阅读说明：本技术 一种含有鹧鸪叶提取物的洗发液及其制备方法 (Shampoo containing Mallotus oblongifolius muell-Arg extract and preparation method thereof ) 是由 张文利 于 2018-05-29 设计创作，主要内容包括：本发明公开了一种含有鹧鸪叶提取物的洗发液及其制备方法。所述洗发液包含鹧鸪叶提取物、表面活性剂、保湿剂、调理剂、增稠剂、增泡剂、添加剂、香精和水。所述的制备方法包括以下步骤：制备鹧鸪叶提取物粉末；按重量配比取蒸馏水加入搅拌罐中,开始搅拌,将蒸馏水加热至45-50℃；将上述鹧鸪叶提取物粉末和保湿剂按所述比例混合,并放入水中充分混合搅拌,制成混合水溶液；随后按比例加入表面活性剂、调理剂、增粘剂、增泡剂、添加剂、香精,混合均匀,得洗发液。本发明的含有鹧鸪叶提取物的洗发液蕴含植物提取精华,滋润补水、止痒护发,改善毛发粗糙等问题,使头发莹润亮泽。对头发发黄、发焦、头发天稀疏无光、防白发、经常掉头发、头发开叉、起头皮屑、有一定功效。(the invention discloses a shampoo containing Mallotus oblongifolius muell-Arg extract and a preparation method thereof. The shampoo comprises Mallotus oblongifolius extract, surfactant, humectant, conditioner, thickener, foam promoter, additive, essence and water. The preparation method comprises the following steps: preparing Mallotus oblongifolius extract powder; adding distilled water into a stirring tank according to the weight ratio, starting stirring, and heating the distilled water to 45-50 ℃; mixing the above Mallotus oblongifolius extract powder and humectant at a certain ratio, adding into water, mixing, and making into mixed water solution; and then adding a surfactant, a conditioner, a tackifier, a foam booster, an additive and essence according to a proportion, and uniformly mixing to obtain the shampoo. The shampoo containing the Mallotus furetianus extract contains plant extract essence, moistens and replenishes water, relieves itching and protects hair, solves the problems of rough hair and the like, and enables the hair to be bright and glossy. Has certain effects on yellow hair, scorched hair, thin hair, white hair prevention, frequent hair loss, split hair and scurf generation.)

1. A shampoo containing Mallotus oblongifolius extract is characterized by comprising the Mallotus oblongifolius extract, a surfactant, a humectant, a conditioner, a thickening agent, a foam booster, an additive, an essence and water.

2. The shampoo containing the partridge leaf extract as claimed in claim 1, wherein the partridge leaf extract in the shampoo is 5-40% by weight, preferably 15-25% by weight; 1-10% of surfactant, preferably 2-5%; the humectant is 5-30%, preferably 15-20%; 1-10% of a conditioner, preferably 3-7%; the foam booster is 0.1-4%, preferably 0.5-3%; 1 to 5 percent of thickening agent, preferably 1.5 to 2.5 percent; 0.1-2% of additive, preferably 0.5-1%; 0.1-2% of essence, preferably 0.5-1%; the amount of water is 60 to 80%, preferably 65 to 70%.

3. The shampoo containing the partridge leaf extract as claimed in claim 1, wherein the moisturizer is one or more of glycerin, propylene glycol, sorbitol, polyethylene glycol, and sodium pyrrolidone carboxylate.

4. the shampoo containing the partridge leaf extract as claimed in claim 1, wherein the surfactant is one or more of natural coconut oil fatty alcohol ether sodium sulfate, fatty alcohol ether sodium sulfosuccinate, cocamidopropyl betaine, cocamide DEA, sodium cocoyl glycinate, polyquaternium-7 and polyquaternium-47.

5. The shampoo containing the partridge leaf extract as claimed in claim 1, wherein the moisturizer is one or more of glycerin, propylene glycol, sorbitol, polyethylene glycol, and sodium pyrrolidone carboxylate.

6. The shampoo containing partridge leaf extract as claimed in claim 1, wherein the conditioner is one or more of guar gum, quaternized silicone polysaccharide, decyl glucoside.

7. The shampoo containing partridge leaf extract as claimed in claim 1, wherein the suds booster is sodium laureth sulfate.

