Kneading device capable of detecting pressure and dispersion degree and method for manufacturing same
阅读说明:本技术 能够检测压力及分散度的混炼装置及其制造方法 (Kneading device capable of detecting pressure and dispersion degree and method for manufacturing same ) 是由 齐藤久司 木岛敬昌 于 2020-02-10 设计创作,主要内容包括:本发明的课题在于提供一种即使在混炼处理中也能够准确且直接地确认混炼装置内的混炼物的状态的混炼装置。为了解决上述课题,提供一种混炼装置,其使分散质分散于非导电性材料中,其特征在于,具备:压力测量部,具有与由所述非导电性材料和所述分散质构成的混炼物接触的受压部,并且测量施加于由所述非导电性材料和所述分散质构成的混炼物的压力值;及判定部,根据所述压力测量部所测量的压力值来判定所述非导电性材料中的所述分散质的分散状态。(The invention provides a kneading device which can accurately and directly confirm the state of a kneaded material in the kneading device even in a kneading process. In order to solve the above problem, a kneading apparatus for dispersing a dispersoid in a non-conductive material is provided, comprising: a pressure measuring section having a pressure receiving section that is in contact with a kneaded product composed of the non-conductive material and the dispersoid, and measuring a pressure value applied to the kneaded product composed of the non-conductive material and the dispersoid; and a determination unit that determines a dispersion state of the dispersoid in the non-conductive material based on the pressure value measured by the pressure measurement unit.)
1. A kneading apparatus for dispersing a dispersoid in a non-conductive material, comprising:
a pressure measuring section having a pressure receiving section that is in contact with a kneaded product composed of the non-conductive material and the dispersoid, and measuring a pressure value applied to the kneaded product composed of the non-conductive material and the dispersoid; and
a determination unit that determines a dispersion state of the dispersoid in the non-conductive material based on the pressure value measured by the pressure measurement unit.
2. The kneading apparatus according to claim 1,
the dispersoid is a dispersoid with conductivity,
the kneading apparatus further comprises an electrical characteristic measuring unit having an electrode unit that is in contact with the kneaded product composed of the non-conductive material and the conductive dispersoid, and a voltage applying unit that applies a predetermined voltage for measurement between a pair of electrodes included in the electrode unit, and measuring an electrical characteristic value of the kneaded product,
the determination section corrects a relationship between the electrical characteristic value measured by the electrical characteristic measurement section and a dispersion state using the pressure value measured by the pressure measurement section, thereby determining the dispersion state of the dispersoid having conductivity in the non-conductive material.
3. The kneading apparatus according to claim 2,
further comprising a temperature measuring unit having a thermosensitive part that comes into contact with a kneaded product composed of the non-conductive material and the conductive dispersoid and measuring a temperature value of the kneaded product composed of the non-conductive material and the conductive dispersoid,
the determination unit corrects a relationship between an electrical characteristic value measured by the electrical characteristic measurement unit and a dispersion state using a pressure value measured by the pressure measurement unit and a temperature value measured by the temperature measurement unit, thereby determining a dispersion state of the dispersoid having conductivity in the non-conductive material.
4. The kneading apparatus according to claim 3,
the electrical characteristic measuring unit and the pressure measuring unit are disposed in close proximity to each other.
5. The kneading apparatus according to any one of claims 2 to 4,
the electrode portion has a cylindrical shape, and the pressure receiving portion is disposed inside the cylindrical electrode portion.
6. A method for producing a kneaded product by dispersing a dispersoid in a non-conductive material, the method comprising:
a pressure measurement step of measuring a pressure value applied to a kneaded product composed of the non-conductive material and the dispersoid; and
a determination step of determining a dispersion state of the dispersoid in the non-conductive material based on the pressure value measured in the pressure measurement step.
Technical Field
The present invention relates to a kneading apparatus for uniformly mixing two or more substances in all fields of chemical industry, plastic industry, pharmaceutical industry, and the like.
Background
A kneading apparatus is widely used, and for example, in the production of rubber products, an internal kneading apparatus is used in a step of mixing and kneading a raw material rubber and an additive such as an additive ingredient or a filler to produce a compounded rubber. For example, patent document 1 describes a horizontal twin-shaft kneading apparatus in which two mixing chambers are arranged in parallel, the two mixing chambers are connected to each other via a region below a ram and a region above a bridge, and a plurality of rotor blades having shape characteristics are attached to each of the two mixing chambers. In this horizontal twin-shaft kneading apparatus, the rotors are arranged parallel to each other and are rotatable, and by rotating these rotors in opposite directions to each other, the kneaded material can be transferred between the mixing spaces.
