阅读说明：本技术 一种火棘牙膏及其制备方法 (Pyracantha fortuneana toothpaste and preparation method thereof ) 是由 黄克霞 祝义伟 周令国 陈秋生 邹严俊杰 曾涛 于 2019-12-03 设计创作，主要内容包括：本发明公开了一种火棘牙膏,包括如下重量份的原料：4-6份火棘总黄酮提取物,1-3份维生素C,6-8份缓蚀剂、18-20份摩擦剂、2-3份润湿剂、1-1.5份增稠剂、1.5-2.5份起泡剂、0.2-0.5份甜味剂、0.1-0.5份香精,余量为水,火棘果粉末与乙醇的混合液,经循环超声波装置及后续工艺处理后,得到火棘总黄酮提取物,还公开了所述火棘牙膏的制作方法：常温下将火棘总黄酮提取物、维生素C、糖精钠置于水中进行溶解后加入真空制膏机中,再将丙三醇加入真空制膏机中制备液料；取碳酸钙、二氧化硅、羧甲基纤维素钠和月桂醇硫酸酯钠搅拌制得粉料；将制备好的粉料加入液料中,并加入薄荷香精,再经过搅拌、抽真空、灌装、封尾等处理制得火棘牙膏,以满足人们对抑菌和美白的牙膏的需求。(The invention discloses pyracantha fortuneana toothpaste which comprises the following raw materials in parts by weight: 4-6 parts of pyracantha fortuneana total flavone extract, 1-3 parts of vitamin C, 6-8 parts of corrosion inhibitor, 18-20 parts of abrasive, 2-3 parts of wetting agent, 1-1.5 parts of thickening agent, 1.5-2.5 parts of foaming agent, 0.2-0.5 part of sweetening agent, 0.1-0.5 part of essence and the balance of water, and mixed liquid of pyracantha fortuneana fruit powder and ethanol are treated by a circulating ultrasonic device and a subsequent process to obtain the pyracantha fortuneana total flavone extract, and the preparation method of the pyracantha fortuneana toothpaste is further disclosed: dissolving pyracantha fortuneana total flavone extract, vitamin C and saccharin sodium in water at normal temperature, adding into a vacuum paste making machine, and adding glycerol into the vacuum paste making machine to prepare a liquid material; mixing calcium carbonate, silicon dioxide, sodium carboxymethylcellulose and sodium lauryl sulfate, and stirring to obtain powder; the prepared powder is added into the liquid material, the mint essence is added, and the pyracantha fortuneana toothpaste is prepared by stirring, vacuumizing, filling, sealing the tail and the like, so that the requirements of people on antibacterial and whitening toothpaste are met.)

1. The pyracantha fortuneana toothpaste is characterized by comprising the following raw materials in parts by weight: 4-6 parts of pyracantha fortuneana total flavone extract, 1-3 parts of vitamin C, 6-8 parts of corrosion inhibitor, 18-20 parts of abrasive, 2-3 parts of wetting agent, 1-1.5 parts of thickening agent, 1.5-2.5 parts of foaming agent, 0.2-0.5 part of sweetening agent, 0.1-0.5 part of essence and the balance of water.

2. The pyracantha fortuneana toothpaste as claimed in claim 1, wherein the corrosion inhibitor is silicon dioxide, the abrasive is calcium carbonate, the wetting agent is glycerol, the thickening agent is sodium carboxymethylcellulose, the foaming agent is sodium lauryl sulfate, the sweetener is sodium saccharin, and the essence is peppermint essence.

3. The pyracantha fortuneana toothpaste as claimed in claim 2, which comprises the following raw materials in parts by weight: 4 parts of pyracantha fortuneana total flavone extract, 3 parts of vitamin C, 8 parts of corrosion inhibitor, 20 parts of abrasive, 3 parts of wetting agent, 1.5 parts of thickening agent, 2.5 parts of foaming agent, 0.5 part of sweetening agent, 0.5 part of essence and the balance of water.

4. The pyracantha fortuneana toothpaste as claimed in claim 3, which comprises the following raw materials in parts by weight: 6 parts of pyracantha fortuneana total flavone extract, 1 part of vitamin C, 6 parts of corrosion inhibitor, 18 parts of abrasive, 2 parts of wetting agent, 1 part of thickening agent, 1.5 parts of foaming agent, 0.2 part of sweetening agent, 0.2 part of essence and the balance of water.

