阅读说明：本技术 高渗透锁水组合物及舒缓保湿面膜液及其制备方法 (High-permeability water-locking composition, soothing and moisturizing mask liquid and preparation method thereof ) 是由 陈炜诗 陈嘉钰 周锐 马飞 慕德明 于 2021-09-09 设计创作，主要内容包括：本申请涉及面膜领域,具体公开了高渗透锁水组合物及舒缓保湿面膜液及其制备方法。高渗透锁水组合物包括组合物A、组合物B、组合物C、舒缓剂、修复剂、保湿剂。面膜液包括高渗透锁水组合物、甘油、丙二醇、海藻糖、透明质酸钠、增稠剂、EDTA二钠、精氨酸、对羟基苯乙酮、1,2-己二醇和水。面膜液制备方法：先制备高渗透锁水组合物；将甘油、一部分丙二醇、海藻糖、透明质酸钠、增稠剂、螯合剂和水混合加热,搅拌均匀得到基础液；降温加入精氨酸搅拌均匀；将剩余丙二醇、对羟基苯乙酮、1,2-己二醇混合加热、搅拌,再加入基础液中搅拌；降温加入高渗透锁水组合物,搅拌均匀,得到面膜液。本申请具有提升面膜液促进面部肌肤吸收的效果。(The application relates to the field of facial masks, and particularly discloses a high-permeability water-locking composition, a soothing and moisturizing facial mask liquid and a preparation method thereof. The high-permeability water-locking composition comprises a composition A, a composition B, a composition C, a soothing agent, a repairing agent and a moisturizing agent. The facial mask liquid comprises a high-permeability water-locking composition, glycerin, propylene glycol, trehalose, sodium hyaluronate, a thickening agent, disodium EDTA, arginine, p-hydroxyacetophenone, 1, 2-hexanediol and water. The preparation method of the mask liquid comprises the following steps: firstly, preparing a high-permeability water-locking composition; mixing and heating glycerin, a part of propylene glycol, trehalose, sodium hyaluronate, a thickening agent, a chelating agent and water, and uniformly stirring to obtain a base solution; cooling, adding arginine and stirring uniformly; mixing the rest propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, heating, stirring, adding into the base solution, and stirring; and cooling, adding the high-permeability water-locking composition, and uniformly stirring to obtain the mask liquid. The application has the effect of promoting facial mask liquid to promote facial skin absorption.)

1. The high-permeability water-locking composition is characterized in that: comprises the following raw materials in percentage by weight:

7.69 to 23.81 percent of composition A, 12.82 to 47.62 percent of composition B, 7.69 to 23.81 percent of composition C, 12.82 to 47.62 percent of soothing agent, 5.13 to 19.05 percent of repairing agent and 7.69 to 23.81 percent of humectant;

the composition A consists of 5-7 wt% of a flower/leaf extract of the alpine leontopodium and a solvent;

the composition B consists of 8-12 wt% of polygonatum extract and a solvent;

the composition C consists of 98-99% wt of lactobacillus/rice fermentation product and solvent.

2. The highly permeable water-retaining composition according to claim 1, wherein: the soothing agent consists of a soothing component and a solvent, wherein the soothing component comprises one or more of a silybum marianum fruit extract, a momordica grosvenori extract, a pseudopterogorgia elisabethae extract, a plumeria alba extract, a water lily flower extract and a opuntia ficus-indica fruit extract.

3. The high-permeability water-locking composition according to claim 2, wherein: the soothing agent consists of 1.6 to 1.8 weight percent of silybum marianum fruit extract, 1.6 to 1.8 weight percent of momordica grosvenori extract, 1.6 to 1.8 weight percent of gorgonia pseudoaltaica extract, 1.6 to 1.8 weight percent of plumeria rubra extract, 1.6 to 1.8 weight percent of water lily flower extract, 1.6 to 1.8 weight percent of prickly pear fruit extract and a solvent.

4. The high-permeability water-locking composition according to claim 1, wherein: the repairing agent consists of a repairing component and a solvent, wherein the repairing component comprises one or more of a gentian root extract, a honeysuckle flower extract, a wild chrysanthemum flower extract, a corydalis tuber extract, a field mint extract and a sophora flavescens root extract.

5. The high-permeability water-locking composition according to claim 1, wherein: the humectant consists of a moisturizing component and a solvent, wherein the moisturizing component comprises one or more of xylitol, centella asiatica extract and tremella extract.

6. A soothing moisturizing mask liquid comprising the high permeability water-locking composition of any of claims 1-5, wherein: comprises the following raw materials in percentage by weight:

phase A: 2-4% of glycerin, 4-6% of propylene glycol, 0.5-1.5% of trehalose, 0.03-0.07% of sodium hyaluronate, 0.2-0.25% of thickening agent and 0.02-0.04% of EDTA disodium;

phase B: arginine 0.1-0.15%;

and C phase: 0.9 to 1.0 percent of propylene glycol, 0.45 to 0.5 percent of p-hydroxyacetophenone and 0.45 to 0.5 percent of 1, 2-hexanediol;

phase D: 2.1 to 3.9 percent of high-permeability water-locking composition;

the balance being water.

7. A soothing and moisturizing mask liquid according to claim 6, which is characterized in that: the weight percentage of the arginine is 0.125-0.135%.

8. A soothing and moisturizing mask liquid according to claim 7, which is characterized in that: the thickening agent comprises one or two of carbomer and sclerotium rolfsii gum.

9. A method of preparing a soothing and moisturizing mask solution according to any of claims 6-8, comprising the steps of:

step one, preparing a high-permeability water-locking composition: mixing and stirring the composition A, the composition B, the composition C, the soothing agent, the repairing agent and the humectant uniformly to obtain a high-permeability water-retaining composition for later use;

mixing glycerol and propylene glycol, adding the residual raw materials of the phase A, heating to 80-85 ℃, and stirring until particles are completely dissolved to obtain a base solution;

step three, cooling to 60-65 ℃, adding the phase B raw material into the base solution, and stirring until the phase B raw material is completely dissolved and has no particles;

step four, mixing the phase C raw materials, heating to 50-55 ℃, uniformly stirring, adding into the base solution, and stirring until the phase C raw materials are completely dissolved and have no particles;

and step five, cooling to 40-45 ℃, adding the high-permeability water-locking composition prepared in the step one into the base solution, and uniformly stirring to obtain the soothing and moisturizing mask solution.

Technical Field

The invention relates to the field of masks, in particular to a high-permeability water-locking composition, a soothing and moisturizing mask liquid and a preparation method thereof.

Background

The facial mask is an important category of skin care products and is a common skin care product for people. The existing facial masks on the market are very various in types and different in effects, and the principle of the facial mask is that the facial mask is covered on the face of a user and kept for 15-25 minutes, various substances in facial mask liquid permeate into the horny layer of the epidermis of the face, and the skin of the face is repaired in a targeted manner such as moisturizing, soothing, brightening, anti-oxidation and the like, so that the skin becomes soft, bright and elastic. In the using process of the facial mask, the facial mask liquid usually needs a certain time to permeate into the horny layer of the facial epidermis to be absorbed and utilized, the absorption effect of the facial mask liquid by the skin greatly influences the effect of the facial mask liquid on the facial skin, and the existing facial mask liquid has a great space for promoting absorption.

Disclosure of Invention

In order to improve the absorption effect of the facial mask liquid on promoting facial skin, the application provides the high-permeability water-locking composition, the soothing and moisturizing facial mask liquid and the preparation method thereof.

In a first aspect, the present application provides a high-permeability water-retaining composition, which adopts the following technical scheme:

a high-permeability water-locking composition comprises the following raw materials in percentage by weight:

7.69 to 23.81 percent of composition A, 12.82 to 47.62 percent of composition B, 7.69 to 23.81 percent of composition C, 12.82 to 47.62 percent of soothing agent, 5.13 to 19.05 percent of repairing agent and 7.69 to 23.81 percent of humectant;

the composition A consists of 5-7 wt% of a flower/leaf extract of the alpine leontopodium and a solvent;

the composition B consists of 8-12 wt% of polygonatum extract and a solvent;

the composition C consists of 98-99% wt of lactobacillus/rice fermentation product and solvent.

By adopting the technical scheme, a plurality of high-permeability colloid groups are formed under the combined action of the composition A containing the extract of the flowers/leaves of the leontopodium alpinum, the composition B containing the extract of the polygonatum odoratum and the composition C containing the lactobacillus/rice fermentation product, when the high-permeability water-locking composition is contacted with the facial skin, the high-permeability colloid groups can rapidly permeate into cells in the deep layer of the skin, a path similar to a high-speed channel is formed on the face, and substances such as a moisturizing agent, a soothing agent, a repairing agent and the like in the high-permeability water-locking composition can be wrapped by the colloid groups and enter the cells in the deep layer of the skin, so that the cells in the deep layer of the skin can be rapidly and sufficiently supplemented with water and repaired; the high-permeability colloid groups promote the skin to absorb the high-permeability water-locking composition, and can improve the skin care efficiency.

Preferably, the soothing agent consists of a soothing component and a solvent, wherein the soothing component comprises one or more of a silybum marianum fruit extract, a momordica grosvenori extract, an willow coral extract, a plumeria alba extract, a water lily flower extract and a opuntia ficus-indica fruit extract.

Preferably, the soothing agent consists of 1.6 to 1.8 weight percent of silybum marianum fruit extract, 1.6 to 1.8 weight percent of momordica grosvenori extract, 1.6 to 1.8 weight percent of gorgonia pseudolaris extract, 1.6 to 1.8 weight percent of plumeria rubra extract, 1.6 to 1.8 weight percent of nymphaea alba extract, 1.6 to 1.8 weight percent of opuntia chinensis extract and a solvent.

By adopting the technical scheme, the phenolic hydroxyl group of the silymarin in the silybum marianum fruit extract has anti-lipid peroxidation activity, not only can keep the structure of collagen in skin unchanged, but also is beneficial to stabilizing the structure of high-permeability colloid groups; mogroside, amino acid, flavone, etc. contained in the extract of Momordica grosvenori is beneficial to enhancing the activity of the extract component of Polygonatum odoratum in composition B; diterpene glycosides contained in the extract of Epilobium angustifolium can relieve the redness of skin; the plumeria rubra extract contains sterol, plumeria glycoside, scopoletin and other various lipid alcohols, the water lily flower extract contains various saccharides and alcohols, and the plumeria rubra extract and the water lily flower extract act together to be beneficial to enhancing the compatibility of the soothing agent and skin cells; the opuntia ficus-indica extract can promote the generation of skin growth factors, has the function of activating skin, activates skin cells to further promote the permeation of high-permeability colloid groups, and achieves the effect of promoting skin absorption.

The silybum marianum fruit extract, the momordica grosvenori extract and other plant extracts are cooperatively matched according to a specific proportion, so that a cooperative compounding effect can be generated, all component substances and high-permeability colloid groups in the moisturizing and relieving process can be uniformly dispersed in the process of permeating into deep cells of the skin, the absorption capacity of the skin is improved, the skin absorption is more balanced, and the balance of the high-permeability water-locking composition on the skin repairing effect is also improved.

Preferably, the repairing agent consists of a repairing component and a solvent, wherein the repairing component comprises one or more of gentian root extract, honeysuckle flower extract, wild chrysanthemum flower extract, corydalis tuber extract, wild mint extract and sophora flavescens root extract.

By adopting the technical scheme, the gentian root extract has a promoting effect on the secretion of epidermal cell cholesterol, and can improve the state of oily rough skin; the flos Lonicerae extract can change sebum composition, and has effects of regulating skin oiliness and softening skin; the wild chrysanthemum extract can restrain the activity of 5 a-reductase and can astringe pores to reduce oil; the gentian root extract, the honeysuckle flower extract and the wild chrysanthemum flower extract have synergistic effect, and have prominent effect on conditioning the skin oiliness.

The rhizoma corydalis extract contains corydalis A, tetrahydropalmatine and propylene, and has analgesic and tranquilizing effects; the herba Menthae extract contains various components such as volatile oil, flavone, organic acid and amino acids, and has certain inhibiting effect on fungi and viruses; the rhizoma corydalis extract and herba Menthae extract are helpful for skin antibacterial and anti-inflammatory.

The herba menthae extract also has the effect of promoting the production of collagen, the radix sophorae flavescentis extract also has the effect of promoting the proliferation of fibroblasts, and the combination of the herba menthae extract and the radix sophorae flavescentis extract is beneficial to relieving damaged cells of skin.

The repairing agent is formed by mixing various plant extracts such as a gentian root extract, a corydalis tuber extract and the like, and realizes comprehensive repair of skin from multiple aspects of skin grease, antibiosis and antiphlogosis and cell repair. In addition, the components such as brass, amino acid and the like contained in the repairing agent are also beneficial to being integrated into the high-permeability colloidal group, so that the stability of the high-permeability colloidal group is enhanced, and the absorption promoting effect of the high-permeability colloidal group on the skin is improved.

Preferably, the humectant consists of a moisturizing component and a solvent, and the moisturizing component comprises one or more of xylitol, centella asiatica extract and tremella extract.

By adopting the technical scheme, the xylitol has the functions of long-acting water replenishing and moisture preserving; the centella asiatica extract mainly contains asiaticoside and madecassoside, can tighten the connecting part of epidermis and dermis, can soften skin, and is helpful for the skin to absorb xylitol; the water-soluble high-molecular heteropolysaccharide in the tremella extract has excellent moisture retention and film-forming properties, can be fused with xylitol to improve the moisture retention effect, and can increase the content of colloid in high-permeability colloid groups, thereby enhancing the stability of the colloid groups. The substances in the humectant promote each other to penetrate into deep cells of the face to play a remarkable moisturizing effect, and the water retention performance of the cells is improved from the deep layer.

In a second aspect, the technical scheme adopted by the soothing and moisturizing mask liquid containing the high-permeability water-locking composition is as follows:

a soothing and moisturizing mask liquid containing a high-permeability water-locking composition comprises the following raw materials in percentage by weight:

phase A: 2-4% of glycerin, 4-6% of propylene glycol, 0.5-1.5% of trehalose, 0.03-0.07% of sodium hyaluronate, 0.2-0.25% of thickening agent and 0.02-0.04% of EDTA disodium;

phase B: arginine 0.1-0.15%;

and C phase: 0.9 to 1.0 percent of propylene glycol, 0.45 to 0.5 percent of p-hydroxyacetophenone and 0.45 to 0.5 percent of 1, 2-hexanediol;

phase D: 2.1 to 3.9 percent of high-permeability water-locking composition;

the balance of water.

Preferably the thickener is one or more of an ammonium acryloyldimethyltaurate/VP copolymer, a carbomer and a sclerotium rolfsii gum.

By adopting the technical scheme, the high-permeability water-locking composition can promote the absorption of facial skin, the high-permeability water-locking composition permeates into skin horny layers and dermal cells to deeply relieve and moisturize the facial skin cells, and trehalose, sodium hyaluronate and glycerin are mutually matched to form a protective film on the skin surface, so that the skin outer layer is conditioned and locked. The high-permeability water-locking composition in the facial mask liquid, trehalose, sodium hyaluronate and the like act together to respectively perform soothing and repairing on the skin from the deep layer and the surface of the skin under the double-pipe condition, so that the facial mask liquid has a good absorption effect and a remarkable soothing and water-locking effect.

Preferably, the weight percentage of the arginine is 0.125-0.135%.

By adopting the technical scheme, arginine is basic amino acid which is necessary in human body, and the arginine can play a role in providing immunity, adjusting acid-base moisture and balancing grease to skin; when the weight percentage of arginine in the facial mask liquid is 0.125-0.135%, the arginine has better cooperative effect, so that the acid-base balance of the whole facial mask liquid system is better, the high-permeability water-locking composition is favorably fused with other components in the facial mask liquid, and a part of arginine can be fused into a high-permeability colloid group, so that the dispersion uniformity of the colloid group can be better improved, and the uniform absorption of facial skin is promoted; but also can promote the colloid group to penetrate into the fibroblast of the dermis layer, and improve the absorption effect of the skin.

Preferably, the thickening agent comprises one or both of carbomer and sclerotium rolfsii.

By adopting the technical scheme, carbomer molecules are used as carboxyl groups and combined with one or more than two hydroxyl groups to form hydrogen bonds for thickening, the neutralized carbomer is an excellent gel matrix, and the carbomer can increase the cohesiveness of a colloid group, thereby being beneficial to improving the structural stability of the colloid group and simultaneously being beneficial to improving the cohesive action between the high-permeability water-locking composition and other components in the mask liquid; the sclerotium rolfsii gum is a natural polymer of natural capsule-shaped glucan polysaccharide, is favorable for controlling the viscosity of the facial mask liquid and maintaining the stability of the facial mask liquid system, and has good cohesiveness with colloid groups, so that the cohesiveness between other components in the facial mask liquid and the colloid groups is improved.

In a third aspect, the application provides a preparation method of a soothing and water-locking mask liquid containing a high-permeability water-locking composition, and the following technical scheme is adopted:

a preparation method of a soothing and moisturizing mask liquid containing a high-permeability water-locking composition comprises the following steps:

step one, preparing a high-permeability water-locking composition: mixing and stirring the composition A, the composition B, the composition C, the soothing agent, the repairing agent and the humectant uniformly to obtain a high-permeability water-retaining composition for later use;

mixing glycerol and propylene glycol, adding the residual raw materials of the phase A, heating to 80-85 ℃, and stirring until particles are completely dissolved to obtain a base solution;

step three, cooling to 60-65 ℃, adding the phase B raw material into the base solution, and stirring until the phase B raw material is completely dissolved and has no particles;

step four, mixing the phase C raw materials, heating to 50-55 ℃, uniformly stirring, adding into the base solution, and stirring until the phase C raw materials are completely dissolved and have no particles;

and step five, cooling to 40-45 ℃, adding the high-permeability water-locking composition prepared in the step one into the base solution, and uniformly stirring to obtain the soothing and moisturizing mask solution.

By adopting the technical scheme, firstly, glycerol and propylene glycol are added into an emulsifying pot, and the glycerol and the propylene glycol are used as solvent base materials of the mask liquid and are used for dissolving other components; adding trehalose, sodium hyaluronate, a thickening agent and EDTA disodium into a solvent base material, and uniformly mixing the materials in the process of heating to 80-85 ℃ to form a mask base solution with the functions of relieving and moisturizing; cooling to 60-65 deg.C, adding arginine, and neutralizing and regulating the basic solution with arginine at the temperature range; mixing and heating the p-hydroxyacetophenone, the propylene glycol and the 1, 2-hexanediol to uniformly mix the p-hydroxyacetophenone, the propylene glycol and the 1, 2-hexanediol, adding the mixture of the p-hydroxyacetophenone, the propylene glycol and the 1, 2-hexanediol into the base liquid, and uniformly dispersing the mixed solution of the p-hydroxyacetophenone, the propylene glycol and the propylene glycol in the base liquid to improve the integral oxidation resistance and corrosion resistance of the base liquid; and finally, after the temperature is reduced to 40-45 ℃, the high-permeability water-locking composition is added into the base solution, water is supplemented and released at a proper temperature, the influence of the temperature on volatile substances in the high-permeability water-locking composition is reduced, the high-permeability water-locking composition and substances in the base solution interact with each other, and the optimal improvement of the moisture retention and release performance of the facial mask solution is completed.

In summary, the present application includes at least one of the following beneficial technical effects:

1. the high-permeability water-locking composition comprises a composition A containing an extract of flowers/leaves of leontopodium alpinum, a composition B containing an extract of polygonatum odoratum and a composition C containing a lactobacillus/rice fermentation product, wherein a plurality of high-permeability colloid groups can be formed under the synergistic action of the composition A, the composition B and the composition C, when the composition A, the composition B and the composition C are in contact with facial skin, the high-permeability colloid groups can rapidly permeate into the horny layer of the skin, a path similar to a high-speed channel is formed on the face, and substances such as a moisturizing agent, a soothing agent, a repairing agent and the like in the high-permeability water-locking composition are wrapped by the colloid groups, so that the high-permeability colloid groups rapidly enter deep cells of the skin to repair and supplement water for the deep cells of the skin. The high-permeability colloid groups improve the absorption capacity of the skin, enhance the absorption capacity of the skin, and can absorb sufficient nutrition in a short time, thereby improving the skin care efficiency;

2. the mask liquid comprises a base liquid composed of trehalose, sodium hyaluronate, glycerol and the like and a moisturizing and soothing effect, the high-permeability water-locking composition improves the absorption effect of skin, each component in the high-permeability water-locking composition extends into deep cells to carry out deep repair on the cells, and the trehalose and the like in the base liquid condition the outer layer of the skin, so that the soothing and moisturizing effect of the mask liquid is greatly improved.

Detailed Description

The present application will be described in further detail with reference to the following examples.

The information on the source of the raw materials used in the following experimental examples and comparative experimental examples is shown in Table 1.

TABLE 1

Preparation example

Preparation example 1

The preparation example discloses a preparation method of a composition A, which comprises the following specific steps: adding 5kg of the extract of the flowers/leaves of the alpine leontopodium, 70kg of butanediol and 25kg of water into an emulsifying pot, mixing, and stirring for 5 minutes at normal temperature and the rotating speed of 30r/min to obtain the composition A.

Preparation example 2

The preparation example discloses a preparation method of a composition A, which comprises the following specific steps: adding 7kg of the extract of the flowers/leaves of the alpine leontopodium, 70kg of butanediol and 23kg of water into an emulsifying pot, mixing, and stirring for 5 minutes at normal temperature and the rotating speed of 30r/min to obtain the composition A.

Preparation example 3

The preparation example discloses a preparation method of a composition B, which comprises the following steps: adding 8kg of rhizoma Polygonati Odorati extract, 20kg of butanediol, 5kg of 1, 2-hexanediol and 67kg of water into an emulsifying pot, mixing, and stirring at normal temperature and rotation speed of 35r/min for 5 min to obtain composition B.

Preparation example 4

The preparation example discloses a preparation method of a composition B, which comprises the following steps: adding 12kg of rhizoma Polygonati Odorati extract, 20kg of butanediol, 3kg of 1, 2-hexanediol and 65kg of water into an emulsifying pot, mixing, and stirring at normal temperature and rotation speed of 35r/min for 5 min to obtain composition B.

Preparation example 5

The preparation example discloses a preparation method of a composition C, which comprises the following specific steps: 98kg of lactobacillus/rice fermentation product, 1kg of 1, 2-pentanediol, and 1kg of 1, 2-hexanediol were added to an emulsifying pot, and mixed, and stirred at normal temperature and rotation speed of 35r/min for 5 minutes to obtain composition C.

Preparation example 6

The preparation example discloses a preparation method of a composition C, which comprises the following specific steps: 99kg of lactobacillus/rice fermentation product, 0.5kg of 1, 2-pentanediol, and 0.5kg of 1, 2-hexanediol were added to an emulsifying pot and mixed, and stirred at normal temperature at a rotation speed of 35r/min for 5 minutes to obtain composition C.

Preparation example 7

In the preparation example, the soothing agent is three-flower anti-blue essence which is composed of 0.5 wt% of peach flower extract, 0.5 wt% of lotus flower extract, 0.5 wt% of shrubalthea flower extract, 37.5 wt% of glycerin, 3 wt% of propylene glycol, 0.5 wt% of 1, 2-ethylene glycol, 0.5 wt% of caprylyl glycol and 57 wt% of water.

Preparation example 8

The preparation example discloses a preparation method of a soothing and slowing agent, which comprises the following specific steps: adding 1.6kg of herba Silybi Mariani extract, 18kg of butanediol, 4kg of hexanediol and 76.4kg of water into an emulsifying pot, mixing, and stirring at normal temperature and rotation speed of 30r/min for 5 min to obtain the soothing agent.

Preparation example 9

The preparation example discloses a preparation method of a soothing and slowing agent, which comprises the following specific steps: adding fructus Siraitiae Grosvenorii extract 1.6kg, herba Salicornia Herbacea extract 1.6kg, butanediol 18kg, 1kg, 2-hexanediol 4kg and water 74.8kg into emulsifying pot, mixing, and stirring at normal temperature and rotation speed of 30r/min for 5 min to obtain the soothing agent.

Preparation example 10

The preparation example discloses a preparation method of a soothing and slowing agent, which comprises the following specific steps: adding 1.6kg of Plumeria rubra extract, 1.8kg of flos Nymphaeae extract, 1.8kg of opuntia ficus-indica extract, 18kg of butanediol, 4kg of 1, 2-hexanediol and 72.8kg of water into an emulsifying pot, mixing, and stirring at normal temperature and the rotation speed of 30r/min for 5 minutes to obtain the soothing agent.

Preparation example 11

The preparation example discloses a preparation method of a soothing and slowing agent, which comprises the following specific steps: adding 1kg of silybum marianum fruit extract, 1kg of momordica grosvenori fruit extract, 1kg of gorgonian extract, 1kg of plumeria rubra extract, 1kg of water lily flower extract, 1kg of opuntia ficus-indica fruit extract, 18kg of butanediol, 4kg of 1, 2-hexanediol and 72kg of water into an emulsifying pot, mixing, and stirring for 5 minutes at the normal temperature and the rotating speed of 30r/min to obtain the soothing agent.

Preparation example 12

The difference between the present preparation example and preparation example 11 is that: 1.6kg of silybum marianum fruit extract, 1.6kg of momordica grosvenori extract, 1.6kg of gorgonia pseudopterodonta extract, 1.6kg of plumeria alba extract, 1.8kg of nymphaea alba extract, 1.8kg of opuntia ficus linn fruit extract and 68kg of water.

Preparation example 13

The difference between the present preparation example and preparation example 11 is that: the content of the silybum marianum fruit extract is 1.8kg, the content of the momordica grosvenori fruit extract is 1.8kg, the content of the gorgonia pseudoaltaica extract is 1.8kg, the content of the plumeria alba extract is 1.8kg, the content of the water lily flower extract is 1.6kg, the content of the opuntia ficus-indica fruit extract is 1.6kg and the content of water is 67.6 kg.

Preparation example 14

The difference between the present preparation example and preparation example 11 is that: replacing 1.8kg of the gorgonia pseudopterogorgii extract with 1.8kg of the sarcandra glabra extract; 1.6kg of the white water lily flower extract was replaced with 1.6kg of the fucus extract.

Preparation example 15

The difference between this preparation and preparation 14 is that: 1.8kg of the gorgonia pseudopterospori extract was replaced with 1.8kg of the paeonia lactiflora root extract.

Preparation example 16

In the preparation example, the repairing agent is golden chamomile flower water.

Preparation example 17

The preparation example discloses a preparation method of a repairing agent, which comprises the following specific steps: adding 3kg of radix gentianae extract, 0.5kg of honeysuckle extract, 0.5kg of wild chrysanthemum extract, 0.5kg of rhizoma corydalis extract, 0.5kg of herba menthae extract, 0.5kg of sophora flavescens root extract, 0.5kg of 1, 2-pentanediol, 0.5kg of octaethylene glycol, 17.5kg of propylene glycol and 76kg of water into an emulsifying pot for mixing, and stirring for 5 minutes at the normal temperature and the rotating speed of 35r/min to obtain the repairing agent.

Preparation example 18

The humectant in the preparation example is VKFerrm 201 skin nourishing lotion produced by Biotech GmbH of Blueyu Chuang (Guangzhou) and comprises lactobacillus/North American eriodictyon fermentation product extract 33 wt%, hydrolyzed rice extract 32 wt%, rice wine lees water 33 wt%, 1, 2-hexanediol 1.5 wt%, and 1, 2-pentanediol 0.2 wt%.

Preparation example 19

The preparation example discloses a preparation method of a humectant, which comprises the following specific steps: adding 7.5kg of xylitol, 35kg of dehydrated xylitol, 15kg of centella asiatica extract, 25kg of tremella extract, 1.5kg of 1, 2-hexanediol and 16kg of water into an emulsifying pot, mixing, and stirring at the normal temperature and the rotation speed of 30r/min for 5 minutes to obtain the humectant.

Examples

Examples 1 to 5

The high-permeability water-locking composition comprises: composition A, composition B, composition C, soothing agent, repairing agent, moisturizing agent and solvent.

The preparation method of the high-permeability water-locking composition comprises the following steps: and adding the composition A, the composition B, the composition C, the soothing agent, the repairing agent and the humectant which are prepared in the preparation example into an emulsifying pot together, and carrying out homogeneous dispersion for 5 minutes at normal temperature and at the rotation speed of 550r/min to obtain the high-permeability water-locking composition.

The amounts of the respective raw material components (unit: kg) of the high permeability water-locking compositions of examples 1 to 5 are specified in Table 2 (in the table, "\" is regarded as not added).

TABLE 2

Examples 6 to 13

A method for preparing a high-permeability water-locking composition, which is different from the embodiment 5 in that: the soothing agents prepared in preparation examples 8-15 were respectively selected as the soothing agents.

The soothing agents used in examples 6-13 are detailed in Table 3

TABLE 3

Example 14

A method for preparing a high-permeability water-locking composition, which is different from the embodiment 5 in that: the repairing agent prepared in preparation example 17 was used as the repairing agent.

Example 15

A method for preparing a high-permeability water-locking composition, which is different from the embodiment 5 in that: the humectant is prepared in preparation example 19.

Examples 16 to 18

The high-permeability water-locking composition comprises: composition A, composition B, composition C, soothing agent, repairing agent, moisturizing agent and solvent.

The preparation method of the high-permeability water-locking composition comprises the following steps: and adding the composition A, the composition B, the composition C, the soothing agent, the repairing agent and the humectant which are prepared in the preparation example into an emulsifying pot together, and carrying out homogeneous dispersion for 5 minutes at normal temperature and at the rotation speed of 550r/min to obtain the high-permeability water-locking composition.

The amounts (unit: kg) of the raw material components of the high permeability water-locking composition in examples 16 to 18 are shown in Table 3.

TABLE 4

Comparative example

Comparative example 1

A method for preparing a high-permeability water-locking composition, which is different from the composition prepared in the example 5 in that: the extract of flowers/leaves of leontopodium alpinum in composition a was replaced with an equal amount of water.

Comparative example 2

A method for preparing a high-permeability water-locking composition, which is different from the composition prepared in the example 5 in that: replacing the extract of Yuzhu in composition B with water.

Comparative example 3

A method for preparing a high-permeability water-locking composition, which is different from the composition prepared in the example 5 in that: the lactobacillus/rice fermentation product in composition C was replaced with an equal amount of water.

Comparative example 4

A method for preparing a high-permeability water-locking composition, which is different from the composition prepared in the example 5 in that: the extract of flowers/leaves of leontopodium alpinum in composition a, the extract of polygonatum odoratum in composition B and the lactobacillus/rice fermentation product in composition C were replaced with the same amount of water.

Comparative example 5

A method for preparing a high-permeability water-locking composition, which is different from the composition prepared in the example 5 in that: the soothing agent was replaced with an equal amount of water.

Examples of the experiments

Experimental example 1

The experimental example discloses a soothing and moisturizing mask liquid containing a high-permeability water-locking composition, which comprises the following raw materials in parts by weight:

phase A: 2kg of glycerin, 4kg of propylene glycol, 0.5kg of trehalose, 0.03kg of sodium hyaluronate, 0.2kg of acryloyl dimethyl taurate/VP copolymer and 0.02kg of EDTA disodium;

phase B: 0.1kg of arginine;

and C phase: 1.0kg of propylene glycol, 0.5kg of p-hydroxyacetophenone and 0.5kg of 1, 2-hexanediol;

phase D: 2.1kg of high-permeability water-locking composition;

89.05kg of water.

The experimental example also discloses a preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition, which comprises the following steps:

step one, selecting the high-permeability water-locking composition prepared in the embodiment 1 for standby;

adding 2kg of glycerol, 4kg of propylene glycol and 89.05kg of water into an emulsifying pot, adding 0.5kg of trehalose, 0.03kg of sodium hyaluronate, 0.2kg of ammonium acryloyldimethyl taurate/VP copolymer and 0.02kg of EDTA disodium, stirring and heating to 80 ℃, preserving heat for 25 minutes, and homogenizing for 3 minutes at the rotating speed of 750r/min until particles are completely dissolved to obtain a base solution;

step three, cooling to 60 ℃, adding 0.1kg of arginine into the base solution, and stirring for 15 minutes at the rotating speed of 35 r/min; step four, mixing and heating 1.0kg of propylene glycol, 0.5kg of p-hydroxyacetophenone and 0.5kg of 1, 2-hexanediol to 55 ℃, stirring for 3 minutes, adding into an emulsifying pot, mixing, and stirring at the rotating speed of 35r/min until particles are completely dissolved;

and step five, cooling to 40 ℃, adding 2.1kg of the high-permeability water-locking composition obtained in the step one into an emulsifying pot, stirring for 15 minutes at the rotating speed of 35r/min, and filtering and discharging by using a 200-mesh filter screen to obtain the mask liquid.

Experimental example 2

The experimental example discloses a soothing and moisturizing mask liquid containing a high-permeability water-locking composition, which comprises the following raw materials in parts by weight:

phase A: 4kg of glycerin, 6kg of propylene glycol, 1.5kg of trehalose, 0.07kg of sodium hyaluronate, 0.25kg of acryloyl dimethyl taurate/VP copolymer and 0.04kg of EDTA disodium;

phase B: 0.15kg of arginine;

and C phase: 0.9kg of propylene glycol, 0.45kg of p-hydroxyacetophenone and 0.45kg of 1, 2-hexanediol;

phase D: 3.9kg of high-permeability water-locking composition;

82.29kg of water.

The experimental example also discloses a preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition, which comprises the following steps:

step one, selecting the high-permeability water-locking composition prepared in the embodiment 1 for standby;

adding 4kg of glycerol, 6kg of propylene glycol and 82.29kg of water into an emulsifying pot, adding 1.5kg of trehalose, 0.07kg of sodium hyaluronate, 0.25kg of ammonium acryloyldimethyl taurate/VP copolymer and 0.04kg of EDTA disodium, stirring and heating to 85 ℃, keeping the temperature for 25 minutes, and homogenizing for 3 minutes under the condition that the rotating speed is 750r/min until particles are completely dissolved to obtain a base solution;

step three, cooling to 65 ℃, adding 0.15kg of arginine into the base solution, and stirring for 15 minutes at the rotating speed of 35 r/min;

step four, mixing and heating 0.9kg of propylene glycol, 0.45kg of p-hydroxyacetophenone and 0.45kg of 1, 2-hexanediol to 50 ℃, stirring for 3 minutes, adding into an emulsifying pot, mixing, and stirring at the rotating speed of 35r/min until particles are completely dissolved;

and step five, cooling to 45 ℃, adding 3.9kg of the high-permeability water-locking composition obtained in the step one into an emulsifying pot, stirring for 15 minutes at the rotating speed of 35r/min, and filtering and discharging by using a 200-mesh filter screen to obtain the mask liquid.

Experimental examples 3 to 19

A preparation method of a soothing and moisturizing mask liquid containing a high-permeability water-locking composition is different from that of experimental example 2 in that: in step one, the highly permeable water-retaining compositions prepared in examples 2-18 were used, respectively.

Experimental example 20

The preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition is different from that of experimental example 18 in that: the content of water in the second step is 82.315kg, and the content of arginine in the third step is 0.125 kg.

Experimental example 21

The preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition is different from that of experimental example 18 in that: the content of water in the second step is 82.305kg, and the content of arginine in the third step is 0.135 kg.

Experimental example 22

The preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition is different from that of experimental example 18 in that: replacing 0.25kg of the acryloyldimethyl taurate/VP copolymer in step two with an equal amount of carbomer.

Experimental example 23

The preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition is different from that of experimental example 18 in that: replacing 0.25kg of the ammonium acryloyldimethyltaurate/VP copolymer obtained in the second step with the same amount of sclerotium rolfsii gum.

Experimental example 24

The preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition is different from that of experimental example 18 in that: and replacing 0.25kg of the acryloyl dimethyl taurate/VP copolymer in the step two by 0.13kg of carbomer and 0.12kg of sclerotium rolfsii.

Experimental example 25

The preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition is different from that of experimental example 18 in that: the water content in the second step is 82.315 kg; replacing 0.25kg of acryloyl dimethyl taurate/VP copolymer in the second step with 0.13kg of carbomer and 0.12kg of sclerotium rolfsii; the arginine content in the third step is 0.125 kg.

Experimental example 26

The experimental example discloses a soothing and moisturizing mask liquid containing a high-permeability water-locking composition, which comprises the following raw materials in parts by weight:

phase A: 3kg of glycerin, 5kg of propylene glycol, 1kg of trehalose, 0.05kg of sodium hyaluronate, 0.13kg of carbomer, 0.1kg of sclerotium rolfsii and 0.03kg of EDTA disodium;

phase B: 0.13kg of arginine;

and C phase: 0.9kg of propylene glycol, 0.45kg of p-hydroxyacetophenone and 0.45kg of 1, 2-hexanediol;

phase D: 3.2kg of high-permeability water-locking composition;

85.56kg of water.

The experimental example also discloses a preparation method of the soothing and moisturizing mask liquid containing the high-permeability water-locking composition, which comprises the following steps:

step one, selecting the high-permeability water-locking composition prepared in the embodiment 1 for standby;

adding 3kg of glycerol, 5kg of propylene glycol and 85.56kg of water into an emulsifying pot, adding 1kg of trehalose, 0.05kg of sodium hyaluronate, 0.13kg of carbomer, 0.1kg of sclerotium rolfsii and 0.03kg of EDTA disodium, stirring and heating to 85 ℃, keeping the temperature for 25 minutes, and homogenizing for 3 minutes under the condition that the rotating speed is 750r/min until no particles are completely dissolved to obtain a base solution;

step three, cooling to 65 ℃, adding 0.13kg of arginine into the base solution, and stirring for 15 minutes at the rotating speed of 35 r/min;

step four, mixing and heating 0.9kg of propylene glycol, 0.45kg of p-hydroxyacetophenone and 0.45kg of 1, 2-hexanediol to 50 ℃, stirring for 3 minutes, adding into an emulsifying pot, mixing, and stirring at the rotating speed of 35r/min until particles are completely dissolved;

and step five, cooling to 45 ℃, adding 3.2kg of the high-permeability water-locking composition obtained in the step one into an emulsifying pot, stirring for 15 minutes at the rotating speed of 35r/min, and filtering and discharging by using a 200-mesh filter screen to obtain the mask liquid.

Comparative Experimental examples 1 to 5

A preparation method of a soothing and moisturizing mask liquid containing a high-permeability water-locking composition is different from that of experimental example 6 in that: in the first step, the high-permeability water-locking composition prepared in the comparative examples 1-5 is respectively selected.

Performance test

1. Facial skin absorption rate test: the same-standard non-woven fabric facial mask paper with the absorption rate of 90% is soaked in the facial mask solutions prepared in the experimental examples 1-26 and the comparative experimental examples 1-5 respectively for 24h and then taken out to serve as a test group, a commercially available brand of water-releasing and water-locking facial mask serves as a control group, and the water contents of the facial masks of the test group and the control group are consistent within an allowable error range (+ -1%). 160 test subjects with no obvious difference between skin quality and facial skin moisture content were selected: dividing every 5 persons of 155 testers into the same test group, using the same test group to test samples prepared by the same experimental example in the test group, and averaging test results; the remaining 5 subjects used as a control group to try the control group mask, and the test results were averaged. After washing the cheek with warm water for 10 minutes, measuring the water content of the skin cuticle at the forehead of a test person of each test group in batches by using a Callegari Soft5.5 skin cuticle water content tester under the conditions of room temperature and humidity of 75-80%, and recording as an initial value; and then, respectively applying the facial masks of the test group and the control group to the face of the test group and the control group, lifting the facial mask at the forehead of the test user when the facial mask is used for 5 minutes, wiping the facial mask solution at the forehead clean by using a paper towel, and measuring the moisture content of the stratum corneum at the forehead of the test user by using a tester, and recording the moisture content as 5 minutes. After collecting and arranging a plurality of groups of data, analyzing and comparing the increment of the moisture content of the skin cuticle of the face of the test person (5-minute moisture content-initial value) in 5 minutes after the facial mask is applied by the test group and the control group, thereby detecting the effect of the facial mask liquid of the experimental examples 1-23 and the comparative experimental examples 1-5 on promoting the skin absorption, wherein the larger the increment of the moisture content of the skin cuticle in 5 minutes is, the better the skin absorption effect is proved.

2. The moisture retention effect test of the mask comprises the following steps: on the basis of the test 1, after the 160 testers apply the facial mask for 15 minutes, taking down the facial mask, cleaning the facial mask liquid remained on the face, measuring the water content of the skin cuticle at the forehead of each test group of testers in batches by adopting a Callegari Soft5.5 skin cuticle water content tester, and recording the water content as a basic value; measuring the water content of the facial skin cuticle of the testees of the test group and the control group after the testees are stood for 30 minutes at room temperature and humidity of 75-80%, recording as the water content of 30 minutes, and calculating the 30-minute loss (the base value is-30 minutes water content); after the test subjects had stood in the room for 60 minutes, the water content of the stratum corneum of the face skin of the test subjects and the control subjects was measured and recorded as the water content for 60 minutes, and the amount of run-off for 60 minutes (base value-60 minute water content) was calculated. And recording data, collecting and sorting a plurality of groups of data, averaging the test results of each group, and taking the mask for 30 minutes and 60 minutes to ensure that the loss of the water content of the horny layer of the face skin of the testee is smaller, so that the water loss of the skin is less in the same time of 30 minutes and 60 minutes, and the moisturizing effect of the mask is better.

