Preparation method of plant pulp glue solution for building

文档序号:1667933 发布日期:2019-12-31 浏览:29次 中文

阅读说明:本技术 一种建筑用植物浆胶液的制备方法 (Preparation method of plant pulp glue solution for building ) 是由 盘登科 潘明德 向耿辉 季金苟 谢方奎 于 2019-09-19 设计创作,主要内容包括:本发明公开了一种建筑用植物浆胶液的制备方法,由以下质量份的各物质组成:2.0-9.0份的聚乙烯醇(PVA)、0.2-0.6份的润滑剂、0.2-0.6份的羧甲基纤维素钠(CMC)、0.007-0.045份的交联剂、0.005-0.02份的防触变剂、0.01-0.06份的增稠剂、0.02-0.04份的缓凝剂、小于0.01份的消泡剂、0.08-0.25份的防腐剂、90-97.5份的水。优点在于:本发明通过交联反应得到的植物浆胶液解决了传统胶水拌合双飞粉流挂、施工困难、填充性差等难题,可彻底排除引入1级致癌物石棉的可能性,好施工、更环保、是普通腻子胶水的理想更新换代产品,具有较大的市场应用前景。(The invention discloses a preparation method of plant pulp glue solution for buildings, which comprises the following substances in parts by mass: 2.0-9.0 parts of polyvinyl alcohol (PVA), 0.2-0.6 part of lubricant, 0.2-0.6 part of sodium carboxymethylcellulose (CMC), 0.007-0.045 part of cross-linking agent, 0.005-0.02 part of anti-thixotropic agent, 0.01-0.06 part of thickening agent, 0.02-0.04 part of retarder, less than 0.01 part of defoaming agent, 0.08-0.25 part of preservative and 90-97.5 parts of water. Has the advantages that: the plant pulp glue solution obtained through the cross-linking reaction solves the problems of sagging, difficult construction, poor filling property and the like of the traditional glue solution mixed with double flying powder, can thoroughly eliminate the possibility of introducing 1-grade carcinogen asbestos, is good in construction, more environment-friendly, is an ideal updated product of common putty glue, and has a great market application prospect.)

1. A plant pulp glue solution for buildings is composed of the following substances in parts by mass:

2. the plant size solution for building as claimed in claim 1, wherein the polyvinyl alcohol (PVA) is one or more of polyvinyl alcohol 2488, polyvinyl alcohol 2099 or polyvinyl alcohol 1792.

3. The plant size solution for building as claimed in claim 1, wherein the lubricant is low molecular weight polyacrylamide with a molecular weight of 100-400 ten thousand.

4. The plant mucilage solution for construction as claimed in claim 1, wherein the viscosity of the sodium carboxymethyl cellulose (CMC) is 1500-5000 mPa.s.

5. The plant pulp glue solution for building as claimed in claim 1, which is characterized in that: the cross-linking agent is one or more of boric acid, sodium tripolyphosphate or phosphoric acid; the anti-thixotropic agent is ammonium polyphosphate or melamine; the thickening agent is high molecular weight polyacrylamide with the molecular weight of 800-1600 ten thousand; the retarder is one or more of citric acid or sodium gluconate; the defoaming agent is one or more of dibutyl phosphate or tributyl phosphate.

6. The construction plant size solution according to claim 1, wherein the preservative is one or more of Methylisothiazolinone (MIT), isothiazolinone (CMIT) or Benzisothiazolinone (BIT).

7. The preparation method of the plant pulp glue solution for the building as claimed in claims 1-6, characterized in that: the preparation method comprises the following steps:

1) adding water into PVA at a concentration of 0.05-0.08g/g, heating to 90-95 deg.C, stirring for more than 40min to dissolve, and cooling to 80-85 deg.C.

2) Dissolving boric acid into 0.005-0.01g/g aqueous solution, dripping into PVA solution under stirring for 5-10min, and reacting for 20-30min after dripping. The stirring speed was 300 revolutions/min. Cooling to below 50 deg.C to obtain clear and transparent solution.

3) And (3) sequentially adding the dissolved lubricant, the CMC, the anti-thixotropic agent, the thickening agent, the citric acid, the dibutyl phosphate and the BIT into the solution obtained in the step 2), adding water for quantification, and uniformly stirring to obtain the plant pulp glue solution.

