阅读说明：本技术 一种美白去皱的皮肤调理剂、面膜及其制备方法 (Skin conditioner and mask for whitening and removing wrinkles and preparation method thereof ) 是由 范玉菡 温伟红 莫霖霭 于 2019-12-03 设计创作，主要内容包括：本发明提供了一种美白去皱的皮肤调理剂、面膜及其制备方法。所述皮肤调理剂按重量份计包括：0.01-0.5份α-熊果苷、1-5份烟酰胺、0.01-1份氨乙基次膦酸、0.01-0.2份富勒烯、0.01-1份乙酰基六肽-8、0.01-1份密蒙花提取物和0.01-1份乳酸杆菌/大米发酵产物。所述面膜按质量百分比计包括：1-14％上述美白去皱的皮肤调理剂、2.5-10％保湿剂、0.1-0.3％pH调节剂和0.06-0.45％增稠剂,余量为水。本发明提供的面膜,通过合理配伍多种有效成分,针对黑色素与皱纹的内在成因,抑制黑色素的生成,同时降低皮肤中胶原蛋白分解酶的活性,改善皱纹,实现美白去皱的功效。(The invention provides a skin conditioner for whitening and removing wrinkles, a mask and a preparation method thereof, wherein the skin conditioner comprises, by weight, 0.01-0.5 part of α -arbutin, 1-5 parts of nicotinamide, 0.01-1 part of aminoethyl phosphinic acid, 0.01-0.2 part of fullerene, 0.01-1 part of acetyl hexapeptide-8, 0.01-1 part of a butterflybush flower extract and 0.01-1 part of lactobacillus/rice fermentation product.)

1. The skin conditioner for whitening and removing wrinkles is characterized by comprising the following components in parts by weight:

0.01-0.5 part of α -arbutin, 1-5 parts of nicotinamide, 0.01-1 part of aminoethyl phosphinic acid, 0.01-0.2 part of fullerene, 0.01-1 part of acetyl hexapeptide-8, 0.01-1 part of buddleja officinalis extract and 0.01-1 part of lactobacillus/rice fermentation product.

2. The skin conditioner according to claim 1, further comprising 0.01-1 part of a root extract of sophora flavescens ait, 0.01-1 part of a root extract of glycyrrhiza inflata, 0.01-1 part of a root extract of scutellaria baicalensis, and 0.01-1 part of an extract of aloe barbadensis leaf.

3. The whitening and wrinkle-removing mask is characterized by comprising the following components in percentage by mass:

1-14% of the skin conditioner of claim 1 or 2, 2.5-10% of a moisturizer, 0.1-0.3% of a pH modifier, and 0.06-0.45% of a thickener, the balance being water.

4. The whitening and wrinkle-removing mask according to claim 3, wherein the humectant is any one or a combination of two or more of carbomer, butanediol, erythritol, sodium hyaluronate or 1, 2-hexanediol;

preferably, the pH adjusting agent is triethanolamine;

preferably, the thickener is disodium edetate and/or hydrolyzed sclerotium rolfsii gum.

5. The whitening wrinkle-removing mask according to claim 3 or 4, further comprising 0.01 to 0.03% of a solubilizer and 0.01 to 0.02% of a fragrance;

preferably, the solubilizer is hydrogenated castor oil;

preferably, the hydrogenated castor oil is PEG-40 hydrogenated castor oil.

6. The whitening wrinkle-removing mask according to any one of claims 3 to 5, further comprising 0.4 to 0.7% of an antioxidant;

preferably, the antioxidant is p-hydroxyacetophenone.

7. The whitening wrinkle-removing mask according to any one of claims 3 to 6, which comprises the following components in percentage by weight:

1-14% of a skin conditioner according to claim 1 or 2, 0.1-0.3% carbomer, 2-8% butylene glycol, 0.01-0.5% erythritol, 0.01-0.2% sodium hyaluronate, 0.4-0.7% 1, 2-hexanediol, 0.1-0.3% triethanolamine, 0.01-0.05% disodium edetate, 0.05-0.4% hydrolyzed sclerotium rolfsii gum, 0.4-0.7% p-hydroxyacetophenone, 0.01-0.03% solubilizer and 0.01-0.02% fragrance, the balance being water.

