阅读说明：本技术 一种防霉藤条的制备方法 (Preparation method of mildew-proof rattan ) 是由 李明 李东猛 于 2021-10-18 设计创作，主要内容包括：本发明涉及一种防霉藤条的制备方法,属于藤制品加工技术领域,该处理方法包括藤条采收、浸泡防霉液、微波加热、烘制处理和负压浸漆工序。利用藤条采收后仍保持活性可继续进行光合作用和呼吸作用,将防霉液送入藤条的内部,在后续烘干过程中,内部水分蒸发,将防霉成分弥散至整个藤条中,使得整个藤条机体都具有防霉效果,之后采用微波加热处理,对藤条内部进行灭菌并杀死蛀虫及虫卵,此外,烘制过程中,在藤条表面重复喷洒防霉液并烘干,在藤条表面形成强防霉层,防止藤条感染霉菌发生霉变,采用抽真空将藤条表面细小裂纹中的空气抽出,卸压后面漆填充进藤条裂纹之间,将藤条有效与外界环境隔开,防止霉菌侵入藤条导致霉变。(The invention relates to a preparation method of mildew-proof rattan, belonging to the technical field of rattan product processing. Still keep the activity after utilizing the rattan to gather and can continue to carry out photosynthesis and respiration, the inside of rattan is sent into to mould proof liquid, in follow-up stoving in-process, inside moisture evaporates, disperse mould proof composition to whole rattan in, make whole rattan organism all have mould proof effect, later adopt microwave heating to handle, disinfect and kill moth and ovum to the rattan inside, furthermore, in the baking process, repeatedly spray mould proof liquid and dry on the rattan surface, form strong mould proof layer on the rattan surface, prevent that the rattan from infecting the mould and taking place to milden, adopt the air in the tiny crackle of evacuation with rattan surface to take out, the finish is filled into between the rattan crackle after the release, effectively separate the rattan with external environment, prevent that mould from invading the rattan and lead to milden.)

1. The preparation method of the mildew-proof rattan is characterized by comprising the following steps:

step 1: collecting fresh rattan bundles for standby;

step 2: soaking the bottom of the rattan collected in the step 1 in mildew-proof liquid, and soaking and culturing for 2-3d in a shady and ventilated environment;

and step 3: removing impurity branches, vine leaves and skins of the rattans soaked in the step 2, and then heating by microwave;

and 4, step 4: weaving and forming the rattans processed in the step 3, and then baking;

and 5: and (4) immersing the rattan processed in the step (4) into a sealing tank filled with finish paint, vacuumizing the sealing tank, maintaining the pressure, releasing the pressure, taking out the rattan, leveling the finish paint, and naturally curing to obtain the mildew-proof rattan.

2. The method for preparing the mildew-proof rattan according to claim 1, wherein in the step 1, the rattan is cut off at an inclination of 45 degrees when being harvested.

3. The method for preparing the mildew-proof rattan according to claim 1, wherein in the step 2, the rattan is soaked in the mildew-proof solution to a depth of 30-50 cm.

4. The preparation method of the mildew-proof rattan according to claim 1, wherein the mildew-proof solution is a diluent of an extract of wormwood and camphor tree leaves, and the preparation process comprises the following steps:

step A1: adding fresh wormwood and camphor tree leaves into a stamping machine according to the dosage-mass ratio of 1:2.5-4, adding tap water which is 0.5 times of the total weight of the wormwood and the camphor tree leaves, stamping and filtering to obtain stamping liquid;

step A2: heating the stamping liquid to 35-42 ℃, stirring and concentrating to half of the original volume, and then pouring into an activated carbon filter element for decolorization to obtain mother liquor;

step A3: and blending the mother liquor and tap water according to the volume ratio of 1:20-25 to obtain the mildew-proof liquid.

5. The method for preparing the mildew-proof rattan according to claim 1, wherein in the step 3, the surface temperature of the rattan is controlled to be 75-85 ℃ during microwave heating, and the treatment time is 20-30 min.

6. The preparation method of the mildew-proof rattan according to claim 1, wherein in the step 4, the specific operation process of the baking treatment is as follows: and (3) drying the rattan at the temperature of 110-.

