阅读说明：本技术 一种火龙果园内实蝇防治液及其制备方法和应用 (Trypetid prevention and treatment liquid and its preparation method and application in a kind of flue orchard ) 是由 郑伟 王彬 韦家平 黄家改 黄国全 蒋邦念 韦堂倩 李兴忠 于 2019-08-30 设计创作，主要内容包括：本发明公开了一种火龙果园内实蝇防治液,由以下原料制成：黄花杜鹃、透骨草、草木灰、地肤子、皂角树叶、除虫菊花、银杏外种皮、使君子、马齿苋、松针片、侧柏叶、烟草提取液、雷公藤提取液,还公开了其制备方法和应用。本发明的实蝇防治液原料来源广,制备简单,且能够准确有效杀灭实蝇,使火龙果园内实蝇发生率低至2％,火龙果产量得到了提高,商品果率可以提高到90％以上,亩收入可以增加600元以上,取得良好的经济效益。(The invention discloses trypetids in a kind of flue orchard to prevent and treat liquid, be prepared from the following raw materials: chrysanthemum cuckoo, lopseed, plant ash, the fruit of summer cypress, Chinese honey locust leaf, pyrethrum flowers, gingko episperm, the fruit of Rangoon creeper, purslane, pine needle piece, cacumen biotae, tobacco extract, tripterygium wilfordii extracting solution also disclose preparation method and application.Trypetid prevention and treatment liquid raw material sources of the invention are wide, preparation is simple, and can accurate and effective kill trypetid, make in flue orchard trypetid incidence down to 2%, dragon fruit yield is improved, commodity fruit rate can be improved to 90% or more, and mu income can increase by 600 yuan or more, obtain good economic benefit.)

1. trypetid prevents and treats liquid in a kind of flue orchard, which is characterized in that be made of raw material from the following weight: chrysanthemum cuckoo 120 ~160 parts, 155~195 parts of lopseed, 150~200 parts of plant ash, 130~170 parts of the fruit of summer cypress, Chinese honey locust leaf 200~250 Part, 85~125 parts of pyrethrum flowers, 225~265 parts of gingko episperm, 45~85 parts of the fruit of Rangoon creeper, 55~95 parts of purslane, pine needle 50~100 parts of piece, 50~100 parts of cacumen biotae, 180~230 parts of tobacco extract, 200~250 parts of tripterygium wilfordii extracting solution.

2. trypetid prevents and treats liquid in a kind of flue orchard according to claim 1, which is characterized in that by the original of following parts by weight Material is made: 130~150 parts of chrysanthemum cuckoo, 165~185 parts of lopseed, 160~190 parts of plant ash, 140~160 parts of the fruit of summer cypress, 210~240 parts of Chinese honey locust leaf, 95~115 parts of pyrethrum flowers, 235~255 parts of gingko episperm, 55~75 parts of the fruit of Rangoon creeper, dent 65~85 parts of amaranth, 60~90 parts of pine needle piece, 60~90 parts of cacumen biotae, 190~220 parts of tobacco extract, tripterygium wilfordii extracting solution 210 ~240 parts.

3. trypetid prevents and treats liquid in a kind of flue orchard according to claim 1, which is characterized in that by the original of following parts by weight Material is made: 140 parts of chrysanthemum cuckoo, 175 parts of lopseed, 175 parts of plant ash, 150 parts of the fruit of summer cypress, 225 parts of Chinese honey locust leaf, Dalmatian chrysanthemum Spend 100 parts, 245 parts of gingko episperm, 65 parts of the fruit of Rangoon creeper, 75 parts of purslane, 75 parts of pine needle piece, 75 parts of cacumen biotae, tobacco extraction 205 parts of liquid, 225 parts of tripterygium wilfordii extracting solution.