5. The pyracantha fortuneana toothpaste as claimed in claim 4, wherein the preparation method of the pyracantha fortuneana toothpaste comprises the following steps:

adding the pyracantha fortuneana total flavone extract, the vitamin C and the saccharin sodium into water with the formula amount at normal temperature, dissolving, adding into a vacuum paste making machine, weighing glycerol, adding into the vacuum paste making machine, and stirring and mixing uniformly to prepare a liquid material;

weighing calcium carbonate, silicon dioxide, sodium carboxymethylcellulose and sodium lauryl sulfate, adding into a reaction vessel, and stirring to obtain powder;

and adding the prepared powder into a liquid material mixture of a vacuum paste making machine, adding the weighed mint essence, stirring, and starting a vacuum pump of the paste making machine to vacuumize until the paste making is finished.

Pouring the paste out of the vacuum paste making machine, filling the paste into a toothpaste hose, and sealing the tail by using a tail sealing machine to obtain the pyracantha fortuneana toothpaste.

6. The method for preparing pyracantha fortuneana toothpaste as claimed in claim 5, wherein the method for preparing the pyracantha fortuneana total flavone extract comprises the following steps:

weighing a pyracantha powder sample;

adding an ethanol solution into a pyracantha powder sample to obtain a first mixed solution;

extracting the first mixed solution by using a circulating ultrasonic device to obtain a second mixed solution;

and carrying out suction filtration on the second mixed solution to obtain clear liquid, and carrying out rotary evaporation to remove the ethanol solvent to obtain the pyracantha fortuneana total flavone extract.

7. The method of claim 5, wherein the vacuum is maintained at a pressure of greater than-0.095 MPa.

8. The method as claimed in claim 6, wherein the parameters of the circulating ultrasonic device are set to power of 1000-.

9. The method of claim 6, wherein the first mixture is a mixture of pyracantha powder and ethanol solution, and the second mixture is a mixture of flavonoids released from cracked pyracantha and ethanol solution.

Technical Field

The invention relates to the technical field of oral care, in particular to pyracantha fortuneana toothpaste and a preparation method thereof.

Background

The Chinese medicinal herbs of Yunnan province, Hunan Zhi Yao Zhi, Sichuan Zhi Yao, Yunnan Chinese herbal medicine and Chinese medicinal dictionary have good compatibility, sour, sweet and astringent taste of pyracantha fortuneana, mild nature, liver, stomach and large intestine channels, and fruits, leaves and roots can be used as medicaments, and have the effects of clearing away heat and toxic materials, promoting blood circulation and stopping bleeding, treating wind-fire toothache and the like. The pyracantha fortuneana fruit is rich in flavonoids and the pericarp contains anthocyanin. Researches find that the flavonoid and anthocyanin have various pharmacological effects of inhibiting bacteria, diminishing inflammation, resisting oxidation, removing free radicals, resisting viruses, stopping bleeding and the like.

The toothpaste is an indispensable thing in daily life, and the types and brands of the toothpaste on the market are numerous. Professional medical statistical data shows that 90% of adults in China have oral problems of different degrees, such as oral ulcer, gingival swelling and pain, bleeding, atrophy, decayed teeth and the like, and the problems are spreading rapidly, and the oral small problems are not enough to go to hospitals, but greatly disturb the mood of people, so that the consumption demand of toothpaste for inhibiting and whitening teeth is generated.

Disclosure of Invention

The invention provides pyracantha fortuneana toothpaste and a preparation method thereof, aiming at solving the consumption demand of people who have requirements on tooth bacteriostasis and whitening.

The pyracantha fortuneana toothpaste comprises the following raw materials in parts by weight: 4-6 parts of pyracantha fortuneana total flavone extract, 1-3 parts of vitamin C, 6-8 parts of corrosion inhibitor, 18-20 parts of abrasive, 2-3 parts of wetting agent, 1-1.5 parts of thickening agent, 1.5-2.5 parts of foaming agent, 0.2-0.5 part of sweetening agent, 0.1-0.5 part of essence and the balance of water.

The corrosion inhibitor is silicon dioxide, the abrasive agent is calcium carbonate, the wetting agent is glycerol, the thickening agent is sodium carboxymethylcellulose, the foaming agent is sodium lauryl sulfate, the sweetening agent is saccharin sodium, and the essence is mint essence.

The pyracantha fortuneana toothpaste comprises the following raw materials in parts by weight: 4 parts of pyracantha fortuneana total flavone extract, 3 parts of vitamin C, 8 parts of corrosion inhibitor, 20 parts of abrasive, 3 parts of wetting agent, 1.5 parts of thickening agent, 2.5 parts of foaming agent, 0.5 part of sweetening agent, 0.5 part of essence and the balance of water.