7. The method for preparing the mildew-proof rattan according to claim 6, wherein the spraying amount of the mildew-proof liquid is 15-20 mL/kg.

8. The method for preparing mildew-proof rattan according to claim 1, wherein in the step 5, vacuum is applied to a vacuum degree of 5-7kPa, and the dwell time is 12-17 min.

Technical Field

The invention belongs to the technical field of rattan product processing, and particularly relates to a preparation method of a mildew-proof rattan.

Background

The rattan plaited product is a handcraft widely spread among China, and is a 'plaited basket, a plaited basket and a family' because the raw material source of the technology is very wide. Rattan woven ware is of various types, including various types such as mats, baskets, dustpans, basketries, rattan boxes, shallow baskets, basket baskets, strainer, and food trays. A variety of products such as laundry baskets, flower pot sets, picnic cutlery baskets, hanging baskets, lampshades, kennels, cat nests, bird nests, etc. have been formed through advanced processing and development.

Rattan products take rattans as main raw materials, but the rattans are easy to grow insects and mildew and rot in the using process, so that the service life of the woven products is shortened. Therefore, the rattan needs to be treated before using, and the chemical agent is mostly used for soaking treatment at present, but the chemical agent is often stronger in toxicity and more serious in residue, and toxic residues are often caused to leak in the use process of woven fabrics, so that the health of a user is affected.

Disclosure of Invention

In order to overcome the technical problems mentioned in the background technology, the invention aims to provide a preparation method of mildew-proof rattan.

The purpose of the invention can be realized by the following technical scheme:

the preparation method of the mildew-proof rattan comprises the following steps:

step 1: mature fresh rattans are cut down from the roots at an angle of 45 degrees and harvested, so that the rattans can absorb mildew-proof liquid later, and then are bundled for later use;

step 2: soaking the bottom of the rattan bundled up in a mildew-proof solution, controlling the soaking depth of the rattan in the mildew-proof solution to be 30-50cm, placing the rattan in a shady ventilation environment for soaking and culturing for 2-3d, keeping the activity of the rattan after being cut down, continuously performing photosynthesis and respiration on the miscellaneous branches and rattan leaves on the rattan, absorbing water from the bottom of the rattan, sucking the mildew-proof solution into the rattan through a conduit in the rattan, and performing mildew prevention on the interior of the rattan;

and step 3: removing impurity branches, rattan leaves and skins of the rattan processed in the step 2, then placing the rattan into microwave heating equipment for heating, killing moth and worm eggs in the rattan, preventing the rattan from being eaten by moth silkworms in the subsequent processing process, integrally heating the rattan through microwave heating, avoiding toughness reduction caused by excessive water loss of the rattan, and facilitating weaving and processing of the rattan;

and 4, step 4: weaving and molding the rattan processed in the step 3 according to design requirements, and then placing the woven rattan into drying equipment for drying treatment;

and 5: and (4) immersing the rattan processed in the step (4) into a sealing tank filled with finish paint, vacuumizing the sealing tank, maintaining the pressure, pumping out air in fine cracks on the surface of the rattan, removing bubbles from the finish paint, releasing the pressure, filling the finish paint between the cracks on the surface of the rattan, enabling the rattan to be densely filled with the finish paint, effectively separating the rattan from the external environment, preventing the rattan from mildewing, taking out the rattan after the pressure is released, leveling, and naturally curing to obtain the mildew-proof rattan.

Further, the mildew-proof liquid is a diluent of the extracts of the wormwood and the camphor tree leaves, and the preparation process is as follows:

step A1: adding fresh wormwood and camphor tree leaves into a stamping machine according to the dosage-mass ratio of 1:2.5-4, adding tap water which is 0.5 times of the total weight of the wormwood and the camphor tree leaves, stamping and filtering to obtain stamping liquid;

step A2: heating the stamping liquid to 35-42 ℃, stirring and concentrating to half of the original volume, then pouring the stamping liquid into an activated carbon filter element for decoloring to obtain a mother liquid, and adsorbing and decoloring through activated carbon to avoid the phenomenon that the rattans are dyed after the dark mildew-proof liquid is absorbed so as to influence the appearance of the rattans;

step A3: and blending the mother liquor and tap water according to the volume ratio of 1:20-25 to obtain the mildew-proof liquid.

