阅读说明：本技术 一种共轭亚油酸的防皲裂唇膏及其制备方法 (Conjugated linoleic acid anti-chapping lipstick and preparation method thereof ) 是由 何海芬 于 2020-06-15 设计创作，主要内容包括：本发明涉及一种共轭亚油酸的防皲裂唇膏,由以下重量份的各组分组成：矿酯30～85份,棕榈酸乙基己酯2～10份,共轭亚油酸2～10份,植物甾醇/辛基十二醇月桂酰谷氨酸酯2～5份,藜麦籽油0.5～3份,小果咖啡籽油0.1～1份,混合提取物1～5份,橄榄油1～10份,澳洲坚果油1～5份,白蜂蜡2～8份,微晶蜡5～10份,小烛树蜡2～5份,香精0.01～0.02份；还公开了其制备方法。本发明的优点在于：将共轭亚油酸应用在唇膏属于首创,对研究开发具有多种生理功能的防皲裂唇膏具有长远意义；共轭亚油酸有非常好的透皮性,可以有效防止唇部皲裂。(The invention relates to a conjugated linoleic acid anti-chapping lipstick which comprises the following components in parts by weight: 30-85 parts of mineral ester, 2-10 parts of ethylhexyl palmitate, 2-10 parts of conjugated linoleic acid, 2-5 parts of phytosterol/octyldodecanol lauroyl glutamate, 0.5-3 parts of quinoa seed oil, 0.1-1 part of small fruit coffee seed oil, 1-5 parts of mixed extract, 1-10 parts of olive oil, 1-5 parts of macadamia nut oil, 2-8 parts of white beeswax, 5-10 parts of microcrystalline wax, 2-5 parts of candelilla wax and 0.01-0.02 part of essence; its preparing process is also disclosed. The invention has the advantages that: the conjugated linoleic acid is applied to the lipstick, which is the first creation and has long-term significance for researching and developing anti-chapping lipsticks with various physiological functions; the conjugated linoleic acid has good transdermal property, and can effectively prevent lip chap.)

1. The conjugated linoleic acid anti-chapping lipstick is characterized in that: the composition comprises the following components in parts by weight: 30-85 parts of mineral ester, 2-10 parts of ethylhexyl palmitate, 2-10 parts of conjugated linoleic acid, 2-5 parts of phytosterol/octyldodecanol lauroyl glutamate, 0.5-3 parts of quinoa seed oil, 0.1-1 part of small fruit coffee seed oil, 1-5 parts of mixed extract, 1-10 parts of olive oil, 1-5 parts of macadamia nut oil, 2-8 parts of white beeswax, 5-10 parts of microcrystalline wax, 2-5 parts of candelilla wax and 0.01-0.02 part of essence.

2. The conjugated linoleic acid anti-chapping lipstick according to claim 1, wherein: the paint consists of the following components in percentage by weight: 58 parts of mineral ester, 6 parts of ethylhexyl palmitate, 6 parts of conjugated linoleic acid, 4 parts of phytosterol/octyldodecanol lauroyl glutamate, 2 parts of quinoa seed oil, 0.5 part of small-fruit coffee seed oil, 3 parts of mixed extract, 6 parts of olive oil, 3 parts of macadamia nut oil, 5 parts of white beeswax, 7 parts of microcrystalline wax, 3 parts of candelilla wax and 0.015 part of essence.

3. The conjugated linoleic acid anti-chapping lipstick according to claim 1 or 2, wherein: the mixed extract is at least two extracts of propolis extract, beeswax extract, rice extract, candelilla wax extract and jojoba seed extract.

4. The method for preparing the conjugated linoleic acid anti-chapping lipstick as claimed in any one of claims 1 to 3, wherein: the method comprises the following steps:

s1, weighing materials in parts by weight except for essence by using a clean anhydrous beaker;

s2, uniformly mixing the weighed materials, and placing the materials in an electric heating furnace for preheating until the raw materials are completely melted;

s3, cooling in air, cooling to 80 ℃, adding essence, and slowly stirring uniformly;

s4, pouring the uniformly stirred solution into a lipstick filling mold, wherein the filling temperature is 80-95 ℃, standing for 10-20 min after filling, and cooling and solidifying;

and S5, demolding to obtain the lipstick.

5. The method for preparing conjugated linoleic acid anti-chapping lipstick according to claim 4, wherein: in step S2, the preheating temperature does not exceed 120 ℃.

6. The method for preparing conjugated linoleic acid anti-chapping lipstick according to claim 4, wherein: in the step S3, during stirring, the stirring speed is 10-14 rpm, and a forward and reverse rotation alternative stirring method is adopted, wherein the forward and reverse rotation switching time is 1-2 min.