4. trypetid prevents and treats liquid in a kind of described in any item flue orchards according to claim 1~3, it is characterised in that: the cigarette The preparation method of careless extracting solution is: the deionized water of 5~6 times of its quality being added into clean tobacco, impregnates 45~50h, greatly Baked wheaten cake opens rear small fire and decocts 55~70min, and filtering and removing slag are added the lime of the quality such as tobacco, stir evenly, obtain the tobacco Extracting solution.

5. trypetid prevents and treats liquid in a kind of described in any item flue orchards according to claim 1~3, it is characterised in that: the thunder Public rattan extracting solution: clean tripterygium wilfordii being put into the ethanol solution that 5~6 times of its quality and mass concentration are 85%, and immersion 2~ After 3h, 7~9h of refluxing extraction at 65~70 DEG C, filtering, it is 1.21~1.28 that filtrate decompression, which is concentrated into relative density, obtains institute State tripterygium wilfordii extracting solution.

6. the preparation method of trypetid prevention and treatment liquid in a kind of flue orchard, which comprises the steps of:

(1) lopseed, the fruit of summer cypress, gingko episperm, the fruit of Rangoon creeper and pine needle piece are weighed in parts by weight, are cleaned after draining away the water, The ethanol solution that the quality such as gingko episperm and mass concentration are 95% is added and adds gingko episperm after impregnating 70~80h The deionized water that 12~15 times of quality decocts 10~13h, and after being cooled to 65~70 DEG C, ultrasonic wave extraction, filtering and removing slag are obtained Extracting solution A；

(2) chrysanthemum cuckoo, Chinese honey locust leaf, pyrethrum flowers and cacumen biotae are weighed in parts by weight, are cleaned after draining away the water, admixture The deionized water that 5~6 times of matter gross mass turns small fire and decocts 7~8h after high fire is boiled, the total matter of substance is added into filter residue for filtering The deionized water of 3~4 times of amount decocts 8~10h, is separated by filtration filtrate and filter residue, merges filtrate twice, obtains extracting solution B；

(3) purslane is cleaned after draining away the water, is sent into juice extractor and squeezes, obtains purslane juice；

(4) temperature is added in plant ash is in 85~100 DEG C of deionized water, and stirring dissolves plant ash sufficiently, with 100~ The filtering of 150 mesh filter bags, filtrate cooled to room temperature obtain plant ash solution；

(5) by tobacco extract, tripterygium wilfordii extracting solution, the extracting solution A of step (1), the extracting solution B of step (2), step (3) The mixing of the plant ash solution of purslane juice and step (4) stirs 20~25min in the case where revolving speed is 2000~2500r/min, quiet 25~30h is set, filtrate is collected by filtration, is purified liquid；

(6) vacuum-concentrcted is carried out to the scavenging solution of step (5) using Rotary Evaporators, be concentrated into relative density be 1.02~ 1.06, it obtains trypetid in the flue orchard and prevents and treats liquid.

7. the preparation method of trypetid prevention and treatment liquid in a kind of flue orchard according to claim 6, it is characterised in that: in step (1), the power of the ultrasonic wave extraction is 145~175W, and extraction time is 40~50min, and Extracting temperature is 60~70 DEG C.

8. the preparation method of trypetid prevention and treatment liquid in a kind of flue orchard according to claim 6, it is characterised in that: in step (6), the temperature of the vacuum-concentrcted is 70~80 DEG C, and vacuum degree is 0.1~0.3Mpa.

9. trypetid prevents and treats liquid in flue orchard made from a kind of preparation method as described in claim 1~8.

10. the application of trypetid prevention and treatment liquid in flue orchard according to claim 9, it is characterised in that: be applied to dragon fruit The prevention and treatment of trypetid in the prevention and treatment of pest and disease damage in garden, especially flue orchard.

Technical field

The present invention relates in crop pest control technical field more particularly to a kind of flue orchard trypetid prevention and treatment liquid and Preparation method and application.

Background technique

Dragon fruit is also known as Hylocereus undatus, passion plant, is Cactaceae triangular prism platymiscium, and fruit is oval, diameter 10- 12cm, appearance are red or yellow, there is the thallus of green rounded triangle, and white, red or yellow pulp have black kind Son.Dragon fruit is full of nutrition, special taste, it contains the rare vegetable albumin of general plant and anthocyanidin, dimension abundant Raw element and water-soluble dietary fiber.In its natural state, fruit is in summer and autumn maturation, sweet, succulence.In recent years, dragon fruit is to collect It eats, watch, being machined in integrated emerging fruit, quite getting consumer reception.

Trypetid, Tephritidae, fruitflies；Fruitfly, the common name of Diptera Acalyptratae Tephritidae, trypetid are subordinate to Belong to Diptera (Diptera) Tephritidae (Tephritidae), about 500 belong to more than 4500 known to the world.1992, White and " the FruitFlies ofEconomic Significance:Their Identification that Elson-Harris is collaborateed And Bionomics " it comes out, the whole world, which is described, with the trypetid meter 26 of economic significance belongs to 233 kinds.

Currently, the document about prevention and treatment trypetid drug has, such as:

1, patent application CN201710751723.9 discloses a kind of citrus fruit fly prevention and treatment liquid and preparation method thereof, warp It crosses and controls brown sugar, white wine, light-coloured vinegar, metrifonate, water according to certain proportion, so that the trapping effect of insect prevention liquid significantly increases By force, it improves to citrus fruit fly control efficiency, reduces citrus planting cost.

2, patent application CN201610799263.2, disclose it is a kind of prevent and treat Lo Han Guo fruit fly medical fluid and its preparation side Method and application method, in parts by weight, by 2~6 parts of light-coloured vinegar, 10~18 parts of brown sugar, 12~20 parts of metrifonate and water 30~50 Part is prepared.It cooks the preparation method comprises the following steps: brown sugar is added in the pot for filling water, until all melting to brown sugar, is subsequently added into Light-coloured vinegar stirs evenly, and obtains mixed liquor；It smashs into metrifonate to pieces 80~200 targeted fine powders, and metrifonate fine powder is added to mixed Close liquid in stir evenly to get.Liquid medicine applying effect of the invention is preferable, can effectively trap and kill the fruit fly of Siraitia grosvenorii, and The dosage of medical fluid is less, greatly reduces the cost of prevention and treatment fruit fly.

3, patent application CN201710883977.6, disclose it is a kind of prevent and treat citrus fruit fly medicament and its preparation side Method is made of raw material from the following weight: 20-40 parts of jamestownweed leaf, 20-30 parts of lemon eucalyptus leaf, 10-20 parts of chenopodium ambrosiodies, ginkgo 12-16 parts of leaf, 8-14 parts of tungoiltree juvenile leaf, 8-14 parts of Chinese alangium leaf, 6-10 parts of sweetscented oleander leaf, 6-12 parts of bunge pricklyash leaf, 4-10 parts of tobacco leaf, 15-25 parts of lilac daphne, 9-15 parts of Rhododendron molle, radix euphorbiae lantu flower 10-20 parts, 18-24 parts of coriaceous cotoneaster root, 15-21 parts of derris root, preservative 4- 6 parts.The pharmaceutical production simple process, it is easy to use, phytotoxicity is not generated to crops, non agricultural chemical residuum is free from environmental pollution, has Drug substance stable, strong drug action, the feature of lasting period length.

4, patent application CN201811052000.0, a kind of fruit fly medicament and preparation method thereof, the original of fruit fly medicament Expect component by mass percentage, comprising: attractant 5%~10%, insecticidal constituent 0.5%~1.0%, emulsifier 2%~ 5%, coemulsifier 2%~5%, solubilizer 1%~3%, surplus is water；Preparation method is comprising steps of by attractant, desinsection Ingredient and emulsifier mix in proportion, and the water of one third is then added with vigorous stirring, co-emulsifier is added after ten minutes Agent continues stirring 20 minutes, adds excess water and solubilizer and obtains fruit fly medicament after stirring 30 minutes.The present invention will draw Lure, insecticidal constituent emulsifier simultaneously wrap up, and uniform solution medicament is made, constantly broken with the volatilization of moisture in medicament Cream releases attractant and insecticidal constituent；Its technical principle is to slow down the rate of release of methyl eugenol by emulsifying technology, Extend and the time is trapped and killed to fruit fly.

But scheme disclosed in document above is not particularly suited for trypetid in flue orchard and prevents and treats, and the above pest and disease damage is anti- Control mode；With the expansion of cultivated area, flue orchard cultivation management is not in place or high-temperature high humidity season management measure less than Position is easy to cause pumpkin fruit fly and citrus fruit fly outburst in flue orchard.And flue orchard pumpkin fruit fly and citrus fruit fly are once Outburst, can cause greater loss to dragon fruit farmer.

Summary of the invention

It is an object of the invention to: in view of the above problems, provide in a kind of flue orchard trypetid prevention and treatment liquid and its Preparation method and application effectively mitigate trypetid and endanger flue fruits.

In order to achieve the above-mentioned object of the invention, The technical solution adopted by the invention is as follows:

Trypetid prevents and treats liquid in a kind of flue orchard, is made of raw material from the following weight: 120~160 parts of chrysanthemum cuckoo, thoroughly 155~195 parts of bone grass, 150~200 parts of plant ash, 130~170 parts of the fruit of summer cypress, 200~250 parts of Chinese honey locust leaf, pyrethrum flowers 85~125 parts, 225~265 parts of gingko episperm, 45~85 parts of the fruit of Rangoon creeper, 55~95 parts of purslane, 50~100 parts of pine needle piece, 50~100 parts of cacumen biotae, 180~230 parts of tobacco extract, 200~250 parts of tripterygium wilfordii extracting solution.

Further, trypetid prevents and treats liquid in a kind of flue orchard, is made of raw material from the following weight: chrysanthemum Du 130~150 parts of cuckoo, 165~185 parts of lopseed, 160~190 parts of plant ash, 140~160 parts of the fruit of summer cypress, Chinese honey locust leaf 210~ 240 parts, 95~115 parts of pyrethrum flowers, 235~255 parts of gingko episperm, 55~75 parts of the fruit of Rangoon creeper, 65~85 parts of purslane, pine 60~90 parts of faller gill, 60~90 parts of cacumen biotae, 190~220 parts of tobacco extract, 210~240 parts of tripterygium wilfordii extracting solution.

Further, trypetid prevents and treats liquid in a kind of flue orchard, is made of raw material from the following weight: chrysanthemum Du 140 parts of cuckoo, 175 parts of lopseed, 175 parts of plant ash, 150 parts of the fruit of summer cypress, 225 parts of Chinese honey locust leaf, 100 parts of pyrethrum flowers, ginkgo 245 parts of exosper, 65 parts of the fruit of Rangoon creeper, 75 parts of purslane, 75 parts of pine needle piece, 75 parts of cacumen biotae, 205 parts of tobacco extract, Thunder God 225 parts of rattan extracting solution.

Further, the preparation method of the tobacco extract is: 5~6 times of its quality being added into clean tobacco Deionized water impregnates 45~50h, and small fire decocts 55~70min after high fire is boiled, and the stone of the quality such as tobacco is added in filtering and removing slag Ash stirs evenly, and obtains the tobacco extract.

Further, the tripterygium wilfordii extracting solution: clean tripterygium wilfordii is put into 5~6 times of its quality and mass concentration is In 85% ethanol solution, after impregnating 2~3h, 7~9h of refluxing extraction at 65~70 DEG C is filtered, and filtrate decompression is concentrated into phase It is 1.21~1.28 to density, obtains the tripterygium wilfordii extracting solution.

