阅读说明：本技术 一种含有黄皮提取物的烟用香精、制备方法及应用 (Cigarette essence containing clausena lansium extract, preparation method and application ) 是由 朱丛戎 邱光明 刘如灿 李朝荣 王毅 周远祥 周胜 杨文敏 赵玉轩 陶文生 马明 于 2019-08-30 设计创作，主要内容包括：本发明公开了一种含有黄皮提取物的烟用香精、制备方法及应用,涉及烟用香精技术领域,一种含有黄皮提取物的烟用香精,包括以下重量份的原料：95Vol％酒精20-50份、黄皮果提取物5-20份、黄皮叶提取物7-25份、乙基麦芽酚0.2-0.8份、树苔浸膏3-8份、烟草提取物0.5-3份、甲基紫罗兰酮0.1-0.3份、蜂蜜10-30份、丙二醇补足至100份。本发明的一种含有黄皮提取物的烟用香精,能赋予卷烟较为明显的特征香气、香气谐调自然,提升香气的质感与清晰度；增加青、熟甜香韵,清新、雅度,使得卷烟抽吸的整体品质得到提升。(the invention discloses a cigarette essence containing a clausena lansium extract, a preparation method and an application, and relates to the technical field of cigarette essences, wherein the cigarette essence containing the clausena lansium extract comprises the following raw materials in parts by weight: 20-50 parts of 95 Vol% alcohol, 5-20 parts of wampee fruit extract, 7-25 parts of wampee leaf extract, 0.2-0.8 part of ethyl maltol, 3-8 parts of tree moss extract, 0.5-3 parts of tobacco extract, 0.1-0.3 part of methyl ionone, 10-30 parts of honey and the balance of propylene glycol to 100 parts. The cigarette essence containing the clausena lansium extract can endow cigarettes with obvious characteristic aroma and harmonious and natural aroma, and improve the texture and definition of the aroma; the green and cooked sweet note is added, and the freshness and elegance are improved, so that the overall quality of cigarette smoking is improved.)

1. The cigarette essence containing the clausena lansium extract is characterized by comprising the following raw materials in parts by weight: 20-50 parts of 95 Vol% alcohol, 5-20 parts of wampee fruit extract, 7-25 parts of wampee leaf extract, 0.2-0.8 part of ethyl maltol, 3-8 parts of tree moss extract, 0.5-3 parts of tobacco extract, 0.1-0.3 part of methyl ionone, 10-30 parts of honey and the balance of propylene glycol to 100 parts.

2. The tobacco flavor containing the clausena lansium extract as claimed in claim 1, is characterized by mainly comprising the following raw materials in parts by weight: 30 parts of 95 Vol% alcohol, 10 parts of Chinese wampee fruit extract, 15 parts of Chinese wampee leaf extract, 0.6 part of ethyl maltol, 6 parts of tree moss extract, 2 parts of tobacco extract, 0.2 part of methyl ionone, 20 parts of honey and the balance of propylene glycol to 100 parts.

3. The tobacco flavor containing the clausena lansium extract as claimed in claim 1, wherein the clausena lansium extract is prepared by soaking and reflux-extracting the clausena lansium with 30-70 Vol% alcohol, then concentrating under reduced pressure, and finally carrying out Maillard reaction.

4. The tobacco flavor containing the clausena lansium extract as claimed in claim 1, wherein the clausena lansium leaf extract is prepared by pulverizing and sieving clausena lansium leaves, soaking and extracting the leaves with 30-70 Vol% ethanol under reflux, and then concentrating the leaves under reduced pressure.

5. A preparation method of cigarette essence containing wampee extract is characterized by comprising the following steps: respectively weighing 20-50 parts of 95 Vol% alcohol, 5-20 parts of Chinese wampee fruit extract, 7-25 parts of Chinese wampee leaf extract, 0.2-0.8 part of ethyl maltol, 3-8 parts of tree moss extract, 0.5-3 parts of tobacco extract, 0.1-0.3 part of methyl ionone, 10-30 parts of honey and propylene glycol to complement to 100 parts by weight, and mixing and stirring uniformly at room temperature to obtain the tobacco essence.