Patent document 1: japanese laid-open patent publication No. 4-166222
In kneading of rubber and the like, it is necessary to finely divide the additive and uniformly disperse the additive in the rubber raw material, and thus poor dispersion causes deterioration in the quality of the rubber product.
Therefore, in the internal kneading apparatus, the kneading time, the temperature inside the kneading apparatus, the power consumption, the position of the ram, and other externally observable values are measured, and the kneading process is managed when these values reach predetermined values, thereby maintaining the product quality constant. However, these values are merely indirect representations of the state of the kneaded product, and it is not clear what state the kneaded product is actually in. On the other hand, as a method of directly checking the state of the kneaded material, there is a method of opening the internal kneading apparatus, sampling a part of the kneaded material, and performing a predetermined inspection of the sampled kneaded material, but this is not preferable from the viewpoint of work efficiency.
Therefore, a kneading apparatus capable of accurately confirming the state of a kneaded material without sampling the kneaded material is desired.
Disclosure of Invention
That is, an object of the present invention is to provide a kneading apparatus capable of accurately confirming the state of a kneaded material in the kneading apparatus even during a kneading process.
The present inventors have conducted intensive studies on the above problems, and as a result, have obtained the following findings: in the kneading apparatus, the dispersion state of the dispersoid in the kneaded material can be accurately determined based on the pressure value applied to the kneaded material composed of the non-conductive material and the dispersoid. The present invention has been accomplished based on this finding.
That is, the present invention relates to a kneading apparatus and a method for producing a kneaded product as follows.
In order to solve the above problem, the present invention provides a kneading apparatus for dispersing a dispersoid in a non-conductive material, the kneading apparatus comprising: a pressure measuring section having a pressure receiving section that is in contact with a kneaded product composed of the non-conductive material and the dispersoid, and measuring a pressure value applied to the kneaded product composed of the non-conductive material and the dispersoid; and a determination unit that determines a dispersion state of the dispersoid in the non-conductive material based on the pressure value measured by the pressure measurement unit.
In a kneaded product containing a dispersoid, an index indicating a dispersion state of the dispersoid varies depending on a pressure value applied to the kneaded product. Therefore, according to the kneading apparatus, the dispersion state of the dispersoid in the kneaded material is determined based on the pressure value applied to the kneaded material, and therefore, the dispersion state of the kneaded material can be accurately determined.
In addition, an embodiment of the kneading apparatus according to the present invention is characterized in that the dispersoid is a conductive dispersoid, the kneading apparatus further includes an electrical characteristic measurement unit that has an electrode unit that comes into contact with a kneaded product composed of a non-conductive material and the conductive dispersoid, and a voltage application unit that applies a predetermined voltage for measurement between a pair of electrodes included in the electrode unit, and measures an electrical characteristic value of the kneaded product, and the determination unit determines the dispersion state of the conductive dispersoid in the non-conductive material by correcting a relationship between the electrical characteristic value measured by the electrical characteristic measurement unit and the dispersion state using a pressure value measured by the pressure measurement unit.
In a kneaded product containing a dispersoid having conductivity, an index indicating a dispersion state of the dispersoid varies depending on a pressure value applied to the kneaded product. Therefore, according to the above feature, the electrical characteristic value of the kneaded material containing the dispersoid having conductivity is measured, the dispersion state of the dispersoid having conductivity in the kneaded material is measured from the electrical characteristic value, and the correction is performed based on the pressure value measured by the pressure measuring unit, whereby the dispersion state of the kneaded material can be confirmed directly and accurately.
In addition, an embodiment of the kneading apparatus according to the present invention is characterized in that the kneading apparatus further includes a temperature measuring unit that has a heat sensitive portion that is in contact with the kneaded product composed of the non-conductive material and the dispersoid having conductivity, and that measures a temperature value of the kneaded product composed of the non-conductive material and the dispersoid having conductivity, and the determining unit determines the dispersion state of the dispersoid having conductivity in the non-conductive material by correcting a relationship between the electrical characteristic value measured by the electrical characteristic measuring unit and the dispersion state using a pressure value measured by the pressure measuring unit and a temperature value measured by the temperature measuring unit.
