阅读说明：本技术 一种玫瑰花水制备方法 (Preparation method of rose water ) 是由 尹帅 于 2021-10-15 设计创作，主要内容包括：本发明公开了一种玫瑰花水制备方法,涉及玫瑰花水领域。该玫瑰花水制备方法,其制备方法包括原料熬制、原料蒸馏、原料过滤、花水制备和花水装瓶五个步骤,该玫瑰花水制备方法,通过白藓皮提取物能够在使用玫瑰花水的过程中不仅能够将其当香水进行使用,同时还具有止痒的作用,从而这样设置能够极大程度的提高玫瑰花水在使用的实用性,在通过柑橘提取物在夏季使用玫瑰花水时,能够达到一定的驱蚊效果,减少夏季蚊虫较多被蚊虫叮咬的情况,进一步的提高了玫瑰花水使用时的多样性和实用性,增加玫瑰花水的实用效果,便于后续对其进行销售,有利于推广和使用,苯氧乙醇能够增加玫瑰花水的存储时间,能够有效的提高玫瑰花水的保质期。(The invention discloses a preparation method of rose water, and relates to the field of rose water. The preparation method of the rose water comprises five steps of raw material boiling, raw material distillation, raw material filtration, flower water preparation and flower water bottling, the preparation method of flos Rosae Rugosae water can use cortex Dictamni Radicis extract as perfume in the process of using flos Rosae Rugosae water, meanwhile, the rose water also has the function of relieving itching, thereby greatly improving the practicability of the rose water in use, when the rose water is used in summer through the citrus extract, a certain mosquito repelling effect can be achieved, the situation that mosquitoes are bitten by mosquitoes in summer is reduced, the variety and the practicality of rose water when further having improved the use increase the practical function of rose water, are convenient for follow-up selling it, are favorable to promoting and using, and phenoxyethanol can increase the save time of rose water, can the effectual shelf life who improves rose water.)

1. The preparation method of the rose water is characterized by comprising the following raw materials in parts by weight: 180 parts of rose petal 150, 80-110 parts of purified water, 10-15 parts of white rose essence, 3-5 parts of glycerol, 3-6 parts of dipropylene glycol, 4-6 parts of propylene glycol, 2-4 parts of EDTA disodium, 1-5 parts of aminomethyl propanol, 4-8 parts of phenoxyethanol, 1-3 parts of preservative, 5-7 parts of musk tincture, 2-5 parts of cortex dictamni extract and 3-6 parts of citrus extract, and the preparation method comprises the following steps:

s1 decocting the raw materials

Cleaning rose petals with clear water, removing excessive water stain on the rose petals, taking out a sand pot, placing the prepared rose petals in the sand pot, pouring prepared purified water into the sand pot, slowly boiling with slow fire, rotating the purified water and the rose petals in the sand pot during the process of slowly boiling with slow fire, and turning off the fire before the purified water is not boiled;

s2 distillation of raw materials

Placing the decocted rose petals and rose water in a distiller, heating the distiller for 5-8min, collecting distilled liquid generated by the rose water after heating, and standing for 20-30min after collecting for cooling;

s3, filtering the raw materials

Filtering the rose petals and the rose water after distillation and cooling for the first time through gauze, filtering the rose water for the second time through new gauze after filtering, adding the white rose essence, the dittany bark extract and the citrus extract into the rose water after filtering, stirring, waiting for the cooling of the rose water after stirring, sealing the mouth through a preservative film after cooling, and standing for 12-24 hours;

s4 preparation of flower water

Taking out the placed rose water, placing the rose water in a stirrer, sequentially adding glycerol, dipropylene glycol, propylene glycol, EDTA disodium, aminomethyl propanol, phenoxyethanol and musk tincture, stirring, adding a preservative, stirring again, and filtering the rose water by using gauze after stirring;

s5 bottling the flower water

Adding 75% ethanol into a glass bottle, placing the glass bottle into an ultrasonic oscillator, oscillating, adding the prepared rose water, and sealing the glass.

2. The method for preparing rose water according to claim 1, wherein: in the step of decocting the raw materials, the rose petals are boiled for 5min to 10 min.

3. The method for preparing rose water according to claim 1, wherein: in the raw material filtering step, the gauze for the first filtering is 180 meshes in 100 and 300 meshes in 200.

4. The method for preparing rose water according to claim 1, wherein: the temperature in the standing step of filtering the raw materials is 15-25 ℃, and the stirring speed of the rose water is 50-60 r/min.

5. The method for preparing rose water according to claim 1, wherein: the gauze used in the step of preparing the flower water is 400 meshes, and the stirring speed is 80-100 r/min.