Further, in the step 3, the surface temperature of the rattan is controlled to be 75-85 ℃ during microwave heating through an infrared thermometer and adjustment of microwave frequency, the treatment time is 20-30min, and under the treatment condition, the rattan water loss speed is low, and moths and eggs can be effectively killed.

Further, in step 4, the specific operation process of the baking treatment is as follows: drying the rattan at the temperature of 110-.

Further, in the step 5, the vacuum degree after vacuumizing is 5-7kPa, and the pressure maintaining time is 12-17 min.

The invention has the beneficial effects that:

1. the invention soaks the bottom end of the rattan gathered in the mildew-proof liquid extracted from the wormwood and the camphor tree leaves, the activity of the rattan is still kept after being gathered, the photosynthesis and the respiration can be continuously carried out, the mildew-proof liquid is sent into the rattan, the internal water is evaporated in the subsequent drying process, the mildew-proof component is dispersed into the whole rattan, so that the whole rattan body has the mildew-proof effect, then the microwave heating treatment is adopted to sterilize the inside of the rattan and kill moth and worm eggs, in addition, in the drying process, the mildew-proof liquid is repeatedly sprayed on the surface of the rattan and dried, a strong mildew-proof layer is formed on the surface of the rattan, and the rattan is prevented from being infected by mildew.

2. According to the invention, the rattan subjected to baking treatment is immersed in the finish paint, and the vacuum pumping and pressure maintaining are carried out, so that air in fine cracks on the surface of the rattan is pumped out, meanwhile, air bubbles are removed from the finish paint, then the pressure is relieved, the finish paint is filled among the cracks on the surface of the rattan, the rattan is tightly filled with the finish paint, the rattan is effectively isolated from the external environment, and mildew caused by mold invasion into the rattan is prevented.

3. The invention provides a mildew-proof liquid which is extracted from camphor tree leaves and wormwood, and is simple in extraction operation, environment-friendly and nontoxic.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

In the embodiment, the finish paint is an epoxy resin anticorrosive finish paint provided by Tianjin Hainanlong chemical company Limited.

Example 1

The mildew-proof liquid prepared in this example is specifically implemented as follows:

step A1: collecting 10kg of fresh wormwood and 25kg of fresh camphor tree leaves, adding the fresh wormwood and the fresh camphor tree leaves into a stamping machine, taking 17.5kg of tap water, evenly dividing the tap water into three parts, adding one part of tap water for stamping each time, stamping for three times, stamping for 5min each time, taking out stamping liquid each time, and then mixing the three stamping liquids;

step A2: pouring the stamping liquid collected in the step A1 into a heating tank, stirring and heating to 35 ℃ at the rotating speed of 120r/min until the stamping liquid is heated until the stamping liquid is concentrated to half of the volume before heating, then pouring the concentrated liquid into an activated carbon filter element for filtering, and taking the filtrate as mother liquid;

step A3: and blending the mother solution and tap water according to the volume ratio of 1:20 to obtain the mildew-proof liquid.

Example 2

The mildew-proof liquid prepared in this example is specifically implemented as follows:

step A1: collecting 10kg of fresh wormwood and 30kg of fresh camphor tree leaves, adding the fresh wormwood and the fresh camphor tree leaves into a stamping machine, taking 20kg of tap water, averagely dividing the tap water into three parts, adding one part of tap water for stamping each time, stamping for three times, stamping for 6min each time, taking out stamping liquid each time, and then mixing the three stamping liquids;

step A2: pouring the stamping liquid collected in the step A1 into a heating tank, stirring and heating to 38 ℃ at the rotating speed of 120r/min until the stamping liquid is heated until the stamping liquid is concentrated to half of the volume before heating, then pouring the concentrated liquid into an activated carbon filter element for filtering, and taking the filtrate as mother liquid;

step A3: and blending the mother solution and tap water according to the volume ratio of 1:23 to obtain the mildew-proof liquid.