3. Evaluating the soothing effect of the facial mask: 30 testers with skin having face redness are selected, the face redness degree of the testers is similar, the testers are 18-45 years old, both men and women have 10 people, the testers are divided into 3 groups, the experimental example 26, the comparative experimental example 5 and the control group are respectively used for face masks, the face masks are applied for 15 minutes at 10 pm every day, after one week, the experimental example 26, the comparative experimental example 5 and the control group are respectively graded according to the skin redness reduction condition and the use feeling, and the evaluation standards are as follows:

1 minute-the degree of facial redness did not decrease after one week of use, with essentially no effect;

2 minutes, namely the degree of facial redness is reduced after one week of use, but the reduction effect is not obvious;

3 minutes, namely the degree of facial redness is reduced after one week of use, and the reduction effect is obvious;

4 minutes, namely the degree of facial redness is reduced after three days of use, and the reduction effect is more obvious;

and 5 points, the degree of the face redness is reduced when the face is used on the second day, and the reduction effect is obvious.

The specific assay data for assays 1-3 are detailed in tables 5-11.

TABLE 5

According to the test data of the experimental examples 1-6 and the control group in table 5, the moisture content of the skin stratum corneum of the facial mask prepared in the experimental examples 1-6 is greater than that of the control group after being applied for 5 minutes, and the increase of the moisture content of the skin stratum corneum of the experimental examples 1-6 from the initial value after being applied for 5 minutes is greater than that of the control group, which indicates that the facial mask prepared in the experimental examples 1-6 has better moisturizing and absorbing effects compared with the commercially available facial mask.

The comparison of the moisture content values in the same time after the facial masks are removed in the experimental examples 1-6 and the control group can be used for obtaining that the moisture content of the skin cuticle after the facial masks are removed in the experimental examples 1-6 for 30 minutes and 60 minutes is greater than that of the skin cuticle after the facial masks are removed in the control group for 30 minutes and 60 minutes, and the moisture content loss of the skin cuticle in the experimental examples 1-6 for 30 minutes and 60 minutes is less than that of the skin cuticle in the control group for 30 minutes and 60 minutes, which indicates that the facial mask liquid prepared in the experimental examples 1-6 has stronger water locking and moisturizing capabilities compared with the commercially available facial mask liquid.

TABLE 6

According to the test data of the experimental example 6 and the comparative experimental examples 1 to 4 in table 6, when the three substances of the herb Hibiscus sabdariffa flower/leaf extract, the Yuzhu extract and the lactobacillus/rice fermentation product are not added or one of the three substances is removed in the facial mask liquid of the comparative experimental examples 1 to 4, the increase of the moisture content of the horny layer of the skin after the facial mask liquid prepared by the comparative experimental examples 1 to 4 is far smaller than the value of the experimental example 6 after the facial mask liquid is applied for 5 minutes by a test person, which indicates that the facial mask liquid prepared by the comparative experimental examples 1 to 4 has weak capability of promoting the absorption of the skin; the water content loss of the skin cuticle after 30 and 60 minutes of facial mask removal in comparative experiment examples 1-4 is greater than that of the skin cuticle after 30 and 60 minutes of facial mask removal in experiment example 6, which shows that the water locking and moisturizing effects of the facial mask liquid prepared in comparative experiment examples 1-4 are poorer than that of experiment example 5.

According to the analysis of the inventor, a plurality of high-permeability colloid groups are formed under the synergistic effect of the composition A containing the extract of the flowers/leaves of the alpine leontopodium, the composition B containing the extract of the polygonatum odoratum and the composition C containing the lactobacillus/rice fermentation product in the high-permeability water-locking composition, when the components of the high-permeability water-locking composition in facial mask liquid are contacted with the facial skin of a test person, the high-permeability colloid groups can rapidly permeate into deep cells of the skin, and substances such as a moisturizing agent, a soothing agent, a repairing agent and the like in the high-permeability water-locking composition are wrapped by the colloid groups and rapidly enter the skin cells along with the colloid groups, so that the absorption of the high-permeability water-locking composition by the skin is promoted, and the absorption capacity of the skin is improved; the moisturizing agent, the soothing agent, the repairing agent and the colloid group in the high-permeability water-locking composition enter deep cells of the skin together, so that the facial skin can be deeply repaired and moisturized, the nutrient components are not easy to lose, and the soothing and moisturizing effects of the facial mask liquid are remarkable.

In comparative experimental examples 1-4, one of the three substances is absent or the three substances are not added, the synergistic effect of the three substances disappears, the help of high-permeability colloid groups formed under the synergistic effect of the three substances is lost, and substances such as a moisturizing agent, a soothing agent, a repairing agent and the like in the high-permeability water-locking composition cannot go deep into the deep layer of the skin, so that the absorption capacity of the skin is reduced, the substances such as the moisturizing agent, the soothing agent, the repairing agent and the like floating on the surface run off quickly, and the water retention and locking and soothing repairing effects of the facial mask liquid are reduced.

TABLE 7

According to the test data of the experimental example 6 and the experimental examples 7-14 in the table 7, the increase of the water content of the skin cuticle after the mask is applied for 5 minutes in the experimental examples 11-12 is obviously larger than the increase of the water content of the skin cuticle after the mask is applied for 5 minutes in the experimental examples 6 and 7-10, which shows that when the soothing agent in the experimental examples 11-12 is prepared from the silybum marianum fruit extract, the momordica grosvenori extract, the gorgonia pseudosciaefolia extract, the plumeria alba extract, the nymphaea alba extract and the opuntia ficus-indica extract in a specific ratio, the prepared mask liquid has a good effect of moisturizing and promoting the skin absorption. The numerical value of the 5-minute water content increase amount of the facial mask liquid prepared in the experimental examples 13-14 is similar to that of the experimental examples 7-10 and is smaller than that of the experimental examples 11-12, which shows that after the substances in the soothing agent are replaced by the substances, the water replenishing and absorption promoting effect of the facial mask liquid prepared in the experimental examples 13-14 is weakened, and the remarkable effect of the facial mask liquid prepared in the experimental examples 11-12 on the water replenishing and absorption promoting effect of the skin cannot be achieved.

As can be seen from the test data of comparative example 5 and examples 6 to 14 in Table 7, the increase in the moisture content of the skin stratum corneum after 5 minutes of application of the mask of comparative example 5 was significantly smaller than the increase in the moisture content of the skin stratum corneum after 5 minutes of application of the mask of examples 6 to 14, indicating that the ability to moisturize and promote absorption of the mask solution prepared in comparative example 5 was greatly reduced when the soothing agent component was not added to comparative example 5.

According to the analysis of the inventor, the plant extracts such as the silybum marianum fruit extract and the momordica grosvenori fruit extract in the soothing agent are cooperatively matched according to a specific proportion, so that a cooperative compounding effect can be generated, the component substances and the high-permeability colloid groups in the high-permeability water-locking composition can be uniformly dispersed in the process of permeating into deep cells of the skin, and the absorption capacity of the skin is improved. When the substances are not added or replaced in the formula, the synergistic effect of the substances in a specific ratio cannot be realized, so that the water-replenishing absorption-promoting effect of the prepared facial mask liquid cannot be improved.