6. The method for preparing rose water according to claim 1, wherein: in the step of bottling the flower water, the frequency of an ultrasonic oscillator is 0.5-3.0MHZ, and the oscillation time is 5-8 min.

7. The method for preparing rose water according to claim 1, wherein: in the step of bottling the rose water, the amount of the rose water added into the glass bottle is 0.05 percent of the total solution of the rose water.

Technical Field

The invention relates to the technical field of rose water, in particular to a preparation method of rose water.

Background

Roses always represent meaningful love, whether in first love, hot love or in a marital hall, and the roses are believed to play an important role in the roses absolutely, so that a lot of people search for the rose-fragrance perfume, the rose-fragrance perfume becomes a perfume which cannot be missed by numerous perfume manufacturers absolutely, the rose is put into a sealed glass bottle to be placed in the sun in the early-stage rose perfume production process, and a few drops of rose perfume can be obtained after a plurality of months.

Disclosure of Invention

Technical problem to be solved

Aiming at the defects of the prior art, the invention provides the preparation method of the rose water, which has longer quality guarantee period, can reduce the infection of the rose water and the body of partial people, and solves the problems of single effect and lower practicability of the rose water in use.

(II) technical scheme

In order to achieve the purpose, the invention provides the following technical scheme:

a preparation method of rose water comprises the following raw materials in proportion: 180 parts of rose petal 150, 80-110 parts of purified water, 10-15 parts of white rose essence, 3-5 parts of glycerol, 3-6 parts of dipropylene glycol, 4-6 parts of propylene glycol, 2-4 parts of EDTA disodium, 1-5 parts of aminomethyl propanol, 4-8 parts of phenoxyethanol, 1-3 parts of preservative, 5-7 parts of musk tincture, 2-5 parts of cortex dictamni extract and 3-6 parts of citrus extract, and the preparation method comprises the following steps:

step one, boiling raw materials

Cleaning rose petals with clear water, removing excessive water stain on the rose petals, taking out a sand pot, placing the prepared rose petals in the sand pot, pouring prepared purified water into the sand pot, slowly boiling with slow fire, rotating the purified water and the rose petals in the sand pot during the process of slowly boiling with slow fire, and turning off the fire before the purified water is not boiled;

step two, raw material distillation

Placing the decocted rose petals and rose water in a distiller, heating the distiller for 5-8min, collecting distilled liquid generated by the rose water after heating, and standing for 20-30min after collecting for cooling;

step three, filtering the raw materials

Filtering the rose petals and the rose water after distillation and cooling for the first time through gauze, filtering the rose water for the second time through new gauze after filtering, adding the white rose essence, the dittany bark extract and the citrus extract into the rose water after filtering, stirring, waiting for the cooling of the rose water after stirring, sealing the mouth through a preservative film after cooling, and standing for 12-24 hours;

step four, flower water preparation

Taking out the placed rose water, placing the rose water in a stirrer, sequentially adding glycerol, dipropylene glycol, propylene glycol, EDTA disodium, aminomethyl propanol, phenoxyethanol and musk tincture, stirring, adding a preservative, stirring again, and filtering the rose water by using gauze after stirring;

step five, bottling the flower water

Adding 75% ethanol into a glass bottle, placing the glass bottle into an ultrasonic oscillator, oscillating, adding the prepared rose water, and sealing the glass.

Preferably, the rose petals in the first step are boiled for 5min to 10 min.

Preferably, the gauze used in the first filtration in the second step is 180 meshes in 100 meshes, and the gauze used in the second filtration is 300 meshes in 200 meshes.

Preferably, the temperature in the standing step two is 15-25 ℃, and the stirring speed of the rose water is 50-60 r/min.

Preferably, the gauze used in the third step is 400 meshes, and the stirring speed is 80-100 r/min.

Preferably, the frequency of the ultrasonic oscillator in the fourth step is 0.5-3.0MHZ, and the oscillation time is 5-8 min.

Preferably, the amount of the rose water added into the glass bottle in the fourth step is 0.05 percent of the total solution of the rose water.

(III) advantageous effects

Compared with the prior art, the invention provides a preparation method of rose water, which has the following beneficial effects:

1. this preparation method of rose water, cooperation through ultrasonic oscillator and ethanol is used, can disinfect the glass bottle that rose water used, can avoid containing pathogenic microorganism in the glass bottle like this, thereby can avoid pathogenic microorganism and rose water to mix and lead to the in-process pathogenic microorganism at use rose water infringes the human body, cause the condition of human infection, set up the safety of assurance rose water when using that can very big degree like this, reduce the condition because of the production skin infection of using rose water, improve the security of human body when using rose water.