8. the shampoo containing the partridge leaf extract as claimed in claim 1, wherein the thickener is one or more of sodium chloride, ammonium chloride, sodium sulfate, guar hydroxypropyltrimonium chloride.

9. the shampoo containing Mallotus oblongifolius muell-Arg 1, wherein the shampoo comprises one or more of Polygonum multiflorum Thunb extract, Bonnate Spirulina powder, and Rose solution.

10. A method for preparing a shampoo containing partridge leaf extract according to any one of claims 1 to 9, comprising the steps of:

(1) Preparing Mallotus oblongifolius extract powder;

(2) Adding distilled water into a stirring tank according to the weight ratio, starting stirring, and heating the distilled water to 45-50 ℃;

(3) Mixing the above Mallotus oblongifolius extract powder and humectant at a certain ratio, adding into water, mixing, and making into mixed water solution;

(4) And then adding a surfactant, a conditioner, a tackifier, a foam booster, an additive and essence according to a proportion, and uniformly mixing to obtain the shampoo.

Technical Field

the invention belongs to a washing product, and particularly relates to a shampoo containing mallotus oblongifolius muell-Arg extract and a preparation method thereof.

background

The shampoo is also called shampoo, shampoo or shampoo, is a basic hair and scalp care cosmetic product which is widely applied, and is one of essential living goods in daily life of people. Generally, a mixed salt of triethanolamine of fatty alcohol sulfate and amine hydroxide, lauric acid isopropanolamide, formaldehyde, polyoxyethylene, lanolin, perfume, coloring material and water are used as raw materials. The main types at present can be classified into transparent types, pearl types and opaque types according to the transparency; can be classified into conditioning shampoo, neutral shampoo, oily shampoo, dry shampoo, dandruff removing shampoo, hair dyeing shampoo, etc. according to functions. The shampoo in the market is added with certain additives and chemical synthesis detergents, and the scalp is excessively degreased due to improper use, so that the root of hair is itchy and inflamed, and the hair quality is damaged.

Mallotus oblongifolius is a plant of Mallotus genus of Euphorbiaceae family, is rarely sexual and drought-resistant, and is favored to grow in stone seams of barren mountains and malls. Mallotus oblongifolius has a thousands of years of eating history in Hainan, is mainly distributed in mountainous areas, hills and coastal areas of Hainan, takes Wanning east mountain as a prosperity, and is a tea substitute beverage plant and a medicinal plant with national characteristics and regional characteristics in Hainan. Mallotus oblongifolius muell-Arg, Mallotus oblongifolius TuArg and Mallotus oblongifolius TuArg are peculiar wild plants with round leaves and sweet taste, and the height of the tree is generally more than 1 to 3 meters, and can even reach 10 meters. The partridge leaves grow mutually, the upper parts of branches grow oppositely, the leaves are in a round oval shape, the length of the leaves is 5-15 cm, the top end of the leaves is sharp, the edges of the leaves are all green and are in wave-shaped teeth, a few transparent veins are arranged on the back surface of the leaves, the veins are in a feather shape, and the length of a petiole is 1-3 cm. Mallotus oblongifolius muell-Arg has peculiar medicinal fragrance, has the effects of clearing heat and detoxicating, clearing heat and quenching thirst, helping digestion and benefiting gallbladder, reducing blood pressure, losing weight, strengthening spleen and nourishing stomach, and can also prevent and treat cold. In recent years, new research and research on partridge leaves have been carried out.

Mallotus oblongifolius muell-Arg contains 18 kinds of amino acids essential to human body, such as tryptophan, threonine, lysine, alanine, glutamic acid, proline and the like, and plays a main role in brain development, detoxification, protein metabolism and the like. The partridge leaves are rich in various vitamins such as vitamin A, vitamin C, vitamin E and the like, and have the functions of resisting wrinkles, immunizing, metabolizing and the like; the partridge leaves are rich in various trace elements such as calcium, potassium, zinc, iron, fluorine, selenium, phosphorus, magnesium, sodium, barium and the like, not only have good health-care effect, but also have good medicinal value, and have positive effects on the growth and development of human bodies, the improvement of bone hardness, cartilage growth and the like, so that the partridge leaves have high development and utilization values.