6. The method for preparing the cigarette flavor containing the clausena lansium extract as claimed in claim 5, wherein the method for preparing the clausena lansium extract specifically comprises the following steps:

Coarse extraction: taking 500g of wampee fruit, adding 4-7L of 30-70 Vol% alcohol, mincing with a juicer for 1min, heating and refluxing for 1-3h, and then concentrating under reduced pressure to 30-50% of the original volume to obtain a coarse extract of the wampee fruit extract for later use;

refining: taking 100g of crude extract of wampee fruit extract, adding 2-8g of amino acid, and reacting at pH 7.5-9.0 and temperature 75-90 deg.C for 1-5h to obtain wampee fruit extract.

7. The method for preparing the tobacco flavor containing the clausena lansium extract as claimed in claim 6, wherein the amino acid is any one of proline, glycine, leucine, phenylalanine, glutamic acid and tryptophan.

8. The preparation method of the cigarette essence containing the clausena lansium extract as claimed in claim 5, wherein the preparation method of the clausena lansium leaf extract comprises the following steps: taking 500g of Chinese wampee leaves, drying in an oven at 50 ℃ for 2h, crushing, sieving with a 100-mesh sieve, adding 3-6L of 30-70 Vol% alcohol, heating and refluxing for 1-3h, and then concentrating under reduced pressure to 20-40% of the original volume to obtain the Chinese wampee leaf extract.

9. The use of the tobacco flavor containing the clausena lansium extract in cigarettes according to any one of claims 1 to 4, wherein the tobacco flavor is added into the tobacco shreds of the cigarettes in an amount of 0.1 to 1 percent of the mass of the tobacco shreds.

Technical Field

The invention relates to the technical field of tobacco essence, in particular to tobacco essence containing clausena lansium extract, a preparation method and application.

Background

Earlier, people have utilized the extracts of flowers and plants or tea leaves as tobacco additives, and have conducted extensive research on the aspects of improving the cigarette quality, increasing the cigarette flavor and taste, and the like. Researchers can concentrate the momordica grosvenori extract into cigarette additives by decompression, and the cigarette additives are added into the polypropylene filter tip adhesive according to a certain proportion to prepare the polypropylene filter tip, so that the effects of increasing aroma, improving the comfort level of cigarettes and reducing smoking harm can be achieved; the novel hawthorn spice prepared by Zhang Qisong and the like not only maintains the characteristic aroma of the hawthorn, but also increases the brewing aroma and the fruit aroma, has typical style, can effectively remove miscellaneous gases, improves and modifies the aroma of cigarettes, makes the smoke soft and has the effect of obviously improving the smoke quality; the tomato composite enzymolysis extract such as the poplar bud and the like can soften smoke, enrich tobacco fragrance, increase fresh and sweet feeling and reduce irritation after being applied to tobacco shreds, and is beneficial to the improvement of cigarette smoking quality. The fruit raw materials have respective characteristic fragrance, different fruits have different tastes and physiological effects, the fruit flavor enhancer is endowed with stronger characteristics when being applied to cigarettes, and the fruit flavor enhancer can be compatible with the flavor blending technology of the cigarettes, so that abundant extract raw material sources are provided.

Clausena lansium (Lour.) Skeels is a evergreen fruit tree of Clausena genus of Rutaceae family, is native to southern China, is planted more in Guangdong, Guangxi, Fujian and Taiwan, and is widely applied to ancient and modern Chinese herbal medicine books in China. The wampee fruit is sour, sweet and delicious, has unique flavor, higher nutritive value and health care function, has the effects of promoting qi circulation and helping digestion, and can be used for treating food retention, fullness and dyspnea, and the like. Researches show that the clausena lansium pulp contains various chemical components such as rich alkaloids, coumarins, volatile oils and flavonoids, and has biological activities in multiple aspects such as oxidation resistance, liver protection, blood sugar reduction, insect killing, bacteriostasis, weeding and the like. At present, the application direction of the clausena lansium extract mainly lies in the technical field of medicine or cosmetics, and reports in the field of tobacco essence are hardly seen.

in addition, in the planting process of the wampee, branches are trimmed once in summer and winter every year, the waste branches generated by the trimming can be burnt only as firewood, resources are wasted, and the environment is polluted. The reported chemical compositions in wampee leaves are: in recent years, the Chinese wampee leaves are reported to have various biological activities of protecting liver, promoting intelligence, resisting bacteria, reducing blood fat, reducing blood sugar and the like. Therefore, the discarded Chinese wampee leaves actually have very high utilization value, and if the trimmed Chinese wampee leaves can be reused, the added value of the Chinese wampee leaves is greatly increased.

