阅读说明：本技术 一种高稳定性珍珠闪光丙烯墨水及其制备方法 (High-stability pearl flashing propylene ink and preparation method thereof ) 是由 张瀚 张胜红 于 2021-07-28 设计创作，主要内容包括：本发明涉及墨水制备的技术领域,特别是涉及一种高稳定性珍珠闪光丙烯墨水及其制备方法,其在暗环境中对使用珍珠闪光丙烯墨水制作的画作进行光照后,整个画面出现特别辉亮的视觉效果,能够更加突出绘画艺术品的感染力,吸引力；先将增稠剂和消泡剂加注进入蒸馏水中,经溶胀、加热搅拌至溶解,加入丙烯酸聚合物乳剂合并后搅拌均匀制成粘合剂,在粘合剂中加入颜料浆搅拌均匀,然后再加入分散剂搅拌均匀成粗浆料,将粗浆料加入到三辊研磨机料斗中研磨后加入杀菌剂、30目玻璃微珠和320目玻璃微珠,再从真空搅拌机中搅拌即可。(The invention relates to the technical field of ink preparation, in particular to high-stability pearl flash acrylic ink and a preparation method thereof, wherein after a painting made of the pearl flash acrylic ink is illuminated in a dark environment, the whole painting has a particularly bright visual effect, so that the infectivity and the attraction of the painting artwork can be more prominent; firstly, adding a thickening agent and a defoaming agent into distilled water, swelling, heating and stirring until the thickening agent and the defoaming agent are dissolved, adding an acrylic polymer emulsion, mixing, uniformly stirring to prepare an adhesive, adding a pigment slurry into the adhesive, uniformly stirring, then adding a dispersing agent, uniformly stirring to obtain a coarse slurry, adding the coarse slurry into a hopper of a three-roll grinder, grinding, adding a bactericide, 30-mesh glass beads and 320-mesh glass beads, and stirring from a vacuum stirrer.)

1. The high-stability pearl flashing propylene ink and the preparation method thereof are characterized in that the formula proportion comprises the following main components in parts by mass: 30-50 parts of acrylic polymer emulsion, 8-25 parts of distilled water, 0.5-2.0 parts of thickening agent, 5-30 parts of pigment slurry, 0.1-0.5 part of defoaming agent, 0.5-2.0 parts of dispersing agent, 0.2-2 parts of bactericide, 1-5 parts of 30-mesh glass beads and 4-10 parts of 320-mesh glass beads,

firstly, adding a thickening agent and a defoaming agent into distilled water, swelling, heating and stirring until the thickening agent and the defoaming agent are dissolved, adding an acrylic polymer emulsion, mixing, uniformly stirring to prepare an adhesive, adding a pigment slurry into the adhesive, uniformly stirring, then adding a dispersing agent, uniformly stirring to obtain a coarse slurry, adding the coarse slurry into a hopper of a three-roller grinder, grinding, adding a bactericide, 30-mesh glass beads and 320-mesh glass beads, and stirring from a vacuum stirrer.

2. The high-stability pearl flash propylene ink and the preparation method thereof according to claim 1, wherein the high-stability pearl flash propylene ink is processed by the following processing steps:

s1, adding 0.5-2.0 parts of thickening agent and 0.1-0.5 part of defoaming agent into 8-25 parts of distilled water, swelling for 6-12 hours, heating to 80-90 ℃, and heating for 0.5-1 hour to prepare adhesive glue solution;

s2, adding 30-50 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive;

s3, adding 5-30 parts of pigment slurry into the adhesive, stirring for 1-2 hours, then adding 0.5-2.0 parts of dispersing agent, and stirring uniformly to obtain a coarse slurry;

s4, adding the coarse slurry into a hopper of a three-roll grinder for grinding, and grinding for 3-5 times by the three-roll grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 10 mu m;

s5, adding 0.2-2 parts of bactericide, 1-5 parts of 30-mesh glass beads and 4-10 parts of 320-mesh glass beads into the ground color slurry, stirring for 2-3 hours in a vacuum stirrer, and uniformly stirring;

and S6, guiding the ink liquid obtained by stirring to flow into a storage barrel to obtain the finished product.

3. The highly stable pearl glitter acrylic ink and the preparation method thereof according to claim 1, wherein the thickener is one of polyacrylamide thickener, white carbon black, bentonite, organic bentonite, activated calcium carbonate, hydrogenated castor oil, calcium stearate, aluminum stearate, zinc stearate and polymerized vegetable oil.

4. The highly stable pearl glitter acrylic ink and the method of manufacturing the same according to claim 1, wherein the antifoaming agent is one of monoamide, bisamide, trialkyl melamine, cyanuric chloride melamine, aliphatic amine, monoalkyl, dialkyl phosphate and fluorinated alkyl phosphate.

5. The highly stable pearl glitter propylene ink and the preparation method thereof according to claim 2, wherein the cooling temperature of the roller is 38-42 ℃.

6. The high-stability pearl flash acrylic ink and the preparation method thereof as claimed in claim 2, wherein the vacuum degree of the vacuum stirrer is-0.092 to-0.096 MPa, and the stirring speed is 180 to 210 r/min.

7. The high-stability pearl flash acrylic ink and the preparation method thereof according to claim 1, wherein the glass beads are high-brightness organic glass beads, are light in weight and are easy to suspend.

8. The highly stable pearl glitter propylene ink and the preparation method thereof according to claim 1, wherein the dispersant is one of polyethylene oxide, low viscosity methyl silicone oil, lecithin and derivatives thereof.

Technical Field

The invention relates to the technical field of ink preparation, in particular to high-stability pearl flashing propylene ink and a preparation method thereof.

Background

Acrylic ink is a drawing pigment, a dispersible pigment made of polymethyl methacrylate (PMMA) dissolved in mineral spirits, supplemented with pigments, sometimes called pure acrylic or plastic pigments. Because of the characteristics of easy film formation, easy dyeing, good rigidity, weak polarity, high transparency and the like of PMMA, the ink performance is superior to that of a polymeric pigment prepared by containing propylene and other water-soluble resins. The characteristics of the acrylic ink are that the acrylic ink does not yellow and is quick to dry, and the acrylic ink is easy to wash away by mineral alcohol or turpentine, so that the acrylic ink is suitable for repairing paintings in painting preservation work, is used for repairing damaged or smeared parts, such as repairing and protecting of Brilliant murals, and is very difficult work.

The existing acrylic pigment product for fine arts only presents a general visual effect when being illuminated in a dark environment, cannot reflect the color of the pigment, has low drawing aesthetic degree, and cannot reflect the artistic charm because the formed fine arts and artworks lack the aesthetic feeling of appreciation. If the art is dark and dull, the eyes of people are difficult to attract. The pearl flash microspheres are ingeniously applied and dispersed in the acrylic ink, so that the painted artworks and artworks are lifelike and flash, and the artistic paper has an aesthetic feeling of being on a piece of natural paper.

Disclosure of Invention

In order to solve the technical problems, the invention provides the high-stability pearl flashing propylene ink and the preparation method thereof. The painting made by the ink has a particularly bright visual effect after being illuminated in a dark environment, and can more highlight the infectivity and the attraction of the painting artworks, so that the painting artworks are vivid, and figures and other artistic images jump on the paper.

The invention relates to a high-stability pearl flashing propylene ink and a preparation method thereof, wherein the formula comprises the following components in parts by mass: 30-50 parts of acrylic polymer emulsion, 8-25 parts of distilled water, 0.5-2.0 parts of thickening agent, 5-30 parts of pigment slurry, 0.1-0.5 part of defoaming agent, 0.5-2.0 parts of dispersing agent, 0.2-2 parts of bactericide, 1-5 parts of 30-mesh glass beads and 4-10 parts of 320-mesh glass beads,

firstly, adding a thickening agent and a defoaming agent into distilled water, swelling, heating and stirring until the thickening agent and the defoaming agent are dissolved, adding an acrylic polymer emulsion, mixing, uniformly stirring to prepare an adhesive, adding a pigment slurry into the adhesive, uniformly stirring, then adding a dispersing agent, uniformly stirring to obtain a coarse slurry, adding the coarse slurry into a hopper of a three-roller grinder, grinding, adding a bactericide, 30-mesh glass beads and 320-mesh glass beads, and stirring from a vacuum stirrer.

The invention relates to a high-stability pearl flashing propylene ink and a preparation method thereof, which is characterized by comprising the following processing steps:

s1, adding 0.5-2.0 parts of thickening agent and 0.1-0.5 part of defoaming agent into 8-25 parts of distilled water, swelling for 6-12 hours, heating to 80-90 ℃, and heating for 0.5-1 hour to prepare adhesive glue solution;

s2, adding 30-50 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive;

s3, adding 5-30 parts of pigment slurry into the adhesive, stirring for 1-2 hours, then adding 0.5-2.0 parts of dispersing agent, and stirring uniformly to obtain a coarse slurry;

s4, adding the coarse slurry into a hopper of a three-roll grinder for grinding, and grinding for 3-5 times by the three-roll grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 10 mu m;

s5, adding 0.2-2 parts of bactericide, 1-5 parts of 30-mesh glass beads and 4-10 parts of 320-mesh glass beads into the ground color slurry, stirring for 2-3 hours in a vacuum stirrer, and uniformly stirring;

and S6, guiding the ink liquid obtained by stirring to flow into a storage barrel to obtain the finished product.

The invention discloses high-stability pearl flashing acrylic ink and a preparation method thereof.

The invention discloses high-stability pearl flashing acrylic ink and a preparation method thereof.

The invention relates to high-stability pearl flashing propylene ink and a preparation method thereof, which are characterized in that the cooling temperature of a roller is 38-42 ℃.

The invention relates to high-stability pearl flash propylene ink and a preparation method thereof, which are characterized in that the working vacuum degree of a vacuum stirrer is-0.092 to-0.096 MPa, and the stirring rotating speed is 180 to 210 r/min.

The high-stability pearl flashing acrylic ink and the preparation method thereof are characterized in that the glass beads are high-brightness organic glass beads, are light in weight and are easy to suspend.

The invention relates to high-stability pearl flashing propylene ink and a preparation method thereof.

The invention has the beneficial effects that: firstly, adding a thickening agent and a defoaming agent into distilled water, swelling, heating and stirring until the thickening agent and the defoaming agent are dissolved, adding an acrylic polymer emulsion, mixing, uniformly stirring to prepare an adhesive, adding a pigment slurry into the adhesive, uniformly stirring, then adding a dispersing agent, uniformly stirring to obtain a coarse slurry, adding the coarse slurry into a hopper of a three-roller grinder, grinding, adding a bactericide, 30-mesh glass beads and 320-mesh glass beads, and stirring from a vacuum stirrer; because the high-refraction glass beads are used in the ink formula, when light irradiates on the surfaces of the beads, the light is condensed on the special reflecting layer at the focus of the glass beads due to the high refraction effect of the glass beads, and the reflecting layer reflects the light, so that very bright reflected light can be seen, the light transmits through the ink film when being reflected, the color of the ink is reflected, after the pearl flash acrylic ink is used for drawing, after the light is used for illumination in a dark environment, the whole picture has a particularly bright visual effect, and the infectivity and the attraction of a drawing artwork can be more highlighted.

Detailed Description

The following examples are given to further illustrate the embodiments of the present invention. The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.

Adding 0.5-2.0 parts of thickening agent and 0.1-0.5 part of defoaming agent into 8-25 parts of distilled water, swelling for 6-12 hours, heating to 80-90 ℃, and heating for 0.5-1 hour to prepare adhesive glue solution; adding 30-50 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive; adding 5-30 parts of pigment slurry into the adhesive, stirring for 1-2 hours, then adding 0.5-2.0 parts of dispersing agent, and uniformly stirring to obtain crude slurry; adding the coarse slurry into a hopper of a three-roller grinder for grinding, and grinding for 3-5 times by the three-roller grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 10 mu m; adding 0.2-2 parts of bactericide, 1-5 parts of 30-mesh glass beads and 4-10 parts of 320-mesh glass beads into the ground color slurry, stirring for 2-3 hours in a vacuum stirrer, and uniformly stirring; the ink liquid obtained by stirring is guided to flow into the storage barrel, and the finished product is obtained.

Example 1

Adding 0.5 part of thickening agent and 0.5 part of defoaming agent into 20 parts of distilled water, swelling for 6 hours, heating to 80 ℃, and heating for 0.5 hour to prepare an adhesive glue solution; adding 45 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive; adding 22 parts of pigment slurry into the adhesive, stirring for 1 hour, adding 1 part of dispersing agent, and uniformly stirring to obtain crude slurry; adding the coarse slurry into a hopper of a three-roller grinder for grinding, and grinding for 3 times by the three-roller grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 10 mu m; adding 1 part of bactericide, 2 parts of 30-mesh glass beads and 8 parts of 320-mesh glass beads into the ground color slurry, stirring for 2 hours in a vacuum stirrer, and uniformly stirring; the ink liquid obtained by stirring is guided to flow into the storage barrel, and the finished product is obtained.

