阅读说明：本技术 一种牡丹纯露及其制备方法 (Peony hydrolat and preparation method thereof ) 是由 陈占锋 王军英 周锐 于 2021-07-26 设计创作，主要内容包括：本发明公开了一种牡丹纯露及其制备方法,由以下组分构成,包括A组分34.28%,B组分0.02%,C组分2%,D组分63.3%和E组分0.4%,所述A组分包括去离子水,EDTA 二钠,聚乙二醇-8,丙二醇,甘油和甘草酸二钾,所述B组分包括氨甲基丙醇,所述C组分包括丙二醇,对羟基苯乙酮和1,2-己二醇,所述D组分包括牡丹花水,牡丹提取物,马齿苋提取物和芍药根提取物,所述E组分包括增溶剂和香精,本发明具有补水保湿、淡化细纹、抗氧化、抗过敏、淡化色斑、提亮肤色、延缓衰老等功效,能够适用于各种肤质和人群,具有广阔的应用前景,有利于推广应用。(The invention discloses a peony hydrolat and a preparation method thereof, which comprises 34.28 percent of component A, 0.02 percent of component B, 2 percent of component C, 63.3 percent of component D and 0.4 percent of component E, the component A comprises deionized water, EDTA disodium, polyethylene glycol-8, propylene glycol, glycerol and dipotassium glycyrrhizinate, the component B comprises aminomethyl propanol, the component C comprises propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, the D component comprising peony water, a peony extract, a purslane extract and a peony root extract, the E component comprises a solubilizer and essence, and the skin care cream has the effects of moisturizing, fading fine lines, resisting oxidation, resisting allergy, fading color spots, brightening skin color, delaying senescence and the like, can be suitable for various skins and crowds, has a wide application prospect, and is beneficial to popularization and application.)

1. The peony hydrosol is characterized by being composed of a component A of 34.28%, a component B of 0.02%, a component C of 2%, a component D of 63.3% and a component E of 0.4%, wherein the component A comprises deionized water, EDTA disodium, polyethylene glycol-8, propylene glycol, glycerol and dipotassium glycyrrhizinate, the component B comprises aminomethyl propanol, the component C comprises propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, the component D comprises peony water, a peony extract, a purslane extract and a peony root extract, and the component E comprises a solubilizer and essence.

2. The peony hydrolat according to claim 1, wherein the mass ratio of the raw materials in the component A is as follows: 28.21% of deionized water, 0.02% of EDTA disodium, 81% of polyethylene glycol, 3% of propylene glycol, 2% of glycerol and 0.05% of dipotassium glycyrrhizinate.

3. The peony hydrolat according to claim 1, wherein the mass ratio of the raw materials in the component B is as follows: aminomethyl propanol 0.02%.

4. The peony hydrolat according to claim 1, wherein the mass ratio of the raw materials in the component C is as follows: 1 percent of propylene glycol, 0.5 percent of p-hydroxyacetophenone and 0.5 percent of 1, 2-hexanediol.

5. The peony hydrolat according to claim 1, wherein the mass ratio of the raw materials in the component D is as follows: 61% of peony flower water, 1.5% of peony extract, 0.3% of purslane extract and 0.5% of peony root extract.

6. The peony hydrolat according to claim 1, wherein the mass ratio of the raw materials in the component E is as follows: 0.3 percent of solubilizer and 0.1 percent of essence.

7. A method for preparing the peony hydrolat as claimed in any one of claims 1-6, comprising the steps of:

s1: sequentially adding the phase A raw materials into an emulsifying pot, stirring and heating to 80-85 ℃ at the rotating speed of 30-35r/min, and keeping the temperature for 20-30min until the materials are uniformly dissolved and no particles exist;

s2: cooling to 65-70 deg.C, adding B phase raw material, stirring for 15-20min to completely uniform without particles;

s3: cooling to 40-45 deg.C, mixing the raw materials of phase C uniformly, heating to 50-55 deg.C to dissolve, adding into emulsifying pot, and stirring to completely uniform without particles;

s4: cooling to 38-40 deg.C, sequentially adding the D phase raw materials into an emulsifying pan, and stirring for 10-15 min;

s5: cooling to 38-40 deg.C, mixing the raw materials of phase E, stirring, adding into emulsifying pot, and stirring for 10-15 min;

s6: sampling and inspecting, and filtering and discharging by a 200-mesh filter screen after the inspection is qualified.

