阅读说明：本技术 温感面膜及其制备方法 (Temperature-sensitive mask and preparation method thereof ) 是由 莫美玲 于 2021-08-20 设计创作，主要内容包括：本发明涉及日用化妆品技术领域,具体而言,涉及一种温感面膜及其制备方法,所述温感面膜,按照重量份数计,包括以下组分：胡椒籽提取物0.001份～0.1份,吴茱萸提取物0.001份～0.2份,姜根油0.001份～1份,多元醇50份～60份,赋脂剂5份～20份,乳化剂0.2份～10份,增稠剂0.2份～3份,水20份～30份。(The invention relates to the technical field of daily cosmetics, and particularly relates to a temperature-sensitive facial mask and a preparation method thereof, wherein the temperature-sensitive facial mask comprises the following components in parts by weight: 0.001 to 0.1 portion of pepper seed extract, 0.001 to 0.2 portion of evodia rutaecarpa extract, 0.001 to 1 portion of ginger oil, 50 to 60 portions of polyalcohol, 5 to 20 portions of fat-imparting agent, 0.2 to 10 portions of emulsifier, 0.2 to 3 portions of thickener and 20 to 30 portions of water.)

1. The temperature-sensitive mask is characterized by comprising the following components in parts by weight:

2. the warming mask as claimed in claim 1, wherein the content of tetrahydropiperine in the pepper seed extract is 95-100% by mass.

3. The temperature-sensitive mask as claimed in claim 1, wherein the evodiamine content of the evodiamine extract is 0.004-0.015% by mass, and the rutaecarpine content is 0.003-0.008% by mass.

4. The temperature-sensing facial mask as claimed in claim 1, wherein the gingerol in the ginger root oil accounts for 0.5-5% by mass.

5. The warming mask as claimed in claim 1, wherein the mass ratio of the pepper seed extract, the evodia rutaecarpa extract and the ginger root oil is 1: (1-2): (2-5).

6. The warming mask pack according to any one of claims 1 to 5, wherein said polyhydric alcohol is one or more selected from the group consisting of glycerin, butylene glycol, propylene glycol and polyethylene glycol.

7. The warming mask pack according to any one of claims 1 to 5, wherein the lipid-imparting agent is one or more selected from squalane, caprylic/capric triglyceride, meadowfoam seed oil, olive oil, jojoba seed oil and macadamia nut oil.

8. The warming mask pack according to any one of claims 1 to 5, wherein said thickener is one or more selected from xanthan gum, sclerosant, carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer and sodium acrylic acid copolymer.

9. The warming mask pack according to any one of claims 1 to 5, wherein the emulsifier is one or more selected from the group consisting of polyglyceryl-10 stearate, polyglyceryl-10 oleate, polyglyceryl-6-distearate, polyglyceryl-6-dioleate, polyglyceryl-3-diisostearate, polyglyceryl-10-diisostearate and sucrose polystearate.

10. A method for preparing the temperature-sensitive mask according to any one of claims 1 to 9, comprising the steps of:

mixing an emulsifier, polyol, a thickening agent and water, heating to 60-80 ℃, and keeping the temperature for more than 20min to obtain a solution A;

adding a fat-imparting agent into the solution A under the condition of continuing heat preservation, and homogenizing, emulsifying and dispersing to obtain a solution B;

cooling the solution B to 30-40 ℃, and sequentially adding pepper seed extract, evodia rutaecarpa extract and ginger root oil.

Technical Field

The invention relates to the technical field of daily cosmetics, and particularly relates to a temperature-sensitive facial mask and a preparation method thereof.

Background

The facial mask is a convenient and quick skin care product, and can achieve certain beautifying effect after being applied or smeared on the face for 15-30 minutes. The mask has the efficacy principle that when the moist mask is applied to the face, substances in the mask tightly wrap the skin, so that the skin is isolated from the outside air, water slowly permeates into the horny layer of the epidermis, and meanwhile, the water in the mask is prevented from being lost quickly, cells of the horny layer can fully absorb the water in the moist environment, collagen of deep cells can fully absorb the water, so that the skin is soft, the elasticity is increased, particularly in cold and dry winter, the skin is most prone to water loss, but in the low-temperature environment, the heat of the skin can be taken away due to the volatilization and heat absorption of the water on the face of the general mask, and the use frequency of the mask in winter is greatly reduced. Moreover, the mask is generally directly applied to the face, has large water content and low temperature, is easy to cause stimulation to the face to cause diseases such as apoplexy and the like, and simultaneously, the cold face mask causes shrinkage of pores, the absorption of the mask is not good, and the using effect of the mask is influenced.

The warm (hot, warm and warm) facial mask can induce vasodilatation, accelerate blood microcirculation of deep layer of skin, increase oxygenation of epidermal skin cells, promote penetration and absorption of active ingredients by matching with massage, improve activity of the epidermal skin cells, achieve the effect of improving texture and surface gloss of the skin, greatly facilitate use in winter and nourish the skin. However, the traditional temperature sensing facial mask has strong irritation, too strong heat sense, too long heat sense retention time and not mild enough.

Disclosure of Invention

Based on the above, the invention provides the facial mask which can improve the skin and has a temperature sensing effect.

The invention provides a temperature-sensitive mask which comprises the following components in parts by weight: 0.001 to 0.1 portion of pepper seed extract, 0.001 to 0.2 portion of evodia rutaecarpa extract, 0.001 to 1 portion of ginger oil, 50 to 60 portions of polyalcohol, 5 to 20 portions of fat-imparting agent, 0.2 to 10 portions of emulsifier, 0.2 to 3 portions of thickener and 20 to 30 portions of water.

In one embodiment, the content of the tetrahydropiperine in the pepper seed extract is 95-100% by mass.

In one embodiment, the evodiamine content of the evodiamine extract is 0.004-0.015 wt%, and the rutaecarpine content is 0.003-0.008 wt%.

In one embodiment, the gingerol in the ginger root oil accounts for 0.5-5% by mass.

In one embodiment, the mass ratio of the pepper seed extract, the evodia rutaecarpa extract and the ginger root oil is 1: (1-2): (2-5).

In one embodiment, the polyol is selected from one or more of glycerol, butylene glycol, propylene glycol and polyethylene glycol.

In one embodiment, the fatliquoring agent is selected from one or more of squalane, caprylic/capric triglyceride, meadowfoam seed oil, olive oil, jojoba seed oil and macadamia nut oil.

In one embodiment, the thickening agent is selected from one or more of xanthan gum, scleroglucan, carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer, and sodium acrylic acid copolymer.

In one embodiment, the emulsifier is selected from one or more of polyglyceryl-10 stearate, polyglyceryl-10 oleate, polyglyceryl-6-distearate, polyglyceryl-6-dioleate, polyglyceryl-3-diisostearate, and sucrose polystearate.

In another aspect of the present invention, a preparation method of the temperature-sensitive mask is provided, which includes the following steps:

mixing an emulsifier, polyol, a thickening agent and water, heating to 60-80 ℃, and keeping the temperature for more than 20min to obtain a solution A;

adding a fat-imparting agent into the solution A under the condition of continuing heat preservation, and homogenizing, emulsifying and dispersing to obtain a solution B;

cooling the solution B to 30-40 ℃, and sequentially adding pepper seed extract, evodia rutaecarpa extract and ginger root oil.

Compared with the prior art, the invention has the following beneficial effects:

the ginger root oil contains a large amount of gingerol, which can combine with capsaicin receptor (TRPV1, ion channel) in cell membrane to generate heat sensation with strong heat sensation, but the heat sensation is quickly relieved after use, compared with vanillyl butyl ether, the gingerol does not cause vasodilatation and pain sensation and is mild. The pepper seed extract contains a large amount of tetrahydropiperine, and can increase the fluidity of lipid bilayers. The alkaloid in fructus evodiae extract has effects of inducing vasodilatation and improving microcirculation. According to the warm mask provided by the invention, the pepper seed extract, the fructus evodiae extract and the ginger root oil are used in a combined manner, and the pepper seed extract and the fructus evodiae extract synergistically promote gingerol molecules to enter the skin through different permeation-promoting mechanisms, so that the effect of warming can be achieved by adding a small amount of ginger root oil. Meanwhile, the pepper seed extract also has a certain heating effect and has the function of thermal sense synergistic interaction with the ginger root oil. The facial mask has mild heating and skin care effects after being applied to the face by further combining other components, and brings pleasant use feeling to consumers.

Detailed Description

Reference will now be made in detail to embodiments of the invention, one or more examples of which are described below. Each example is provided by way of explanation, not limitation, of the invention. In fact, it will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the scope or spirit of the invention. For instance, features illustrated or described as part of one embodiment, can be used on another embodiment to yield a still further embodiment.

It is therefore intended that the present invention cover the modifications and variations of this invention provided they come within the scope of the appended claims and their equivalents. Other objects, features and aspects of the present invention are disclosed in or are apparent from the following detailed description. It is to be understood by one of ordinary skill in the art that the present discussion is a description of exemplary embodiments only, and is not intended as limiting the broader aspects of the present invention.

Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.

The terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.

Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first" or "second" may explicitly or implicitly include at least one such feature. In the description of the invention, "a plurality" means at least two, e.g., two, three, etc., unless explicitly specified otherwise. In the description of the present invention, "a plurality" means at least one, e.g., one, two, etc., unless specifically limited otherwise.

Other than as shown in the operating examples, or where otherwise indicated, all numbers expressing quantities of ingredients, physical and chemical properties, and so forth used in the specification and claims are to be understood as being modified in all instances by the term "about". For example, unless indicated to the contrary, the numerical parameters set forth in the foregoing specification and attached claims are approximations that can be suitably varied by those skilled in the art in seeking to obtain the desired properties utilizing the teachings disclosed herein. The use of numerical ranges by endpoints includes all numbers within that range and any range within that range, for example, 1 to 5 includes 1, 1.1, 1.3, 1.5, 2, 2.75, 3, 3.80, 4, and 5, and the like.

The embodiment of the invention provides a temperature-sensitive mask which comprises the following components in parts by weight: 0.001 to 0.1 portion of pepper seed extract, 0.001 to 0.2 portion of evodia rutaecarpa extract, 0.001 to 1 portion of ginger oil, 50 to 60 portions of polyalcohol, 5 to 20 portions of fat-imparting agent, 0.2 to 10 portions of emulsifier, 0.2 to 3 portions of thickener and 20 to 30 portions of water.

The ginger root oil contains a large amount of gingerol, which can combine with capsaicin receptor (TRPV1, ion channel) in cell membrane to generate heat sensation with strong heat sensation, but the heat sensation is quickly relieved after use, compared with vanillyl butyl ether, the gingerol does not cause vasodilatation and pain sensation and is mild. The pepper seed extract contains a large amount of tetrahydropiperine, and can increase the fluidity of lipid bilayers. The alkaloid in fructus evodiae extract has effects of inducing vasodilatation and improving microcirculation. The two components synergistically promote gingerol molecules to enter the skin through different permeation-promoting mechanisms, so that the effect of warming can be achieved by adding a small amount of ginger root oil. Meanwhile, the pepper seed extract also has a certain heating effect and has the function of thermal sense synergistic interaction with the ginger root oil. According to the warm mask, the pepper seed extract, the fructus evodiae extract and the ginger root oil are used in a combined mode, and other components are combined, so that the warm mask has mild heating and skin care effects after being applied to the face, and pleasant use feeling is brought to consumers.

In some embodiments, the content of the tetrahydropiperine in the pepper seed extract is 95-100% by weight.

In some embodiments, the content of evodiamine in the fructus evodiae extract is 0.004-0.015% by mass, and the content of rutaecarpine in the fructus evodiae extract is 0.003-0.008% by mass.

In some embodiments, the gingerol in the ginger root oil is 0.5-5% by weight.

In some embodiments, the mass ratio of the pepper seed extract, the evodia rutaecarpa extract and the ginger root oil may be 1: (1-2): the ratio of (2) to (5) may be, for example, 1:1:2, 1:1.875:3.75, or 1:2: 5.

In some preferred embodiments, the weight part of the ginger root oil in the temperature-sensitive mask is 0.001 to 0.3.

Polyol means a compound having 2 or more hydroxyl groups. The polyol is not particularly limited, and may include, but is not limited to, polyethylene glycol, propylene glycol, butylene glycol, hexylene glycol, glycerin, diglycerin, diethylene glycol, dipropylene glycol, 1, 2-pentanediol, sorbitol, xylitol, and combinations thereof. The polyol is preferably a polyol which is liquid at normal temperature and pressure. In some preferred embodiments, the polyol is selected from one or more of glycerol, butylene glycol, propylene glycol, and polyethylene glycol.

The fat-endowing agent has the functions of conditioning skin lipid and repairing skin. The lipid-imparting agents may include, but are not limited to, highly branched saturated or unsaturated alkanes: such as the all-methyl-substituted hexadecane and docosane isomers, 2,4,4,6,6,8, 8-dimethyl-10-methylundecane, 2,4,4,6, 6-dimethyl-8-methylnonane; fatty acid esters: such as isopropyl isostearate, hexyl laurate, isohexyl laurate, isopropyl palmitate, hexyl palmitate, decyl oleate, isodecyl oleate, hexyldecyl stearate, isopropyl isostearate, dihexyldecyl adipate, etc.; di-and trialkyl and alkenyl esters: such as isocetyl stearoyloxystearate, diisopropyl adipate, citric tristearate; polyol esters: such as ethylene glycol mono and di-fatty acid esters, diethylene glycol mono and di-fatty acid esters, polyethylene glycol mono and di-fatty acid esters, propylene glycol mono and di-fatty acid esters, polypropylene glycol monooleate, polypropylene glycol 2000 monostearate, and the like; oil esters: such as glycerides derived from natural castor oil, sunflower oil, cottonseed oil, corn oil, olive oil, cod liver oil, squalane, sweet almond oil, avocado oil, shea butter, palm oil, meadowfoam seed oil, olive oil, jojoba seed oil and macadamia nut oil, sesame oil and lanolin, caprylic/capric triglycerides, synthetic triolein and tristearin dilaurate, and the like; organic polymers: such as polybutene, polyisopropene, polybutadiene, isobutylene and butene copolymers, and the like. In some preferred embodiments, the fatliquoring agent is selected from one or more of squalane, caprylic/capric triglyceride, meadowfoam seed oil, olive oil, jojoba seed oil and macadamia nut oil.

Thickeners function to increase viscosity, stability of the ingredients and to achieve a fluid state for ease of use. The thickener may include, but is not limited to, gelatin, sodium caseinate, guar gum, acacia gum, pectin, agar, carrageenan, gellan gum, xanthan gum, sclerotium rolfsii gum, carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer, sodium acrylic acid copolymer, and the like. In some preferred embodiments, the thickener is selected from one or more of xanthan gum, sclerotium rolfsii, carbomer, acrylic acid/C10-30 alkanol acrylate crosspolymer and sodium acrylic acid copolymer. In some preferred embodiments, the thickener is selected from sodium acrylate copolymer.

The emulsifier is also not particularly limited, and alternative examples are anionic emulsifiers, nonionic emulsifiers, and betaine-type emulsifiers.

Examples of such emulsifiers may include, but are not limited to, sorbitan olivine oleate, polyglycerol-10 stearate, polyglycerol-10 oleate, polyglycerol-6 distearate, polyglycerol-6 dioleate, polyglycerol-3-diisostearate, polyglycerol-10-diisostearate, sodium stearoyl lactylate, glycerol stearate, sucrose polystearate, hydrogenated lecithin, cetearyl alcohol, ceteareth, cetearyl glucoside, PEG-100 stearate, glycerol stearate/PEG-100 stearate, sorbitan sesquioleate, isosteareth-20, PEG-10 campesterol, laureth-7, polyglycerol-3 methylglucose distearate, PEG/PPG-10/1 polydimethylsiloxane, Polyglycerol-3 diisostearate, steareth-20, ceteth-20, polysorbate-60, polyoxyethylene hydrogenated castor oil, coco glucoside, macrogol laurate, lecithin, polyglycerol-10 myristate.

In some preferred embodiments, the emulsifier is selected from one or more of polyglyceryl-10 stearate, polyglyceryl-10 oleate, polyglyceryl-6-distearate, polyglyceryl-6-dioleate, polyglyceryl-3-diisostearate, polyglyceryl-10-diisostearate, and sucrose polystearate. In some more preferred embodiments, the emulsifier is selected from polyglyceryl-10 stearate.

In addition, the emulsifying system of the invention is not limited to the above components, but other ingredients that can be used in a possible cosmetic or dermatological product may also be added, such as: whitening additives, skin conditioners, soothing agents, pH adjusters, chelating agents, other antioxidants, and the like.

In another aspect of the present invention, a method for preparing the temperature-sensitive facial mask is provided, which comprises the following steps:

mixing an emulsifier, polyol, a thickening agent and water, heating to 60-80 ℃, and keeping the temperature for more than 20min to obtain a solution A;

adding a fat-imparting agent into the solution A under the condition of continuing heat preservation, and homogenizing, emulsifying and dispersing to obtain a solution B;

cooling the solution B to 30-40 ℃, and sequentially adding pepper seed extract, evodia rutaecarpa extract and ginger root oil.

In another aspect of the invention, the use method of the temperature-sensitive mask is further provided, and the mask is applied to the face. Furthermore, after being applied, the face massage can be combined to promote absorption and enhance the effect.

The temperature-sensitive mask of the present invention will be described in further detail with reference to specific examples. The present invention is intended to be further described in detail to assist those skilled in the art and researchers to further understand the present invention, and the technical conditions and the like do not limit the present invention. Any modification made within the scope of the claims of the present invention is within the scope of the claims of the present invention. The examples, which are not specifically illustrated, employ drugs and equipment, all of which are conventional in the art. The experimental procedures, in which specific conditions are not indicated in the examples, were carried out according to conventional conditions, such as those described in the literature, in books, or as recommended by the manufacturer. The parts referred to below are parts by weight. The related raw materials are as follows:

the pepper seed extract is Cosmoperine CH (product name) from Sabinsa corporation;

the fructus evodiae extract is Gatuline Radiance (product name) of Gattefose (manufacturer);

the ginger root oil is ginger oleoresin (product name) of Kaibo Biotech Co., Ltd, Anhui.

Example 1

The temperature-sensitive facial mask comprises the following raw materials:

5 parts of caprylic/capric triglyceride, 5 parts of squalane, 1 part of polyglycerol-10 stearate, 50 parts of glycerol, 10 parts of butanediol, 0.2 part of acrylic acid (ester) copolymer sodium, 0.1 part of ginger root oil, 0.05 part of pepper seed extract, 0.1 part of fructus evodiae extract and 28.55 parts of deionized water.

The preparation method comprises the following steps:

1. preparing raw materials according to the weight ratio, uniformly mixing polyglycerol-10 stearate, glycerol, butanediol, acrylic acid (ester) copolymer sodium and deionized water, heating to 60 ℃, and preserving heat for 25min to obtain a solution A.

2. And (3) under the condition of continuously keeping the temperature, adding caprylic/capric triglyceride and squalane into the solution A, and homogenizing, emulsifying and dispersing to obtain a solution B.

3. Cooling to 30 deg.C, sequentially adding semen Piperis extract, fructus evodiae extract, and ginger root oil, stirring, and dispersing.

4. Cooling to room temperature, stirring, vacuumizing to below 0.01MPa, removing air, and packaging.

Example 2

The temperature-sensitive facial mask comprises the following raw materials:

10 parts of caprylic/capric triglyceride, 2 parts of polyglycerol-10 stearate, 45 parts of glycerol, 20 parts of butanediol, 1.5 parts of acrylic acid (ester) copolymer sodium, 0.3 part of ginger root oil, 0.08 part of pepper seed extract, 0.15 part of fructus evodiae extract and 20.97 parts of deionized water.

The preparation method comprises the following steps:

1. preparing raw materials according to the weight ratio, uniformly mixing polyglycerol-10 stearate, glycerol, butanediol, acrylic acid (ester) copolymer sodium and deionized water, heating to 60 ℃, and preserving heat for 25min to obtain a solution A.

2. And (3) under the condition of continuing heat preservation, adding caprylic acid/capric acid triglyceride into the solution A, and homogenizing, emulsifying and dispersing to obtain a solution B.

3. Cooling to 30 deg.C, sequentially adding semen Piperis extract, fructus evodiae extract, and ginger root oil, stirring, and dispersing.

4. Cooling to room temperature, stirring, vacuumizing to below 0.01MPa, removing air, and packaging.

Example 3

The temperature-sensitive facial mask comprises the following raw materials:

5 parts of meadowfoam seed oil, 8 parts of squalane, 5 parts of polyglycerol-10 stearate, 60 parts of glycerol, 1 part of acrylic acid (ester) copolymer sodium, 0.5 part of ginger root oil, 0.1 part of pepper seed extract, 0.2 part of fructus evodiae extract and 20.2 parts of deionized water.

The preparation method comprises the following steps:

1. preparing raw materials according to the weight ratio, uniformly mixing polyglycerol-10 stearate, glycerol, acrylic acid (ester) copolymer sodium and deionized water, heating to 60 ℃, and preserving heat for 25min to obtain a solution A.

2. And (3) under the condition of continuously keeping the temperature, adding the white pond flower seed oil into the solution A, and homogenizing, emulsifying and dispersing to obtain a solution B.

3. Cooling to 30 deg.C, sequentially adding semen Piperis extract, fructus evodiae extract, and ginger root oil, stirring, and dispersing.

4. Cooling to room temperature, stirring, vacuumizing to below 0.01MPa, removing air, and packaging.

Comparative example 1

The temperature-sensitive facial mask comprises the following raw materials:

10 parts of caprylic/capric triglyceride, 2 parts of polyglycerol-10 stearate, 50 parts of glycerol, 10 parts of butanediol, 1 part of acrylic acid (ester) copolymer sodium, 0.1 part of ginger root oil and 26.9 parts of deionized water.

The preparation method comprises the following steps:

1. preparing raw materials according to the weight ratio, uniformly mixing polyglycerol-10 stearate, glycerol, butanediol, acrylic acid (ester) copolymer sodium and deionized water, heating to 60 ℃, and preserving heat for 25min to obtain a solution A.

2. And (3) under the condition of continuing heat preservation, adding caprylic acid/capric acid triglyceride into the solution A, and homogenizing, emulsifying and dispersing to obtain a solution B.

3. Cooling to 30 deg.C, adding ginger root oil, stirring and dispersing.

4. Cooling to room temperature, stirring, vacuumizing to below 0.01MPa, removing air, and packaging.

Comparative example 2

The temperature-sensitive facial mask comprises the following raw materials:

3 parts of caprylic/capric triglyceride, 7 parts of jojoba seed oil, 1 part of polyglycerol-10 stearate, 40 parts of glycerol, 20 parts of butanediol, 1.5 parts of acrylic acid (ester) copolymer sodium, 0.1 part of pepper seed extract, 0.1 part of fructus evodiae extract and 27.3 parts of deionized water.

The preparation method comprises the following steps:

1. preparing raw materials according to the weight ratio, uniformly mixing polyglycerol-10 stearate, glycerol, butanediol, acrylic acid (ester) copolymer sodium and deionized water, heating to 60 ℃, and preserving heat for 25min to obtain a solution A.

2. And (3) adding caprylic/capric triglyceride and jojoba seed oil into the solution A under the condition of continuing heat preservation, and homogenizing, emulsifying and dispersing to obtain a solution B.

3. Cooling to 30 deg.C, sequentially adding semen Piperis and fructus evodiae extract, stirring and dispersing.

4. Cooling to room temperature, stirring, vacuumizing to below 0.01MPa, removing air, and packaging.

Comparative example 3

The temperature-sensitive facial mask comprises the following raw materials:

3 parts of meadowfoam seed oil, 7 parts of jojoba seed oil, 1 part of polyglycerol-10 stearate, 40 parts of glycerol, 20 parts of 1, 3-propylene glycol, 1.5 parts of acrylic acid (ester) copolymer sodium, 0.1 part of pepper seed extract, 0.1 part of ginger root oil and 27.3 parts of deionized water.

The preparation method comprises the following steps:

1. preparing raw materials according to the weight ratio, uniformly mixing polyglycerol-10 stearate, glycerol, 1, 3-propylene glycol, acrylic acid (ester) copolymer sodium and deionized water, heating to 60 ℃, and preserving heat for 25min to obtain a solution A.

2. And (3) under the condition of continuing heat preservation, adding the white pond flower seed oil and the jojoba seed oil into the solution A, and homogenizing, emulsifying and dispersing to obtain a solution B.

3. Cooling to 30 deg.C, sequentially adding semen Piperis extract and ginger root oil, stirring and dispersing.

4. Cooling to room temperature, stirring, vacuumizing to below 0.01MPa, removing air, and packaging.

Comparative example 4

The temperature-sensitive facial mask comprises the following raw materials:

3 parts of meadowfoam seed oil, 7 parts of squalane, 5 parts of polyglycerol-10 stearate, 40 parts of glycerol, 20 parts of 1, 3-propylene glycol, 1.5 parts of acrylic acid (ester) copolymer sodium, 0.1 part of fructus evodiae extract, 0.1 part of ginger root oil and 23.3 parts of deionized water.

The preparation method comprises the following steps:

1. preparing raw materials according to the weight ratio, uniformly mixing polyglycerol-10 stearate, glycerol, 1, 3-propylene glycol, acrylic acid (ester) copolymer sodium and deionized water, heating to 60 ℃, and preserving heat for 25min to obtain a solution A.

2. And (3) under the condition of continuously keeping the temperature, adding the white pond flower seed oil and squalane into the solution A, and homogenizing, emulsifying and dispersing to obtain a solution B.

