阅读说明：本技术 一种臭氧油及其制备方法 (Ozone oil and preparation method thereof ) 是由 王梅 于 2021-08-23 设计创作，主要内容包括：本发明公开的属于臭氧油技术领域,具体为一种臭氧油及其制备方法,S1：采用PEM膜用低压直流导通固态膜电极的正负两极电解去离子水,水在特殊的阳极溶液界面上以质子交换的形式被分离为氢氧分子,氢从阴极溶液界面上直接被排放,氧分子在阳极介面上因高密度电流产生的电子激发而获得能量,并聚合成臭氧分子,将臭氧分子进行收集,从而得到臭氧,S2：将橄榄油加入到臭氧油固化反应器中,并向臭氧油固化反应器中通入步骤S1中得到的臭氧,使臭氧与橄榄油结合,本发明的臭氧油制备工艺操作简单,制备流程较少,降低了臭氧油的制备成本,从而能够相应降低臭氧油的售价,便于臭氧油的推广使用,方便开拓市场。(The invention belongs to the technical field of ozone oil, and particularly relates to ozone oil and a preparation method thereof, wherein S1: adopting a PEM membrane to conduct positive and negative electrodes of a solid membrane electrode through low-voltage direct current to electrolyze deionized water, separating water into hydroxyl molecules in a proton exchange mode on a special anode solution interface, directly discharging hydrogen from a cathode solution interface, obtaining energy by exciting the oxygen molecules on the anode interface due to electrons generated by high-density current, polymerizing the energy into ozone molecules, and collecting the ozone molecules to obtain ozone, S2: the olive oil is added into the ozone oil curing reactor, and the ozone obtained in the step S1 is introduced into the ozone oil curing reactor, so that the ozone and the olive oil are combined.)

1. An ozone oil, characterized in that: the ozone oil raw material is prepared from the following components in parts by weight:

60-106 parts of ozone, 850 parts of olive oil 800-.

2. The ozone oil of claim 1, wherein: the ozone oil raw material is prepared from the following components in parts by weight:

60 parts of ozone, 800 parts of olive oil, 4 parts of linoleic acid, 8 parts of linolenic acid, 3 parts of arachidonic acid, 6 parts of oleic acid and 10 parts of peppermint oil.

3. The ozone oil of claim 1, wherein: the ozone oil raw material is prepared from the following components in parts by weight:

83 parts of ozone, 825 parts of olive oil, 5 parts of linoleic acid, 9 parts of linolenic acid, 4 parts of arachidonic acid, 7 parts of oleic acid and 12 parts of peppermint oil.

4. The ozone oil of claim 1, wherein: the ozone oil raw material is prepared from the following components in parts by weight:

106 parts of ozone, 850 parts of olive oil, 6 parts of linoleic acid, 10 parts of linolenic acid, 5 parts of arachidonic acid, 8 parts of oleic acid and 14 parts of peppermint oil.

5. A process for the preparation of an ozonized oil according to any one of claims 1 to 4, characterized in that: the method comprises the following steps:

s1: adopting a PEM membrane to conduct positive and negative electrodes of a solid membrane electrode by low-voltage direct current to electrolyze deionized water, separating water into oxyhydrogen molecules in a proton exchange mode on a special anode solution interface, directly discharging hydrogen from a cathode solution interface, obtaining energy by exciting the oxygen molecules on the anode interface due to electrons generated by high-density current, polymerizing the energy into ozone molecules, and collecting the ozone molecules to obtain ozone;

s2: adding olive oil into an ozone oil curing reactor, and introducing the ozone obtained in the step S1 into the ozone oil curing reactor to combine the ozone with the olive oil;

s3: and (4) adding linoleic acid, linolenic acid, arachidonic acid, oleic acid and peppermint oil into the olive oil obtained in the step S2, and then stirring to obtain the ozone oil.

S4: and (5) sterilizing the ozone oil obtained in the step (S3), and bottling and sealing the ozone oil after the sterilization is finished.

6. The process of claim 5, wherein the ozone oil is prepared by the following steps: in the step S3, the stirring time is 30-40 min.