8. The method for preparing peony hydrolat according to claim 7, wherein the stirring speed in each of S2, S3, S4 and S5 is 30-35 r/min.

Technical Field

The invention relates to the technical field of cosmetics, and particularly relates to peony hydrolat and a preparation method thereof.

Background

The hydrolat, also called water essential oil, refers to a 100% saturated distillation stock solution separated during the extraction of essential oil in the distillation extraction process, is a byproduct of essential oil, has natural and pure components and light and pleasant fragrance, and is a condensed water solution obtained by distilling aromatic plants. The pure dew contains a small amount of essential oil components and water-soluble substances in all plants, has hundreds of plant water-soluble substances, contains mineral nutrients which are lacked by the essential oil, has the characteristic of low concentration and is easily absorbed by skin, is mild and non-irritating, can be used for moisturizing every day, and can also replace pure water to prepare various facial masks and the like.

Paeoniflorin has the reputation of king in flowers and very beautiful fragrance. However, the peony seed oil is only used as an ornamental flower since ancient times, the root bark (namely the cortex moutan) of the traditional Chinese medicinal material is mainly taken, in recent years, with the fact that peony seed oil enters new resource food ranks, the peony planting area is increased in geometric progression, the yield of the peony is large, and in order to fully utilize the waste resource, a plurality of experts and scholars successively carry out comprehensive research on the components and the application of the peony. The results show that the peony essential oil, the peony fresh flower water and the peony flower extract are high-quality raw materials of daily chemical products. Therefore, there is an urgent need to develop a peony hydrolat and a preparation method thereof to satisfy the pursuit of female consumers for beauty.

In view of the above, the present invention is particularly proposed.

Disclosure of Invention

The invention aims to provide peony hydrolat which has the effects of moisturizing, fading fine lines, resisting oxidation, resisting allergy, fading color spots, brightening skin color, delaying senescence and the like, can be suitable for various skin types and crowds, has a wide application prospect, and is beneficial to popularization and application.

In order to achieve the purpose, the peony hydrosol provided by the invention comprises a component A of 34.28%, a component B of 0.02%, a component C of 2%, a component D of 63.3% and a component E of 0.4%, wherein the component A comprises deionized water, disodium EDTA, polyethylene glycol-8, propylene glycol, glycerol and dipotassium glycyrrhizinate, the component B comprises aminomethyl propanol, the component C comprises propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, the component D comprises peony water, a peony extract, a purslane extract and a peony root extract, and the component E comprises a solubilizer and a essence.

Preferably, the component A comprises the following raw materials in percentage by mass: 28.21% of deionized water, 0.02% of EDTA disodium, 81% of polyethylene glycol, 3% of propylene glycol, 2% of glycerol and 0.05% of dipotassium glycyrrhizinate.

Preferably, the mass ratio of the raw materials in the component B is as follows: aminomethyl propanol 0.02%.

Preferably, the mass ratio of the raw materials in the component C is as follows: 1 percent of propylene glycol, 0.5 percent of p-hydroxyacetophenone and 0.5 percent of 1, 2-hexanediol.

Preferably, the mass ratio of the raw materials in the component D is as follows: 61% of peony flower water, 1.5% of peony extract, 0.3% of purslane extract and 0.5% of peony root extract.

Preferably, the mass ratio of the raw materials in the component E is as follows: 0.3 percent of solubilizer and 0.1 percent of essence.