8. A method for preparing a whitening and wrinkle-removing mask according to any one of claims 3 to 7, comprising the steps of:

(1) mixing water, a thickening agent and a humectant, and homogenizing to obtain a homogeneous liquid;

(2) and (2) mixing the homogenized solution obtained in the step (1) with the rest components, and filling into an aluminum foil bag in which non-woven fabrics are placed in advance to obtain the whitening and wrinkle-removing facial mask.

9. The preparation method according to claim 8, wherein the temperature of the mixing and homogenizing in the step (1) is 80-85 ℃ and the time is 5-10 min;

preferably, the mixing and homogenizing in the step (1) are carried out in a vacuum emulsifying pot;

preferably, the mixing in step (2) is carried out at a temperature of 40-45 ℃ for a time of 5-10 min.

10. The method of manufacturing according to claim 8 or 9, comprising the steps of:

(1) adding water, thickener and humectant into vacuum emulsifying pan, mixing and homogenizing at 80-85 deg.C for 5-10min to obtain homogeneous solution;

(2) and (2) cooling the homogenized liquid obtained in the step (1) to 40-45 ℃, then adding the rest components, stirring and mixing for 5-10min, cooling to below 38 ℃, discharging, and filling into an aluminum foil bag in which non-woven fabrics are placed in advance to obtain the whitening and wrinkle-removing facial mask.

Technical Field

The invention belongs to the technical field of care products, particularly relates to a mask and a preparation method thereof, and particularly relates to a skin conditioner for whitening and removing wrinkles, a mask and a preparation method thereof.

Background

A plurality of pigment cells are distributed at the lower layer of the epidermis of a human body, the pigment cells form melanin through the catalytic oxidation of tyrosinase in the body, and the increase of the melanin in the skin leads to the darkening of the skin color. According to the influence degree on the pigmentation of human skin, the main method for realizing the whitening purpose of the whitening cosmetic is to inhibit and eliminate melanin. Meanwhile, as people age, metabolism of the human body begins to slow down, the number of fibroblasts in the human body gradually decreases, and collagen and elastic fibrin secreted by the human body gradually decrease and break due to oxidation, so that a supporting component for the epidermis disappears, the epidermis is unevenly collapsed, the dermis layer begins to thin, the elasticity of the skin is poor, and wrinkles can be generated. The accumulation of melanin and the generation of wrinkles largely affect the surface state of skin, and thus achieving whitening and anti-wrinkle have been the main objectives of skin care products.

The facial mask is a skin care product capable of cleaning and protecting the face and simultaneously caring the facial skin, and has the functions of isolating the facial skin from the outside air, inhibiting water evaporation, softening the horny layer of the epidermis, enlarging pores, improving the blood circulation of the facial skin, enhancing the absorption of nutrient substances and achieving the effect of improving the physiological function of the skin. By adding different active ingredients into the facial mask, the facial mask can realize different skin care functions, such as functions of deep cleaning, moisturizing, whitening, anti-wrinkle, acne removal and the like.

CN102988239A discloses a skin-care wrinkle-removing mask cream, which is composed of the following components in parts by weight: 13-16 parts of methyl glycol, 8-15 parts of nipagin methanol, 7-11 parts of hexadecanol, 3-13 parts of sodium stearate, 8-11 parts of mint, 4-8 parts of aloe and the balance of water. The invention can make the face skin smooth and bright, has obvious effect of eliminating wrinkles, has the effect of moistening the skin, has no toxic or harmful raw materials, no side effect, and is safe and reliable.

CN108245476A discloses a whitening and spot-fading mask and a preparation method thereof, the whitening and spot-fading mask comprises high-concentration beauty fluid, mask paper paste and a packaging bag, wherein the high-concentration beauty fluid comprises a gel, a humectant, a preservative, emollient oil, a pH regulator, a whitening and spot-fading substance and the balance of distilled water, and the whitening and spot-fading substance comprises pearl powder, vitamin E, water-soluble β -glucan, protein powder, saffron crocus and lutein.