8. The construction plant size solution as claimed in claim 7, wherein the PVA in step 1) is PVA 2099.

9. The plant pulp glue solution for building as claimed in claim 7, wherein the cross-linking agent in step 2) is boric acid.

10. The plant pulp glue solution for buildings according to claim 7, characterized in that the retarder in the step 3) is citric acid; the defoaming agent is dibutyl phosphate; the preservative is BIT.

Technical Field

The invention relates to the technical field of glue solution, in particular to a preparation method of plant pulp glue solution for buildings.

Background

The putty (filling mud) is a decorative setting material for leveling the surface of a wall body, is thick paste paint and is an essential product before painting. Is applied on the primer or directly applied on the object to remove the defects of high and low unevenness on the surface of the object to be coated. The filler is mainly heavy calcium carbonate, talcum powder and the like, and common putty glue is usually added to improve the adhesiveness of the filler. Can fill the working surface with partial depression and can also scrape the whole surface. The traditional glue is mixed with double flying powder and flows, the construction is difficult, the filling property is poor, and 1-grade carcinogen asbestos can be introduced possibly to harm the bodies of constructors.

In order to solve the problems, a preparation method of plant pulp glue solution for buildings is provided.

Disclosure of Invention

The invention aims to solve the problems in the background art and provides a preparation method of plant pulp glue solution for buildings.

In order to achieve the purpose, the invention adopts the following technical scheme: a plant pulp glue solution for buildings is composed of the following substances in parts by mass:

in the plant size liquid for building, the polyvinyl alcohol (PVA) is one or more of polyvinyl alcohol 2488, polyvinyl alcohol 2099 and polyvinyl alcohol 1792.

In the plant size liquid for buildings, the lubricant is low molecular weight polyacrylamide with the molecular weight of 100-400 ten thousand.

In the plant size liquid for construction, the viscosity of the sodium carboxymethyl cellulose (CMC) is 1500-5000 mPa.s.

In the plant pulp glue solution for the building, the cross-linking agent is one or more of boric acid, sodium tripolyphosphate or phosphoric acid; the anti-thixotropic agent is ammonium polyphosphate or melamine; the thickening agent is high molecular weight polyacrylamide with the molecular weight of 800-1600 ten thousand; the retarder is one or more of citric acid or sodium gluconate; the defoaming agent is one or more of dibutyl phosphate or tributyl phosphate.

In the above-mentioned one construction plant pulp liquid, the preservative is one or more of Methylisothiazolinone (MIT), isothiazolinone (CMIT) or Benzisothiazolinone (BIT).

In the preparation method of the plant pulp glue solution for the building, the preparation method comprises the following steps:

1) adding water into PVA at a concentration of 0.05-0.08g/g, heating to 90-95 deg.C, stirring for more than 40min to dissolve, and cooling to 80-85 deg.C.

2) Dissolving boric acid into 0.005-0.01g/g aqueous solution, dripping into PVA solution under stirring for 5-10min, and reacting for 20-30min after dripping. The stirring speed was 300 revolutions/min. Cooling to below 50 deg.C to obtain clear and transparent solution.

3) And (3) sequentially adding the dissolved lubricant, the CMC, the anti-thixotropic agent, the thickening agent, the citric acid, the dibutyl phosphate and the BIT into the solution obtained in the step 2), adding water for quantification, and uniformly stirring to obtain the plant pulp glue solution.

In the above preparation method of the plant pulp liquid for construction, the PVA in step 1) is polyvinyl alcohol 2099.

In the preparation method of the plant pulp glue solution for the building, the cross-linking agent in the step 2) is boric acid.

In the preparation method of the plant pulp glue solution for the building, the retarder in the step 3) is citric acid; the defoaming agent is dibutyl phosphate; the preservative is BIT.

Compared with the prior art, the preparation method of the plant pulp glue solution for the building has the advantages that:

the plant pulp glue solution for the building, which is obtained through the cross-linking reaction, solves the problems of sagging, difficult construction, poor filling property and the like of the double-flying powder mixed by the traditional glue solution, can thoroughly eliminate the possibility of introducing 1-grade carcinogen asbestos, is good in construction, more environment-friendly, is an ideal updated product of common putty glue, and has a great application prospect.

Detailed Description

The following examples are for illustrative purposes only and are not intended to limit the scope of the present invention.

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