in the application aspect of the mallotus oblongifolius leaves at present, the leaves are mainly used for making tea drinks, such as: the patent number is CN200910135176.7, and the patent name is Chinese patent of "a bag of partridge tea", this patent adopts partridge tea as the main raw material, adopts chrysanthemum, lemon as supplementary raw materials, when keeping original special flavor of partridge tea, has improved the quality of product, has improved the product taste, has improved the product added value of partridge tea effectively. For example, the patent No. CN201210052585.2, entitled "francolin tea liquid beverage", uses francolin tea as a main raw material, and is prepared from chrysanthemum, medlar, lemon and the like, thereby solving the problems of singleness, original bulkiness, difficulty in controlling product quality, short shelf life and the like of the existing francolin tea product, and having the effects of good taste, more comprehensive nutrition, improvement of quality of the processed product of francolin tea, prolongation of shelf life and the like.

Therefore, at present, the application of partridge leaves is basically to prepare tea drinks, but the application in other aspects is less. At present, no published report of a shampoo related research prepared by the partridge leaf extract is found at home and abroad.

disclosure of Invention

the invention provides a shampoo containing mallotus oblongifolius muell-Arg extract and a preparation method thereof, aiming at overcoming the defects of the existing shampoo technology. The shampoo contains plant extract essence, and has effects of moistening and replenishing water, relieving itching and caring hair, improving hair roughness, and making hair bright and lustrous. The shampoo disclosed by the invention contains a large amount of protein, folic acid, pantothenic acid, aminobenzoic acid, selenium, lecithin, vitamin A, vitamin E, vitamin B2 and vitamin C, and has certain effects on yellowing and scorching of hair, thinning and dull hair, preventing white hair, frequently losing hair, splitting hair and scurf.

the invention mainly aims to provide a shampoo containing Mallotus furetianus leaf extract, which comprises the Mallotus furetianus leaf extract, a surfactant, a humectant, a conditioner, a thickening agent, a foam booster, an additive, an essence and water.

preferably, the shampoo containing the partridge leaf extract comprises 5-40% of the partridge leaf extract, preferably 15-25% of the partridge leaf extract in percentage by weight; 1-10% of surfactant, preferably 2-5%; the humectant is 5-30%, preferably 15-20%; 1-10% of a conditioner, preferably 3-7%; the foam booster is 0.1-4%, preferably 0.5-3%; 1 to 5 percent of thickening agent, preferably 1.5 to 2.5 percent; 0.1-2% of additive, preferably 0.5-1%; 0.1-2% of essence, preferably 0.5-1%; the amount of water is 60 to 80%, preferably 65 to 70%.

In another preferred example, the humectant is one or a combination of glycerin, propylene glycol, sorbitol, polyethylene glycol and sodium pyrrolidone carboxylate.

in another preferred example, the surfactant is one or a combination of more of natural coconut oil fatty alcohol ether sodium sulfate, fatty alcohol ether sodium sulfosuccinate, cocamidopropyl betaine, cocamide DEA, sodium cocoyl glycinate, polyquaternium-7 and polyquaternium-47.

In another preferred example, the humectant is one or a combination of glycerin, propylene glycol, sorbitol, polyethylene glycol and sodium pyrrolidone carboxylate.

In another preferred embodiment, the conditioning agent is one or more of guar gum, quaternary ammonium siloxane polysaccharide and decyl glucoside.

In another preferred embodiment, the foam booster is sodium laureth sulfate.

In another preferred embodiment, the thickening agent is one or a combination of sodium chloride, ammonium chloride, sodium sulfate and guar gum hydroxypropyl trimethyl ammonium chloride.

in another preferred embodiment, the shampoo comprises one or more of polygonum multiflorum extract, ponaster powder and rose water.

in another preferred embodiment, the shampoo containing the partridge leaf extract is prepared according to a proper proportion, and comprises the components of partridge leaf extract, sodium laureth sulfate, decyl glucoside, cocamidopropyl betaine, cocamide DEA, sodium cocoyl glycinate, polyquaternium-7, polyquaternium-47, PEG-7 glyceryl cocoate, glycerol, sodium lauryl sulfate, guar hydroxypropyl trimonium chloride, POLYGONUM MULTIFLORUM (Polygonum MULTIFLORUM) extract, Bolina SPIRULINA (Spirulina PLATENSIS) powder, rose (ROSA RUGOSA) flower water, lactic acid, essence, sodium chloride, DMDM (antibacterial agent) and water.