2. This preparation method of rose water, can not only use it as perfume at the in-process that uses rose water through the dittany bark extract product, still have the effect of relieving itching simultaneously, thereby the practicality of improvement rose water that can very big degree is using is set up like this, when using rose water in summer through the oranges and tangerines extract product, can reach certain mosquito repellent effect, reduce the more condition of being stung by the mosquito of mosquito in summer, further improvement variety and the practicality when rose water uses, increase the practical effect of rose water, be convenient for follow-up sell it, be favorable to promoting and using.

3. This preparation method of rose water through using the impurity of getting rid of rose water that can be very big degree after the cubic gauze filters rose water, can effectual improvement rose water quality after production, avoids off-the-shelf rose water inside to produce the floccule of sediment when using, has added phenoxyethanol in the rose water simultaneously, can increase the save time of rose water, can effectual improvement rose water's shelf life.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The first embodiment is as follows:

a preparation method of rose water comprises the following raw materials in proportion: 150 parts of rose petals, 80 parts of purified water, 10 parts of white rose essence, 3 parts of glycerol, 3 parts of dipropylene glycol, 4 parts of propylene glycol, 2 parts of EDTA disodium, 1 part of aminomethyl propanol, 4 parts of phenoxyethanol, 1 part of preservative, 5 parts of musk tincture, 2 parts of cortex dictamni extract and 3 parts of citrus extract, wherein the preparation method comprises the following steps:

step one, boiling raw materials

Cleaning rose petals with clear water, removing excessive water stain on the rose petals, taking out a sand pot, placing the prepared rose petals in the sand pot, pouring prepared purified water into the sand pot, slowly boiling with slow fire, turning off the fire before the purified water is not boiled, and boiling the rose petals for 8 min;

step two, raw material distillation

Placing the decocted rose petals and rose water in a distiller, heating the distiller for 5min, collecting distilled liquid generated by the rose water after heating, and standing for 20min after collecting to cool;

step three, filtering the raw materials

Filtering the rose petals and the rose water after distillation and cooling for the first time through gauze, filtering the rose water for the second time through new gauze after filtering, adding the white rose essence, the dittany bark extract and the citrus extract into the rose water after filtering, stirring, waiting for cooling the rose water after stirring, sealing the cooled rose water through a preservative film, standing for 12 hours, wherein the temperature in the standing is 15 ℃, the stirring speed of the rose water is 50r/min, the gauze for the first filtering is 100 meshes, and the gauze for the second filtering is 200 meshes;

step four, flower water preparation

Taking out the placed rose water, placing the rose water in a stirrer, sequentially adding glycerol, dipropylene glycol, propylene glycol, EDTA disodium, aminomethyl propanol, phenoxyethanol and musk tincture, stirring, adding a preservative, stirring again, filtering the rose water by using gauze after stirring, wherein the used gauze is 400 meshes, and the stirring speed is 80 r/min;

step five, bottling the flower water

Adding 75% ethanol into a glass bottle, placing the glass bottle into an ultrasonic oscillator, oscillating, adding the prepared rose water, and sealing the glass, wherein the frequency of the ultrasonic oscillator is 0.5MHZ, the oscillation time is 5min, and the rose water added into the glass bottle in the step of bottling the rose water accounts for 0.05% of the total rose water solution.

Example two:

a preparation method of rose water comprises the following raw materials in proportion: 165 parts of rose petals, 95 parts of purified water, 12 parts of white rose essence, 4 parts of glycerol, 5 parts of dipropylene glycol, 5 parts of propylene glycol, 3 parts of EDTA disodium, 3 parts of aminomethyl propanol, 6 parts of phenoxyethanol, 2 parts of preservative, 5 parts of musk tincture, 3 parts of cortex dictamni extract and 4 parts of citrus extract, wherein the preparation method comprises the following steps:

step one, boiling raw materials

Cleaning rose petals with clear water, removing excessive water stain on the rose petals, taking out a sand pot, placing the prepared rose petals in the sand pot, pouring prepared purified water into the sand pot, slowly boiling with slow fire, turning off the fire before the purified water is not boiled, and boiling the rose petals for 8 min;

step two, raw material distillation

Placing the decocted rose petals and rose water in a distiller, heating the distiller for 6min, collecting distilled liquid generated by the rose water after heating, and standing for 25min after collecting to cool;

step three, filtering the raw materials

Filtering the rose petals and the rose water after distillation and cooling for the first time through gauze, filtering the rose water for the second time through new gauze after filtering, adding the white rose essence, the dittany bark extract and the citrus extract into the rose water after filtering, stirring, waiting for cooling the rose water after stirring, sealing the cooled rose water through a preservative film, standing for 12 hours, wherein the temperature in the standing is 20 ℃, the stirring speed of the rose water is 55r/min, the gauze for the first filtering is 150 meshes, and the gauze for the second filtering is 250 meshes;

step four, flower water preparation

Taking out the placed rose water, placing the rose water in a stirrer, sequentially adding glycerol, dipropylene glycol, propylene glycol, EDTA disodium, aminomethyl propanol, phenoxyethanol and musk tincture, stirring, adding a preservative, stirring again, filtering the rose water by using gauze after stirring, wherein the used gauze is 400 meshes, and the stirring speed is 90 r/min;

step five, bottling the flower water

Adding 75% ethanol into a glass bottle, placing the glass bottle into an ultrasonic oscillator, oscillating, adding the prepared rose water, and sealing the glass, wherein the frequency of the ultrasonic oscillator is 2MHZ, the oscillation time is 6min, and the amount of the rose water added into the glass bottle in the step of bottling the rose water is 0.05% of the total solution of the rose water.

Example three:

a preparation method of rose water comprises the following raw materials in proportion: 180 parts of rose petals, 110 parts of purified water, 15 parts of white rose essence, 5 parts of glycerol, 6 parts of dipropylene glycol, 6 parts of propylene glycol, 4 parts of EDTA disodium, 5 parts of aminomethyl propanol, 8 parts of phenoxyethanol, 3 parts of preservative, 7 parts of musk tincture, 5 parts of cortex dictamni extract and 6 parts of citrus extract, and the preparation method comprises the following steps:

step one, boiling raw materials

Cleaning rose petals with clear water, removing excessive water stain on the rose petals, taking out a sand pot, placing the prepared rose petals in the sand pot, pouring prepared purified water into the sand pot, slowly boiling with slow fire, turning off the fire before the purified water is not boiled, and boiling the rose petals for 10 min;

step two, raw material distillation

Placing the decocted rose petals and rose water in a distiller, heating the distiller for 8min, collecting distilled liquid generated by the rose water after heating, and standing for 30min after collecting to cool;

step three, filtering the raw materials

Carrying out primary filtration on the rose petals and the rose water after distillation and cooling through gauze, carrying out secondary filtration on the rose water by using new gauze after filtration, adding white rose essence, dittany bark extract and citrus extract into the rose water after filtration, stirring, waiting for cooling of the rose water after stirring, sealing by using a preservative film after cooling, standing for 12 hours, wherein the temperature in the standing is 25 ℃, the stirring speed of the rose water is 60r/min, the gauze for primary filtration is 180 meshes, and the gauze for secondary filtration is 300 meshes;

step four, flower water preparation

Taking out the placed rose water, placing the rose water in a stirrer, sequentially adding glycerol, dipropylene glycol, propylene glycol, EDTA disodium, aminomethyl propanol, phenoxyethanol and musk tincture, stirring, adding a preservative, stirring again, filtering the rose water by using gauze after stirring, wherein the used gauze is 400 meshes, and the stirring speed is 100 r/min;

step five, bottling the flower water

Adding 75% ethanol into a glass bottle, placing the glass bottle into an ultrasonic oscillator, oscillating, adding the prepared rose water, and sealing the glass, wherein the frequency of the ultrasonic oscillator is 3.0MHZ, the oscillation time is 8min, and the rose water added into the glass bottle in the step of bottling the rose water accounts for 0.05% of the total rose water solution.

Therefore, the rose essence is adopted as a raw material in most of the prior rose water, so that the rose fragrance is strong after the rose water is prepared, sensory discomfort is easily caused when the rose water is used too much, and meanwhile, the prior rose water has single function and low practicability and is not easy to store when in use; the preparation method of the rose water can sterilize the glass bottle used by the rose water by matching the ultrasonic oscillator with the ethanol, so that pathogenic microorganisms contained in the glass bottle can be avoided, the condition that the pathogenic microorganisms invade the human body and cause human body infection in the process of using the rose water due to the mixing of the pathogenic microorganisms and the rose water can be avoided, the safety of the rose water in use can be greatly ensured, the condition of skin infection caused by the use of the rose water is reduced, the safety of the human body in the use of the rose water is improved, the dittany bark extract can be used as perfume in the process of using the rose water and has the effect of relieving itching, the practicability of the rose water in use can be greatly improved, and the citrus extract can be used in summer when the rose water is used, can reach certain mosquito repellent effect, reduce the more condition that is bitten by the mosquito of summer mosquito, further improvement variety and practicality when rose water uses, increase the practical function of rose water, be convenient for follow-up selling it, be favorable to promoting and using, use the cubic gauze to filter the impurity of getting rid of rose water that can be very big degree after the rose water, can effectual improvement rose water quality after production, avoid off-the-shelf rose water inside to produce the floccule that deposits when using, simultaneously add phenoxy ethanol in the rose water, can increase the save time of rose water, can effectual improvement rose water's shelf life.