7. The method for preparing conjugated linoleic acid anti-chapping lipstick according to claim 4, wherein: in step S4, the angle of the lipstick filling mold is 20-40 degrees.

8. The method for preparing conjugated linoleic acid anti-chapping lipstick according to claim 4, wherein: in step S5, when demolding, the specific steps are: and (3) placing the filling part of the aluminum mold base of the lipstick filling mold above a vacuumizing machine, starting the vacuumizing machine, and stirring, so that demolding can be carried out.

9. The method for preparing conjugated linoleic acid anti-chapping lipstick according to claim 4, wherein: in step S5, when demolding, the specific steps are: and putting the lipstick filling mold with the lipstick into a refrigerator for 15-25 min, and taking out to be demoulded.

Technical Field

The invention relates to the technical field of cosmetics, in particular to a conjugated linoleic acid anti-chapping lipstick and a preparation method thereof.

Background

The research on various position and space isomers of Conjugated Linoleic Acid (CLA) which is a series of essential fatty acids with position and geometric isomers shows that the physiological activity of the Conjugated Linoleic Acid is mainly expressed in the following aspects: 1) anti-cancer effect; 2) preventing cardiovascular diseases; 3) losing weight; 4) an immune modulating function; 5) improving bone quality; 6) regulating blood sugar. Conjugated linoleic acid has been increasingly focused on its research because of its multiple physiological functions. The edible level of conjugated linoleic acid is always a concern for developers at present, and the safety of the lipstick is always a concern, and the conjugated linoleic acid has various health-care functions, but the anti-chapping function of the conjugated linoleic acid in the lipstick is not known at present. Therefore, the conjugated linoleic acid anti-chapping lipstick prepared has long-term significance.

Disclosure of Invention

The invention aims to overcome the defects of the prior art and provides a conjugated linoleic acid anti-chapping lipstick and a preparation method thereof.

The purpose of the invention is realized by the following technical scheme:

the conjugated linoleic acid anti-chapping lipstick comprises the following components in parts by weight: 30-85 parts of mineral ester, 2-10 parts of ethylhexyl palmitate, 2-10 parts of conjugated linoleic acid, 2-5 parts of phytosterol/octyldodecanol lauroyl glutamate, 0.5-3 parts of quinoa seed oil, 0.1-1 part of small fruit coffee seed oil, 1-5 parts of mixed extract, 1-10 parts of olive oil, 1-5 parts of macadamia nut oil, 2-8 parts of white beeswax, 5-10 parts of microcrystalline wax, 2-5 parts of candelilla wax and 0.01-0.02 part of essence.

Further, the conjugated linoleic acid anti-chapping lipstick consists of the following components in percentage by weight: 58 parts of mineral ester, 6 parts of ethylhexyl palmitate, 6 parts of conjugated linoleic acid, 4 parts of phytosterol/octyldodecanol lauroyl glutamate, 2 parts of quinoa seed oil, 0.5 part of small-fruit coffee seed oil, 3 parts of mixed extract, 6 parts of olive oil, 3 parts of macadamia nut oil, 5 parts of white beeswax, 7 parts of microcrystalline wax, 3 parts of candelilla wax and 0.015 part of essence.

Further, the mixed extract is at least two extracts of propolis extract, beeswax extract, rice extract, candelilla wax extract and jojoba seed extract.

The preparation method of the conjugated linoleic acid anti-chapping lipstick comprises the following steps:

s1, weighing materials in parts by weight except for essence by using a clean anhydrous beaker;

s2, uniformly mixing the weighed materials, and placing the materials in an electric heating furnace for preheating until the raw materials are completely melted;

s3, cooling in air, cooling to 80 ℃, adding essence, and slowly stirring uniformly;

s4, pouring the uniformly stirred solution into a lipstick filling mold, wherein the filling temperature is 80-95 ℃, standing for 10-20 min after filling, and cooling and solidifying;

and S5, demolding to obtain the lipstick.

Further, in step S2, the preheating temperature does not exceed 120 ℃.

Further, in step S3, the stirring speed is 10-14 rpm, and the forward and reverse rotation alternative stirring method is adopted, and the forward and reverse rotation switching time is 1-2 min.

Further, in step S4, the angle of the lipstick filling mold is 20-40 °.

Further, in step S5, when demolding, the specific steps are: and (3) placing the filling part of the aluminum mold base of the lipstick filling mold above a vacuumizing machine, starting the vacuumizing machine, and stirring, so that demolding can be carried out.

Further, in step S5, when demolding, the specific steps are: and putting the lipstick filling mold with the lipstick into a refrigerator for 15-25 min, and taking out to be demoulded.

The invention has the following advantages:

1. the conjugated linoleic acid is applied to the lipstick, which belongs to the initiative and has long-term significance for researching and developing the anti-chapping lipstick with various physiological functions.