in another preferred embodiment, the partridge leaves selected for use in the present invention are selected from the group consisting of Hainan Qiongzhong, Ledong, Baotin, Tongshi mountain, Wanning eastern mountain and Wenchang Turbon, and preferably the Wanning eastern mountain and Wenchang Turbon.

another main object of the present invention is to provide a method for preparing a shampoo containing mallotus oblongifolius extract, which comprises the following steps: preparing Mallotus oblongifolius extract powder; adding distilled water into a stirring tank according to the weight ratio, starting stirring, and heating the distilled water to 45-50 ℃; mixing the above Mallotus oblongifolius extract powder and humectant at a certain ratio, adding into water, mixing, and making into mixed water solution; and then adding a surfactant, a conditioner, a tackifier, a foam booster, an additive and essence according to a proportion, and uniformly mixing to obtain the shampoo.

The partridge leaf extract is prepared according to the following method:

(1) selecting Mallotus oblongifolius muell-Arg, cleaning, drying, pulverizing, sieving, and making into Mallotus oblongifolius muell-Arg coarse powder;

(2) heating and refluxing the mallotus oblongifolius coarse powder obtained in the step (1) with water to extract to obtain a water extract;

(3) Filtering the water extracting solution in the step (2), and concentrating to obtain a concentrated solution;

(4) adding the concentrated solution obtained in the step (3) into ethanol, standing for a period of time, and filtering to obtain an alcohol precipitation solution;

(5) recovering ethanol from the ethanol precipitation solution, and concentrating to obtain concentrated solution;

(6) passing the concentrated solution in the step (5) through macroporous adsorption resin, eluting with water, discarding the eluent, eluting with ethanol, collecting the eluent, recovering ethanol, and concentrating under reduced pressure to obtain extract;

(7) and (4) drying and crushing the extract in the step (6) to obtain the partridge leaf extract.

preferably, the partridge leaf extract is prepared by the following method:

(1) Selecting, cleaning, drying and crushing Mallotus oblongifolius muell-Arg, then sieving with a 20-40 mesh sieve, and taking the sieved substances to obtain Mallotus oblongifolius muell-Arg coarse powder for later use;

(2) heating and refluxing the mallotus oblongifolius coarse powder obtained in the step (1) with water to extract to obtain a water extract;

(3) filtering the water extracting solution obtained in the step (2), and concentrating until the relative density is 1.0-1.2 to obtain a concentrated solution;

(4) Adding the concentrated solution obtained in the step (3) into 90-95% ethanol until the alcohol concentration is 50-80%, standing for 4-6 h, and filtering to obtain an alcohol precipitation solution;

(5) Recovering ethanol from the ethanol precipitation solution, and concentrating the ethanol precipitation solution until the relative density is 1.0-1.1 to obtain a concentrated solution;

(6) passing the concentrated solution in the step (5) through macroporous adsorption resin, eluting with 1-5 times of water, discarding the eluent, eluting with 1-5 times of 5-10% ethanol, collecting the eluent, recovering ethanol, and concentrating under reduced pressure until the relative density is 1.0-1.2 to obtain an extract;

(7) And (4) drying and crushing the extract in the step (6) by microwave to obtain the partridge leaf extract.

In another preferred embodiment, the preparation of the partridge leaf extract comprises the following specific operation steps:

(1) Selecting, cleaning, drying and crushing Mallotus oblongifolius muell-Arg, then sieving with a 20-mesh sieve, and taking the sieved product to obtain Mallotus oblongifolius muell-Arg coarse powder for later use;

(2) Heating and refluxing the mallotus oblongifolius coarse powder obtained in the step (1) with water to extract to obtain a water extract;

(3) filtering the water extracting solution obtained in the step (2), and concentrating until the relative density is 1.0-1.2 to obtain a concentrated solution;

(4) Adding the concentrated solution obtained in the step (3) into 90-95% ethanol until the alcohol concentration is 50-80%, standing for 4-6 h, and filtering to obtain an alcohol precipitation solution;

(5) recovering ethanol from the ethanol precipitation solution, and concentrating the ethanol precipitation solution until the relative density is 1.0-1.1 to obtain a concentrated solution;

(6) passing the concentrated solution in the step (5) through macroporous adsorption resin, eluting with 1-5 times of water, discarding the eluent, eluting with 1-5 times of 5-10% ethanol, collecting the eluent, recovering ethanol, and concentrating under reduced pressure until the relative density is 1.0-1.2 to obtain an extract;

(7) And (4) drying and crushing the extract in the step (6) by microwave to obtain the partridge leaf extract.

