Visual electric dehydration and electric desalting experimental device

文档序号:758542 发布日期:2021-04-06 浏览:48次 中文

阅读说明:本技术 一种可视化电脱水电脱盐实验装置 (Visual electric dehydration and electric desalting experimental device ) 是由 刘建春 刘家诚 姚磊 王洪福 韦伟 张立新 于 2020-11-23 设计创作,主要内容包括:本发明公开了一种可视化电脱水电脱盐实验装置,包括分离器、加热管和沉淀罐,分离器底部通过螺栓连接有支架,加热管和沉淀罐依次通过螺栓连接在支架上端,加热管进液管通过管道与分离器出液口连通,加热管出液口通过管道与沉淀罐连通,支架下端一侧通过螺栓连接有储液罐;本发明通过将分离器、加热管和沉淀罐安装在支架上,同时在支架底部安装储液罐与沉淀罐对接,在分离器内部安装带有通孔结构的分配板,在分配板中间安装插板,调整插板在分配板中间的位置,使得插板与分配板侧壁开设的通孔错开,改变通孔的大小,从而调整通孔分散的油液的颗粒大小,适应不同状态的油液分散工作。(The invention discloses a visual electric dehydration and electric desalination experimental device which comprises a separator, a heating pipe and a settling tank, wherein the bottom of the separator is connected with a support through a bolt; the separator, the heating pipe and the settling tank are arranged on the support, the liquid storage tank is arranged at the bottom of the support and is in butt joint with the settling tank, the distributing plate with the through hole structure is arranged in the separator, the inserting plate is arranged in the middle of the distributing plate, the position of the inserting plate in the middle of the distributing plate is adjusted, the inserting plate and the through hole formed in the side wall of the distributing plate are staggered, and the size of the through hole is changed, so that the size of oil particles dispersed by the through hole is adjusted, and the oil dispersing device is suitable for oil dispersing.)

1. The utility model provides a visual electric dehydration electric desalting experimental apparatus, includes separator (1), heating pipe (2) and gunbarrel (3), its characterized in that: the bottom of the separator (1) is connected with a support (4) through a bolt, the heating pipe (2) and the settling tank (3) are sequentially connected to the upper end of the support (4) through bolts, a liquid inlet pipe of the heating pipe (2) is communicated with a liquid outlet of the separator (1) through a pipeline, the liquid outlet of the heating pipe (2) is communicated with the settling tank (3) through a pipeline, and one side of the lower end of the support (4) is connected with a liquid storage tank (5) through a bolt;

the separator is characterized in that a distribution plate (6) is welded on one side inside the separator (1), the distribution plate (6) is of a hollow structure, a plug board (7) is inserted into a middle cavity of the distribution plate (6), the same through holes (8) are formed in the side walls of the distribution plate (6) and the plug board (7), a motor (9) is connected to the top of the separator (1) through bolts, a lead screw (10) is connected to the side wall of the top of the separator (1) through a bearing, the upper end of the lead screw (10) is connected with a main shaft of the motor (9) through a coupler, the lower end of the lead screw (10) is inserted into the inner side of a middle through groove of the plug board (7), a ball nut (11) is connected to the lower end of the lead screw (10;

separator (1) inside intermediate position has electrode plate (12) through bolted connection, separator (1) lateral wall intermediate position is logical groove structure, just separator (1) lateral wall middle logical groove lateral wall is packaged with baffle (13), it has glass board (14) to package in the middle of baffle (13), glass board (14) are located electrode plate (12) outside.

2. The visual electric dehydration and electric desalting experimental device according to claim 1, characterized in that: the side wall of the support (4) is connected with a temperature control switch (15) through a bolt, and the temperature control switch (15) is electrically connected with the heating pipe (2) through a lead.

3. The visual electric dehydration and electric desalting experimental device according to claim 1, characterized in that: the side wall of the distribution plate (6) is provided with a strip-shaped groove (16), the middle of the strip-shaped groove (16) is connected with a pointer (17) in a sliding and clamping mode, and the end portion of the pointer (17) is located on the side wall of the glass plate (14).

4. The visual electric dehydration and electric desalting experimental device according to claim 3 is characterized in that: the end part of the pointer (17) is connected to the side wall of the inserting plate (7) through a bolt, and the length of the strip-shaped groove (16) is smaller than that of the inserting plate (7).

5. The visual electric dehydration and electric desalting experimental device according to claim 3 is characterized in that: the side wall of the glass plate (14) is pasted with a scale plate (18), and the tip of the pointer (17) is positioned on one side of the scale line of the scale plate (18).

6. The visual electric dehydration and electric desalting experimental device according to claim 1, characterized in that: the bottom of the separator (1) and the bottom of the settling tank (3) are welded with sewage pipeline structures of the same specification, and the lower end of the sewage pipeline is hermetically provided with a valve (19).

7. The visual electric dehydration and electric desalting experimental device according to claim 1, characterized in that: the side wall of the lower end of the side wall of the bracket (4) is connected with a reversing switch (20) through a bolt, and the reversing switch (20) is electrically connected with the motor (9) through a wire.

Technical Field

The invention relates to the technical field of crude oil processing, in particular to a visual electric dehydration and electric desalting experimental device.

Background

The crude oil entering the refinery, although being dewatered at the field, still contains a greater or lesser amount of salt and water. The salts (such as sodium chloride, calcium chloride, magnesium chloride and the like) contained in the crude oil are mostly dissolved in water to form water-in-oil emulsion; also a small fraction of salt crystals are suspended in the oil. In order not to affect the crude oil processing, the crude oil is desalted and dehydrated in the first step after entering the plant. The method for removing the crude oil is to add a small amount of water (about 5 percent) to be fully mixed, to make salt completely dissolved in the water, then to add a selected demulsifier, to make water drops grow under the action of an electric field and obtain sedimentation separation under a certain condition (the temperature is properly high to reduce the crude oil temperature, and the pressure is higher than the temperature by F and the saturated vapor pressure of the oil is 0.1-0.35 MPa). This process is known as desalting and dewatering of crude oil. Desalting and dewatering are carried out simultaneously. The demulsifiers used are chemicals, so they are also called crude oil chemical desalting and dewatering, and also called crude oil electric desalting and dewatering under the electric field.

In the prior art, crude oil is in the refining process, because the distributing plate part in the separator is fixed inside the separator, the through-hole size of distributing plate lateral wall is fixed, and the distributing plate is inconsistent to the dispersion effect of the crude oil of different concentrations, and the lower fluid of concentration need disperse with less through-hole, and the effect is just good, uses the distributing plate of large aperture to lead to the dispersion efficiency to reduce, and inconvenient observation moreover.

Therefore, the invention is necessary to invent a visual electric dehydration and electric desalting experimental device.

Disclosure of Invention

The invention aims to provide a visual electric dehydration and electric desalting experimental device which has the advantages that a visual window part is added for observing the reaction state in a separator, meanwhile, an inserting plate assembly is added for matching and adjusting the size of a through hole in the side wall of a distributing plate, and the problem that the existing distributing plate has inconsistent dispersion effects on crude oil with different concentrations is solved.

In order to achieve the purpose, the invention provides the following technical scheme: a visual electric dehydration and electric desalination experimental device comprises a separator, a heating pipe and a settling tank, wherein the bottom of the separator is connected with a support through a bolt, the heating pipe and the settling tank are sequentially connected to the upper end of the support through bolts, a liquid inlet pipe of the heating pipe is communicated with a liquid outlet of the separator through a pipeline, the liquid outlet of the heating pipe is communicated with the settling tank through a pipeline, and one side of the lower end of the support is connected with a liquid storage tank through a bolt;

a distribution plate is welded on one side inside the separator, the distribution plate is of a hollow structure, an insertion plate is inserted into a middle cavity of the distribution plate in an inserted manner, the distribution plate and the side wall of the insertion plate are provided with the same through hole, the top of the separator is connected with a motor through a bolt, the side wall of the top of the separator is connected with a lead screw through a bearing, the upper end of the lead screw is connected with a motor spindle through a coupler, the lower end of the lead screw is inserted into the inner side of a middle through groove of the insertion plate, the lower end of the lead screw is in threaded connection with;

the separator is characterized in that a plate electrode is connected to the middle of the inside of the separator through a bolt, the middle of the outer side wall of the separator is of a through groove structure, a partition plate is packaged on the side wall of the through groove in the middle of the outer side wall of the separator, a glass plate is packaged in the middle of the partition plate, and the glass plate is located on the outer side of the plate electrode.

Preferably, the side wall of the bracket is connected with a temperature control switch through a bolt, and the temperature control switch is electrically connected with the heating pipe through a lead.

Preferably, the side wall of the distribution plate is provided with a strip-shaped groove, the middle of the strip-shaped groove is connected with a pointer in a sliding and clamping mode, and the end part of the pointer is located on the side wall of the glass plate.

Preferably, the end part of the pointer is connected to the side wall of the inserting plate through a bolt, and the length of the strip-shaped groove is smaller than that of the inserting plate.

Preferably, a scale plate is adhered to the side wall of the glass plate, and the pointer tip is positioned on one side of the scale line of the scale plate.

Preferably, the bottom of the separator and the bottom of the sedimentation tank are welded with sewage pipeline structures with the same specification, and the lower end of the sewage pipeline is hermetically provided with a valve.

Preferably, the lateral wall of the lower end of the lateral wall of the bracket is connected with a reversing switch through a bolt, and the reversing switch is electrically connected with the motor through a wire.

Compared with the prior art, the invention has the following beneficial effects:

1. according to the invention, the separator, the heating pipe and the precipitation tank are arranged on the bracket, and meanwhile, the liquid storage tank is arranged at the bottom of the bracket and is butted with the precipitation tank, so that oil liquid precipitated and separated from the precipitation tank is conveniently conveyed into the liquid storage tank for subsequent purification treatment;

2. the invention installs the distributing plate with the through hole structure in the separator, when the oil enters from the end of the separator, when the oil passes through the through holes in the middle of the distributing plate, the oil can be gradually dispersed into a certain size along with the limit of the through holes and passes through the middle of the through holes, then on the other side of the through hole, part of the oil liquid can be gathered and combined again, part of impurities are separated from the oil liquid and are precipitated to the bottom of the separator, a plug board is arranged in the middle of the distributing board, a motor is arranged at the top of the separator and connected with a screw rod on the side wall of the separator, the power supply of the motor is switched on, the motor can drive the screw rod to rotate, the ball nut drives the inserting plate to move along the middle groove of the distributing plate, the position of the inserting plate in the middle of the distributing plate is adjusted, the inserting plate is staggered with the through hole formed in the side wall of the distributing plate, the size of the through hole is changed, thereby adjusting the particle size of the oil dispersed by the through holes and adapting to the oil dispersion work in different states; the electrode plates are additionally arranged inside the separator and are electrified, so that oil liquid inside the separator can be electrified, the mixture added inside the separator is matched, water and salt substances in the oil liquid are subjected to electrolytic separation, and the oil in the oil liquid is conveniently separated from impurities.

Drawings

FIG. 1 is a schematic structural view of the present invention;

FIG. 2 is a schematic diagram of the internal components of the present invention;

FIG. 3 is a schematic view of a distributor plate assembly according to the present invention;

FIG. 4 is a schematic top view of a distributor plate assembly according to the present invention.

In the figure: 1. a separator; 2. heating a tube; 3. a settling tank; 4. a support; 5. a liquid storage tank; 6. a distribution plate; 7. inserting plates; 8. a through hole; 9. a motor; 10. a screw rod; 11. a ball nut; 12. an electrode plate; 13. a partition plate; 14. a glass plate; 15. a temperature control switch; 16. a strip-shaped groove; 17. a pointer; 18. a scale plate; 19. a valve; 20. a reversing switch.

Detailed Description

The following detailed description of the present invention is given for the purpose of better understanding technical solutions of the present invention by those skilled in the art, and the present description is only exemplary and explanatory and should not be construed as limiting the scope of the present invention in any way.

It should be noted that: like reference numbers and letters refer to like items in the following figures, and thus, once an item is defined in one figure, it need not be further defined and explained in subsequent figures.

It is to be understood that the terms "center," "upper," "lower," "left," "right," "vertical," "horizontal," "inner," "outer," and the like are used in a generic and descriptive sense only and not for purposes of limitation, the terms "center," "upper," "lower," "left," "right," "vertical," "horizontal," "inner," "outer," and the like are used in the generic and descriptive sense only and not for purposes of limitation, as the term is used in the generic and descriptive sense, and not for purposes of limitation, unless otherwise specified or implied, and the specific reference to a device or element is intended to be a reference to a particular element, structure, or component. Furthermore, the terms "first," "second," "third," and the like are used solely to distinguish one from another and are not to be construed as indicating or implying relative importance.

Furthermore, the terms "horizontal", "vertical", "overhang" and the like do not imply that the components are required to be absolutely horizontal or overhang, but may be slightly inclined. For example, "horizontal" merely means that the direction is more horizontal than "vertical" and does not mean that the structure must be perfectly horizontal, but may be slightly inclined.

In the description of the present invention, it should also be noted that, unless otherwise explicitly specified or limited, the terms "disposed," "mounted," "connected," and "connected" are to be construed broadly and may, for example, be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.