2. The conjugated linoleic acid has good transdermal property, can effectively prevent lip chap, and has quick response and better effect compared with the products sold in the market.

3. The invention can also soften dead skin and effectively prevent cheilitis.

Detailed Description

The invention is further described below with reference to examples, but the scope of the invention is not limited to the following.

[ example 1 ]:

the conjugated linoleic acid anti-chapping lipstick comprises the following components in parts by weight: 30 parts of mineral ester, 10 parts of ethylhexyl palmitate, 10 parts of conjugated linoleic acid, 2 parts of phytosterol/octyldodecanol lauroyl glutamate, 3 parts of quinoa seed oil, 0.1 part of small-fruit coffee seed oil, 5 parts of mixed extract, 1 part of olive oil, 5 parts of macadamia nut oil, 2 parts of white beeswax, 10 parts of microcrystalline wax, 2 parts of candelilla wax and 0.02 part of essence.

Further, the mixed extract is at least two extracts of propolis extract, beeswax extract, rice extract, candelilla wax extract and jojoba seed extract.

The preparation method of the conjugated linoleic acid anti-chapping lipstick comprises the following steps:

s1, weighing materials in parts by weight except for essence by using a clean anhydrous beaker;

s2, uniformly mixing the weighed materials, and placing the materials in an electric heating furnace for preheating at a temperature not exceeding 120 ℃ until the raw materials are completely melted;

s3, air cooling, cooling to 80 ℃, adding essence, slowly stirring uniformly at a stirring speed of 10rpm, and adopting a forward and reverse rotation alternative stirring method, wherein the forward and reverse rotation switching time is 2 min;

s4, pouring the uniformly stirred solution into a lipstick filling mold, wherein the angle of the lipstick filling mold is 20 degrees, the filling temperature is 80 ℃, standing for 20min after filling, and cooling and solidifying;

and S5, demolding, namely placing the filling part of the aluminum mold base of the lipstick filling mold above a vacuumizing machine, starting the vacuumizing machine to stir, and demolding to obtain the lipstick.

[ example 2 ]:

the conjugated linoleic acid anti-chapping lipstick consists of the following components in percentage by weight: 58 parts of mineral ester, 6 parts of ethylhexyl palmitate, 6 parts of conjugated linoleic acid, 4 parts of phytosterol/octyldodecanol lauroyl glutamate, 2 parts of quinoa seed oil, 0.5 part of small-fruit coffee seed oil, 3 parts of mixed extract, 6 parts of olive oil, 3 parts of macadamia nut oil, 5 parts of white beeswax, 7 parts of microcrystalline wax, 3 parts of candelilla wax and 0.015 part of essence.

Further, the mixed extract is at least two extracts of propolis extract, beeswax extract, rice extract, candelilla wax extract and jojoba seed extract.

The preparation method of the conjugated linoleic acid anti-chapping lipstick comprises the following steps:

s1, weighing materials in parts by weight except for essence by using a clean anhydrous beaker;

s2, uniformly mixing the weighed materials, and placing the materials in an electric heating furnace for preheating at a temperature not exceeding 120 ℃ until the raw materials are completely melted;

s3, air cooling, cooling to 80 ℃, adding essence, slowly stirring uniformly at a stirring speed of 12rpm, and adopting a forward and reverse rotation alternative stirring method, wherein the forward and reverse rotation switching time is 1.5 min;

s4, pouring the uniformly stirred solution into a lipstick filling mold, wherein the angle of the lipstick filling mold is 30 degrees, the filling temperature is 88 ℃, standing for 15min after filling, and cooling and solidifying;

and S5, demolding, namely putting the lipstick filling mold with the lipstick into a refrigerator integrally, and taking out after 25min to obtain the lipstick.

[ example 3 ]:

the conjugated linoleic acid anti-chapping lipstick comprises the following components in parts by weight: 50 parts of mineral ester, 8 parts of ethylhexyl palmitate, 4 parts of conjugated linoleic acid, 4 parts of phytosterol/octyldodecanol lauroyl glutamate, 2 parts of quinoa seed oil, 0.7 part of small-fruit coffee seed oil, 4 parts of mixed extract, 6 parts of olive oil, 2 parts of macadamia nut oil, 6 parts of white beeswax, 7 parts of microcrystalline wax, 3 parts of candelilla wax and 0.017 part of essence.

Further, the mixed extract is at least two extracts of propolis extract, beeswax extract, rice extract, candelilla wax extract and jojoba seed extract.