3. Cooling to 30 deg.C, sequentially adding fructus evodiae extract and rhizoma Zingiberis recens root oil, stirring, and dispersing.

4. Cooling to room temperature, stirring, vacuumizing to below 0.01MPa, removing air, and packaging.

Comparative example 5

Comparative example 5 the materials and preparation method were substantially the same as those of example 1, except that ginger root oil, pepper seed extract and evodia rutaecarpa extract were equally replaced with vanillyl butyl ether.

The preparation methods of examples 1 to 3 and comparative examples 1 to 4 have the following raw material mixture ratio list:

TABLE 1

Sensory performance tests and moisturizing effect tests were performed on the temperature-sensitive masks prepared in examples 1 to 3 and comparative examples 1 to 5 as samples.

The sensory test results are shown in table 2 below.

The test method comprises the following steps:

and (5) trial investigation, wherein the number of people for each sample trial is 50, and the number of people for each sample trial is not less than 35 after abnormal exclusion. The trial effect adopts subjective scoring (1-10 points). The score is calculated statistically as follows: .

TABLE 2

Note: the above scores are average scores of effective scores.

The temperature sense refers to the strength of the heat sense felt by the tester. No thermal sensation is given for 0-2 minutes, slight thermal sensation is given for 2-4 minutes, moderate thermal sensation is given for 4-6 minutes, strong thermal sensation is given for 6-8 minutes, and strong thermal sensation is given for 8-10 minutes.

Experience refers to the degree of satisfaction of the tester with the sample. 0-2 points are not satisfactory, 2-4 points are not satisfactory, 4-6 points are basically satisfactory, 6-8 points are satisfactory, and 8-10 points are very satisfactory.

As can be seen from table 2 above, the same amount of ginger root oil was used in example 1 and comparative example 1, and the components promoting the absorption of ginger root oil, such as pepper seed extract and evodia rutaecarpa extract, were not added in comparative example 1, and the temperature feeling was significantly lower than that in example 1.

Comparative example 2 only used pepper seed extract and evodia rutaecarpa extract, and no ginger root oil, although having a certain warming effect, the feeling of warmth was low.

Example 1 used the same amount of ginger root oil as comparative examples 3 and 4, comparative example 3 did not add evodia rutaecarpa extract, comparative example 4 did not add pepper seed extract, and the temperature was significantly lower than that of example 1.

Compared with the comparative example 5, the comparative example 5 has strong heat feeling, but has high irritation, and can cause skin irritation reaction to influence the safety of the product.

Therefore, the warming effect comes from the synergistic effect of the ginger root oil, the pepper seed extract and the fructus evodiae extract, the warming strength and the warming property are both most suitable for consumers to use, the effect is milder than that of a common heating agent, namely vanillyl butyl ether, and the product is provided with more excellent experience.

And (3) testing the moistening effect:

testing an instrument: moisture test probes.

The test method comprises the following steps: the number of people for each sample to be tested is 50, and the number of people after abnormal exclusion is not less than 35. Before the test, the subject needs to clean his arms, wipe it clean with dry facial tissue, and after cleaning, sit in a constant temperature and humidity room with temperature of 22 + -1 deg.C and humidity of 50 + -5% for 30min, and keep it relaxed. The upper arm skin is selected for skin moisture content test in the experiment. The test subjects applied the test product to the test area, left for 20 minutes, washed off, and wiped dry. Skin moisture was measured 30min, 2h, 4h after application and compared to before application. The moisture content data was averaged for all subjects.

The test results are given in the following table:

of these, comparative example 5 has no test data because some of the test subjects felt strong irritancy and did not stay for 20 minutes.

The moisture test result shows that the product has good moisturizing and nourishing effects on the skin, the heating penetration enhancer can achieve the effect of influencing and promoting the penetration and absorption of substances, and further the moisturizing and nourishing effects of the product are also improved.

Therefore, the mask product provided by the invention has mild temperature, excellent skin care effect and better comprehensive experience.

The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.

The above-mentioned embodiments only express several embodiments of the present invention, so as to understand the technical solutions of the present invention specifically and in detail, but not to be understood as the limitation of the protection scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. It should be understood that the technical solutions provided by the present invention, which are obtained by logical analysis, reasoning or limited experiments, are within the scope of the appended claims. Therefore, the protection scope of the patent of the invention is subject to the content of the appended claims, and the description can be used for explaining the content of the claims.