阅读说明：本技术 炮仗花复合香精及其在牙膏中的应用 (Composite essence of fire-cracker flower and its application in toothpaste ) 是由 贾强 伍第政 王欢 万红霞 董蕾 欧爱芬 江津津 于 2019-10-29 设计创作，主要内容包括：本发明公开了一种炮仗花复合香精及其在牙膏中的应用,该炮仗花复合香精由10～20份炮仗花提取物、18～37份天然薄荷脑、30～47份薄荷素油、0.8～1.7份茴香油、0.4～0.8份丁香酚和0.5～1.3份留兰香油混合制得。本发明的炮仗花复合香精香气浓郁、稳定而留长,且具有消肿止痛、活血散瘀、祛痱止痒、提神醒脑之功效。将其应用到牙膏中,针对牙龈红肿以及牙龈出血具有良好的缓解效果。(The invention discloses a polygonum branch flower composite essence and application thereof in toothpaste, wherein the polygonum branch flower composite essence is prepared by mixing 10-20 parts of polygonum branch flower extract, 18-37 parts of natural menthol, 30-47 parts of peppermint oil, 0.8-1.7 parts of fennel oil, 0.4-0.8 part of eugenol and 0.5-1.3 parts of spearmint oil. The polygonum cuspidatum flower composite essence disclosed by the invention is strong in fragrance, stable and long in remaining, and has the effects of relieving swelling and pain, promoting blood circulation to remove blood stasis, removing miliaria, relieving itching, refreshing and restoring consciousness. The toothpaste is applied to toothpaste, and has good relieving effect on gingival swelling and gingival bleeding.)

1. The composite essence of the fire cracker flower is characterized by being prepared by mixing the following components in parts by weight:

the preparation method of the polygonum cuspidatum extract comprises the following steps:

mixing the polygonum capitatum, 40-75% ethanol solution and purified water, soaking for 36-48 h under the vacuum degree of-0.050-0.060 MPa, heating and decocting for 4-5 h, and filtering to obtain filtrate and filter residue; decolorizing the filtrate, and concentrating to obtain rhizoma Polygoni Cuspidati extract.

2. The fire-fighting stick flower composite essence according to claim 1, which is characterized in that: the mass ratio of the polygonum cuspidatum flower to the ethanol solution to the purified water is (0.60-1.25) to (0.45-0.85) to (3.5-4.5).

3. The fire-fighting stick flower composite essence according to claim 1, which is characterized in that: the heating decoction is carried out for 4.5 hours at 65-85 ℃.

4. The fire-fighting stick flower composite essence according to claim 1, which is characterized in that: the concentration is carried out at 70-100 ℃.

5. The use of the complex essence of polygonum cuspidatum of any one of claims 1-4 in toothpaste.

6. A toothpaste characterized by comprising 1.5-2.5% (w/w) of the polygonum branch composite essence according to any one of claims 1-4.

7. The toothpaste according to claim 6, characterized in that it is prepared from the following ingredients in percentage by mass:

8. a method of preparing a toothpaste as claimed in claim 7, comprising the steps of:

a. dissolving sodium lauryl sulfate in purified water to form a mixture D1;

b. dispersing sodium carboxymethylcellulose in silicon dioxide to form a mixture D2;

c. uniformly mixing trisodium phosphate, sodium saccharin, sodium monofluorophosphate and the mixture D1, and heating for 5-10 min to form a mixture D3;

d. uniformly mixing sorbitol with the mixture D2, and heating for 5-10 min to form a mixture D4;

e. adding the mixture D3 and D4 into an emulsifying pot, adding essence of the natural polygonum capitatum extract, uniformly mixing, stirring for 3-5 min under vacuum to prepare paste, and filling into a composite tube.

9. The method of claim 8, wherein: and c, heating at 50-70 ℃.

10. The method of claim 8, wherein: and d, heating at the temperature of 60-70 ℃.

Technical Field

The invention belongs to the field of natural product application, and particularly relates to a polygonum cuspidatum flower composite essence and application thereof in toothpaste.

Background

Toothpaste is a daily necessity and has a long history. With the development of society, various types of toothpastes are coming out, and the application of natural extracts as active ingredients to toothpastes to solve related oral problems has become a mainstream hot spot in the market.