The pyracantha fortuneana toothpaste comprises the following raw materials in parts by weight: 6 parts of pyracantha fortuneana total flavone extract, 1 part of vitamin C, 6 parts of corrosion inhibitor, 18 parts of abrasive, 2 parts of wetting agent, 1 part of thickening agent, 1.5 parts of foaming agent, 0.2 part of sweetening agent, 0.2 part of essence and the balance of water.

The invention also provides a preparation method of the pyracantha fortuneana toothpaste, which comprises the following steps:

adding the pyracantha fortuneana total flavone extract, the vitamin C and the saccharin sodium into water with the formula amount at normal temperature, dissolving, adding into a vacuum paste making machine, weighing glycerol, adding into the vacuum paste making machine, and stirring and mixing uniformly to prepare a liquid material;

weighing calcium carbonate, silicon dioxide, sodium carboxymethylcellulose and sodium lauryl sulfate, adding into a reaction vessel, and stirring to obtain powder;

and adding the prepared powder into a liquid material mixture of a vacuum paste making machine, adding the weighed mint essence, stirring, and starting a vacuum pump of the paste making machine to vacuumize until the paste making is finished.

And pouring the paste out of the vacuum paste making machine, filling the paste into a toothpaste hose, and sealing the tail by using a tail sealing machine to obtain the pyracantha fortuneana toothpaste.

The preparation method of the pyracantha fortuneana total flavone extract comprises the following steps:

weighing a pyracantha powder sample;

adding an ethanol solution into a pyracantha powder sample to obtain a first mixed solution;

extracting the first mixed solution by using a circulating ultrasonic device to obtain a second mixed solution;

and carrying out suction filtration on the second mixed solution to obtain clear liquid, and carrying out rotary evaporation to remove the ethanol solvent to obtain the pyracantha fortuneana total flavone extract.

Wherein the vacuum degree of the vacuum is kept above-0.095 MPa.

Wherein, the parameters of the circulating ultrasonic device are set to power of 1000-3000W and time of 30-60 min.

The first mixed solution is the mixture of pyracantha powder and an ethanol solution, and the second mixed solution is the mixture of flavonoids released after the pyracantha is cracked and the ethanol solution.

The invention has the beneficial effects that: the flavonoid substances and the anthocyanin have various pharmacological effects of bacteriostasis, inflammation diminishing, oxidation resistance, free radical removal, virus resistance, hemostasis and the like, the total flavone in the pyracantha fortuneana peel and pulp is extracted by adopting a circulating ultrasonic extraction method, a certain amount of vitamin C is compounded, and the vitamin C is added into a toothpaste base material to develop the pyracantha fortuneana toothpaste with bacteriostasis and whitening effects so as to meet the consumption requirements of people on the toothpaste with bacteriostasis and whitening effects on teeth.

Drawings

In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.

Fig. 1 is a flow structure schematic diagram of a preparation method of pyracantha fortuneana toothpaste of embodiment 1 of the invention and the preparation method thereof.

Fig. 2 is a schematic flow structure diagram of a preparation method of the pyracantha fortuneana total flavone extract of example 1 of the pyracantha fortuneana toothpaste and the preparation method thereof of the present invention.

Fig. 3 is a flow structure schematic diagram of a preparation method of pyracantha fortuneana toothpaste of embodiment 2 of the invention and the preparation method thereof.

Fig. 4 is a flow structure diagram of a preparation method of the pyracantha fortuneana total flavone extract of example 2 of the pyracantha fortuneana toothpaste and the preparation method thereof of the present invention.

Fig. 5 is a flow structure schematic diagram of a preparation method of pyracantha fortuneana toothpaste of embodiment 3 of the invention and the preparation method thereof.

Fig. 6 is a flow structure schematic diagram of a preparation method of pyracantha fortuneana total flavone extract of example 3 of the pyracantha fortuneana toothpaste and the preparation method thereof of the present invention.

Fig. 7 is a flow structure schematic diagram of a preparation method of pyracantha fortuneana toothpaste of example 4 of the pyracantha fortuneana toothpaste and the preparation method thereof of the present invention.

Fig. 8 is a flow structure diagram of a preparation method of the pyracantha fortuneana total flavonoid extract of example 4 of the pyracantha fortuneana toothpaste and the preparation method thereof of the present invention.

Detailed Description

Reference will now be made in detail to embodiments of the present invention, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are illustrative and intended to be illustrative of the invention and are not to be construed as limiting the invention.