阅读说明：本技术 一种无激素和抗生素的缓解鼻炎的组合物和制备方法 (The composition and preparation method of the alleviation rhinitis of a kind of no hormone and antibiotic ) 是由 黄志新 陈超 于 2019-09-11 设计创作，主要内容包括：本发明涉及一种无激素和抗生素的缓解鼻炎的组合物,所述组合物的主要原料为以木麻黄的树干或枝杈为原料制取的木酢液。本发明所提供的缓解鼻炎的组合物,其主要成分是木麻黄木酢液,利用木酢液所具有的强力杀菌、消炎、杀病毒、渗透和收敛等作用,可起到促进呼吸道表皮粘膜细胞收敛,消肿通窍的作用,可有效缓解鼻塞、多涕、嗅觉下降、头痛头昏等表面症状,对鼻炎有很好的辅助康复效果。优选地,所述组合物为乳膏,该乳膏包含木麻黄二次蒸馏木酢液、蜂蜡、石蜡油、薄荷脑、甘油、氮酮、BHT、305乳化剂、Oliven1000等成分,乳膏产品整体呈现柔和光滑、轻质、不油腻易吸收、无刺激性的特点,且对缓解患者鼻炎症状的效果也十分迅速和明显。(The present invention relates to a kind of composition of the alleviation rhinitis of no hormone and antibiotic, the primary raw material of the composition is using the trunk of horse-tail or branch as the pyroligneous liquor of waste.The composition provided by the present invention for alleviating rhinitis, its main component is horse-tail pyroligneous liquor, using strong disinfecting, anti-inflammatory possessed by pyroligneous liquor, kills the virus, permeates and Thyme Extract, it can play and promote the convergence of respiratory tract epidermis mucomembranous cell, reduce swelling sensible effect, the surface symptoms such as nasal obstruction, more tears, smell decline, headache and dizziness can be effectively relieved, have good recovering aid effect to rhinitis.Preferably, the composition is emulsifiable paste, the emulsifiable paste includes the ingredients such as horse-tail second distillation pyroligneous liquor, beeswax, paraffin oil, menthol, glycerol, azone, BHT, 305 emulsifiers, Oliven1000, soft smooth, lightweight is integrally presented in cream products, non-greasy easily absorbs, nonirritant feature, and also very rapidly and obvious to the effect of reduction of patient Rhinitis Symptoms.)

1. a kind of composition of the alleviation rhinitis of no hormone and antibiotic, which is characterized in that the primary raw material of the composition is Using the trunk of horse-tail or branch as the pyroligneous liquor of waste.

2. composition according to claim 1, which is characterized in that the pyroligneous liquor is horse-tail second distillation pyroligneous liquor, It is prepared as follows:

By the trunk of horse-tail or branch through 350-400 DEG C of anaerobic high temperature pyrolysis, generated gas-liquid is cooling, stand after The claret liquid substance arrived, this is casuarina equisetifolia wood jealous woman stoste, by this casuarina equisetifolia wood jealous woman stoste again through second distillation, mistake after distillation Filter, obtains second distillation pyroligneous liquor；Vapo(u)rizing temperature is 98-102 DEG C, and second distillation pyroligneous liquor is relative to casuarina equisetifolia wood jealous woman stoste Yield is no more than 80%.

3. composition according to claim 2, which is characterized in that the composition is emulsifiable paste, and it is secondary that it includes horse-tails Distill pyroligneous liquor 25-50wt%, wax 1.5-2.5wt%, grease 1.5-2.5% wt%, solvent 1.5-2.5wt%, freshener 0.5- 1.5wt%, moisturizer 3-7wt%, bleeding agent 1.5-2.5 wt%, antioxidant 0.5-1.5wt% and emulsifier 2-4wt%, surplus are Pure water.

4. composition according to claim 2, which is characterized in that the composition is emulsifiable paste, and it includes following components:

Horse-tail second distillation pyroligneous liquor 25-50wt%；

Beeswax 1.5-2.5wt%；

Paraffin oil 1.5-2.5% wt%；

DMSO 1.5-2.5 wt%；

Menthol 0.5-1.5 wt%；

Glycerol 3-7 wt%；

Azone 1.5-2.5 wt%；

BHT 0.5-1.5 wt%；

305 emulsifier 0.5-1.5wt%；

Oliven1000 1.5-2.5wt%；

Surplus is distilled water or pure water.

5. composition according to claim 2, which is characterized in that the composition is emulsifiable paste.

6. a kind of preparation method of the alleviation rhinitis emulsifiable paste of no hormone and antibiotic, which comprises the following steps:

S1: preparing the wooden jealous woman stoste: the trunk of horse-tail or branch dissection be put into pyrolysis oven, and at 350-400 DEG C and isolation is empty It is pyrolyzed 14-20 hours under gas, the smoke mixture drawn in pyrolysis oven is condensed, stratification obtains claret liquid substance For casuarina equisetifolia wood jealous woman stoste；

S2: it preparation horse-tail second distillation pyroligneous liquor: by casuarina equisetifolia wood jealous woman stoste again through second distillation, filters, obtains after distillation Second distillation pyroligneous liquor；Vapo(u)rizing temperature be 98-102 DEG C, second distillation pyroligneous liquor relative to casuarina equisetifolia wood jealous woman stoste yield not More than 80%；

S3: according to horse-tail second distillation pyroligneous liquor 25-50%, beeswax 1.5-2.5%, paraffin oil 1.5-2.5%, DMSO 1.5- 2.5%, menthol 0.5-1.5%, glycerol 3-7%, azone 1.5-2.5%, BHT 0.5-1.5%, 305 emulsifier 0.5-1.5% and Oliven1000 1.5-2.5% prepares each raw material,

Above each raw material is handled as follows:

First menthol, BHT are dissolved in DMSO, add glycerol and azone, heating water bath is to 70-80 DEG CLiquid；By beeswax, Paraffin oil and OLIVEN1000 mixing are heated up to 70-80 DEG C of thorough meltLiquid；By pure water plus horse-tail second distillation wood Jealous woman liquid mixes, and being heated to 70-80 DEG C isLiquid；It willLiquid is addedIt, will after liquid mixesLiquid is added, and stirring is cooled to 40-50 DEG C, 305 emulsifiers are added, stirs evenly to room temperature and alleviates the emulsifiable paste of rhinitis.

Technical field

The present invention relates to the composition for alleviating rhinitis, the alleviation rhinitis of especially a kind of no hormone, antibiotic and preservative Composition and preparation method.

Background technique

Rhinitis, that is, nasal cavity inflammatory disease is virus, bacterium, allergen, various physical and chemical factors and certain systemic diseases The inflammation of caused bronchia mucosal.The main pathological change of rhinitis is bronchia mucosal hyperemia, swelling, exudation, hyperplasia, atrophy or bad It waits indefinitely.Virus infection is its primary cause of disease, or secondary bacterial infection on the basis of virus infection.It has been known that there is more than 100 kinds of viruses It can cause this disease, most commonly rhinovirus, followed by influenza and parainfluenza virus, adenovirus, coronavirus, Coxsackie virus And mucus and paramyxovirus etc..Viral transmission mode mainly passes through respiratory tract sucking, followed by passes through contaminated body or food Object enters body.The main inhalant allergen such as pollen, fungi, dermatophagoides pteronyssinus, animal scurf, room dust.Rhinitis Symptoms have very A variety of, the type according to rhinitis is different, and Rhinitis Symptoms are also different, mainly there is rhinitis chronic and acute rhinitis.

In the emulsifiable paste or spray product of current some alleviation rhinitis, it will usually which the fungicide containing pure chemistry ingredient resists The ingredients such as inflammation, antibiotic, some are added to hormone even for allergic rhinitis.In addition, the rhinitis of some pure Chinese herbal medicine types Emulsifiable paste or spray are stored for the ease of room temperature and obtain compared with long shelf life, can also adding preservative agent.For example, in some alleviation noses In scorching product, contains four water, eight Boratex as fungicide, bergapten and be used for anti-inflammatory and antalgic ingredient, but four water, eight boric acid Sodium has certain toxicity, and bergapten has phototoxicity, stimulation and the pigment of mucous membrane or skin can be caused by solar radiation It is calm.Other purely play cleaning nasal cavity, such as seawater nasal cavity cleaning agent, although almost without side-effects, to depth by For the patient of rhinitis puzzlement, the effect for alleviating Rhinitis Symptoms is very limited, tends not to comparatively fast alleviate pain.

Product as rhinitis, it will usually there is part to enter respiratory tract, therefore the nose that hypotoxicity low side effect is healthier Scorching product will increasingly be favored by people, and particularly with some constitutions slightly weak person, such as infant, the safety of rhinitis product is to disappear Expense person first has to consideration.And existing product or effect are unobvious or how much containing some malicious accessory ingredients, it is more more Add ideal rhinitis product for consumer's unrestricted choice.

Summary of the invention

(1) technical problems to be solved

In order to solve the above problem of the prior art, the present invention be desirable to provide a kind of safety is higher, healthier, toxic side effect more Composition product low and that Rhinitis Symptoms can be effectively relieved.

The object of the present invention is to provide the compositions and preparation method of the alleviation rhinitis of a kind of no hormone and antibiotic.

(2) technical solution

In order to achieve the above object, the main technical schemes that the present invention uses include:

On the one hand, the present invention provides a kind of composition of the alleviation rhinitis of no hormone and antibiotic, and primary raw material is with the wooden fiber crops Yellow trunk or branch is the pyroligneous liquor of waste.

Preferred embodiment according to the present invention, the pyroligneous liquor are horse-tail second distillation pyroligneous liquor, as follows Preparation:

By the trunk of horse-tail or branch through 350-400 DEG C of anaerobic high temperature pyrolysis, generated gas-liquid is cooling, stand after The claret liquid substance arrived, this is casuarina equisetifolia wood jealous woman stoste, by this casuarina equisetifolia wood jealous woman stoste again through second distillation, mistake after distillation Filter, obtains second distillation pyroligneous liquor；Vapo(u)rizing temperature is 98-102 DEG C, and second distillation pyroligneous liquor is relative to casuarina equisetifolia wood jealous woman stoste Yield is no more than 80%.

Wherein, 3.5-4.5% containing phenols, organic acid 1.5-2.5% in horse-tail second distillation pyroligneous liquor.

Preferred embodiment according to the present invention, the composition are emulsifiable paste, and it includes horse-tail second distillation pyroligneous liquor 25- 50wt%, wax 1.5-2.5wt%, grease 1.5-2.5% wt%, solvent 1.5-2.5 wt%, freshener 0.5-1.5 wt%, moisturizing Agent 3-7 wt%, bleeding agent 1.5-2.5 wt%, antioxidant 0.5-1.5 wt% and emulsifier 2-4wt%, surplus are pure water.

Preferred embodiment according to the present invention, the composition are emulsifiable paste, and it includes following components:

Horse-tail second distillation pyroligneous liquor 25-50wt%；

Beeswax 1.5-2.5wt%；

Paraffin oil 1.5-2.5% wt%；

DMSO 1.5-2.5 wt%；

Menthol 0.5-1.5 wt%；

Glycerol 3-7 wt%；

Azone 1.5-2.5 wt%；

BHT 0.5-1.5 wt%；

305 emulsifier 0.5-1.5wt%；

Oliven1000 1.5-2.5wt%；

Surplus is distilled water or pure water.

For emulsifiable paste compared to spray or nasal cavity cleaning liquid, the time rested on bronchia mucosal is relatively permanent therefore right In the patient perplexed by rhinitis, it is applied to nasal membrane position, effect is obvious and relaxation effect works quickly, can effectively delay Solve rhinitis caused by nasal obstruction, more tears, smell decline, headache and dizziness symptom, to acute and chronic rhinitis caused by a variety of causes, atrophy Property rhinitis, nasosinusitis, nose tinea etc., there is good recovering aid effect.Inhibition bacterium ingredient contained by it can inhibit harmful bacteria and exist The effect of respiratory tract infection further prevents the respiratory tract infection (cold cough, tonsils inflammation, pneumonia) caused by rhinitis Etc. complication.

On the other hand, the present invention provides a kind of preparation method of the alleviation rhinitis emulsifiable paste of no hormone and antibiotic comprising Step:

S1: preparing the wooden jealous woman stoste: the trunk of horse-tail or branch dissection be put into pyrolysis oven, and at 350-400 DEG C and isolation is empty It is pyrolyzed 14-20 hours under gas, the smoke mixture drawn in pyrolysis oven is condensed, stratification obtains claret liquid substance For casuarina equisetifolia wood jealous woman stoste；

S2: it preparation horse-tail second distillation pyroligneous liquor: by casuarina equisetifolia wood jealous woman stoste again through second distillation, filters, obtains after distillation Second distillation pyroligneous liquor (1.5-2.5% containing organic acid, phenols 3.5-4.5%)；Vapo(u)rizing temperature is 98-102 DEG C, second distillation wood jealous woman Liquid phase is no more than 80% for the yield of casuarina equisetifolia wood jealous woman stoste；

S3: according to horse-tail second distillation pyroligneous liquor 25-50%, beeswax 1.5-2.5%, paraffin oil 1.5-2.5%, DMSO 1.5- 2.5%, menthol 0.5-1.5%, glycerol 3-7%, azone 1.5-2.5%, BHT 0.5-1.5%, 305 emulsifier 0.5-1.5% and Oliven1000 1.5-2.5% prepares each raw material, and above each raw material is handled as follows:

First menthol, BHT are dissolved in DMSO, add glycerol and azone, heating water bath is to 70-80 DEG CLiquid；By beeswax, Paraffin oil and OLIVEN1000 mixing are heated up to 70-80 DEG C of thawing and areLiquid；It will be wooden with second distillation in pure water plus horse-tail Jealous woman liquid mixes, and being heated to 70-80 DEG C isLiquid；It willLiquid is addedIt, will after liquid mixesLiquid is added, and stirring is cooled to 40-50 DEG C, 305 emulsifiers are added, stir evenly to room temperature, are adjusted to predetermined weight with pure water to get the emulsifiable paste of rhinitis is alleviated.

The definition of pyroligneous liquor:

The condensate recovery liquid of pyroligneous liquor thermal decomposition of wood ingredient during firing charcoal has special smoke aroma, is in acidity, PH value 3 or so, to be faint yellow to bronzing, pyroligneous liquor main component is the substances such as organic acid, phenols, ketone, furans.But no The pyroligneous liquor ingredient and effect obtained with timber is very different.Pyroligneous liquor is a kind of multi-element biologic for not adding any other composition Preparation, it is taken at naturally, for human body.

(3) beneficial effect

The beneficial effects of the present invention are:

The present invention is waste wood jealous woman stoste using the trunk or branch of horse-tail, by the wooden jealous woman stoste again through second distillation, mistake After the rectification process such as filter, for making the main component of the emulsifiable paste or ointment of alleviating rhinitis.

The emulsifiable paste provided by the present invention for alleviating rhinitis, main component is horse-tail pyroligneous liquor, is had using pyroligneous liquor Some strong disinfectings anti-inflammatory, kill the virus, permeate and Thyme Extract, can play and promote the convergence of respiratory tract epidermis mucomembranous cell, disappear It swells sensible effect, the surface symptoms such as nasal obstruction, more tears, smell decline, headache and dizziness can be effectively relieved；Meanwhile to a variety of causes Caused acute and chronic rhinitis, atrophic rhinitis, nasosinusitis, nose tinea etc. have good recovering aid effect, and bactericidal effect can Inhibit mushroom in respiratory tract infection, to by virus, bacterium or fungi etc. cause rhinitis chronic and acute rhinitis have convergence well, Anti-inflammatory and sensible alleviation and other effects.In addition, the emulsifiable paste provided by the present invention for alleviating rhinitis is free of antibiotic, hormone and anti-corrosion Agent, the toxic side effect that safety is higher, extremely low, the infant etc. weaker suitable for constitution.

Preferably, in the emulsifiable paste of alleviation rhinitis of the invention, can also include beeswax, menthol, in addition to be used as adhesive agent, It adjusts viscosity and improves except smell, itself also have the effects that inducing astrigency, anti-inflammatory, antipruritic, analgesic, mitigation edema, and menthol There are also sensible restoring consciouness, alleviate because of symptom dizzy caused by rhinitis snuffles.DMSO in formula also has anti-inflammatory analgetic effect.Azone, DMSO, OLIVEM 1000 can play the role of promoting functional component osmotic absorption jointly, improve emulsifiable paste components utilising rate and rise Imitate speed；Each ingredient is the non-stimulated ingredient of hypotoxicity in cream formulation, and especially OLIVEM 1000 is a kind of high-quality emulsification Agent, safe and non-stimulating property.Soft smooth, lightweight is integrally presented in cream products, non-greasy easily absorbs, nonirritant feature, and It is also very rapidly and obvious to the curative effect of reduction of patient Rhinitis Symptoms.

Specific embodiment

In order to preferably explain the present invention, in order to understand, below by specific embodiment, present invention work is retouched in detail It states.

The present invention relates to the emulsifiable pastes and preparation method thereof that a kind of no hormone, antibiotic, preservative can be relieved rhinitis.The emulsifiable paste Primary raw material be pyroligneous liquor.Pyroligneous liquor is to issue heat in 350-400 DEG C of anaerobic high temperature using branches such as horse-tails as raw material Cracking, the claret liquid substance that generated gas-liquid obtains after cooling, standing.This is the wooden jealous woman stoste, then through second distillation, The purification link such as filtering obtains second distillation pyroligneous liquor.

The wooden jealous woman sap is a kind of in quality raw materials forestry waste processing and generated during resource utilization, is a kind of Not plus the multi-element biologic preparation of any other composition, it is taken at naturally, for nature.Horse-tail is the common tree in China torrid areas Kind horse-tail tree.Horse-tail, Chinese medicine name.For Casuarinaceae plant horse-tail (Casuarina equisetifoliaForst.) Young browse or bark.It is distributed in Guangxi, Guangdong, Fujian, Taiwan coastal area.It is bitter, pungent, it is warm-natured.It is return lung, large intestine, small Intestines warp.With ventilating the lung and relieving cough, the effect of promoting qi circulation and relieving pain, warming middle energizer to stop diarrhea, dampness removing.Cold, fever, cough are treated, hernia, abdominal pain is let out It rushes down, dysentery, difficult urination, the illnesss such as tinea pedis pyogenic infections.

Using horse-tail second distillation purification pyroligneous liquor as primary raw material, with other waxes, grease, freshener, moisturizer, The compoundings such as bleeding agent, antioxidant, emulsifier can be made into emulsifiable paste, be applied on bronchia mucosal, can play and promote respiratory tract epidermis The surface symptoms such as nasal obstruction, more tears, smell decline, headache and dizziness can be effectively relieved in mucomembranous cell convergence, sensible effect of reducing swelling； Meanwhile to acute and chronic rhinitis caused by a variety of causes, atrophic rhinitis, nasosinusitis, nose tinea etc., there is good recovering aid to imitate Fruit, bactericidal effect are able to suppress mushroom in respiratory tract infection, prevent respiratory disease.

According to the present invention, in a preferred embodiment, the emulsifiable paste for alleviating rhinitis includes following component: horse-tail is secondary Distill pyroligneous liquor 25-50wt%；Beeswax 1.5-2.5wt%；Paraffin oil 1.5-2.5% wt%；DMSO 1.5-2.5 wt%；Menthol 0.5-1.5 wt%；Glycerol 3-7 wt%；Azone 1.5-2.5 wt%；BHT 0.5-1.5 wt%；305 emulsifier 0.5-1.5wt%； Oliven1000 1.5-2.5wt%；

Surplus is distilled water or pure water.

The each component of above-mentioned emulsifiable paste component has all carried out comprehensive selection and has determined after investigating, in the hope of preparation in selection Alleviation rhinitis emulsifiable paste, effect can reach ideal optimal, comprising: alleviate the onset time of rhinitis curative effect, smear posterula Comfort, smell, the irritation to mucous membrane, safety, appearance of its cream products of mucous membrane etc..

In the emulsifiable paste component, the characteristics of each component, is as follows:

Beeswax has the characteristics that good tackness, transmissibility, emulsibility, slickness, emulsifies with easy after alkali effect, after emulsification It can dissolve each other with oil and in conjunction with other ingredients, itself also there is inducing astrigency, sore, myogenic, the effect of analgesic.It is main in emulsifiable paste It plays and increases adhesion, play stability, adjust stickiness, reduce the effects of greasy feeling.Paraffin oil has moisturizing, cleaning, work The effect of cost, quick-drying is reduced for filler.

DMSO is that one kind had not only been dissolved in water but also had been dissolved in the particularly important aprotic polar solvent of organic solvent, itself has and disappears The effects of inflammation relieves pain, diuresis, calm, can be used as the raw material and carrier of drug main component, itself also has transdermal enhancer With the effect of antifreezing agent.

It is also a kind of disinfectant that menthol, which is a kind of freshener,.When topical application, has and promote blood circulation and anti-inflammatory, antipruritic etc. Effect, can be used for anti-inflammatory, antipruritic, analgesic, mitigate edema etc., restoring consciouness can be also promoted, caused by alleviating or mitigating because of rhinitis snuffles Headache and dizziness symptom.

Glycerol is a kind of moisturizer, and the ingredient that pyroligneous liquor, menthol etc. can be made mainly to work is glutinous in skin or nasal cavity Film surface stops time enough and is able to transdermal penetration absorption.In addition, glycerol property is very soft, bronchia mucosal can be improved to slow The adaptability of rhinitis emulsifiable paste is solved, nasal cavity comfort and patient compliance are improved.For experiencing all sorts of the patient of rhinitis puzzlement, glycerol is helped In the reparation of bronchia mucosal damage.

BHT is a kind of antioxidant, can prevent from causing rotten substance because of oxidation, preferably uses food-grade in this application BHT, safety are higher.Azone is a kind of bleeding agent, is ok jointly with chemosmotic DMSO, OLIVEM 1000 Play the role of promoting the diffusion of effective component transdermal penetration.

305 emulsifiers and Oliven1000(olive oil spermaceti alcohol ester) be emulsifier, emulsifier can increase emulsifiable paste at The stability and homogeneity divided avoid placing layering.Wherein, 305 emulsifiers by polyacrylamide (and) aliphatic alcohol polyethenoxy Ether composition is a kind of thickening of emulsifiable paste shape, emulsification and stabilizer, has the advantages that swelling is fireballing, can be made into gel in moment, The creams as made from it, sense of touch is splendid, and soft and very smooth, viscosity still maintains stable after the shearing of long period；And it is long Phase is exposed under ultraviolet light, and viscosity still remains stable.

OLIVEM 1000 is a new generation's emulsifier as derived from olive oil, is free of EO, mild emulsifier can be in emulsifiable paste Inside forms liquid crystal structure, easily painting exhibition, obtains salubrious, and silky feel while has a moisture-keeping functions, all advantages it is equal because Olive oil is derived from for it.In all natural oils, olive oil is and the highest grease of skin compatibility, and OLIVEM 1000 have followed all advantages of olive oil, so that final products is had unique skin sense with splendid percutaneous permeability.It can The loss for wearing the severe edema due to hypofunction of the spleen point is significantly reduced, to assign emulsifiable paste long-acting and short-acting moisture-keeping functions.The cream modulated with OLIVEM 1000 The great gloss of cream is fine and smooth and have unique, soft, salubrious sense of touch comprising a large amount of greases.Its advantage mainly has (1) steady Fixed emulsion will not influence the stability of product comprising a large amount of natural oils；(2) height moisturizing: oleophilic moiety is derived from Olive oil, high skin absorption, height moisturizing, the reticular structure of studies have shown that liquid crystal is to the short-term of skin and long-term Moisture retention is improved, because the moisture total amount for including in this configuration is close to 70%, and all moisture are applied in cream Exhibition, reticular structure can be released immediately after breaking, be absorbed by the skin, and here it is the emulsifiable pastes deployed with OLIVEM 1000 on the skin The reason of generation is salubrious, refrigerant skin sense.(3) safe and non-stimulating: to carry out human body patch with 10% 1000 aqueous dispersions of Olivem Experiment, chorioallantoic membrane experiment, Olivem 1000 is completely nonirritant as the result is shown.

The present invention also provides the preparation methods of a kind of no hormone and the alleviation rhinitis emulsifiable paste of antibiotic comprising step:

S1: preparing the wooden jealous woman stoste: the trunk of horse-tail or branch dissection be put into pyrolysis oven, and at 350-400 DEG C and isolation is empty It is pyrolyzed 14-20 hours under gas, the smoke mixture drawn in pyrolysis oven is condensed, stratification obtains claret liquid substance For casuarina equisetifolia wood jealous woman stoste；

S2: it preparation horse-tail second distillation pyroligneous liquor: by casuarina equisetifolia wood jealous woman stoste again through second distillation, filters, obtains after distillation Second distillation pyroligneous liquor (1.5-2.5% containing organic acid, phenols 3.5-4.5%)；Vapo(u)rizing temperature is 98-102 DEG C, second distillation wood jealous woman Liquid phase is no more than 80% for the yield of casuarina equisetifolia wood jealous woman stoste；

S3: according to horse-tail second distillation pyroligneous liquor 25-50%, beeswax 1.5-2.5%, paraffin oil 1.5-2.5%, DMSO 1.5- 2.5%, menthol 0.5-1.5%, glycerol 3-7%, azone 1.5-2.5%, BHT 0.5-1.5%, 305 emulsifier 0.5-1.5% and Oliven1000 1.5-2.5% prepares each raw material, and above each raw material is handled as follows:

First menthol, BHT are dissolved in DMSO, add glycerol and azone, heating water bath is to 70-80 DEG CLiquid；By beeswax, Paraffin oil and OLIVEN1000 mixing are heated up to 70-80 DEG C of thorough meltLiquid；By pure water plus horse-tail second distillation wood Jealous woman liquid mixes, and being heated to 70-80 DEG C isLiquid；It willLiquid is addedIt, will after liquid mixesLiquid is added, and stirring is cooled to 40-50 DEG C, 305 emulsifiers are added, stir evenly to room temperature, being adjusted to predetermined weight with pure water, (each ingredient is aforementioned in emulsifiable paste made from making Within the scope of listed relative content), the emulsifiable paste for alleviating rhinitis is made, hose is bottled or poured into emulsifiable paste.

Wherein in step S1, under normal circumstances, after smoke mixture condensation, stratification 6 months or more is needed, is layered To three layers, the claret liquid substance of middle layer is required casuarina equisetifolia wood jealous woman stoste.

Being layered at the top of liquid is foam and dross, and bottom is fine slag.When collection, the foam and dross at top can be first removed, so After pump out middle layer, part of the bottom containing fine slag then remains the smoke mixture for containing condensation again next time.Wine Red liquid obtains supernatant liquid after tentatively filtering, then is distilled twice, second distillation pyroligneous liquor is obtained by filtration (containing organic Sour 1.5-2.5%, phenols 3.5-4.5%).Horse-tail second distillation pyroligneous liquor is used to make the product for alleviating rhinitis.

The following are the specific embodiments of the preparation method of the emulsifiable paste of the alleviation rhinitis of a kind of antibiotic-free of the present invention and hormone.