Giant knotweed, another name: 1, ricefield eel vines; latin name: pyrostegia venusta (Ker-Gawl.) Miers, Bignoniaceae, Bighead cane vine of genus Polygonum, has 3-pronged tendrils. Leaf generation; stamen grows in the middle of the corolla tube, filaments are shaped, and anthers are forked. The ovary is cylindrical, the quilt is fine and soft, the style is thin, the stigma is lingulate and flat, and the style and the filament extend out of the corolla. The fruit is in a shape of a boat, seeds are arranged in multiple rows in the fruit, the seeds have wings, the fruit is thin and the flowering period is long. Native south American Brazil has been widely cultivated as a garden ornamental vine in tropical Asia. Researches show that the phenolic substances in the polygonum cuspidatum extract have antibacterial, anti-caries and antioxidant activities. The cambium flower is used as a conventional tonic for treating any inflammatory disease in the traditional Brazilian medicine, and has the effects of resisting tumors and regulating metabolic disorder. Therefore, the development of the daily necessities of the firecracker which are deeply liked by people has strong application prospect.

Disclosure of Invention

The invention aims to provide the polygonum cuspidatum flower composite essence with the effects of relieving swelling and pain, promoting blood circulation to remove blood stasis, removing miliaria, relieving itching and refreshing brain.

The invention also aims to provide the application of the polygonum cuspidatum flower composite essence in toothpaste.

The purpose of the invention is realized by the following technical scheme:

the composite essence of the fire cracker flower is prepared by mixing the following components in parts by weight:

the preparation method of the polygonum cuspidatum extract comprises the following steps:

mixing the polygonum capitatum, 40-75% ethanol solution and purified water, soaking for 36-48 h under the vacuum degree of-0.050-0.060 MPa, heating and decocting for 4-5 h, and filtering to obtain filtrate and filter residue; decolorizing the filtrate, and concentrating to obtain rhizoma Polygoni Cuspidati extract;

preferably, the mass ratio of the polygonum cuspidatum flower to the ethanol solution to the purified water is (0.60-1.25): (0.45-0.85): (3.5-4.5);

the heating decoction is preferably carried out for 4.5 hours at 65-85 ℃;

the concentration is preferably performed at 70-100 ℃.

The polygonum cuspidatum flower composite essence is applied to toothpaste, has the effects of clearing heat, reducing internal heat, diminishing inflammation, removing halitosis and the like, and particularly has a good relieving effect on gingival swelling and gingival bleeding.

A toothpaste contains 1.5-2.5% (w/w) of rhizoma Polygoni Cuspidati flower composite essence;

the toothpaste is prepared from the following components in percentage by mass:

the preparation method of the toothpaste comprises the following steps:

a. dissolving sodium lauryl sulfate in purified water to form a mixture D1;

b. dispersing sodium carboxymethylcellulose in silicon dioxide to form a mixture D2;

c. uniformly mixing trisodium phosphate, sodium saccharin, sodium monofluorophosphate and the mixture D1, and heating for 5-10 min to form a mixture D3;

d. uniformly mixing sorbitol with the mixture D2, and heating for 5-10 min to form a mixture D4;

e. adding the mixtures D3 and D4 into an emulsifying pot, adding essence of the natural polygonum capitatum extract, uniformly mixing, stirring for 3-5 min under vacuum to prepare paste, and filling into a composite tube;

preferably, the heating temperature in the step c is 50-70 ℃, and the heating temperature in the step d is 60-70 ℃.

Compared with the prior art, the invention has the following advantages and effects:

1. the polygonum cuspidatum flower composite essence disclosed by the invention is strong in fragrance, stable and long in remaining, and has the effects of relieving swelling and pain, promoting blood circulation to remove blood stasis, removing miliaria, relieving itching, refreshing and restoring consciousness.

2. The toothpaste containing the polygonum cuspidatum flower composite essence can play roles in clearing heat, reducing internal heat, diminishing inflammation, removing halitosis and the like, and particularly has a good relieving effect on gingival swelling and gingival bleeding. The main component is natural extract, so the Chinese medicinal composition has natural functions of diminishing inflammation, relieving pain and stopping bleeding and has no side effect. Meanwhile, the health care wine is suitable for the old, the young, the women and the children, and is beneficial and harmless after being used for a long time.

3. The toothpaste of the invention has simple preparation process and is suitable for industrial production.

Detailed Description

The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto.