阅读说明：本技术 香料模块配方、以及用于加热不燃烧卷烟的香料和加热不燃烧卷烟的制备方法 (Fragrance module formula and fragrance for heating the cigarette that do not burn and heating are not burnt the preparation method of cigarette ) 是由 史健阳 黄玉川 郭林清 赵德清 包毅 郑怡 于 2019-09-18 设计创作，主要内容包括：本发明公开了香料模块配方、以及用于加热不燃烧卷烟的香料和加热不燃烧卷烟的制备方法,涉及加热不燃烧卷烟技术领域。该香料模块配方包括产香主体10-90份、溶剂10-90份、烟草提取物2-50份、增香剂0.5-70份和矫味剂0.1-50份；产香主体选自草本主香、果味饮品主香和花香主香中的至少一种。香料的制备方法,其以上述香料模块配方为原料,通过简单的混合制备得到香料；加热不燃烧卷烟的制备方法,包括将上述方法制备得到的香料加载至加热不燃烧卷烟中,制备得到的加热不燃烧卷烟具有独特的香特征,且不含不愉快的杂气,抽吸口感十分理想。(Fragrance the invention discloses fragrance module formula and for heating the cigarette that do not burn and heating are not burnt the preparation method of cigarette, are related to heating and are not burnt technical field of cigarettes.The fragrance module formula includes fragrant 10-90 parts of the main body of production, 10-90 parts of solvent, 2-50 parts of tobacco extract, 0.5-70 parts of fumet and 0.1-50 parts of corrigent；It produces fragrant main body and is selected from least one of draft main note, fruity beverage main note and fragrance of a flower main note.The preparation method of fragrance obtains fragrance by being simply mixed with using above-mentioned fragrance module formula as raw material；The preparation method for the cigarette that do not burn is heated, the fragrance including the above method to be prepared, which is loaded onto, to be heated in the cigarette that do not burn, and the heating being prepared does not burn cigarette with unique fragrant feature, and is free of offending miscellaneous gas, and it is very ideal to aspirate mouthfeel.)

1. a kind of fragrance module formula, which is characterized in that according to parts by weight, including produce fragrant 10-90 parts of main body, solvent 10-90 Part, 2-50 parts of tobacco extract, 0.5-70 parts of fumet and 0.1-50 parts of corrigent；

Preferably, the fragrant main body of the production is selected from least one of draft main note, fruity beverage main note and fragrance of a flower main note；

It is highly preferred that the draft main note is selected from Radix Glycyrrhizae, mustard, wrinkled giant hyssop, fritillary-loquat, green grass cream, old ginger, Schisandra chinensis, Radix Angelicae Sinensis With any one or more in dandelion；

It is highly preferred that the fruity beverage main note be selected from pineapple, lichee, blueberry, muskmelon, sweet orange, strawberry, bergamot pear, coffee, can Can, any one or more in cola, green tea, Dragon Well tea, gin tonic, whiskey and rock sugar pear；

It is highly preferred that the fragrance of a flower main note is selected from Michelia oil, Michelia alba leaf oil, neroli oil, patchouli oil, costus root oil, perfume (or spice) Thatch alcohol, geraniol, linalool, vanillic aldehyde, eugenol, strawberry aldehyde, osmanthus concrete, perilla herb oil, oil of aglaia odorate, Flos micheliae Albae oil, rose One of rare oil and jasmine lactone are a variety of.

2. fragrance module formula according to claim 1, which is characterized in that the fragrance module formula includes producing fragrant main body 40-80 parts, 30-70 parts of solvent, 5-35 parts of tobacco extract, 1-50 parts of fumet and 0.5-30 parts of corrigent；

Preferably, the fragrance module formula include produce fragrant 50-70 parts of main body, 40-60 parts of solvent, 8-25 parts of tobacco extract, 4-35 parts and corrigent 1-20 parts of fumet.

3. fragrance module formula according to claim 1, which is characterized in that the fumet is essential oil, tincture or medicinal extract；

Preferably, the fumet is selected from juniper berry oil, orrisroot oil, onion oil, wintergreen, absinthium, mustard oil, peppery peppermint Oil, thyme oil, oil of bay, cassia oil, aniseed oil, citronellol, geraniol, nerol, dorinone, orange oil, lemon oil, grass Certain kind of berries extract, coffee tincture, almond oil, jasmine oil, bigarabe leaf extract, attar of rose, orange oil, caryophyllus oil, haw thorn extract, Pineapple extract, mace oil, cassia oil, peppermint oil, ginger oil, isoamyl acetate, phenylethyl isovalerate, ethyl isovalerate, second Any one or more in acetoacetic ester, benzaldehyde, vanillic aldehyde, eugenol, strawberry aldehyde, osmanthus concrete and oil of aglaia odorate；

It is highly preferred that the fumet is selected from juniper berry oil, orrisroot oil, onion oil, wintergreen, absinthium, mustard oil, β-greatly At least one of horse ketone and oil of Peppermint.

4. fragrance module formula according to any one of claim 1-3, which is characterized in that the corrigent is selected from fourth two Sour menthyl ester and its derivative, vanillon, honey, Radix Glycyrrhizae extract, frambinone, 2-3 dimethyl pyrazine, ethyl butyrate, Ethylmaltol, ethyl propionate, vanillic aldehyde, furanone, isobutylaldehyde, isovaleric acid, maltol, benzaldehyde, dimethyl suflfate, 2- first Base butyric acid, isopentyl aldehyde, benzyl carbinol, phenylacetic acid, heliotropin, valeric acid, valeral, butanol, butyric acid, benzyl alcohol, ethyl acetate, cucurbit Bar extract, isobutanol, isobutyric acid, methyl cyclopentenyl ketone, 3-hydroxy-2-butanone, sucrose, sorbierite, ethyl lactate, citric acid, witloof Any one or more in extract, α-ionone, lactic acid, pyruvic acid and tea perfume spirane；

Preferably, the corrigent in menthyl succinate and its derivative, vanillon, honey, Radix Glycyrrhizae extract extremely Few one kind.

5. fragrance module formula according to any one of claim 1-3, which is characterized in that the solvent is selected from water, second Any one or more in alcohol, propylene glycol, glycerol, isopropyl myristate and Ergol.

6. fragrance module formula according to any one of claim 1-3, which is characterized in that the fragrance module formula is also Including 0.1-50 parts of stabilizer；Preferably 1-35 parts；More preferably 5-20 parts.

7. fragrance module formula according to claim 6, which is characterized in that the stabilizer be selected from 'alpha '-hydroxy acids, glycerol, Glyceryl triacetate, triethyl citrate, polyethylene glycol, polyoxyethylene, maltitol, xylitol, sorbierite, propylene glycol, oneself Any one or a few in glycol, butanediol, triethylene glycol, polydextrose, tartaric acid, citric acid, benzoic acid and malic acid；

Preferably, the stabilizer is selected from 'alpha '-hydroxy acids, glycerol, glyceryl triacetate, triethyl citrate, benzoic acid and poly- second Any one or a few in glycol.

8. a kind of for heating the preparation method of the fragrance for the cigarette that do not burn, which comprises the following steps:

Each component in fragrance module formula described in any one of claim 1-7 is uniformly mixed.

The preparation method of cigarette 9. a kind of heating is not burnt, which is characterized in that including the fragrance that will be prepared in claim 8 It is loaded onto described heat in the cigarette that do not burn.

The preparation method of cigarette 10. heating according to claim 9 is not burnt, which is characterized in that the heating is not burnt Cigarette includes smoke section, distance piece, temperature descending section and vinegar fibre section；

Wherein, the 0-10% that the smoke section quality is accounted in the additional amount of the smoke section fragrance, in the distance piece fragrance Additional amount accounts for the 0-15% of the distance piece quality, accounts for the 0- of the temperature descending section quality in the additional amount of the temperature descending section fragrance 15%, the 0-8% of the vinegar fibre section quality is accounted in the additional amount of the vinegar fibre section fragrance；

Preferably, the 0.5-5% that the smoke section quality is accounted in the additional amount of the smoke section fragrance, in the distance piece fragrance Additional amount account for the 0.5-10% of the distance piece quality, account for the temperature descending section quality in the additional amount of the temperature descending section fragrance 0.05-4% accounts for the 0.01-3% of the vinegar fibre section quality in the additional amount of the vinegar fibre section fragrance；

Preferably, fragrance is selected from spray coating method, infusion process, cladding process, injection in the addition manner for heating the cigarette temperature descending section that do not burn At least one of method, gel method and absorption method.

Technical field

The present invention relates to heating not to burn technical field of cigarettes, and in particular to fragrance module formula and for heating It does not burn the fragrance of cigarette and heating is not burnt the preparation method of cigarette.

Background technique

With the continuous improvement of people's living standards, people feel the consumption consciousness of tobacco product from initial satisfaction Pursuit of the today to safety.It does not require nothing more than cigarette perfume taste to coordinate to enrich, it is also desirable to which there is unique flavor.

The distinctive flavor of draft can not only combine together with cigarette perfume, additionally it is possible to improve and improve the flavor of cigarette.In addition, The tobacco perfume material of other styles also has to be developed.Heating the cigarette that do not burn is the cigarette kind being popular in recent years, still The style for the cigarette that do not burn is heated also to abundant, to meet the needs of people are to tobacco flavor.

Summary of the invention

The purpose of the present invention is to provide a kind of fragrance module formulas, it is intended to so that fragrance module formula is met heating and not burn The characteristic of cigarette makes the suction mouthfeel diversification for heating the cigarette that do not burn.

Another object of the present invention is to provide a kind of for heating the preparation method of the fragrance for the cigarette that do not burn, method Simple and easy to do, the fragrance being prepared can assign the suction mouthfeel that cigarette individual style is not burnt in heating.

The third object of the present invention is the cigarette tool for providing a kind of preparation method for heating the cigarette that do not burn, being prepared There is the suction mouthfeel of mannerism.

The present invention solves its technical problem and adopts the following technical solutions to realize.

The invention proposes a kind of fragrance module formulas, according to parts by weight, including produce fragrant 10-90 parts of main body, solvent 10- 90 parts, 2-50 parts of tobacco extract, 0.5-70 parts of fumet and 0.1-50 parts of corrigent；

Preferably, it produces fragrant main body and is selected from least one of draft main note, fruity beverage main note and fragrance of a flower main note.

The present invention also proposes a kind of for heating the preparation method of the fragrance for the cigarette that do not burn, comprising the following steps:

Each component in above-mentioned fragrance module formula is uniformly mixed.

The present invention also proposes a kind of preparation method for heating the cigarette that do not burn, including the fragrance that the above method is prepared It is loaded onto and heats in the cigarette that do not burn.

The beneficial effect that the embodiment of the present invention provides a kind of fragrance module formula is: its by produce fragrant main body as major ingredient, It can be assigned with good fiting effects of formation such as tobacco extract, fumet, corrigents with covering miscellaneous gas, coordinating tobacco perfume The unique fragrant feature of product and regular governed essence module formula.

The embodiment of the invention also provides a kind of for heating the preparation method of the fragrance for the cigarette that do not burn, with above-mentioned perfume (or spice) Material module formula is raw material, obtains fragrance by being simply mixed with, and method is simple is suitable for industrial applications.

The embodiment of the invention also provides a kind of preparation methods for heating the cigarette that do not burn, including the above method is prepared into To fragrance be loaded onto heating and do not burn in cigarette, the heating the being prepared cigarette that do not burn has unique fragrant feature, and is free of Offending miscellaneous gas, suction mouthfeel are very ideal.

Specific embodiment

It in order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below will be in the embodiment of the present invention Technical solution be clearly and completely described.The person that is not specified actual conditions in embodiment, according to normal conditions or manufacturer builds The condition of view carries out.Reagents or instruments used without specified manufacturer is the conventional production that can be obtained by commercially available purchase Product.

Below the fragrance to fragrance module formula provided in an embodiment of the present invention and for heating the cigarette that do not burn and add The preparation method of the hot cigarette that do not burn is specifically described.

A kind of fragrance module formula provided in an embodiment of the present invention, according to parts by weight, including fragrant 10-90 parts of the main body of production, 10-90 parts of solvent, 2-50 parts of tobacco extract, 0.5-70 parts of fumet and 0.1-50 parts of corrigent；Preferably, the production is fragrant main Body is selected from least one of draft main note, fruity beverage main note and fragrance of a flower main note, using draft main note, fruity beverage main note and The fragrance module of different-style is prepared in fragrance of a flower main note respectively.

Inventor is respectively optimized the selection of draft main note, fruity beverage main note and fragrance of a flower main note, so that finally The production perfume (or spice) effect for obtaining fragrant module is more preferable.Draft main note is selected from Radix Glycyrrhizae, mustard, wrinkled giant hyssop, fritillary-loquat, green grass cream, old ginger, the five tastes Any one or more in son, Radix Angelicae Sinensis and dandelion.Fruity beverage main note is selected from pineapple, lichee, blueberry, muskmelon, sweet orange, grass Any one or more in the certain kind of berries, bergamot pear, coffee, cocoa, cola, green tea, Dragon Well tea, gin tonic, whiskey and rock sugar pear. Fragrance of a flower main note is selected from Michelia oil, Michelia alba leaf oil, neroli oil, patchouli oil, costus root oil, citronellol, geraniol, fragrant camphor tree In alcohol, vanillic aldehyde, eugenol, strawberry aldehyde, osmanthus concrete, perilla herb oil, oil of aglaia odorate, Flos micheliae Albae oil, attar of rose and jasmine lactone It is one or more.

It should be noted that draft main note is the major ingredient in formula, play the role of introducing herbal fragrance, it is above several Herbaceous material, which compares, to be suitable for heating the cigarette that do not burn.Fruity beverage main note be can be formula in major ingredient, play Introduce the effect of fruity or beverage flavor；Fragrance of a flower main note can also be used as the major ingredient in formula, play the work for introducing fragrance of a flower fragrance With.

It should be noted that it is by produce fragrant main body as major ingredient, formed with tobacco extract, fumet, corrigent etc. Good fiting effect can assign product unique fragrant feature to cover miscellaneous gas, coordinate tobacco perfume.The improvement of formula is removed To consider to coordinate that tobacco is fragrant, covers outside miscellaneous gas, it is also necessary to consider that heating is not burnt the suction temperatures of cigarette, temperature is less than one As electronic cigarette, the fragrance formulations for electronic cigarette are unsuitable for heating and do not burn cigarette.

Inventor further improves the dosage of each component in formula, it is preferable that fragrance module formula includes producing fragrant main body 40-80 parts, 30-70 parts of solvent, 5-35 parts of tobacco extract, 1-50 parts of fumet and 0.5-30 parts of corrigent.It is highly preferred that fragrant Expect that module formula includes producing fragrant 50-70 parts of main body, 40-60 parts of solvent, 8-25 parts of tobacco extract, 4-35 parts of fumet and flavoring 1-20 parts of agent.Formula after optimization by the dosage of regulation each component, make it is miscellaneous contained by major ingredient be so incensed that cover, while making fragrance more Add pleasure, to obtain preferably suction mouthfeel.

You need to add is that the used in amounts of each component in the fragrance module formula provided in the embodiment of the present invention will control In a certain range, if will lead to the decline of suction mouthfeel beyond above range, or even also there is the obvious phenomenon of miscellaneous gas.

Specifically, tobacco extract can be tobacco extract or tobacco flower concrete.Tobacco extract for this formula can To be obtained by extraction, the way of distillation, extraction.Assisted extraction method includes microwave, ultrasound, high temperature etc..Extraction solvent include water, Hydrophilic organic solvent (ethyl alcohol, propylene glycol, methanol, acetone) and lipophilic organic solvent (petroleum ether, chloroform, ether, acetic acid Ethyl ester, dichloroethanes, two polypropylene glycols), Extracting temperature is within 450 DEG C.Common tobacco extract is applicable in the present invention and matches Side, such as flue-cured tobacco, airing tobacco, burley tobaccos, cigar.

Specifically, fumet is essential oil, tincture or medicinal extract, the form of fumet can be it is a variety of, specifically can be according to institute The difference of raw material is selected to select suitable dosage form.

Preferably, fumet is selected from juniper berry oil, orrisroot oil, onion oil, wintergreen, absinthium, mustard oil, peppery peppermint Oil, thyme oil, oil of bay, cassia oil, aniseed oil, citronellol, geraniol, nerol, dorinone, orange oil, lemon oil, grass Certain kind of berries extract, coffee tincture, almond oil, jasmine oil, bigarabe leaf extract, attar of rose, orange oil, caryophyllus oil, haw thorn extract, Pineapple extract, mace oil, cassia oil, peppermint oil, ginger oil, isoamyl acetate, phenylethyl isovalerate, ethyl isovalerate, second Any one or more in acetoacetic ester, benzaldehyde, vanillic aldehyde, eugenol, strawberry aldehyde, osmanthus concrete and oil of aglaia odorate.More than Several raw materials can play the effect for covering miscellaneous gas well, can choose one such or several raw materials.

It is highly preferred that fumet is selected from juniper berry oil, orrisroot oil, onion oil, wintergreen, absinthium, mustard oil, β-greatly At least one of horse ketone and oil of Peppermint.Inventors have found that can not only effectively cover book on Chinese herbal medicine using above several fumet In miscellaneous gas, can also obtain preferably suction mouthfeel.

Further, corrigent is selected from menthyl succinate and its derivative, vanillon, honey, Radix Glycyrrhizae extract, oxybenzene Base butanone, 2-3 dimethyl pyrazine, ethyl butyrate, ethylmaltol, ethyl propionate, vanillic aldehyde, furanone, isobutylaldehyde, isoamyl Acid, maltol, benzaldehyde, dimethyl suflfate, 2-Methyl Butyric Acid, isopentyl aldehyde, benzyl carbinol, phenylacetic acid, heliotropin, valeric acid, penta Aldehyde, butanol, butyric acid, benzyl alcohol, ethyl acetate, fenugreek extract, isobutanol, isobutyric acid, methyl cyclopentenyl ketone, second are even In relation by marriage, sucrose, sorbierite, ethyl lactate, citric acid, chicory extract, α-ionone, lactic acid, pyruvic acid and tea perfume spirane Any one or more.Above several raw materials can play the effect for covering miscellaneous gas well, can choose one such Or several raw materials.

Preferably, corrigent in menthyl succinate and its derivative, vanillon, honey, Radix Glycyrrhizae extract extremely Few one kind.Inventors have found that above several corrigents are for making the suction mouthfeel ten of finally obtained fragrance in inventive formulation Sub-argument is thought, is tasteful perfume material.

Specifically, solvent is any one in water, ethyl alcohol, propylene glycol, glycerol, isopropyl myristate and Ergol Kind is a variety of.Above several common solvents are adapted to dissolve other raw materials, and will not bring offending smell.

In some embodiments, fragrance module formula further includes 0.1-50 parts of stabilizer；Preferably 1-35 parts；More preferably 5-20 parts.The addition of stabilizer facilitates the holding fragrance for keeping raw material more longlasting, and the perfume material being prepared is enable to protect always Hold good smell.

Stabilizer be selected from 'alpha '-hydroxy acids, glycerol, glyceryl triacetate, triethyl citrate, polyethylene glycol, polyoxyethylene, Maltitol, xylitol, sorbierite, propylene glycol, hexylene glycol, butanediol, triethylene glycol, polydextrose, tartaric acid, citric acid, benzene Any one or a few in formic acid and malic acid；Preferably, stabilizer is selected from 'alpha '-hydroxy acids, glycerol, glyceryl triacetate, lemon Any one or a few in lemon triethylenetetraminehexaacetic acid ester, benzoic acid and polyethylene glycol.Inventors have found that being added using above several stabilizers The fragrance for entering the fragrance that can make to be prepared in formula composition keeps more longlasting, and perfume material can be always maintained at after being used for cigarette Preferable suction mouthfeel.In other embodiments, stabilizer further includes some water-soluble high scores with non-newtonian flow volume property Sub- substance (such as guar gum) and substance (such as alginate, cyclodextrin, the D-sorbite liver that can reduce grease surface tension Fatty acid ester).

The embodiment of the invention also provides a kind of for heating the preparation method of the fragrance for the cigarette that do not burn, including following step It is rapid: each component in above-mentioned fragrance module formula is uniformly mixed.In general, each component in fragrance formulations is that liquid is straight It connects and is uniformly mixed；When each component in fragrance formulations has solid-state and liquid, it can dissolve to form liquefied mixture after mixing, Suspension, colloid can also be formed with endless fully dissolved, or be prepared into particle or powder.

The embodiment of the invention also provides a kind of preparation methods for heating the cigarette that do not burn, including the fragrance that will be prepared It is loaded onto and heats in the cigarette that do not burn.You need to add is that the fragrance that is prepared of the embodiment of the present invention can by spray coating method, The methods of fragrant collimation method (fragrant line is not limited to cotton thread, including any filiform that can adhere to fragrance), injection method, infusion method are carried on On tobacco or wrapping paper.Flavoring equipment includes flavoring pump, lavender jar, spice filling etc., wherein straight with essence during flavoring The vessel temp of contact is no more than 150 DEG C.

In some embodiments, heating the cigarette that do not burn includes smoke section, distance piece, temperature descending section and vinegar fibre section；Wherein, In The additional amount of the smoke section fragrance accounts for the 0-10% of the smoke section quality, accounts in the additional amount of the distance piece fragrance described The 0-15% of distance piece quality accounts for the 0-15% of the temperature descending section quality in the additional amount of the temperature descending section fragrance, in the vinegar The additional amount of fine section fragrance accounts for the 0-8% of the vinegar fibre section quality；Preferably, it is accounted in the additional amount of the smoke section fragrance described The 0.5-5% of smoke section quality accounts for the 0.5-10% of the distance piece quality in the additional amount of the distance piece fragrance, described The additional amount of temperature descending section fragrance accounts for the 0.05-4% of the temperature descending section quality, accounts for the vinegar in the additional amount of the vinegar fibre section fragrance The 0.01-3% of fine section quality.The existing cigarette that do not burn that heats generally comprises above-mentioned several parts, makes in the embodiment of the present invention Standby obtained fragrance for heating when not burning cigarette it is noted that each section of loading capacity, loading capacity is too small cannot reach prepare it is special The effect of the cigarette of style, loading capacity is excessive to will appear the suction phenomenon that mouthfeel is bad, smell is excessively strong, or even will appear perfume (or spice) The case where essence exudation.

It should be noted that can dissolve to form liquid after mixing when each component in fragrance formulations has solid-state and liquid Mixture can also form suspension, colloid with endless fully dissolved, or be prepared into particle or powder.If the form of suspension, At 25 DEG C, viscosity should be less than 2000mPas.Preferably, the essence additive heats the cigarette temperature descending section that do not burn described Addition manner be selected from least one of spray coating method, infusion process, cladding process, injection method, gel method and absorption method.

Feature and performance of the invention are described in further detail with reference to embodiments.