7. The process of claim 5, wherein the ozone oil is prepared by the following steps: in the step S4, the sterilization mode adopts ultraviolet sterilization, the sterilization time is 40-60min, and the temperature of the sterilization environment is 20-40 ℃.

8. The process of claim 5, wherein the ozone oil is prepared by the following steps: and in the step S4, after the ozone oil is bottled and sealed, the bottle is refrigerated and stored.

Technical Field

The invention relates to the technical field of ozone oil, in particular to ozone oil and a preparation method thereof.

Background

Ozone oil is based on olive oil, which is rich in 80% oleic acid (18: in ═ 6), and 1.0g of oil can absorb up to 160mg of ozone. Analysis after ozonization the modification characteristics were analyzed by Nuclear Magnetic Resonance (NMR) chromatography and the new carbon signal was found to correlate with a Criegee ozonide peak near 105 ppm. At 130ppm the olefinic carbon signal was completely absent, carbonyl compounds and carboxylic acids were absent, and the conclusion was drawn by combining resonance chromatography data, elemental analysis and High Performance Liquid Chromatography (HPLC). Long-term ozonation results in the formation of a special glycerol trimolecular ozone compound, i.e., an ozonized oil.

The existing ozone oil preparation method is complex, the preparation cost of the ozone oil is high, and the popularization and the use of the ozone oil are not facilitated.

Disclosure of Invention

The invention aims to provide ozone oil and a preparation method thereof, and aims to solve the problems that the existing preparation method of ozone oil in the background art is complex, the preparation cost of ozone oil is high, and the ozone oil is not beneficial to popularization and use.

In order to achieve the purpose, the invention provides the following technical scheme: the ozone oil raw material is prepared from the following components in parts by weight:

60-106 parts of ozone, 850 parts of olive oil 800-.

Preferably, the ozone oil raw material is prepared from the following components in parts by weight:

60 parts of ozone, 800 parts of olive oil, 4 parts of linoleic acid, 8 parts of linolenic acid, 3 parts of arachidonic acid, 6 parts of oleic acid and 10 parts of peppermint oil.

Preferably, the ozone oil raw material is prepared from the following components in parts by weight:

83 parts of ozone, 825 parts of olive oil, 5 parts of linoleic acid, 9 parts of linolenic acid, 4 parts of arachidonic acid, 7 parts of oleic acid and 12 parts of peppermint oil.

Preferably, the ozone oil raw material is prepared from the following components in parts by weight:

106 parts of ozone, 850 parts of olive oil, 6 parts of linoleic acid, 10 parts of linolenic acid, 5 parts of arachidonic acid, 8 parts of oleic acid and 14 parts of peppermint oil.

A preparation process of ozone oil comprises the following steps:

s1: adopting a PEM membrane to conduct positive and negative electrodes of a solid membrane electrode by low-voltage direct current to electrolyze deionized water, separating water into oxyhydrogen molecules in a proton exchange mode on a special anode solution interface, directly discharging hydrogen from a cathode solution interface, obtaining energy by exciting the oxygen molecules on the anode interface due to electrons generated by high-density current, polymerizing the energy into ozone molecules, and collecting the ozone molecules to obtain ozone;

s2: adding olive oil into an ozone oil curing reactor, and introducing the ozone obtained in the step S1 into the ozone oil curing reactor to combine the ozone with the olive oil;

s3: and (4) adding linoleic acid, linolenic acid, arachidonic acid, oleic acid and peppermint oil into the olive oil obtained in the step S2, and then stirring to obtain the ozone oil.

S4: and (5) sterilizing the ozone oil obtained in the step (S3), and bottling and sealing the ozone oil after the sterilization is finished.

Preferably, in the step S3, the stirring time is 30-40 min.

Preferably, in step S4, the sterilization mode is ultraviolet sterilization, the sterilization time is 40-60min, and the sterilization environment temperature is 20-40 ℃.

Preferably, in step S4, the ozone oil is filled in bottles and sealed, and then stored in cold storage.