In a kneaded product containing a dispersoid having conductivity, an index indicating a dispersion state of the dispersoid varies depending on a temperature value of the kneaded product. Therefore, according to the above feature, the electrical characteristic value of the kneaded product including the electrically conductive dispersoid is measured, the dispersion state of the electrically conductive dispersoid in the kneaded product is measured from the electrical characteristic value, and the dispersion state of the kneaded product is corrected using the pressure value measured by the pressure measuring unit and the temperature value measured by the temperature measuring unit, whereby the dispersion state of the kneaded product can be directly and accurately confirmed.
In one embodiment of the kneading apparatus of the present invention, the electrical characteristic measuring unit and the pressure measuring unit are disposed in close proximity to each other.
If an electrical characteristic measuring section for measuring an electrical characteristic value of the kneaded product and a pressure measuring section for measuring a pressure value applied to the kneaded product are provided at positions apart from each other in the apparatus, the electrical characteristic value and the pressure value may be values measured for the kneaded products in different states. According to this kneading apparatus, since the electrical characteristic measuring unit and the pressure measuring unit are disposed close to each other, the electrical characteristic value and the pressure value can be measured with respect to the kneaded material in the same or similar state. Therefore, the kneading apparatus exhibits the following effects: when the characteristic value is corrected using the pressure value, appropriate correction is obtained, and the dispersion state of the kneaded material can be determined more accurately.
In one embodiment of the kneading apparatus of the present invention, the electrode portion has a cylindrical shape, and the pressure receiving portion is disposed inside the cylindrical electrode portion.
According to this kneading apparatus, the pressure value and the electrical characteristic value can be measured at the same position of the kneaded material by arranging the positions at which the pressure value and the electrical characteristic value are measured in a limited manner. Therefore, the kneading apparatus exhibits the following effects: when the characteristic value is corrected using the pressure value, appropriate correction is obtained, and the dispersion state of the kneaded material can be determined more accurately.
In order to solve the above problems, the present invention provides a kneading method for producing a kneaded product by dispersing a dispersoid in a non-conductive material, the method comprising the steps of: a pressure measurement step of measuring a pressure value applied to a kneaded product composed of the non-conductive material and the dispersoid; and a determination step of determining a dispersion state of the dispersoid in the non-conductive material based on the pressure value measured in the pressure measurement step.
According to the method for producing a kneaded product, the dispersion state of the dispersoid having conductivity in the kneaded product is determined based on the pressure value applied to the kneaded product, and therefore, the dispersion state of the kneaded product can be accurately determined.
According to the present invention, it is possible to provide a kneading apparatus capable of accurately and directly confirming the state of a kneaded material in the kneading apparatus even during a kneading process.
Drawings
Fig. 1 is a schematic explanatory view showing the structure of a kneading apparatus according to embodiment 1 of the present invention. Wherein (A) is a front cross-sectional view of the kneading apparatus, and (B) is a plan view of the kneading apparatus.
Fig. 2 is a schematic explanatory view showing a structure of a pressure measuring unit attached to a kneading apparatus according to embodiment 1 of the present invention.
Fig. 3 is a schematic explanatory view showing the configuration of an electrical characteristic measuring unit attached to a kneading apparatus according to embodiment 1 of the present invention. An example of the electrical characteristic measuring unit in which the electrode unit is flush with the inner surface of the mixing chamber is shown.
FIG. 4 is a schematic explanatory view showing another embodiment of an electrical characteristic measuring section attached to a kneading apparatus of the present invention. Wherein (A) is a schematic explanatory view of the electrical characteristic measurement section in a shape in which the electrode section protrudes toward the mixing chamber side, and (B) is a schematic explanatory view of the electrical characteristic measurement section in a shape in which the electrode section recedes toward the outer wall side of the housing.
FIG. 5 is a schematic explanatory view showing the arrangement of a pressure measuring section and an electrical characteristic measuring section attached to the kneading apparatus of the present invention. Wherein (A) is a schematic explanatory view showing a kneading apparatus in which a pressure measuring section and an electrical property measuring section are disposed in a curved surface portion, and (B) is a schematic explanatory view showing a kneading apparatus in which a pressure measuring section and an electrical property measuring section are disposed in a flat surface portion.