Disclosure of Invention

aiming at the problems, the invention aims to design and provide the cigarette essence containing the clausena lansium extract, which can endow the cigarette with more obvious characteristic aroma and harmonious and natural aroma and improve the texture and definition of the aroma; the green and cooked sweet note is added, and the freshness and elegance are improved, so that the overall quality of cigarette smoking is improved.

The invention solves the technical problems by the following technical means:

A cigarette essence containing wampee extract comprises the following raw materials in parts by weight: 20-50 parts of 95 Vol% alcohol, 5-20 parts of wampee fruit extract, 7-25 parts of wampee leaf extract, 0.2-0.8 part of ethyl maltol, 3-8 parts of tree moss extract, 0.5-3 parts of tobacco extract, 0.1-0.3 part of methyl ionone, 10-30 parts of honey and the balance of propylene glycol to 100 parts.

according to the tobacco essence, the clausena lansium fruit extract and the clausena lansium leaf extract are added into the raw materials, and main components of the refined clausena lansium fruit extract and the refined clausena lansium leaf extract enter a human body along with mainstream breath and are absorbed in the smoking process, so that the tobacco essence has the effects of promoting digestion, reducing phlegm and regulating qi, and has the effects of dispelling wind, relieving exterior syndrome, eliminating phlegm and promoting qi circulation, and is used for preventing and treating influenza.

In addition, the research of the inventor shows that because the Chinese wampee fruit extract contains a large amount of carbohydrate, if only the Chinese wampee fruit extract is added into the tobacco essence, when the cigarette is burnt, sweet and greasy taste is brought to smokers, and unfavorable sensory experience is brought to the cigarette, and if only the Chinese wampee leaf extract is added, when the cigarette is burnt, the cigarette brings harsh feeling to smokers and brings unfavorable sensory experience to the cigarette, when the Chinese wampee fruit extract and the Chinese wampee leaf extract are simultaneously added into the tobacco essence according to a certain proportion, sweet and greasy feeling in the Chinese wampee fruit extract and astringent feeling in the Chinese wampee leaf extract are mutually offset and fused, the sweet and greasy feeling in the Chinese wampee fruit extract and the Chinese wampee leaf extract can play a role in complementation and mutual enhancement of application effects, and the Chinese wampee fruit extract and the Chinese wampee leaf extract can be used simultaneously to endow the cigarettes with obvious characteristic aroma and harmonious and natural aroma, so that the texture and definition of the aroma are improved; the green and cooked sweet note is added, and the freshness and elegance are improved, so that the overall quality of cigarette smoking is improved.

Further, the feed mainly comprises the following raw materials in parts by weight: 30 parts of 95 Vol% alcohol, 10 parts of Chinese wampee fruit extract, 15 parts of Chinese wampee leaf extract, 0.6 part of ethyl maltol, 6 parts of tree moss extract, 2 parts of tobacco extract, 0.2 part of methyl ionone, 20 parts of honey and the balance of propylene glycol to 100 parts.

Further, the Chinese wampee fruit extract is prepared by soaking and refluxing the Chinese wampee fruit in 30-70 Vol% alcohol, then carrying out reduced pressure concentration, and finally carrying out Maillard reaction.

