阅读说明：本技术 一种园艺黄荆杀菌剂 (Horticultural negundo chastetree bactericide ) 是由 周德超 于 2019-10-17 设计创作，主要内容包括：本发明公开一种园艺黄荆杀菌剂,其主要由以下重量份比例的组分所制成：园艺黄荆根40-90份、园艺黄荆茎40-85份、园艺黄荆叶35-75份、园艺黄荆花35-45份、园艺黄荆子35-45份、石竹烯25-55份、贝壳粉20-30份、银杏叶3-15份、硼砂l-12份、三叶青1-13份、芦荟1-13份、白炭黑粉3-15份、芒果甙2-10份、异芒果甙5-15份、薄荷2-15份。本发明具有优异的杀菌效果,且对园艺黄荆的根、茎、叶、花、种子的新用途具有指导性意义。(The invention discloses a horticultural negundo chastetree fungicide which is mainly prepared from the following components in parts by weight: 40-90 parts of garden vitex negundo roots, 40-85 parts of garden vitex negundo stems, 35-75 parts of garden vitex negundo leaves, 35-45 parts of garden vitex negundo flowers, 35-45 parts of garden vitex negundo fruits, 25-55 parts of caryophyllene, 20-30 parts of shell powder, 3-15 parts of ginkgo leaves, l-12 parts of borax, 1-13 parts of radix tetrastigme, 1-13 parts of aloe, 3-15 parts of white carbon black powder, 2-10 parts of mangiferin, 5-15 parts of isomangiferin and 2-15 parts of mint. The invention has excellent sterilization effect and has instructive significance for new application of roots, stems, leaves, flowers and seeds of the garden negundo chastetree.)

1. A horticultural negundo chastetree fungicide is characterized by being mainly prepared from the following components in parts by weight: 40-90 parts of garden vitex negundo roots, 40-85 parts of garden vitex negundo stems, 35-75 parts of garden vitex negundo leaves, 35-45 parts of garden vitex negundo flowers, 35-45 parts of garden vitex negundo fruits, 25-55 parts of caryophyllene, 20-30 parts of shell powder, 3-15 parts of ginkgo leaves, l-12 parts of borax, 1-13 parts of radix tetrastigme, 1-13 parts of aloe, 3-15 parts of white carbon black powder, 2-10 parts of mangiferin, 5-15 parts of isomangiferin and 2-15 parts of mint.

2. The bactericide as claimed in claim 1, which is prepared from the following components in parts by weight: 45-85 parts of garden vitex negundo roots, 45-80 parts of garden vitex negundo stems, 40-74 parts of garden vitex negundo leaves, 37-43 parts of garden vitex negundo flowers, 36-43 parts of garden vitex negundo fruits, 22-50 parts of caryophyllene, 23-28 parts of shell powder, 5-13 parts of ginkgo leaves, 2-10 parts of borax, 3-10 parts of radix tetrastigme, 2-11 parts of aloe, 5-11 parts of white carbon black powder, 3-8 parts of mangiferin, 6-13 parts of isomangiferin and 3-12 parts of mint.

3. The bactericide as claimed in claim 1, which is prepared from the following components in parts by weight: 50-82 parts of horticultural vitex negundo roots, 60-78 parts of horticultural vitex negundo stems, 50-72 parts of horticultural vitex negundo leaves, 39-42 parts of horticultural vitex negundo flowers, 38-42 parts of horticultural vitex negundo fruits, 25-45 parts of caryophyllene, 25-27 parts of shell powder, 6-12 parts of ginkgo leaves, 5-8 parts of borax, 4-8 parts of radix tetrastigme, 4-9 parts of aloe, 7-10 parts of white carbon black powder, 4-7 parts of mangiferin, 7-12 parts of isomangiferin and 4-10 parts of mint.