Fig. 6 is a schematic explanatory view showing a configuration of a composite measuring section attached to a kneading apparatus according to
Fig. 7 is a schematic explanatory view showing another embodiment of the composite measurement unit. Wherein (a) is a plan view when the pressure-receiving portion of the composite measurement portion is formed in a substantially quadrangular prism shape and the 1 st electrode, the 2 nd electrode, and the insulating member are formed in a substantially quadrangular cylindrical shape, and (B) is a plan view when the pressure-receiving portion of the composite measurement portion is formed in a substantially quadrangular prism shape and the 1 st electrode, the 2 nd electrode, and the insulating member are formed in a substantially cylindrical shape.
In the figure: 1A, 1B-kneading apparatus, 2-casing, 2 a-inlet, 2B-outlet, 2C-semi-cylindrical left wall, 2 d-semi-cylindrical right wall, 2 e-front wall, 2 f-rear wall, 2 g-inlet cover, 2 h-outlet cover, 3-rotor, 3 a-shaft, 3B-blade, 4-mixing chamber, 5-pressure measuring section, 5 a-pressure receiving section, 5B-buffer section, 5C-pressure sensor, 5 d-guide, 5 e-pressure plate, 5 f-bolt, 6A, 6B, 6C-electrical characteristics measuring section, 6A-1 st electrode section, 6B-2 nd electrode section, 6C-insulating member, 6 d-voltage applying section, 7-temperature measuring part, 8-determining part, 9-composite measuring part, 9 a-pressure part, 9 b-buffer part, 9 c-pressure sensor, 9 d-guide part, 9 e-1 st electrode, 9 f-2 nd electrode, 9 g-insulating part, 9 h-voltage applying part, 9 i-pressing plate, 9 j-bolt, 9 k-pressure part, 9 l-1 st electrode, 9 m-insulating part and 9 n-2 nd electrode.
Detailed Description
Hereinafter, embodiments of the kneading apparatus according to the present invention will be described in detail with reference to the drawings.
The kneading apparatuses described in the embodiments are merely examples for explaining the kneading apparatus according to the present invention, and are not limited thereto.
In the following embodiments, the explanation of the kneading apparatus may be replaced with the explanation of each step of the corresponding method for producing a kneaded product.
The kneading apparatus of the present invention is a kneading apparatus for dispersing a dispersoid in a nonconductive material. The nonconductive material is not particularly limited, but examples thereof include polymer materials such as rubber products, plastic products, and films.
The dispersoid in the present invention is a granular material, and may be a non-conductive dispersoid or a conductive dispersoid. Examples of the nonconductive dispersoid include silica particles and sulfur particles, and examples of the conductive dispersoid include carbon particles and metal powder.
[ 1 st embodiment ]
Fig. 1 is a schematic explanatory view showing the structure of a
As shown in fig. 1 (a), the
The nonconductive material and the dispersoid may be collectively referred to as "kneaded material" or "kneaded material".
As shown in fig. 1 (a) and (B), the
The
When the nonconductive material and the conductive dispersoid are mixed, the resulting kneaded material is discharged from the
The
The rotation direction and speed of the
The size and shape of the blades of the
Further, when the kneading is performed by the
(pressure measuring section)
Fig. 2 is a sectional view for explaining the structure of the
The
The installation position and the number of the
(temperature measuring section)
The
The installation position and the number of the
(electric characteristic measuring section)
Fig. 3 is a schematic explanatory view for explaining the structure of the electrical characteristic measurement unit 6. The electrical characteristic measurement unit 6 includes: a pair of electrodes (a 1 st electrode portion 6a and a 2 nd electrode portion 6b) provided at portions of the
When the voltage applying unit 6d applies a measuring voltage to the pair of electrodes (the 1 st electrode 6a and the 2 nd electrode 6b), a current flows through the kneaded material in contact with the 1 st electrode 6a and the 2 nd electrode 6 b. The electrical characteristic measuring unit 6 then obtains an electrical characteristic value of the current flowing through the kneaded material. Here, the electrical property value is not particularly limited as long as it is a parameter indicating the ease of flowing of the current flowing through the kneaded material, and examples thereof include a current value, a voltage value, and a resistance value.