TABLE 8

According to the detection data of experimental example 6 and experimental example 15 in table 8, the value of the increase of the water content of the skin stratum corneum of the facial mask liquid prepared in experimental example 15 after being applied for 5 minutes is improved compared with the value of experimental example 6, which indicates that the efficacy of the facial mask liquid prepared in experimental example 15 in the aspects of moisturizing and absorption promotion is improved when the facial mask liquid prepared in experimental example 15 is prepared by mixing gentian root extract, honeysuckle flower extract, wild chrysanthemum extract, corydalis tuber extract, wild mint extract and sophora flavescens root extract with a solvent.

The inventor analyzes that the repairing agent is formed by mixing a plurality of plant extracts such as a gentian root extract, a corydalis tuber extract and the like, so that the repairing agent is favorable for repairing the skin in all directions, and components such as brass, amino acid and the like contained in the repairing agent are also favorable for being fused into high-permeability colloid groups, so that the stability of the high-permeability colloid groups is enhanced, and the absorption promoting effect of the high-permeability colloid groups on the skin is improved.

According to the detection data of experimental example 6 and experimental example 16 in table 8, the increase value of the water content of the stratum corneum of the skin of the facial mask liquid prepared in experimental example 16 after being applied for 5 minutes is larger than that of experimental example 6, which indicates that the moisturizing and absorption promoting capability of the facial mask liquid prepared in experimental example 16 is improved; in experimental example 16, the value of the water content loss of the stratum corneum after 30 minutes and 60 minutes after the mask is removed is smaller than that in experimental example 6, which shows that the mask liquid prepared in experimental example 16 has better water locking and moisturizing capabilities.

The inventor analyzes that all the substances in the moisturizing agent mutually promote to penetrate into the deep cells of the face to moisturize the cells, so that the moisture is not easy to lose, the remarkable moisturizing effect is achieved, and the water locking capacity of the cells is improved from the deep layer of the skin.

The numerical value of the water content increase of the horny layer of the skin after the facial mask liquid prepared in the experimental examples 17-19 is applied for 5 minutes is far larger than that of the experimental example 6, which shows that the facial mask liquid prepared in the experimental examples 17-19 has more outstanding water replenishing and absorption promoting capacity; experimental examples 17-19 the values of the water content loss of the horny layer of the skin after 30 minutes and 60 minutes of facial mask removal are smaller than those of the experimental example 6, which shows that the water-locking and moisturizing capabilities of the facial mask liquid prepared in the experimental examples 17-19 are improved. In experimental examples 17 to 19, the better components in the above examples are adopted on the basis of the basic formula of experimental example 6, so that the numerical values of the performance test data of the experimental examples 17 to 19 are greatly improved compared with the numerical values of the experimental example 6, and the combination ratio of the components in the water replenishing and relieving composition in the experimental example 18 is selected as the optimal combination ratio.

TABLE 9

According to the test data of experimental example 18 and experimental examples 20-21 in table 9, the increase of the water content of the horny layer of the skin after 5 minutes of application of the facial mask solutions prepared in experimental examples 20-21 is larger than the data of experimental example 18, which indicates that the facial mask solutions prepared in experimental examples 20-21 have a good effect of promoting water absorption when the mass percentage of arginine in the facial mask solutions is 0.125-0.135%.

The inventor analyzes that when the mass percentage of arginine in the facial mask liquid is 0.125-0.135%, the acid-base regulation effect of arginine is better, so that the high-permeability colloid group and other components in the facial mask liquid are better fused, and a part of arginine can be fused into the high-permeability colloid group, so that the dispersion uniformity of the colloid group can be improved, and the uniform absorption of facial skin is promoted; but also can promote the colloid group to penetrate into the fibroblast of the dermis layer, and improve the absorption effect of the skin.

Watch 10

According to the test data of experimental example 18 and experimental examples 22-24 in table 10, the increase of the water content of the stratum corneum of the skin after 5 minutes of application of the facial mask solutions prepared in experimental examples 22-24 is obviously higher than that of the data of experimental example 18, which shows that the facial mask solutions prepared in experimental examples 22-24 have better moisturizing, absorption promoting, relieving and repairing effects. The numerical value of the water content loss of the horny layer of the skin after the facial mask is removed for 30 minutes in the experimental examples 22-24 is smaller than that in the experimental example 18, which shows that the facial mask liquid prepared in the experimental examples 22-24 can play a certain role in water locking and moisturizing in a short time.

According to the analysis of the inventor, carbomer can increase the cohesiveness of the colloid group, is beneficial to improving the structural stability of the colloid group, enhances the absorption effect of skin and is beneficial to improving the cohesive action between the high-permeability water-locking composition and other components in the mask liquid; the sclerotium rolfsii gum is beneficial to controlling the viscosity of the mask liquid and maintaining the stability of the mask liquid system, and the sclerotium rolfsii gum and the colloid group also have good cohesiveness, so that the cohesiveness between other components in the mask liquid and the colloid group is improved.

The mask liquids prepared in experimental examples 25-26 adopt the better components in the experimental examples, so that the numerical values of performance detection data of the experimental examples 25-26 are greatly improved compared with the numerical values of the experimental example 18, the performance data of the mask liquids prepared in experimental example 25 and experimental example 26 are similar, and the mask liquid prepared in experimental example 26 is used as the optimal example of the application.

The condition of the test subjects with flush and relieved face is classified into the table, which is detailed in table 11.

TABLE 11

According to the scoring values of 30 testers in table 11 on experimental example 26, comparative experimental example 5 and a control group, the composition a prepared in preparation example 1, the composition B prepared in preparation example 4, the composition C prepared in preparation example 5, the soothing agent prepared in preparation example 13, the repairing agent prepared in preparation example 16 and the moisturizing agent prepared in preparation example 19 are selected for experimental example 26, and the total score of the facial mask solution prepared by mixing the high-permeability water-locking composition prepared in preparation example 26 with the substances such as carbomer, sclerotium rolfsii, arginine and the like is more than 4 minutes, so that the high-permeability water-locking composition in the facial mask solution prepared in experimental example 26 is the best in proportion and has the best combined action with other raw material components, and the facial mask solution has a prominent effect on relieving and reducing facial redness.

The components of the soothing agent are removed from the facial mask liquid prepared in the comparative experiment example 5, and the scores of the facial mask liquid prepared in the comparative experiment example 5 are all 2-3 when the silybum marianum fruit extract, the momordica grosvenori fruit extract, the gorgonia pseudopteropi extract, the plumeria rubra extract, the nymphaea alba flower extract and the opuntia ficus chinensis fruit extract in the soothing agent cannot be combined in a specific ratio to generate synergistic effect, so that the facial mask liquid prepared in the comparative experiment example 5 has little effect on relieving and alleviating the problem of facial redness due to the fact that other components in the facial mask liquid lose the soothing components, and cannot achieve the remarkable soothing effect of the facial mask liquid prepared in the experiment example 25.

The scores of the control groups are all 2-3 points, which are lower than the score of the experimental example 26, and the result shows that the facial mask liquid prepared according to the optimal component ratio of the application has a remarkable effect on relieving compared with the commercial facial mask liquid.

The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.