In another preferred embodiment, the preparation of the partridge leaf extract comprises the following specific operation steps:

(1) selecting, cleaning, drying and crushing Mallotus oblongifolius muell-Arg, then sieving with a 30-mesh sieve, and taking the sieved product to obtain Mallotus oblongifolius muell-Arg coarse powder for later use;

(2) Heating and refluxing the mallotus oblongifolius coarse powder obtained in the step (1) with water to extract to obtain a water extract;

(3) Filtering the water extracting solution obtained in the step (2), and concentrating until the relative density is 1.0-1.2 to obtain a concentrated solution;

(4) Adding the concentrated solution obtained in the step (3) into 90-95% ethanol until the alcohol concentration is 50-80%, standing for 4-6 h, and filtering to obtain an alcohol precipitation solution;

(5) Recovering ethanol from the ethanol precipitation solution, and concentrating the ethanol precipitation solution until the relative density is 1.0-1.1 to obtain a concentrated solution;

(6) Passing the concentrated solution in the step (5) through macroporous adsorption resin, eluting with 1-5 times of water, discarding the eluent, eluting with 1-5 times of 5-10% ethanol, collecting the eluent, recovering ethanol, and concentrating under reduced pressure until the relative density is 1.0-1.2 to obtain an extract;

(7) and (4) drying and crushing the extract in the step (6) by microwave to obtain the partridge leaf extract.

In another preferred embodiment, the preparation of the partridge leaf extract comprises the following specific operation steps:

(1) selecting, cleaning, drying and crushing Mallotus oblongifolius muell-Arg, then sieving with a 40-mesh sieve, and taking the sieved product to obtain Mallotus oblongifolius muell-Arg coarse powder for later use;

(2) heating and refluxing the mallotus oblongifolius coarse powder obtained in the step (1) with water to extract to obtain a water extract;

(3) Filtering the water extracting solution obtained in the step (2), and concentrating until the relative density is 1.0-1.2 to obtain a concentrated solution;

(4) adding the concentrated solution obtained in the step (3) into 90-95% ethanol until the alcohol concentration is 50-80%, standing for 4-6 h, and filtering to obtain an alcohol precipitation solution;

(5) recovering ethanol from the ethanol precipitation solution, and concentrating the ethanol precipitation solution until the relative density is 1.0-1.1 to obtain a concentrated solution;

(6) passing the concentrated solution in the step (5) through macroporous adsorption resin, eluting with 1-5 times of water, discarding the eluent, eluting with 1-5 times of 5-10% ethanol, collecting the eluent, recovering ethanol, and concentrating under reduced pressure until the relative density is 1.0-1.2 to obtain an extract;

(7) and (4) drying and crushing the extract in the step (6) by microwave to obtain the partridge leaf extract.

in another preferred example, in the step (6), the macroporous adsorbent resin is one of D101, DM130, GHP-8, XAD-16 and PRP-2A, preferably D101.

according to the technical scheme provided by the invention, the shampoo and the preparation method thereof can fully play the effects of moistening and replenishing water, relieving itching and protecting hair, improving rough hair and the like by adding the partridge leaf extract, and enabling the hair to be bright and glossy.

Detailed Description

The invention discloses a shampoo containing Mallotus oblongifolius muell-Arg extract and a preparation method thereof. The invention takes the partridge leaf extract as the functional component of the shampoo, fully utilizes the pharmacological characteristics of the partridge leaf, and realizes the effects of moistening and moisturizing, relieving itching and protecting hair, improving the problems of rough hair and the like, and enabling the hair to be bright and lustrous. The shampoo disclosed by the invention contains a large amount of protein, folic acid, pantothenic acid, aminobenzoic acid, selenium, lecithin, vitamin A, vitamin E, vitamin B2 and vitamin C, and has certain effects on yellowing and scorching of hair, thinning and dull hair, preventing white hair, frequently losing hair, splitting hair and scurf. The present invention will be further described below by way of specific examples, but it is noted that the present invention is not limited thereto.