Example 3

The mildew-proof liquid prepared in this example is specifically implemented as follows:

step A1: collecting 10kg of fresh wormwood and 40kg of fresh camphor tree leaves, adding the fresh wormwood and the fresh camphor tree leaves into a stamping machine, taking 25kg of tap water, averagely dividing the tap water into three parts, adding one part of tap water for stamping each time, stamping for three times, stamping for 7min each time, taking out stamping liquid each time, and then mixing the three stamping liquids;

step A2: pouring the stamping liquid collected in the step A1 into a heating tank, stirring and heating to 42 ℃ at the rotating speed of 120r/min until the stamping liquid is heated until the stamping liquid is concentrated to half of the volume before heating, then pouring the concentrated liquid into an activated carbon filter element for filtering, and taking the filtrate as mother liquid;

step A3: and blending the mother liquor and tap water according to the volume ratio of 1:25 to obtain the mildew-proof liquid.

Example 4

The embodiment of the preparation of the mildew-proof rattan has the following specific implementation process:

step 1: and (3) harvesting 18 mature fresh rattans, wherein the specific harvesting method comprises the steps of chopping the rattans from the roots of the rattans at an angle of 45 degrees, and bundling 6 rattans into a group by using a bundling belt for later use.

Step 2: soaking the bottoms of a group of bundled rattans in the mildew-proof solution prepared in the example 1, controlling the soaking depth of the rattans in the mildew-proof solution to be 30cm, and placing the rattans in a shady and ventilated environment for soaking and culturing for 2 d;

the activity of the rattan is still kept after the rattan is harvested, the miscellaneous branches and rattan leaves on the rattan continue to perform photosynthesis and respiration, water is absorbed from the bottom of the rattan, and mildew-proof liquid is absorbed into the rattan through a conduit in the rattan to prevent mildew in the rattan;

and step 3: removing impurity branches, vine leaves and skins of the rattan soaked in the step 2, then putting the rattan into microwave heating equipment for heating, controlling the surface temperature of the microwave rattan to be 75 ℃ by using an infrared thermometer and adjusting the microwave frequency, and treating for 20 min;

the microwave heating can kill the moths and eggs in the rattan, so that the moths and the silkworms are prevented from eating the rattan in the subsequent treatment process, the integral rattan can be heated by the microwave heating, the toughness of the rattan is not reduced due to excessive water loss, and the rattan is favorably woven and processed;

and 4, step 4: bending the rattan processed in the step 3 into an annular workpiece, simulating rattan weaving, placing the woven rattan into a drying device for drying treatment, wherein the drying treatment specifically comprises the following steps: controlling the drying temperature to be 110 ℃, taking out the rattans every 8min, spraying the mildew-proof liquid prepared in the embodiment 1 on the surfaces of the rattans, controlling the spraying amount of the mildew-proof liquid to be 15mL/kg, repeating the operation for 3 times, and drying the rattans for 40min to finish the drying treatment;

through drying repeatedly and spraying mould proof liquid, on the one hand at the repeated mould proof composition that adheres to in the surface of rattan, effectively prevent to milden and rot, on the other hand, the mould proof liquid that repeatedly sprays makes the rattan keep toughness in the baking process, eliminates the stress of weaving production gradually, prevents the rattan and dries the fracture.

And 5: immersing the rattan processed in the step 4 into a sealed tank filled with finish paint, vacuumizing the sealed tank to 5kPa, maintaining the pressure for 12min, releasing the pressure, taking out the rattan, leveling, and naturally curing to obtain the mildew-proof rattan;

air in the tiny crackle of rattan surface is taken out through the evacuation, removes the bubble to the finish simultaneously, later release, and the finish paint is filled into between the crackle on rattan surface for the rattan is packed closely knit by the finish paint, separates the rattan effectively with external environment, prevents that the rattan from mildening and rot.