Compared with the prior art, the invention has the beneficial effects that:

1) the preparation process of the ozone oil is simple to operate, the preparation flow is less, and the preparation cost of the ozone oil is reduced, so that the price of the ozone oil can be correspondingly reduced, the ozone oil is convenient to popularize and use, and the market is convenient to develop;

2) the method is characterized in that a PEM membrane is adopted to conduct positive and negative electrodes of a solid membrane electrode through low-voltage direct current to electrolyze deionized water, water is separated into hydrogen and oxygen molecules in a proton exchange mode on a special anode solution interface, hydrogen is directly discharged from a cathode solution interface, the oxygen molecules obtain energy on the anode interface due to the excitation of electrons generated by high-density current and are polymerized into ozone molecules, and the ozone molecules are collected to obtain ozone, so that the collected ozone has high concentration, does not contain nitrogen and oxygen compounds, does not contain carcinogenic substances, and avoids harming the body health of a user.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "top/bottom", and the like, indicate orientations or positional relationships for convenience in describing the present invention and simplifying the description, but do not indicate or imply that the referred device or element must have a particular orientation, be constructed and operated in a particular orientation, and thus should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.

In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "sleeved/connected," "connected," and the like are to be construed broadly, e.g., "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.

The invention provides a technical scheme that: the ozone oil is prepared from the following raw materials in parts by weight:

60-106 parts of ozone, 850 parts of olive oil 800-.

A preparation process of ozone oil comprises the following steps:

s1: adopting a PEM membrane to conduct positive and negative electrodes of a solid membrane electrode by low-voltage direct current to electrolyze deionized water, separating water into oxyhydrogen molecules in a proton exchange mode on a special anode solution interface, directly discharging hydrogen from a cathode solution interface, obtaining energy by exciting the oxygen molecules on the anode interface due to electrons generated by high-density current, polymerizing the energy into ozone molecules, and collecting the ozone molecules to obtain ozone;

s2: adding olive oil into an ozone oil curing reactor, and introducing the ozone obtained in the step S1 into the ozone oil curing reactor to combine the ozone with the olive oil;

s3: and (4) adding linoleic acid, linolenic acid, arachidonic acid, oleic acid and peppermint oil into the olive oil obtained in the step S2, and then stirring to obtain the ozone oil.

S4: and (5) sterilizing the ozone oil obtained in the step (S3), and bottling and sealing the ozone oil after the sterilization is finished.

In the step S3, the stirring time is 30-40 min.

In the step S4, the sterilization mode adopts ultraviolet sterilization, the sterilization time is 40-60min, and the temperature of the sterilization environment is 20-40 ℃.

And in the step S4, after the ozone oil is bottled and sealed, the bottle is refrigerated and stored.

The ozone oil application has the following characteristics:

1. broad spectrum property: ozone has the effect of killing various pathogenic microorganisms such as bacteria, fungi, viruses, molds, mycoplasma, chlamydia, trichomonas vaginalis and the like, and ozone destroys the structure of a microbial membrane by oxidation to realize the sterilization effect.

2. Rapidity: after the ozone reaches a certain degree (the ozone content per gram is 8-9.6mg), pathogenic microorganisms can be killed within seconds to minutes, the disinfectant is the fastest one of the known disinfectants, the ozone content of domestic similar products is lower than 7mg/L at present, and the only product exceeding the value is the Oudeler ozone oil product.

3. Safety: the acute toxicity experiment of ozone shows that LD50 is more than 500mg/kg, is nontoxic, has no stimulation to skin, mucosa and eyes, and has no harm and toxicity to healthy cells due to the strong oxidation balance enzyme system of the healthy cells, and the byproducts of ozone after killing pathogenic microorganisms are oxygen and gaseous water molecules.

4. Penetrability: due to O₃Has small molecular weight, strong penetration to cell tissue, and permeability of 2mm to mucosaTo the inner wall of pathogenic microorganism cells.

5. No drug resistance: because of the action mechanism of ozone, the genetic material of pathogenic microorganisms is directly decomposed, irreversible death occurs, and the medicine is different from common antibiotics and antiviral ointments, so that the medicine resistance is not generated.

6. The dual property: the byproducts generated by ozone killing and killing pathogenic microorganisms are oxygen and gaseous water molecules which can be absorbed by cell tissues, accelerate blood circulation and promote the healing of the skin of an affected part.

The ozone oil also has the following effects:

1. clearing away toxic garbage in vagina and uterus, promoting cell regeneration, contracting vagina, increasing vagina wall elasticity, improving sexual desire, and reproducing virginal state.

2. Remove the hard pigmentation and spots on the face, improve the dark yellow face and make the skin delicate and ruddy.

3. Improving soreness of knee and waist, asthenia, promoting estrogen secretion, activating cell to plump breast, balancing endocrine, and preventing various gynecological diseases caused by vaginal unclean.

4. Recovering vaginal muscle activity, improving vaginal elasticity, tightening vagina, improving sexual feeling, promoting puerperal uterine contraction, promoting metabolism, and eliminating lochia.

5. It can be used for treating senile vaginitis, cervicitis, cervical erosion, endometritis, pelvic inflammatory disease, adnexitis, etc., and infection of mold, Candida, and Candida albicans.

6. It can kill gonococcus, mycoplasma and venereal diseases infected by various viruses, such as condyloma acuminatum, herpes zoster, gonorrhea, etc., and has good effects on female dysmenorrhea, abnormal menstrual period, low libido, and vaginal relaxation.

Example 1:

the method comprises the steps of electrolyzing deionized water by adopting a PEM membrane through a positive electrode and a negative electrode of a solid membrane electrode in a low-voltage direct current mode, separating water into hydrogen and oxygen molecules in a proton exchange mode on a special anode solution interface, directly discharging hydrogen from a cathode solution interface, exciting the oxygen molecules on the anode interface by electrons generated by high-density current to obtain energy, polymerizing the energy into ozone molecules, collecting the ozone molecules to obtain ozone, adding 800g of olive oil into an ozone oil curing reactor, introducing 60g of ozone into the ozone oil curing reactor to combine the ozone with the olive oil, adding 4g of linoleic acid, 8g of linolenic acid, 3g of arachidonic acid, 6g of oleic acid and 10g of mint oil into the olive oil, stirring to obtain the ozone oil, sterilizing the ozone oil, bottling the ozone oil and sealing after the sterilization treatment is finished.

Example 2:

electrolyzing deionized water by adopting a PEM membrane and conducting positive and negative poles of a solid membrane electrode by using low-voltage direct current, separating water into hydrogen and oxygen molecules in a proton exchange mode on a special anode solution interface, directly discharging hydrogen from a cathode solution interface, exciting the oxygen molecules on the anode interface by electrons generated by high-density current to obtain energy, polymerizing the energy into ozone molecules, collecting the ozone molecules to obtain ozone, adding 825g of olive oil into an ozone oil curing reactor, introducing 83g of ozone into the ozone oil curing reactor to combine the ozone with the olive oil, adding 5g of linoleic acid, 9g of linolenic acid, 4g of arachidonic acid, 7g of oleic acid and 12g of mint oil into the olive oil, stirring to obtain the ozone oil, sterilizing the ozone oil, bottling the ozone oil and sealing after the sterilization treatment is finished.

Example 3:

electrolyzing deionized water by adopting a PEM membrane and conducting positive and negative poles of a solid membrane electrode by using low-voltage direct current, separating water into hydrogen and oxygen molecules in a proton exchange mode on a special anode solution interface, directly discharging hydrogen from a cathode solution interface, exciting the oxygen molecules on the anode interface by electrons generated by high-density current to obtain energy, polymerizing the energy into ozone molecules, collecting the ozone molecules to obtain ozone, adding 850g of olive oil into an ozone oil curing reactor, introducing 106g of ozone into the ozone oil curing reactor to combine the ozone with the olive oil, adding 6g of linoleic acid, 10g of linolenic acid, 5g of arachidonic acid, 8g of oleic acid and 14g of mint oil into the olive oil, stirring to obtain the ozone oil, sterilizing the ozone oil, bottling the ozone oil and sealing after the sterilization treatment is finished.

The ozonized oil finally obtained in examples 1 to 3 was subjected to a bacteria inhibition test, with the specific parameters as given in the following table:

while there have been shown and described the fundamental principles and essential features of the invention and advantages thereof, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but is capable of other specific forms without departing from the spirit or essential characteristics thereof; the present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.