A preparation method of peony hydrolat comprises the following steps:

s1: sequentially adding the phase A raw materials into an emulsifying pot, stirring and heating to 80-85 ℃ at the rotating speed of 30-35r/min, and keeping the temperature for 20-30min until the materials are uniformly dissolved and no particles exist;

s2: cooling to 65-70 deg.C, adding B phase raw material, stirring for 15-20min to completely uniform without particles;

s3: cooling to 40-45 deg.C, mixing the raw materials of phase C uniformly, heating to 50-55 deg.C to dissolve, adding into emulsifying pot, and stirring to completely uniform without particles;

s4: cooling to 38-40 deg.C, sequentially adding the D phase raw materials into an emulsifying pan, and stirring for 10-15 min;

s5: cooling to 38-40 deg.C, mixing the raw materials of phase E, stirring, adding into emulsifying pot, and stirring for 10-15 min;

s6: sampling and inspecting, and filtering and discharging by a 200-mesh filter screen after the inspection is qualified.

Preferably, the stirring speed in S2, S3, S4 and S5 is 30-35 r/min.

The peony hydrolat and the preparation method thereof provided by the invention have the following beneficial effects.

1. The skin care product has the effects of moisturizing, fading fine lines, resisting oxidation, resisting allergy, fading color spots, brightening skin color, delaying aging and the like, can be suitable for various skins and crowds, has a wide application prospect, and is beneficial to popularization and application.

2. The components of the invention contain various natural extracts, have no toxic or side effect, are green and safe, have no irritation to skin, can be used by children, old people and pregnant women, have wide application range and have obvious effect.

Detailed Description

The present invention will be further described with reference to specific examples to assist understanding of the invention.

The invention provides peony hydrolat which comprises a component A of 34.28%, a component B of 0.02%, a component C of 2%, a component D of 63.3% and a component E of 0.4%, wherein the component A comprises deionized water, EDTA disodium, polyethylene glycol-8, propylene glycol, glycerol and dipotassium glycyrrhizinate, the component B comprises aminomethyl propanol, the component C comprises propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, the component D comprises peony water, a peony extract, a purslane extract and a peony root extract, and the component E comprises a solubilizer and essence.

The component A comprises the following raw materials in percentage by mass: 28.21% of deionized water, 0.02% of EDTA disodium, 81% of polyethylene glycol, 3% of propylene glycol, 2% of glycerol and 0.05% of dipotassium glycyrrhizinate.

The component B comprises the following raw materials in percentage by mass: aminomethyl propanol 0.02%.

The component C comprises the following raw materials in percentage by mass: 1 percent of propylene glycol, 0.5 percent of p-hydroxyacetophenone and 0.5 percent of 1, 2-hexanediol.

The component D comprises the following raw materials in percentage by mass: 61% of peony flower water, 1.5% of peony extract, 0.3% of purslane extract and 0.5% of peony root extract.

The component E comprises the following raw materials in percentage by mass: 0.3 percent of solubilizer and 0.1 percent of essence.

The invention provides a preparation method of peony hydrolat, which comprises the following steps:

s1: sequentially adding the phase A raw materials into an emulsifying pot, stirring and heating to 80-85 ℃ at the rotating speed of 30-35r/min, and keeping the temperature for 20-30min until the materials are uniformly dissolved and no particles exist;

s2: cooling to 65-70 deg.C, adding B phase raw material, stirring for 15-20min to completely uniform without particles;

s3: cooling to 40-45 deg.C, mixing the raw materials of phase C uniformly, heating to 50-55 deg.C to dissolve, adding into emulsifying pot, and stirring to completely uniform without particles;

s4: cooling to 38-40 deg.C, sequentially adding the D phase raw materials into an emulsifying pan, and stirring for 10-15 min;

s5: cooling to 38-40 deg.C, mixing the raw materials of phase E, stirring, adding into emulsifying pot, and stirring for 10-15 min;

s6: sampling and inspecting, and filtering and discharging by a 200-mesh filter screen after the inspection is qualified.

In the S2, S3, S4 and S5, the stirring speed is 30-35 r/min.