The installation position and the number of the electrical characteristic measuring units 6 are not particularly limited. The installation position is arranged on at least one of the
Further, as for the arrangement of the pair of electrodes (i.e., the 1 st electrode 6a and the 2 nd electrode 6b) of the electrical characteristic measurement section 6, it is preferable to arrange them along the
The material and shape of the 1 st electrode 6a and the 2 nd electrode 6b are not limited as long as they can measure the resistance value of the kneaded material in the mixing
The insulating
The electrical characteristic measuring unit 6 transmits an electrical characteristic value related to the current flowing between the 1 st electrode 6a and the 2 nd electrode 6b to the determining
It is considered that the relationship between the electrical characteristic value and the dispersion state varies depending on the pressure value or the temperature value of the kneaded material. The reason why the phenomenon in which the relationship between the electrical characteristic value and the dispersion state changes depending on the pressure value of the kneaded material is presumed to occur is as follows: when pressure is applied to the kneaded material, the kneaded material is compressed, and the distance of the dispersoid having conductivity in the non-conductive material is varied. That is, when pressure is applied to the kneaded material, the distance of the dispersoid having conductivity becomes small, and the resistance value decreases. The reason why the relationship between the electrical property value and the dispersion state changes depending on the temperature value of the kneaded material is presumed to be as follows: when the temperature value becomes high, the resistance value of the resin decreases. Therefore, the
From the viewpoint of correcting the relationship between the electrical characteristic value and the dispersion state based on the pressure value or the temperature value, it is preferable to obtain the electrical characteristic value, the pressure value, and the temperature value for a kneaded product in the same state. Therefore, it is preferable to dispose the electrical characteristic measuring unit 6, the
When the electrical characteristic measurement unit 6, the
(determination section)
The
The determination in the
Thus, the
The information transmission between the
According to the above features, in the
In embodiment 1, a conductive dispersoid is used as the dispersoid, but a non-conductive dispersoid may be used. In this case, instead of the electrical characteristic measuring unit, for example, the dispersoid may be detected by an optical method to determine the dispersion state, and this may be corrected by using the pressure value and the temperature value.
[ 2 nd embodiment ]
The kneading apparatus 1B according to
Since the configuration other than the
Fig. 6 (a) is a sectional view for explaining the structure of the composite measuring unit 9. The composite measurement unit 9 includes a pressure measurement unit configured to include: a pressure receiving portion 9a provided on the mixing chamber side surface of the
In the composite measuring portion 9, the pressure sensor 9c detects the pressure generated by the contact of the kneaded product during kneading with the pressure receiving portion 9a via the buffer portion 9b, and measures the electrical characteristic value of the current flowing through the kneaded product between the 1 st electrode 9e and the 2 nd electrode 9 f. Accordingly, the pressure value and the electrical characteristic value can be measured at the same portion of the kneaded material, and therefore, the correlation between the pressure value and the electrical characteristic value can be accurately maintained, and the dispersion state of the kneaded material can be confirmed.
The installation position and the number of the composite measuring units 9 are not particularly limited. The installation position is arranged on at least one of the
The materials and shapes of the 1 st electrode 9e, the 2 nd electrode 9f, and the insulating member 9g of the composite measuring unit 9 are not limited as long as they are set so as to be able to measure the electrical property values of the kneaded material in the mixing
The information transmission between the electrical characteristic measuring unit and the pressure measuring unit of the composite measuring unit 9 and the determining
As described above, the kneading apparatus 1B of the present invention measures the pressure value and the electrical characteristic value of the kneaded product in more limited ranges, and can accurately confirm the state of the kneaded product. This can improve the quality control and the work efficiency of a product containing a nonconductive material and a dispersoid having conductivity.
(other embodiment of the composite measuring section)
The shape of the composite measuring portion is not limited to the cylindrical shape shown in fig. 6, and various shapes can be adopted. Fig. 7 shows another embodiment of the composite measuring unit. For example, the composite measurement unit shown in fig. 7 (a) is a composite measurement unit including a pressure receiving portion 9k having a substantially quadrangular prism shape, a 1 st electrode 9l and a 2 nd electrode 9n having substantially quadrangular cylindrical shapes, and an insulating member 9 m. The composite measurement unit shown in fig. 7 (B) is a composite measurement unit including a pressure receiving portion having a substantially rectangular prism shape, and a 1 st electrode 9e, a 2 nd electrode 9f and an insulating member 9g having substantially cylindrical shapes.
The kneading apparatus of the present invention can be used for confirming the dispersion state of a kneaded product in a kneading process in various industrial fields. Specifically, the kneading apparatus of the present invention can improve quality control and work efficiency in a kneading process in which a dispersoid is uniformly dispersed in a non-conductive material such as a kneading material (i.e., a polymer material) of a rubber product.
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