The Chinese wampee fruit extract after the Maillard reaction can overcome the problems of weak characteristic aroma, slight stimulation, slight miscellaneous gas, smoke emission and the like caused by the direct application of the Chinese wampee fruit extract prepared by the conventional method in cigarettes. In addition, the wampee fruit extract contains a large amount of reducing sugar, the reducing sugar with too high content can bring unfavorable sensory experience to cigarettes during combustion, and after the maillard reaction, the reducing sugar and amino acid react to generate a large amount of flavor substances with oxidation resistance, so that the effect of eliminating free radicals in vivo can be achieved, and the positive effect of reducing smoking harm is achieved.

further, the Chinese wampee leaf extract is prepared by crushing and sieving Chinese wampee leaves, soaking and extracting the Chinese wampee leaves by refluxing in 30-70 Vol% alcohol, and then concentrating under reduced pressure.

In addition, the invention also discloses a preparation method of the cigarette essence containing the clausena lansium extract, which comprises the following steps: respectively weighing 20-50 parts of 95 Vol% alcohol, 5-20 parts of Chinese wampee fruit extract, 7-25 parts of Chinese wampee leaf extract, 0.2-0.8 part of ethyl maltol, 3-8 parts of tree moss extract, 0.5-3 parts of tobacco extract, 0.1-0.3 part of methyl ionone, 10-30 parts of honey and propylene glycol to complement to 100 parts by weight, and mixing and stirring uniformly at room temperature to obtain the tobacco essence.

Further, the preparation method of the wampee fruit extract specifically comprises the following steps:

Coarse extraction: taking 500g of wampee fruit, adding 4-7L of 30-70 Vol% alcohol, mincing with a juicer for 1min, heating and refluxing for 1-3h, and then concentrating under reduced pressure to 30-50% of the original volume to obtain a coarse extract of the wampee fruit extract for later use;

Refining: taking 100g of crude extract of wampee fruit extract, adding 2-8g of amino acid, and reacting at pH 7.5-9.0 and temperature 75-90 deg.C for 1-5h to obtain wampee fruit extract.

further, the amino acid is any one of proline, glycine, leucine, phenylalanine, glutamic acid and tryptophan.

Further, the preparation method of the Chinese wampee leaf extract comprises the following steps: taking 500g of Chinese wampee leaves, drying in an oven at 50 ℃ for 2h, crushing, sieving with a 100-mesh sieve, adding 3-6L of 30-70 Vol% alcohol, heating and refluxing for 1-3h, and then concentrating under reduced pressure to 20-40% of the original volume to obtain the Chinese wampee leaf extract.

The invention also discloses application of the tobacco essence containing the clausena lansium extract in cigarettes, and particularly relates to the tobacco essence which accounts for 0.1-1% of the mass of tobacco shreds and is added into the tobacco shreds of the cigarettes.

the invention has the beneficial effects that:

1. according to the cigarette essence containing the clausena lansium extract, the clausena lansium fruit extract and the clausena lansium leaf extract are added into the raw materials, and have the effects of complementation and mutual enhancement of application effects, when the essence is applied to cigarettes, the cigarette can be endowed with obvious characteristic aroma, the aroma is harmonious and natural, and the texture and the definition of the aroma are improved; the green and cooked sweet note is added, and the freshness and elegance are improved, so that the overall quality of cigarette smoking is improved.

2. The main components of the Chinese wampee fruit extract and the Chinese wampee leaf extract added in the invention can enter the human body along with the mainstream breath and be absorbed in the burning and sucking process, thereby having the effects of promoting digestion, reducing phlegm and regulating qi, dispelling wind, relieving exterior syndrome, eliminating phlegm and promoting qi circulation, and being used for preventing and treating influenza.

3. The wampee fruit extract is refined through Maillard reaction, so that the content of reducing sugar in the wampee fruit extract is reduced, and meanwhile, a large amount of generated flavor substances have oxidation resistance and can play a role in removing free radicals in vivo, so that the positive effect on reducing smoking harm is achieved.

4. the preparation method of the tobacco essence is simple, mild in condition, simple in equipment requirement, low in cost, easy to produce in industrialization and suitable for popularization and use.

5. According to the invention, the raw material of the Chinese wampee leaf extract can utilize Chinese wampee leaf on the waste branch of the Chinese wampee tree pruning every year, so that the resource is fully utilized, waste is changed into valuable, and the added value of the Chinese wampee leaf extract is greatly increased.

Detailed Description

The present invention will be described in detail with reference to specific examples below: