, and resisting depression, and can be absorbed by steam; the fig essential oil can effectively cover up the miscellaneous gas of cigarettes, enables the smoke to be soft, has fine fragrance, has the effect of obviously improving the smoke quality and neutralizes the fragrance of the magnolia officinalis oleoresin, and the combination of the three components enables the fragrance to be more layered, and meanwhile, the fat-soluble vitamins are added to be beneficial to health.

Detailed Description

In order to make the present invention more comprehensible, the technical solutions of the present invention are further described below with reference to specific embodiments, but the present invention is not limited thereto.