Further, in a kind of flue orchard trypetid prevention and treatment liquid preparation method, include the following steps:

(1) lopseed, the fruit of summer cypress, gingko episperm, the fruit of Rangoon creeper and pine needle piece are weighed in parts by weight, are cleaned and are drained away the water Afterwards, the ethanol solution that the quality such as gingko episperm and mass concentration are 95% is added to add outside ginkgo after impregnating 70~80h The deionized water of 12~15 times of cortex amount of kind decocts 10~13h, after being cooled to 65~70 DEG C, ultrasonic wave extraction, and filtering and removing slag, Obtain extracting solution A；

(2) chrysanthemum cuckoo, Chinese honey locust leaf, pyrethrum flowers and cacumen biotae are weighed in parts by weight, are cleaned after draining away the water, are added The deionized water for entering 5~6 times of substance gross mass turns small fire and decocts 7~8h after high fire is boiled, substance is added into filter residue for filtering The deionized water that 3~4 times of gross mass decocts 8~10h, is separated by filtration filtrate and filter residue, merges filtrate twice, obtains extracting solution B；

(3) purslane is cleaned after draining away the water, is sent into juice extractor and squeezes, obtains purslane juice；

(4) plant ash is added in the deionized water that temperature is 85~100 DEG C, stirring dissolves plant ash sufficiently, with 100 The filtering of~150 mesh filter bags, filtrate cooled to room temperature obtain plant ash solution；

(5) by tobacco extract, tripterygium wilfordii extracting solution, the extracting solution A of step (1), the extracting solution B of step (2), step (3) mixing of the plant ash solution of purslane juice and step (4), in the case where revolving speed is 2000~2500r/min stirring 20~ 25min stands 25~30h, filtrate is collected by filtration, is purified liquid；

(6) vacuum-concentrcted is carried out using scavenging solution of the Rotary Evaporators to step (5), being concentrated into relative density is 1.02~1.06, it obtains trypetid in the flue orchard and prevents and treats liquid.

Further, in step (1), the power of the ultrasonic wave extraction is 145~175W, extraction time is 40~ 50min, Extracting temperature are 60~70 DEG C.

Further, in step (6), the temperature of the vacuum-concentrcted is 70~80 DEG C, vacuum degree is 0.1~ 0.3Mpa。

Further, trypetid prevents and treats liquid in flue orchard made from a kind of preparation method as described above.

Further, in the flue orchard trypetid prevention and treatment liquid application, applied in flue orchard pest and disease damage it is anti- It controls, the prevention and treatment of trypetid especially in flue orchard.

In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are:

(1) trypetid prevention and treatment liquid raw material sources of the invention are wide, and preparation is simple, and can accurate and effective kill trypetid, make fire Down to 2%, dragon fruit yield is improved trypetid incidence in imperial orchard, and commodity fruit rate can be improved to 90% or more, mu Income can increase by 600 yuan or more, obtain good economic benefit.

(2) prevention and treatment of the application prevention and treatment liquid obtained suitable for pest and disease damage in flue orchard, is especially suitable for flue The prevention and treatment of trypetid in orchard reduces trypetid outburst rate in flue orchard, and the outburst of flue fruit fly is avoided to cause the underproduction；Moreover, Raw material used herein includes the Chinese herbal medicines such as plant ash, pyrethrum flowers, gingko episperm, tobacco extract, can not only be good Trypetid in prevention and treatment garden well, additionally it is possible to effectively prevent the pest and disease damages such as aphid, ant, coccid, prodenia litura, effectively reduce dragon fruit Pest and disease damage incidence in garden.

Specific embodiment

Specific embodiments of the present invention will be described in further detail below, but the invention is not limited to these realities Mode is applied, it is claimed to still fall within the claims in the present invention for any improvement or replacement on the present embodiment essence spirit Range.