Example 5

The embodiment of the preparation of the mildew-proof rattan has the following specific implementation process:

step 1: taking a group of the rattans harvested in the example 4 for standby;

step 2: soaking the bottom of the rattan in the mildew-proof liquid prepared in the embodiment 2, controlling the soaking depth of the rattan in the mildew-proof liquid to be 40cm, and placing the rattan in a shady ventilation environment for soaking and culturing for 3 d;

and step 3: removing impurity branches, vine leaves and skins of the rattan soaked in the step 2, then putting the rattan into microwave heating equipment for heating, and controlling the surface temperature of the microwave rattan to be 80 ℃ by using an infrared thermometer and adjusting the microwave frequency for processing for 25 min;

and 4, step 4: bending the rattan processed in the step 3 into an annular workpiece, simulating rattan weaving, placing the woven rattan into a drying device for drying treatment, wherein the drying treatment specifically comprises the following steps: controlling the drying temperature to be 120 ℃, taking out the rattans every 10min, spraying the mildew-proof liquid prepared in the embodiment 2 on the surfaces of the rattans, controlling the spraying amount of the mildew-proof liquid to be 17mL/kg, repeating the operation for 3 times, and drying the rattans for 35min to finish the drying treatment;

and 5: and (4) immersing the rattan processed in the step (4) into a sealed tank containing finish paint, vacuumizing the sealed tank to 6kPa, maintaining the pressure for 15min, releasing the pressure, taking out the rattan, leveling, and naturally curing to obtain the mildew-proof rattan.

Example 6

The embodiment of the preparation of the mildew-proof rattan has the following specific implementation process:

step 1: taking a group of the rattans harvested in the example 4 for standby;

step 2: soaking the bottom of the rattan in the mildew-proof liquid prepared in the embodiment 3, controlling the soaking depth of the rattan in the mildew-proof liquid to be 50cm, and placing the rattan in a shady ventilation environment for soaking and culturing for 3 d;

and step 3: removing impurity branches, vine leaves and skins of the rattan soaked in the step 2, then putting the rattan into microwave heating equipment for heating, and controlling the surface temperature of the microwave rattan to be 85 ℃ and the treatment time to be 30min by using an infrared thermometer and adjusting the microwave frequency;

and 4, step 4: bending the rattan processed in the step 3 into an annular workpiece, simulating rattan weaving, placing the woven rattan into a drying device for drying treatment, wherein the drying treatment specifically comprises the following steps: controlling the drying temperature to be 130 ℃, taking out the rattans every 12min, spraying the mildew-proof liquid prepared in the embodiment 3 on the surfaces of the rattans, controlling the spraying amount of the mildew-proof liquid to be 20mL/kg, repeating the operation for 3 times, and drying the rattans for 30min to finish the drying treatment;

and 5: and (4) immersing the rattan processed in the step (4) into a sealed tank containing finish paint, vacuumizing the sealed tank to 7kPa, maintaining the pressure for 17min, releasing the pressure, taking out the rattan, leveling, and naturally curing to obtain the mildew-proof rattan.

Taking penicillium citrinum, trichoderma viride and aspergillus niger to be activated according to a use standard, then inoculating the penicillium citrinum, trichoderma viride and aspergillus niger to a PDA culture medium to be cultured, then adding sterile water to prepare bacterial liquid, sterilizing the surfaces of the rattans prepared in the embodiments 4-6 by adopting high-temperature water vapor, then respectively coating the three bacterial liquids on the mildew-proof rattans prepared in the embodiments 4-6, then placing the rattans in a constant-temperature and constant-humidity chamber with the air humidity of 90% and the temperature of 28 ℃, placing for 30 days, taking out the rattans and observing the growth condition of the mildew on the surface, wherein the specific data are shown in the following table 1:

TABLE 1

	Example 4	Example 5	Example 6
				Penicillium citrinum	No visible colony	No visible colony	No visible colony
Trichoderma viride	No visible colony	No visible colony	No visible colony
				Aspergillus niger	No visible colony	No visible colony	No visible colony

As can be seen from Table 1, the rattan treated by the method has no visible mould colony when being inoculated with penicillium citrinum, trichoderma viride and aspergillus niger and placed in a constant temperature and humidity environment for 30 days, and shows excellent mould-proof effect.

In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The foregoing is illustrative and explanatory only and is not intended to be exhaustive or to limit the invention to the precise embodiments described, and various modifications, additions, and substitutions may be made by those skilled in the art without departing from the scope of the invention or exceeding the scope of the claims.