However, most of the existing facial masks have single efficacy, and cannot achieve the whitening and anti-wrinkle effects at the same time, and consumers prefer to obtain a multi-effect facial mask which can achieve the whitening and anti-wrinkle effects at the same time. Therefore, a mask having whitening and wrinkle-removing functions is to be developed to meet the market demand.

Disclosure of Invention

Aiming at the defects in the prior art, the invention aims to provide a skin conditioner for whitening and removing wrinkles, a mask and a preparation method thereof. The skin conditioner and the facial mask provided by the invention can reduce the melanin content of the skin, increase the expression of the fibrin and achieve the effects of whitening and removing wrinkles by reasonably proportioning the components. In order to achieve the purpose, the invention adopts the following technical scheme:

in a first aspect, the invention provides a skin conditioner for whitening and removing wrinkles, which comprises the following components in parts by weight:

0.01-0.5 part of α -arbutin, 1-5 parts of nicotinamide, 0.01-1 part of aminoethyl phosphinic acid, 0.01-0.2 part of fullerene, 0.01-1 part of acetyl hexapeptide-8, 0.01-1 part of BUDDLEJA OFFICINALIS (Buddleja OFFICINALIS) extract and 0.01-1 part of LACTOBACILLUS/rice fermentation product (Lactobacillus/RICE FERMENT).

α -arbutin has effects of inhibiting tyrosinase activity, inhibiting melanin generation and deposition, removing mottle and freckle, and has good therapeutic effect on scar caused by ultraviolet burn, and good antiinflammatory, repairing and whitening effects.

Nicotinamide, also known as nicotinamide, is an amide compound of nicotinic acid, is a skin anti-aging ingredient recognized in the field of beauty skin science, and can relieve and prevent dark, yellowish and vegetable colors of skin generated in the early aging process of skin. And meanwhile, the damaged stratum corneum lipid barrier can be repaired, and the skin resistance is improved.

Compared with α -arbutin, the aminoethyl phosphinic acid does not inhibit tyrosinase, but is responsible for converting tyrosinase into DOPA and DOPA quinone, so that the dopamine can be stabilized, and the conversion of the dopamine into melanin is prevented.

The fullerene can eliminate free radicals and avoid the influence of the free radicals on the skin, so that the problems of darkness, color spots and the like are reduced, the fullerene can prevent wrinkles from being generated and reduce the activity of collagen catabolic enzymes in the skin, so that the decomposition loss of the collagen in the skin is avoided, and the wrinkles can be improved after the wrinkles are generated.

Acetyl hexapeptide-8 is a bioactive peptide, and can inhibit release of glutamate, destroy stability of SNARE (synaptosome associated protein receptor) complex, reduce facial wrinkles caused by muscle contraction, and effectively prevent new wrinkles.

The flos Buddlejae extract is derived from leaf of flos Buddlejae, contains multiple components such as glycyrrhizic acid, has effects of clearing heat and promoting diuresis, and can be used in daily chemical products for effectively regulating skin and improving skin health state.

The lactobacillus/rice fermentation product is a product obtained by fermenting lactobacillus with rice as a substrate, is a lactobacillus metabolite, is very complex rather than single component, is rich in various vitamins and proteins, has balanced nutrient content, inhibits free radicals, improves skin quality, and is an excellent comprehensive conditioner.

The components are creatively combined in a specific proportion, are matched with each other, have synergistic interaction, can effectively lighten melanin and wrinkles by inhibiting and eliminating melanin, increasing fibroblasts, smoothing fine lines and other action mechanisms aiming at the internal and external causes of the melanin and the wrinkles of the skin, and enables the skin to be white, fine and compact.

In the present invention, the α -arbutin is present in an amount of 0.01 to 0.5 parts by weight, and may be, for example, 0.01, 0.02, 0.04, 0.05, 0.08, 0.1, 0.12, 0.15, 0.18, 0.2, 0.25, 0.3, 0.35, 0.4, 0.45 or 0.5 parts by weight.

The nicotinamide is 1-5 parts by weight, and may be, for example, 1 part, 1.2 parts, 1.4 parts, 1.5 parts, 1.8 parts, 2 parts, 2.2 parts, 2.5 parts, 2.8 parts, 3 parts, 3.2 parts, 3.5 parts, 4 parts, 4.2 parts, 4.5 parts, or 5 parts.

The weight portion of the aminoethyl phosphinic acid is 0.01 to 1 part, and may be, for example, 0.01 part, 0.02 part, 0.05 part, 0.08 part, 0.1 part, 0.14 part, 0.18 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part.

The fullerene may be present in an amount of 0.01 to 0.2 parts by weight, for example, 0.01 parts, 0.02 parts, 0.05 parts, 0.08 parts, 0.1 parts, 0.12 parts, 0.14 parts, 0.15 parts, 0.16 parts, 0.18 parts, or 0.2 parts.

The acetyl hexapeptide-8 may be present in an amount of 0.01 to 1 part by weight, for example, 0.01 part, 0.02 part, 0.05 part, 0.08 part, 0.1 part, 0.14 part, 0.18 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, or 1 part.

The weight portion of the buddleja officinalis extract is 0.01-1 part, and may be, for example, 0.01 part, 0.02 part, 0.05 part, 0.08 part, 0.1 part, 0.14 part, 0.18 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part.

The weight portion of the lactobacillus/rice fermentation product is 0.01-1 part, and can be, for example, 0.01 part, 0.02 part, 0.05 part, 0.08 part, 0.1 part, 0.14 part, 0.18 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part, and the like.

As a preferred technical scheme of the invention, the skin conditioner also comprises 0.01-1 part of radix sophorae flavescentis (Sophora angustifolia) root extract, 0.01-1 part of GLYCYRRHIZA INFLATA (Glycyrrhiza INFLATA) root extract, 0.01-1 part of SCUTELLARIA BAICALENSIS (Scutellaria BAICALENSIS) root extract and 0.01-1 part of ALOE BARBADENSIS (Aloe BARBADENSIS) leaf extract.

The sophora flavescens root extract contains active ingredients such as matrine, oxymatrine, hydroxymatrine and the like, and can balance oil secretion, dredge and astringe pores, clear away toxin impurities in skin, relieve skin itch, promote the growth and repair of damaged vascular nerve cells, recover the activity of subcutaneous capillary cells and promote the skin to be compact and smooth.

The collagen component in the glycyrrhiza inflata root extract can enable the skin to be firmer, and meanwhile, the anti-aging component in the glycyrrhiza inflata root extract can obviously resist the deposition of melanin, so that the skin whitening effect is achieved.

The radix scutellariae extract has obvious anti-inflammation and anti-allergy effects and can relieve the skin allergy probability, and the zinc baicalin and the copper baicalin contained in the radix scutellariae extract have obvious scavenging effect on superoxide radical, protect skin cells from being excessively oxidized by the superoxide radical and inhibit the generation of melanin.

The aloe vera leaf extract contains active substances of polysaccharide, amino acid, polypeptide, organic acid, vitamin and other water-soluble components, can obviously enhance the water absorption performance of skin keratinized tissue, can deeply permeate and moisturize, and has extremely strong water replenishing and moisturizing effects.

In the present invention, the weight portion of the extract of the root of sophora flavescens is 0.01 to 1 part, and may be, for example, 0.01 part, 0.02 part, 0.05 part, 0.08 part, 0.1 part, 0.14 part, 0.18 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part.

The licorice root extract is 0.01-1 part by weight, such as 0.01, 0.02, 0.05, 0.08, 0.1, 0.14, 0.18, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9 or 1 part by weight.

The scutellaria root extract is 0.01-1 part by weight, for example, 0.01 part, 0.02 part, 0.05 part, 0.08 part, 0.1 part, 0.14 part, 0.18 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part, etc.