The preparation method of the conjugated linoleic acid anti-chapping lipstick comprises the following steps:

s1, weighing materials in parts by weight except for essence by using a clean anhydrous beaker;

s2, uniformly mixing the weighed materials, and placing the materials in an electric heating furnace for preheating at a temperature not exceeding 120 ℃ until the raw materials are completely melted;

s3, air cooling, cooling to 80 ℃, adding essence, slowly stirring uniformly at a stirring speed of 13rpm, and adopting a forward and reverse rotation alternative stirring method, wherein the forward and reverse rotation switching time is 1.5 min;

s4, pouring the uniformly stirred solution into a lipstick filling mold, wherein the angle of the lipstick filling mold is 33 degrees, the filling temperature is 85 ℃, standing for 12min after filling, and cooling and solidifying;

and S5, demolding, namely placing the filling part of the aluminum mold base of the lipstick filling mold above a vacuumizing machine, starting the vacuumizing machine to stir, and demolding to obtain the lipstick.

Example 4:

the conjugated linoleic acid anti-chapping lipstick comprises the following components in parts by weight: 85 parts of mineral ester, 2 parts of ethylhexyl palmitate, 2 parts of conjugated linoleic acid, 5 parts of phytosterol/octyldodecanol lauroyl glutamate, 0.5 part of quinoa seed oil, 1 part of small-fruit coffee seed oil, 1 part of mixed extract, 10 parts of olive oil, 1 part of macadamia nut oil, 8 parts of white beeswax, 5 parts of microcrystalline wax, 5 parts of candelilla wax and 0.01 part of essence.

Further, the mixed extract is at least two extracts of propolis extract, beeswax extract, rice extract, candelilla wax extract and jojoba seed extract.

The preparation method of the conjugated linoleic acid anti-chapping lipstick comprises the following steps:

s1, weighing materials in parts by weight except for essence by using a clean anhydrous beaker;

s2, uniformly mixing the weighed materials, and placing the materials in an electric heating furnace for preheating at a temperature not exceeding 120 ℃ until the raw materials are completely melted;

s3, air cooling, cooling to 80 ℃, adding essence, slowly stirring uniformly at a stirring speed of 14rpm, and adopting a forward and reverse rotation alternative stirring method, wherein the forward and reverse rotation switching time is 1 min;

s4, pouring the uniformly stirred solution into a lipstick filling mold, wherein the angle of the lipstick filling mold is 40 degrees, the filling temperature is 95 ℃, standing for 10min after filling, and cooling and solidifying;

and S5, demolding, namely putting the lipstick filling mold with the lipstick into a refrigerator integrally, taking out after 15min, and demolding to obtain the lipstick.

Among the above embodiments, embodiment 2 is the most preferred embodiment.

The lipstick produced according to the formulation and preparation described in example 2 was subjected to the following tests:

the experimental method comprises the following steps:

the tester selects: 50 people with dry and chapped lips are selected, wherein 25 women and 25 men are selected. Has no obvious erosion and other complications.

And (3) judging standard: the tester scored the degree of improvement (5 points full score) a: the chap of the mouth and the lip is completely cured and disappears for 5 minutes.

B: has obvious effect, and the chap area is reduced by more than 60 percent and is divided into 4 minutes. C: effective, the chap area is reduced by 30-60% to 2-3 minutes. D: the chap area is not reduced to 0-1 minute by less than 30 percent.

The test method comprises the following steps: a self-control method was used. The subjects were given daily lipsticks for three days, once each day at 8h intervals.

The test results of 50 subjects are scored as follows:

5 points of	4 is divided into	2 to 3 points	0 to 1 point
				30 persons	15 persons	5 persons	0

And (4) conclusion: 60% of the subjects found that the healing effect was very satisfactory, reaching the complete disappearance of the chapped lips in three days. The effect is obvious in 30% of subjects, and the chapped area can be reduced by more than 60% in three days. 10% of the subjects considered the composition to be effective, allowing a 30-60% reduction in chapped area for three days. All subjects considered the composition to have an onset of action for three days, with a faster and better effect than the commercial product.

In the invention, the conjugated linoleic acid is selected from 9t, 11t-18:2 or 9t, 11c-18:2 conjugated linoleic acid. Of the 16 isomers of conjugated linoleic acid, the ratio of 9c, 11t-18: 2. 9t, 11t-18: 2. 10t, 12 c-18:2 and 10c, 12 c-18:2, and the like, wherein the two isomers with strong physiological activity with the most content are 9c, 11t-18: 2. 10t, 12 c-18:2 two isomers. Of particular interest are the isomers c9t11, which, for one, represent more than 80% of the total of the 16 isomers in the natural CLA present in the food; secondly, c9t11 is the only isomer in 16 isomers which can be absorbed by animal cells and deeply enter the phospholipid layer; thirdly, the function of the tl0cl2 isomer in the CLA isomer is stronger than that of the c9t11 isomer.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.