4. The bactericide as claimed in claim 1, which is prepared from the following components in parts by weight: 80 parts of horticultural vitex negundo root, 70 parts of horticultural vitex negundo stem, 70 parts of horticultural vitex negundo leaf, 40 parts of horticultural vitex negundo flower, 40 parts of horticultural vitex negundo fruit, 35 parts of caryophyllene, 26 parts of shell powder, 8 parts of ginkgo leaf, 6 parts of borax, 6 parts of radix tetrastigme, 5 parts of aloe, 8 parts of white carbon black powder, 5 parts of mangiferin, 9 parts of isomangiferin and 8 parts of mint.

5. The fungicide according to any one of claims 1 to 4, wherein said shell powder has a particle size of 12 to 25 mm.

6. The fungicide according to any one of claims 1 to 4, wherein the particle size of said white carbon black powder is 10 to 20 mm.

7. The fungicide according to any one of claims 1 to 4, characterized in that its preparation method comprises the steps of: mixing the garden vitex negundo linn root, the garden vitex negundo linn stem, the garden vitex negundo linn leaf, the garden vitex negundo linn flower and the garden vitex negundo linn fruit according to the weight parts, adding 15-20 times of clear water, decocting for 3-5h at one time, and filtering to remove residues to obtain a first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 10-12 times of clear water, decocting for 2-4 hr, filtering to remove residue to obtain a second filtrate; mixing the first filtrate and the second filtrate, adding the rest raw materials, and stirring at 30-40 deg.C for 40-65min to obtain bactericide.

8. The bactericide as claimed in claim 7, wherein the first decoction is carried out by decocting with strong fire for 0.5-1h, and then decocting with slow fire for 2-4 h.

9. The bactericide as claimed in claim 7, wherein the second decocting is decocting with strong fire for 0.5-1h, and then decocting with slow fire for 1-3 h.

Technical Field

The invention relates to the technical field of gardening negundo chastetree, in particular to a gardening negundo chastetree bactericide.

Background

The horticultural vitex negundo is an excellent variety in vitex agnus-castus, is a small deciduous tree or shrub plant of vitex of Verbenaceae, and has fragrance throughout the plant. Square small branches, dense grey down. The leaves are opposite, palm-shaped to form compound leaves, the edges of the minor leaves are provided with a plurality of saw teeth, the upper part is green, the lower part is light green, and no hair or slight hair exists. The top of the cone-shaped inflorescence is large and bell-shaped, the top has a crown with split teeth which is purplish blue and bright, and the top has a lobe. The fruit is spherical, yellow brown to dark brown, is similar to black pepper seed in shape, has spicy fragrance, and is used as a seasoning in some areas. The flowering period is 6-10 months, and the flowering period in summer and autumn is positive, so that the aromatic plants are strong in ornamental value. Vitex agnus-castus is distributed in temperate or subtropical regions, including the middle part of Asia, the southern Europe, the Mediterranean region and the like, particularly the southern Turkish region has rich Vitex agnus-castus resources, and at present, some regions of China are introduced, such as Jiangsu, Zhejiang, Shanghai, Hubei, Chongqing, Sichuan, Anhui and the like.