The aloe vera leaf extract may be 0.01 to 1 part by weight, for example, 0.01 part, 0.02 part, 0.05 part, 0.08 part, 0.1 part, 0.14 part, 0.18 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part, etc.

In a second aspect, the invention provides a whitening and wrinkle-removing mask, which comprises the following components in percentage by mass:

1-14% of the skin conditioner of the first aspect, 2.5-10% of a humectant, 0.1-0.3% of a pH regulator, 0.06-0.45% of a thickener, and the balance water.

According to the whitening and wrinkle-removing facial mask, the whitening and wrinkle-removing facial mask is prepared by reasonably matching the whitening and wrinkle-removing skin conditioner provided by the first aspect with the moisturizing agent, the pH regulator, the thickening agent and water, wherein the skin conditioner contained in the whitening and wrinkle-removing facial mask can achieve the whitening and wrinkle-removing effects, no preservative is added, the facial mask does not damage the skin through reasonable proportion, and the moisturizing effect is good.

In the present invention, the skin conditioner for whitening and removing wrinkles may be 1 to 14% by weight, for example, 1%, 1.5%, 2%, 2.5%, 3%, 3.5%, 4%, 4.5%, 5%, 6%, 7%, 8%, 9%, 10%, 11%, 12%, 13%, 14% or the like.

The humectant may be present in an amount of 2.5 to 10% by weight, for example 2.5%, 2.8%, 3%, 3.5%, 4%, 4.5%, 5%, 5.5%, 6%, 6.5%, 7%, 7.5%, 8%, 9%, 9.5% or 10% by weight.

The weight percentage of the pH adjuster is 0.1 to 0.3%, and may be, for example, 0.1%, 0.11%, 0.12%, 0.15%, 0.16%, 0.18%, 0.2%, 0.21%, 0.22%, 0.25%, 0.28%, or 0.3%.

The weight percentage of the thickener is 0.06 to 0.45%, and may be, for example, 0.06%, 0.07%, 0.08%, 0.1%, 0.15%, 0.2%, 0.25%, 0.3%, 0.32%, 0.35%, 0.4%, 0.42%, or 0.45%.

According to a preferable technical scheme of the invention, the humectant is any one or a combination of more than two of carbomer, butanediol, erythritol, sodium hyaluronate or 1, 2-hexanediol.

Wherein, carbomer is acrylic acid crosslinked resin obtained by crosslinking pentaerythritol and the like with acrylic acid, and is a very important rheology regulator, neutralized carbomer is an excellent gel matrix, has important purposes of thickening, suspending and the like, has simple process and good stability, and is widely applied to emulsion, cream and gel; erythritol has strong moisture retention and hygroscopicity, can be used as a humectant of cosmetics like glycerin, but sodium hyaluronate has higher penetrating power to skin without greasy and sticky feeling of glycerin, and is helpful for promoting the penetration and absorption of nutrient components by further adding sodium hyaluronate into neck beautifying cream. The resistance of the acetylated sodium hyaluronate to hyaluronidase is 13 times that of the non-acetylated sodium hyaluronate, and the penetration force to skin is stronger.

As a preferable technical scheme of the invention, the pH regulator is triethanolamine.

Preferably, the thickener is disodium ethylenediaminetetraacetate and/or sclerotium rolfsii (scleritium mrolfssii) gum.

In a preferred embodiment of the present invention, the whitening and wrinkle-reducing mask further comprises 0.01 to 0.03% (e.g., 0.01%, 0.012%, 0.015%, 0.018%, 0.02%, 0.022%, 0.025%, 0.028%, 0.03%, etc.) of a solubilizer and 0.01 to 0.02% (e.g., 0.01%, 0.012%, 0.014%, 0.015%, 0.016%, 0.018%, 0.02%, etc.) of a fragrance. The fragrance may be a perfume.

Preferably, the solubilizer is hydrogenated castor oil.

Preferably, the hydrogenated castor oil is PEG-40 hydrogenated castor oil.

Hydrogenated castor oil is a modified castor oil product, is a common high-efficiency solubilizer, and can uniformly disperse oily substances such as essence, essential oil and the like into water to form a stable and transparent solution. According to the epoxy group to be attached, it can be classified into PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PEG-80 hydrogenated castor oil, etc.