The effect comparison test is carried out on the peony hydrolat and the alfu verbena-mefone rosemary hydrolat and the Hanfang rose refined hydrolat which are better in public praise at present, and the test process is as follows:

1. 150 female volunteers aged 40-50 years and having dry facial skin were selected and randomly divided into 3 groups of 50 persons per group. Then, the face of each of the three groups of volunteers is respectively smeared with the peony hydrolat, the alfa-verbena-meyeri rosemary hydrolat and the Han prescription rose refined hydrolat, the dosage is 1ml each time in the morning and evening every day, the three groups of volunteers are fully massaged until being absorbed, the using effect is observed after 3 months, and the moisturizing and moisturizing effects of the three products are shown in Table 1.

TABLE 1 comparison of moisturizing and moisturizing effects of three products

Trial product	Obvious effect/people	General/human effects	No effect/person
				Peony hydrolat	42	8	0
AfuMabian verbena clomefone rosemary hydrolat	15	17	18
				Hanfang rose extract pure dew	12	16	22

As can be seen from table 1, after 3 months of use, in the volunteers who used the peony hydrolat of the present invention, the proportion of the moisturizing effect was 84% for the obvious one, 16% for the general one, and 0 for the non-effective one. In volunteers who used the pure dew of rosemary, the content of the water for moisturizing is only 30%, the content of the water for moisturizing is 34% and the content of the water for moisturizing is 36%. In the volunteers who use the Hanfang rose refined extract hydrolat, the water-retaining and moisturizing effect is only 24 percent, the water-retaining and moisturizing effect is 32 percent in general, and the water-retaining and moisturizing effect is 44 percent in non-effective volunteers. The comparison shows that the peony hydrolat has obvious moisturizing and moisturizing effects and far exceeds the currently better ajavazone rosemary hydrolat and hanfang rose refined hydrolat on the market.

2. 150 female volunteers aged 50-60 years and having obvious fine lines on the face were selected and randomly divided into 3 groups of 50 persons per group. Then, the face of three groups of volunteers is respectively smeared with the peony hydrosol, the alfuz-verbena rosemary hydrosol and the Hanfang rose refined hydrosol of the invention, the dosage is 1ml in the morning and evening every day, the three groups of volunteers are fully massaged until the three groups of volunteers are absorbed, the using effect is observed after 3 months, and the effect of the three products for fading the fine lines is shown in table 2.

TABLE 2 comparison of the effect of the three products for reducing the fine lines

Trial product	Obvious effect/people	General/human effects	No effect/person
				Peony hydrolat	40	10	0
AfuMabian verbena clomefone rosemary hydrolat	18	20	12
				Hanfang rose extract pure dew	16	16	18

As can be seen from Table 2, after 3 months of use, in the volunteers who used the peony hydrolat of the present invention, the effect of fading fine lines was 80% for the obvious effect, 20% for the general effect, and 0 for the non-effect. In volunteers using the African verbena-one rosemary hydrolat, the fine line fading effect is only 36 percent, the fine line fading effect is generally 40 percent, and the fine line fading effect is 24 percent. In volunteers who use Hanfang rose essence lotion, the effect of fading fine lines is only 32%, the effect of fading fine lines is 32% in general, and the effect of fading fine lines is 36% in non-effective volunteers. The comparison shows that the effect of the peony hydrolat for fading fine lines is obvious and far exceeds the currently better albizione rosemary hydrolat and Chinese rose refined hydrolat on the market.

The skin care product has the effects of moisturizing, fading fine lines, resisting oxidation, resisting allergy, fading color spots, brightening skin color, delaying aging and the like, can be suitable for various skins and crowds, has a wide application prospect, and is beneficial to popularization and application. The components of the invention contain various natural extracts, have no toxic or side effect, are green and safe, have no irritation to skin, can be used by children, old people and pregnant women, have wide application range and have obvious effect.

The inventive concept is explained in detail herein using specific examples, which are given only to aid in understanding the core concepts of the invention. It should be understood that any obvious modifications, equivalents and other improvements made by those skilled in the art without departing from the spirit of the present invention are included in the scope of the present invention.