Referring to fig. 1-4, a visual electric dehydration and electric desalination experimental device comprises a separator 1, a heating pipe 2 and a settling tank 3, wherein the bottom of the separator 1 is connected with a support 4 through a bolt, the heating pipe 2 and the settling tank 3 are sequentially connected with the upper end of the support 4 through bolts, a liquid inlet pipe of the heating pipe 2 is communicated with a liquid outlet of the separator 1 through a pipeline, a liquid outlet of the heating pipe 2 is communicated with the settling tank 3 through a pipeline, and one side of the lower end of the support 4 is connected with a liquid storage tank 5 through a bolt;

the separator 1, the heating pipe 2 and the settling tank 3 are arranged on the support 4, meanwhile, the liquid storage tank 5 is arranged at the bottom of the support 4 and is in butt joint with the settling tank 3, oil liquid precipitated and separated from the settling tank 3 is conveniently conveyed into the liquid storage tank 5, subsequent purification treatment is conveniently carried out, the separator 1 is used for separating oil and an oil-gas mixture or oil and emulsion, the separated oil liquid is conveyed into the heating pipe 2 for heating, subsequent dosing and settling reaction is convenient, oil liquid after settling reaction is extracted, and the upper oil liquid is conveyed into the liquid storage tank 5 for storage;

a distributing plate 6 is welded on one side inside the separator 1, the distributing plate 6 is of a hollow structure, an inserting plate 7 is inserted into a middle cavity of the distributing plate 6, the same through hole 8 is formed in the side walls of the distributing plate 6 and the inserting plate 7, the top of the separator 1 is connected with a motor 9 through a bolt, the side wall of the top of the separator 1 is connected with a lead screw 10 through a bearing, the upper end of the lead screw 10 is connected with a main shaft of the motor 9 through a coupler, the lower end of the lead screw 10 is inserted into the inner side of a middle through groove of the inserting plate 7, the lower end of the lead screw 10;

a distribution plate 6 with a through hole 8 structure is arranged in the separator 1, when oil enters from the end part of the separator 1 and passes through the through hole 8 in the middle of the distribution plate 6, the oil can be gradually dispersed into a certain size along with the limit of the through hole 8, the oil passes through the middle of the through hole 8, then part of the oil can be gathered and combined again on the other side of the through hole 8, part of impurities can be separated from the oil and deposited at the bottom of the separator 1, an inserting plate 7 is arranged in the middle of the distribution plate 6, a motor 9 is arranged at the top of the separator 1 and connected with a screw rod 10 on the side wall of the separator 1, the power supply of the motor 9 is switched on, the motor 9 can drive the screw rod 10 to rotate, so that a ball nut 11 drives the inserting plate 7 to move along a middle groove of the distribution plate 6, the position of the inserting plate 7 in the middle of, thereby adjusting the particle size of the oil dispersed by the through holes 8 and adapting to the oil dispersion work in different states;

an electrode plate 12 is connected to the middle position inside the separator 1 through a bolt, the middle position of the outer side wall of the separator 1 is of a through groove structure, a partition plate 13 is packaged on the side wall of the through groove in the middle of the outer side wall of the separator 1, a glass plate 14 is packaged in the middle of the partition plate 13, and the glass plate 14 is located on the outer side of the electrode plate 12.

An electrode plate 12 is added in the separator 1, when the electrode plate 12 is electrified, oil liquid in the separator 1 is electrified, water and salt substances in the oil liquid are electrolyzed and separated by matching with a mixture added in the separator 1, and the oil in the oil liquid is conveniently separated from impurities;

specifically, the side wall of the bracket 4 is connected with a temperature control switch 15 through a bolt, and the temperature control switch 15 is electrically connected with the heating pipe 2 through a lead;

a temperature control switch 15 is installed on the side wall of the support 4, the temperature control switch 15 is used for adjusting the heating temperature of the heating pipe 2 to meet the oil heating requirements of different states, the heating pipe 2 is a conventional heating pipe, the conventional heating pipe 2 is formed by filling an electric heating wire into a seamless metal pipe (a carbon steel pipe, a titanium pipe, a stainless steel pipe and a copper pipe), and a gap part is filled with magnesium oxide powder with good thermal conductivity and insulativity and then is contracted to form a pipe, and the pipe is processed into a pipe shape to facilitate the heating of liquid;

specifically, a strip-shaped groove 16 is formed in the side wall of the distribution plate 6, a pointer 17 is slidably clamped in the middle of the strip-shaped groove 16, the end portion of the pointer 17 is located on the side wall of the glass plate 14, the end portion of the pointer 17 is connected to the side wall of the insertion plate 7 through a bolt, the length of the strip-shaped groove 16 is smaller than that of the insertion plate 7, a scale plate 18 is adhered to the side wall of the glass plate 14, and the tip of the pointer 17 is located on one side;

a strip-shaped groove 16 part is added on the side wall of the distribution plate 6, a pointer 17 is arranged in the middle of the strip-shaped groove 16 and connected with the insertion plate 7, when the insertion plate 7 moves, the pointer 17 can also move up and down along with the insertion plate 7 and is matched with a scale plate 18 arranged on the side wall of the glass plate 14, so that the height of the current position of the insertion plate 7 connected with the pointer 17 can be observed, the mutual staggered distance between the through hole 8 on the side wall of the insertion plate 7 and the through hole 8 on the side wall of the distribution plate 6 is calculated, the size of the through hole 8 is adjusted;

specifically, the bottom of the separator 1 and the bottom of the settling tank 3 are welded with sewage pipeline structures with the same specification, and the lower end of the sewage pipeline is hermetically provided with a valve 19;

valves 19 are arranged on the sewage discharge pipelines at the bottoms of the separator 1 and the settling tank 3, so that the separator 1 and the settling tank 3 can be conveniently cleaned;

specifically, the side wall of the lower end of the side wall of the bracket 4 is connected with a reversing switch 20 through a bolt, and the reversing switch 20 is electrically connected with the motor 9 through a lead;

the lower end of the bracket 4 is provided with a reversing switch 20, the reversing switch 20 is used for adjusting the rotation direction of the motor 9, the motor 9 drives the screw rod 10 to rotate forward and backward, so that the ball nut 11 component drives the inserting plate 7 to correspondingly lift, the staggered size of the inserting plate 7 and the through hole 8 on the side wall of the distributing plate 6 is adjusted, and the crude oil separation work in different states is adapted.

When the device is used, the separator 1, the heating pipe 2 and the settling tank 3 are installed on the support 4, the liquid storage tank 5 is installed at the bottom of the support 4 and is in butt joint with the settling tank 3, oil liquid precipitated and separated from the settling tank 3 is conveniently conveyed into the liquid storage tank 5, subsequent purification treatment is conveniently carried out, the separator 1 is used for separating oil and an oil-gas mixture or oil and emulsion, the separated oil liquid is conveyed into the heating pipe 2 for heating, subsequent dosing and settling reaction is convenient, oil liquid after settling reaction is extracted and conveyed into the liquid storage tank 5 for storage; a distribution plate 6 with a through hole 8 structure is arranged in the separator 1, when oil enters from the end part of the separator 1 and passes through the through hole 8 in the middle of the distribution plate 6, the oil can be gradually dispersed into a certain size along with the limit of the through hole 8, the oil passes through the middle of the through hole 8, then part of the oil can be gathered and combined again on the other side of the through hole 8, part of impurities can be separated from the oil and deposited at the bottom of the separator 1, an inserting plate 7 is arranged in the middle of the distribution plate 6, a motor 9 is arranged at the top of the separator 1 and connected with a screw rod 10 on the side wall of the separator 1, the power supply of the motor 9 is switched on, the motor 9 can drive the screw rod 10 to rotate, so that a ball nut 11 drives the inserting plate 7 to move along a middle groove of the distribution plate 6, the position of the inserting plate 7 in the middle of, thereby adjusting the particle size of the oil dispersed by the through holes 8 and adapting to the oil dispersion work in different states; the electrode plates 12 are additionally arranged in the separator 1, the oil liquid in the separator 1 is electrified by electrifying the electrode plates 12, and water and salt substances in the oil liquid are subjected to electrolytic separation by matching with the mixture added in the separator 1, so that the oil in the oil liquid is conveniently separated from impurities.

The standard parts used in the present application document can be purchased from the market, and can be customized according to the description of the specification and the accompanying drawings, the specific connection mode of each part adopts the conventional means of mature bolts, rivets, welding and the like in the prior art, the machines, parts and equipment adopt the conventional models in the prior art, the control mode is automatically controlled by a controller, the control circuit of the controller can be realized by simple programming of technicians in the field, the present invention belongs to the common knowledge in the field, and the present invention is mainly used for protecting mechanical devices, so the present invention does not explain the control mode and the circuit connection in detail, and the peripheral controllers mentioned in the specification can play a control role for the electric elements mentioned in the text, and the peripheral controllers are conventional known equipment.

It should be noted that, in this document, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

The principles and embodiments of the present invention are explained herein using specific examples, which are presented only to assist in understanding the method and its core concepts of the present invention. It should be noted that there are no specific structures but a few objective structures due to the limited character expressions, and that those skilled in the art may make various improvements, decorations or changes without departing from the principle of the invention or may combine the above technical features in a suitable manner; such modifications, variations, combinations, or adaptations of the invention using its spirit and scope, as defined by the claims, may be directed to other uses and embodiments.

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