Example 2

Adding 2 parts of thickening agent and 0.3 part of defoaming agent into 22 parts of distilled water, swelling for 8 hours, heating to 80 ℃, and heating for 0.5 hour to prepare an adhesive glue solution; adding 36 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive; adding 22 parts of pigment slurry into the adhesive, stirring for 2 hours, adding 0.7 part of dispersing agent, and uniformly stirring to obtain crude slurry; adding the coarse slurry into a hopper of a three-roller grinder for grinding, and grinding for 5 times by the three-roller grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 5 mu m; adding 2 parts of bactericide, 5 parts of 30-mesh glass beads and 10 parts of 320-mesh glass beads into the ground color slurry, stirring for 3 hours in a vacuum stirrer, and uniformly stirring; the ink liquid obtained by stirring is guided to flow into the storage barrel, and the finished product is obtained.

Example 3

Adding 1 part of thickening agent and 0.5 part of defoaming agent into 8 parts of distilled water, swelling for 12 hours, heating to 80 ℃, and heating for 1 hour to prepare an adhesive glue solution; adding 50 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive; adding 30 parts of pigment slurry into the adhesive, stirring for 1 hour, adding 0.5 part of dispersing agent, and uniformly stirring to obtain crude slurry; adding the coarse slurry into a hopper of a three-roller grinder for grinding, and grinding for 5 times by the three-roller grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 8 mu m; adding 1 part of bactericide, 1 part of 30-mesh glass beads and 8 parts of 320-mesh glass beads into the ground color slurry, stirring for 3 hours in a vacuum stirrer, and uniformly stirring; the ink liquid obtained by stirring is guided to flow into the storage barrel, and the finished product is obtained.

Example 4

Adding 2 parts of thickening agent and 0.1 part of defoaming agent into 25 parts of distilled water, swelling for 10 hours, heating to 90 ℃, and heating for 1 hour to prepare an adhesive glue solution; adding 50 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive; adding 12 parts of pigment slurry into the adhesive, stirring for 2 hours, adding 1 part of dispersing agent, and uniformly stirring to obtain crude slurry; adding the coarse slurry into a hopper of a three-roller grinder for grinding, and grinding for 4 times by the three-roller grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 5 mu m; adding 0.9 part of bactericide, 5 parts of 30-mesh glass beads and 4 parts of 320-mesh glass beads into the ground color slurry, stirring for 2 hours in a vacuum stirrer, and uniformly stirring; the ink liquid obtained by stirring is guided to flow into the storage barrel, and the finished product is obtained.

Example 5

Adding 1.5 parts of thickening agent and 0.3 part of defoaming agent into 25 parts of distilled water, swelling for 8 hours, heating to 80 ℃, and heating for 0.5 hour to prepare adhesive glue solution; adding 30 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive; adding 27 parts of pigment slurry into the adhesive, stirring for 2 hours, adding 2 parts of dispersing agent, and uniformly stirring to obtain crude slurry; adding the coarse slurry into a hopper of a three-roller grinder for grinding, and grinding for 3 times by the three-roller grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 5 mu m; adding 0.2 part of bactericide, 4 parts of 30-mesh glass beads and 10 parts of 320-mesh glass beads into the ground color slurry, stirring for 2 hours in a vacuum stirrer, and uniformly stirring; the ink liquid obtained by stirring is guided to flow into the storage barrel, and the finished product is obtained.

Example 6

Adding 1.5 parts of thickening agent and 0.5 part of defoaming agent into 25 parts of distilled water, swelling for 10 hours, heating to 80 ℃, and heating for 1 hour to prepare an adhesive glue solution; adding 50 parts of acrylic polymer emulsion into the adhesive glue solution, and stirring the mixture until the mixture is uniform to prepare an adhesive; adding 5 parts of pigment slurry into the adhesive, stirring for 1 hour, adding 2 parts of dispersing agent, and uniformly stirring to obtain crude slurry; adding the coarse slurry into a hopper of a three-roller grinder for grinding, and grinding for 3 times by the three-roller grinder; the roller is cooled by circulating water, and the fineness of the ground color sizing material is below 10 mu m; adding 1 part of bactericide, 5 parts of 30-mesh glass beads and 10 parts of 320-mesh glass beads into the ground color slurry, stirring for 3 hours in a vacuum stirrer, and uniformly stirring; the ink liquid obtained by stirring is guided to flow into the storage barrel, and the finished product is obtained.

The above description is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, several modifications and variations can be made without departing from the technical principle of the present invention, and these modifications and variations should also be regarded as the protection scope of the present invention.