In a preferred embodiment of the present invention, the whitening and wrinkle-reducing mask further comprises 0.4 to 0.7% (for example, 0.4%, 0.45%, 0.5%, 0.55%, 0.6%, 0.65%, or 0.7%) of an antioxidant.

Preferably, the antioxidant is p-hydroxyacetophenone.

As a preferable technical scheme of the invention, the whitening and wrinkle-removing mask comprises the following components in percentage by weight: 1-14% of the skin conditioner of the first aspect, 0.1-0.3% of carbomer, 2-8% of butanediol, 0.01-0.5% of erythritol, 0.01-0.2% of sodium hyaluronate, 0.4-0.7% of 1, 2-hexanediol, 0.1-0.3% of triethanolamine, 0.01-0.05% of disodium edetate, 0.05-0.4% of hydrolyzed sclerotium rolfsii gum, 0.4-0.7% of p-hydroxyacetophenone, 0.01-0.03% of solubilizer, 0.01-0.02% of aromatic and the balance of water.

In a third aspect, the present invention provides a method for preparing a whitening and wrinkle-removing mask according to the second aspect, wherein the method comprises the following steps:

(1) mixing water, a thickening agent and a humectant, and homogenizing to obtain a homogeneous liquid;

(2) and (2) mixing the homogenized liquid obtained in the step (1) with the rest components, filtering and discharging, and filling into an aluminum foil bag in which non-woven fabrics are placed in advance to obtain the whitening and wrinkle-removing facial mask.

As a preferred embodiment of the present invention, the temperature for mixing and homogenizing in step (1) is 80 to 85 ℃, and may be, for example, 80 ℃, 81 ℃, 82 ℃, 83 ℃, 84 ℃, or 85 ℃; the time is 5-10min, such as 5min, 6min, 7min, 8min, 9min or 10 min.

Preferably, the mixing and homogenizing in the step (1) are carried out in a vacuum emulsifying pot.

Preferably, the temperature of the mixing in the step (2) is 40-45 ℃, for example, 40 ℃, 41 ℃, 42 ℃, 43 ℃, 44 ℃ or 45 ℃ and the like; the time is 5-10min, such as 5min, 6min, 7min, 8min, 9min or 10 min.

As a preferred technical scheme of the invention, the preparation method comprises the following steps:

(1) adding water, thickener and humectant into vacuum emulsifying pan, mixing and homogenizing at 80-85 deg.C for 5-10min to obtain homogeneous solution;

(2) and (2) cooling the homogenized liquid obtained in the step (1) to 40-45 ℃, then adding the rest components, stirring and mixing for 5-10min, cooling to below 38 ℃, discharging, and filling into an aluminum foil bag in which non-woven fabrics are placed in advance to obtain the whitening and wrinkle-removing facial mask.

The recitation of numerical ranges herein includes not only the above-recited numerical values, but also any numerical values between non-recited numerical ranges, and is not intended to be exhaustive or to limit the invention to the precise numerical values encompassed within the range for brevity and clarity.

Compared with the prior art, the invention has the beneficial effects that:

1. the skin conditioner provided by the invention is reasonably compatible with α -arbutin, aminoethyl phosphinic acid and nicotinamide as triple whitening components, can inhibit tyrosinase activity, reduce pigmentation, inhibit dopa enzyme, reduce pigment formation, promote pigment decomposition, whiten and brighten skin;

2. the skin conditioner provided by the invention is compounded with double anti-aging components of fullerene and acetyl hexapeptide-8, the fullerene removes free radicals, provides anti-oxidation protection, delays aging and wrinkles, and the acetyl hexapeptide-8 improves the area and depth of the wrinkles and lightens the wrinkles; meanwhile, the whitening and wrinkle-removing mask provided by the invention has dual effects of whitening and wrinkle resistance, and two skin care requirements can be met by one mask.

Detailed Description

The technical solution of the present invention is further explained by the following embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.