Vitex agnus-castus is one of the commonly used herbs in Europe, and its therapeutic effect on diseases has been recognized in the United states, Germany, Japan, and other countries. Vitex agnus-castus fruits were documented as early as 2500 years ago to be used for the treatment of gynecological disorders such as dysmenorrhea, irregular menstruation, etc., and were said to be commonly used by herders and churches to reduce libido. In addition, since ancient Greece, the fruit has been used as a botanical drug for women's health. In turkey, residents use Vitex agnus-castus leaves to treat abdominal pain, fruits are used for diuresis, dispelling wind, and sedation, while flowers, leaves, and rhizomes are used to treat menstrual cycle disorders; in brazil, vitex agnus-castus is used for religious ceremony and park ornamental plants, and its twigs and fruits are also used for treating stomachache, headache, syphilis, etc.; in Iran folk, Vitex agnus-castus is used to treat milk disorders, convulsions, epilepsy, constipation, etc. Along with the continuous and intensive research on Vitex agnus-castus by foreign scholars, Vitex agnus-castus is gradually discovered to have estrogen-like effect and good curative effect on female diseases, Vitex agnus-castus fruit extract is approved to be used for treating irregular menstruation, premenstrual syndrome and mastalgia in Germany in 1992, and Vitex agnus-castus fruit is loaded into European pharmacopoeia to enable the Vitex agnus-castus fruit to have clear medicinal standards. Vitex agnus-castus contains numerous chemical components with biological activity. Casticin is the main chemical component and the characteristic component of casticin, and the content of casticin in casticin fruits is not less than 0.8 percent and can exert various biological activities such as anti-inflammation, anti-tumor, prolactin secretion inhibition and the like according to the regulation of European pharmacopoeia. The Vitex agnus-castus also contains abundant volatile oil components, mainly including cineole, myrtenol, pinene, sabinene, farnesene, geranene, caryophyllene and alpha-terpinyl acetate; flavones such as apigenin, luteolin, kaempferol-3-O-rutinoside, isoluteolin 6-c- (2-O-trans-caffeoyl) glucoside, vitexin and isoorientin; phenolic acids such as hydroxybenzoic acid, 3, 4-dihydroxybenzoic acid, and the like. In addition, carotenoid, chlorogenic acid, isochlorogenic acid, etc. are contained, and has antioxidant effect.

The research on the garden vitex negundo is mainly focused on the research on the medicinal value of the garden vitex negundo. In the prior art, the root, stem, leaf, flower and seed of the garden vitex negundo has been reported to be used in bactericide, and through research, the root, stem, leaf, flower and seed of the garden vitex negundo has potential bactericidal effect, and can be used as raw material components of bactericide or can obtain unexpected bactericidal effect.

Disclosure of Invention

The purpose of the invention is as follows: the invention aims to provide a horticultural negundo chastetree fungicide, which is used for improving the bactericidal effect of the fungicide and has instructive significance for new application of roots, stems, leaves, flowers and seeds of the horticultural negundo chastetree.

The technical scheme is as follows: the invention relates to a horticultural negundo chastetree fungicide, which is mainly prepared from the following components in parts by weight: 40-90 parts of garden vitex negundo roots, 40-85 parts of garden vitex negundo stems, 35-75 parts of garden vitex negundo leaves, 35-45 parts of garden vitex negundo flowers, 35-45 parts of garden vitex negundo fruits, 25-55 parts of caryophyllene, 20-30 parts of shell powder, 3-15 parts of ginkgo leaves, l-12 parts of borax, 1-13 parts of radix tetrastigme, 1-13 parts of aloe, 3-15 parts of white carbon black powder, 2-10 parts of mangiferin, 5-15 parts of isomangiferin and 2-15 parts of mint.

Preferably, the paint is mainly prepared from the following components in parts by weight: 45-85 parts of garden vitex negundo roots, 45-80 parts of garden vitex negundo stems, 40-74 parts of garden vitex negundo leaves, 37-43 parts of garden vitex negundo flowers, 36-43 parts of garden vitex negundo fruits, 22-50 parts of caryophyllene, 23-28 parts of shell powder, 5-13 parts of ginkgo leaves, 2-10 parts of borax, 3-10 parts of radix tetrastigme, 2-11 parts of aloe, 5-11 parts of white carbon black powder, 3-8 parts of mangiferin, 6-13 parts of isomangiferin and 3-12 parts of mint.

Preferably, the paint is mainly prepared from the following components in parts by weight: 50-82 parts of horticultural vitex negundo roots, 60-78 parts of horticultural vitex negundo stems, 50-72 parts of horticultural vitex negundo leaves, 39-42 parts of horticultural vitex negundo flowers, 38-42 parts of horticultural vitex negundo fruits, 25-45 parts of caryophyllene, 25-27 parts of shell powder, 6-12 parts of ginkgo leaves, 5-8 parts of borax, 4-8 parts of radix tetrastigme, 4-9 parts of aloe, 7-10 parts of white carbon black powder, 4-7 parts of mangiferin, 7-12 parts of isomangiferin and 4-10 parts of mint.

Preferably, the paint is mainly prepared from the following components in parts by weight: 80 parts of horticultural vitex negundo root, 70 parts of horticultural vitex negundo stem, 70 parts of horticultural vitex negundo leaf, 40 parts of horticultural vitex negundo flower, 40 parts of horticultural vitex negundo fruit, 35 parts of caryophyllene, 26 parts of shell powder, 8 parts of ginkgo leaf, 6 parts of borax, 6 parts of radix tetrastigme, 5 parts of aloe, 8 parts of white carbon black powder, 5 parts of mangiferin, 9 parts of isomangiferin and 8 parts of mint.

Preferably, the particle size of the shell powder is 12-25 mm.

Preferably, the particle size of the white carbon black powder is 10-20 mm.

Preferably, the preparation method comprises the following steps: mixing the garden vitex negundo linn root, the garden vitex negundo linn stem, the garden vitex negundo linn leaf, the garden vitex negundo linn flower and the garden vitex negundo linn fruit according to the weight parts, adding 15-20 times of clear water, decocting for 3-5h at one time, and filtering to remove residues to obtain a first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 10-12 times of clear water, decocting for 2-4 hr, filtering to remove residue to obtain a second filtrate; mixing the first filtrate and the second filtrate, adding the rest raw materials, and stirring at 30-40 deg.C for 40-65min to obtain bactericide.

Preferably, the first decoction is carried out by firstly decocting for 0.5-1h with strong fire and then decocting for 2-4h with slow fire.

Preferably, the secondary boiling is to boil for 0.5 to 1 hour by strong fire and then boil for 1 to 3 hours by slow fire.

Compared with the prior art, the invention has the beneficial effects that: the root, stem, leaf, flower and seed of the garden vitex negundo are selected as raw materials, and are matched with caryophyllene, shell powder, ginkgo leaf, borax, radix tetrastigme, aloe, white carbon black powder, mangiferin, isomangiferin, mint and the like, and after the raw materials are combined according to a reasonable proportion, the bactericide has a better synergistic effect, so that the garden vitex negundo has an excellent bactericidal effect. In addition, the invention also has instructive significance for the new application of roots, stems, leaves, flowers and seeds of the garden vitex negundo. In the preferred preparation method, firstly, garden vitex negundo roots, garden vitex negundo stems, garden vitex negundo leaves, garden vitex negundo flowers and garden vitex negundo seeds are mixed, 15-20 times of clear water is added, the mixture is decocted for 3-5 hours for one time, and the residue is filtered to obtain first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 10-12 times of clear water, decocting for 2-4 hr, filtering to remove residue to obtain a second filtrate, and decocting separately to obtain the final product with enhanced synergistic effect, reduced water and time, and reduced cost. Through detection, the average bacteriostasis rate of the antibacterial agent is 94% for staphylococcus aureus, escherichia coli, candida albicans and the like.

Detailed Description

The technical solution of the present invention is described in detail by the following specific examples, but the scope of the present invention is not limited to the examples.

Example 1

A horticultural negundo chastetree fungicide is mainly prepared from the following components in parts by weight: 90 parts of horticultural vitex negundo roots, 40 parts of horticultural vitex negundo stems, 75 parts of horticultural vitex negundo leaves, 45 parts of horticultural vitex negundo flowers, 35 parts of horticultural vitex negundo fruits, 55 parts of caryophyllene, 30 parts of 12mm shell powder, 3 parts of ginkgo leaves, 12 parts of borax, 1 part of radix tetrastigme, 13 parts of aloe, 15 parts of 10mm white carbon black powder, 2 parts of mangiferin, 15 parts of isomangiferin and 2 parts of mint; the preparation method comprises the following steps: mixing the garden vitex negundo linn root, the garden vitex negundo linn stem, the garden vitex negundo linn leaf, the garden vitex negundo linn flower and the garden vitex negundo linn fruit according to the weight parts, adding 20 times of clear water, decocting for 0.5h by strong fire, decocting for 4h by slow fire, and filtering to remove residues to obtain a first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 10 times of clear water, decocting with strong fire for 1 hr, decocting with slow fire for 1 hr, and filtering to remove residue to obtain a second filtrate; mixing the first filtrate and the second filtrate, adding the rest raw materials, and stirring at 40 deg.C for 40min to obtain bactericide.

The root, stem, leaf, flower and seed of the garden vitex negundo are selected as raw materials, and are matched with caryophyllene, shell powder, ginkgo leaf, borax, radix tetrastigme, aloe, white carbon black powder, mangiferin, isomangiferin, mint and the like, and after the raw materials are combined according to a reasonable ratio, the bactericide has a better synergistic effect, so that the embodiment has an excellent sterilizing effect.

Example 2

A horticultural negundo chastetree fungicide is mainly prepared from the following components in parts by weight: 40 parts of garden vitex negundo roots, 85 parts of garden vitex negundo stems, 35 parts of garden vitex negundo leaves, 45 parts of garden vitex negundo flowers, 35 parts of garden vitex negundo fruits, 55 parts of caryophyllene, 20 parts of 25mm shell powder, 15 parts of ginkgo leaves, l parts of borax, 13 parts of radix tetrastigme, 1 part of aloe, 3 parts of 20mm white carbon black powder, 10 parts of mangiferin, 5 parts of isomangiferin and 15 parts of mint; the preparation method comprises the following steps: mixing the garden vitex negundo linn root, the garden vitex negundo linn stem, the garden vitex negundo linn leaf, the garden vitex negundo linn flower and the garden vitex negundo linn fruit according to the weight parts, adding 15 times of clear water, decocting for 1 hour by strong fire, then decocting for 2 hours by slow fire, and filtering to remove residues to obtain a first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 12 times of clear water, decocting with strong fire for 0.5 hr, decocting with slow fire for 3 hr, and filtering to remove residue to obtain a second filtrate; mixing the first filtrate and the second filtrate, adding the rest raw materials, and stirring at 30 deg.C for 65min to obtain bactericide.

The root, stem, leaf, flower and seed of the garden vitex negundo are selected as raw materials, and are matched with caryophyllene, shell powder, ginkgo leaf, borax, radix tetrastigme, aloe, white carbon black powder, mangiferin, isomangiferin, mint and the like, and after the raw materials are combined according to a reasonable ratio, the bactericide has a better synergistic effect, so that the embodiment has an excellent sterilizing effect.

Example 3

A horticultural negundo chastetree fungicide is mainly prepared from the following components in parts by weight: 80 parts of horticultural vitex negundo roots, 70 parts of horticultural vitex negundo stems, 70 parts of horticultural vitex negundo leaves, 40 parts of horticultural vitex negundo flowers, 40 parts of horticultural vitex negundo fruits, 35 parts of caryophyllene, 26 parts of 18mm shell powder, 8 parts of ginkgo leaves, 6 parts of borax, 6 parts of radix tetrastigme, 5 parts of aloe, 8 parts of 15mm white carbon black powder, 5 parts of mangiferin, 9 parts of isomangiferin and 8 parts of mint; the preparation method comprises the following steps: mixing the garden vitex negundo linn root, the garden vitex negundo linn stem, the garden vitex negundo linn leaf, the garden vitex negundo linn flower and the garden vitex negundo linn fruit according to the weight parts, adding 18 times of clear water, decocting for 0.8h by strong fire, decocting for 3h by slow fire, and filtering to remove residues to obtain a first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 11 times of clear water, decocting with strong fire for 0.7 hr, decocting with slow fire for 2 hr, and filtering to remove residue to obtain a second filtrate; mixing the first filtrate and the second filtrate, adding the rest raw materials, and stirring at 35 deg.C for 50min to obtain bactericide.

The root, stem, leaf, flower and seed of the garden vitex negundo are selected as raw materials, and are matched with caryophyllene, shell powder, ginkgo leaf, borax, radix tetrastigme, aloe, white carbon black powder, mangiferin, isomangiferin, mint and the like, and after the raw materials are combined according to a reasonable ratio, the bactericide has a better synergistic effect, so that the embodiment has an excellent sterilizing effect.

Example 4

A horticultural negundo chastetree fungicide is mainly prepared from the following components in parts by weight: 45 parts of garden vitex negundo roots, 80 parts of garden vitex negundo stems, 40 parts of garden vitex negundo leaves, 43 parts of garden vitex negundo flowers, 36 parts of garden vitex negundo fruits, 50 parts of caryophyllene, 23 parts of 16mm shell powder, 13 parts of ginkgo leaves, 2 parts of borax, 10 parts of radix tetrastigme, 2 parts of aloe, 11 parts of 12mm white carbon black powder, 3 parts of mangiferin, 13 parts of isomangiferin and 3 parts of mint; the preparation method comprises the following steps: mixing the garden vitex negundo linn root, the garden vitex negundo linn stem, the garden vitex negundo linn leaf, the garden vitex negundo linn flower and the garden vitex negundo linn fruit according to the weight parts, adding 18 times of clear water, decocting for 0.8h by strong fire, decocting for 3h by slow fire, and filtering to remove residues to obtain a first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 11 times of clear water, decocting with strong fire for 0.7 hr, decocting with slow fire for 2 hr, and filtering to remove residue to obtain a second filtrate; mixing the first filtrate and the second filtrate, adding the rest raw materials, and stirring at 32 deg.C for 45min to obtain bactericide.

The root, stem, leaf, flower and seed of the garden vitex negundo are selected as raw materials, and are matched with caryophyllene, shell powder, ginkgo leaf, borax, radix tetrastigme, aloe, white carbon black powder, mangiferin, isomangiferin, mint and the like, and after the raw materials are combined according to a reasonable ratio, the bactericide has a better synergistic effect, so that the embodiment has an excellent sterilizing effect.

Example 5

A horticultural negundo chastetree fungicide is mainly prepared from the following components in parts by weight: 85 parts of horticultural vitex negundo root, 80 parts of horticultural vitex negundo stem, 40 parts of horticultural vitex negundo leaf, 43 parts of horticultural vitex negundo flower, 36 parts of horticultural vitex negundo fruit, 22 parts of caryophyllene, 28 parts of 18mm shell powder, 5 parts of ginkgo leaf, 10 parts of borax, 3 parts of radix tetrastigme, 11 parts of aloe, 5 parts of 17mm white carbon black powder, 8 parts of mangiferin, 6 parts of isomangiferin and 12 parts of mint; the preparation method comprises the following steps: mixing the garden vitex negundo linn root, the garden vitex negundo linn stem, the garden vitex negundo linn leaf, the garden vitex negundo linn flower and the garden vitex negundo linn fruit according to the weight parts, adding 16 times of clear water, decocting for 0.8h by strong fire, decocting for 3h by slow fire, and filtering to remove residues to obtain a first filtrate; mixing folium Ginkgo, radix Apioris Fortunei, Aloe and herba Menthae, adding 11 times of clear water, decocting with strong fire for 0.7 hr, decocting with slow fire for 2 hr, and filtering to remove residue to obtain a second filtrate; mixing the first filtrate and the second filtrate, adding the rest raw materials, and stirring at 37 deg.C for 60min to obtain bactericide.

The root, stem, leaf, flower and seed of the garden vitex negundo are selected as raw materials, and are matched with caryophyllene, shell powder, ginkgo leaf, borax, radix tetrastigme, aloe, white carbon black powder, mangiferin, isomangiferin, mint and the like, and after the raw materials are combined according to a reasonable ratio, the bactericide has a better synergistic effect, so that the embodiment has an excellent sterilizing effect.

As noted above, while the present invention has been shown and described with reference to certain preferred embodiments, it is not to be construed as limited thereto. Various changes in form and detail may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.