阅读说明：本技术 一种多效修护面膜液及其制备方法 (Multi-effect facial mask repairing liquid and preparation method thereof ) 是由 杨丹 金毅 罗丽华 毛明利 张绮 顾婷 朱玲 朱辰 于 2019-11-27 设计创作，主要内容包括：本发明公开了一种多效修护面膜液,属于化妆品技术领域,其主要成分为由特异性卵黄抗体、神经酰胺、磷脂酰胆碱三者复配后构成的组合物。本发明将特异性卵黄抗体、神经酰胺、磷脂酰胆碱这三者复配并非简单的将三种物质组合在一起,使其三种主要成分单独发挥原本具有的作用,而是能够相辅相成的发挥作用,极大的减少了添加剂种类的使用,减少致敏因素出现的概率,更为安全有效,在滋养肌肤的同时,修护由肌肤过敏或者换季所引起的各种状况。(The invention discloses a multi-effect repairing mask liquid, which belongs to the technical field of cosmetics, and mainly comprises a composition formed by compounding a specific egg yolk antibody, ceramide and phosphatidylcholine. According to the invention, the specific yolk antibody, the ceramide and the phosphatidylcholine are compounded, and the three substances are not simply combined together, so that the three main components of the yolk antibody, the ceramide and the phosphatidylcholine play the original functions independently, but can play complementary roles, so that the use of additive types is greatly reduced, the probability of occurrence of sensitization factors is reduced, the yolk antibody is safer and more effective, and various conditions caused by skin allergy or season change are repaired while the skin is nourished.)

1. The multi-effect facial mask repairing liquid is characterized in that a composition formed by compounding a specific chicken egg yolk antibody, ceramide and phosphatidylcholine is used as a main component.

2. The multi-effect repairing mask liquid according to claim 1, characterized by further comprising other auxiliary components, specifically: chelating agent, humectant, thickener, stabilizer, oat kernel extract, and water.

3. The multi-effect conditioning mask solution of claim 2, wherein the chelating agent is EDTA;

the humectant is at least one of 1, 3-propylene glycol, 1, 2-pentanediol, butanediol, sodium hyaluronate and glycerol;

the thickening agent is sodium acrylate copolymer;

the stabilizer is at least one of propylene glycol and glycerol caprylate;

the water is deionized water.

4. The multi-effect repairing mask liquid according to claims 1-3, wherein the specific chicken egg yolk antibody is a compound specific chicken egg yolk antibody prepared by compounding an escherichia coli chicken egg yolk antibody and a staphylococcus aureus chicken egg yolk antibody in a mass ratio of 1: 1-3.

5. The preparation method of the multi-effect repairing mask liquid according to any one of claims 1 to 4, wherein the raw materials comprise the following components in percentage by mass of the total mass of the composition:

50-90% of deionized water, 0.01-0.05% of chelating agent, 0.1-0.3% of humectant a, 0.1-2% of thickening agent, 0.78-5% of humectant b3, 0.2-0.7% of stabilizer, 0.1-2% of humectant c 2-5%, 0.1-2% of oat kernel extract, 0.1-2% of ceramide, 0.1-2% of phosphatidylcholine and 3-20% of specific egg yolk antibody;

the preparation process comprises the following steps:

(1) adding a chelating agent and a humectant a into deionized water, stirring, heating to 75-95 ℃, sterilizing for 30 minutes until the chelating agent and the humectant are completely dissolved, and preparing a mixed solution A for later use;

(2) uniformly mixing a thickening agent and a humectant B, adding the thickening agent and the humectant B into the mixed solution prepared in the step (1) at the temperature of 75-95 ℃, and stirring at the temperature of 75-95 ℃ until the liquid is uniform and has no particles to obtain a mixed solution B;

(3) uniformly mixing the stabilizer and the humectant C at room temperature until the mixture is transparent and free of particles to obtain a mixed solution C;

(4) stirring the mixed solution B prepared in the step (2) at room temperature, cooling to 60-65 ℃, adding the mixed solution C obtained in the step (3), and stirring uniformly to obtain a mixed solution D;

(5) and after the mixed solution D is cooled to room temperature, sequentially adding the oat kernel extract, the ceramide, the phosphatidylcholine and the specific egg yolk antibody, uniformly stirring, and filtering to remove impurities to obtain a finished product.

6. The preparation method of the multi-effect repairing mask liquid according to claim 5, wherein the humectant a is sodium hyaluronate; the humectant b is at least one of 1, 3-propylene glycol, butanediol and 1, 2-pentanediol; the humectant c is glycerin.

7. The preparation method of the multi-effect repairing mask liquid according to claim 5 or 6, wherein the cooling method for cooling the mixed solution D to room temperature in the step (5) comprises the following steps: and (5) placing the glass tube at room temperature, and cooling the glass tube when the glass tube is normally radiated.

8. The method for preparing the multi-effect facial mask fluid according to claim 5 or 6, wherein in the step (5), the specific chicken egg yolk antibodies are obtained by the following steps: the method comprises the steps of injecting harmful flora antigens into directionally cultured chickens to enable the directionally cultured chickens to obtain effective and independent biological antibodies, carrying out linear transfer of the antibodies in the process of laying eggs of the chickens, enabling the eggs hatched by the directionally cultured chickens to carry protein products with anti-harmful flora, and extracting the components to obtain active biological antibodies.

Technical Field

The invention relates to the technical field of cosmetics, in particular to a multi-effect repairing mask liquid and a preparation method thereof.

Background

The skin is divided into epidermis, dermis and subcutaneous tissue, the epidermis is the outermost layer of the skin and has a protective effect, and the epidermis layer can also be divided into five layers at the same time: stratum corneum, stratum lucidum, stratum granulosum, stratum spinosum, stratum basale, sebaceous membrane. The protection of the skin is mainly provided by the stratum corneum, which is composed of multiple layers of extremely flat cells, is a main barrier for the absorption of chemicals through the skin and the loss of water, is also a main barrier for the invasion of chemicals and microorganisms into the body, has acid and alkali resistance, and plays an important role in the skin guarantee function. We also consider the outermost barrier to direct contact with air outside the stratum corneum of the skin to be our skin surface microorganisms. In daily life, environmental pollution, improper cleaning, various bad facial mask liquid use, physical stimulation, bad living habits and the like all destroy the microbial flora balance on the skin surface, so that the skin generates various stimulations, and the problems of red swelling, fever, pain and itch, tightness, desquamation and the like can be solved. At this time, a safe and effective repairing facial mask liquid needs to be selected to comprehensively care the skin of people.

At present, the facial mask becomes a necessity for daily maintenance of the modern young, and the facial mask products on the market are various in types and various in forms, including a powdery facial mask, a paste facial mask and a film facial mask. The functions of the facial mask are also various, and actually, various chemical reagents are added by a plurality of manufacturers to achieve the effect of publicizing the facial mask, but the facial mask has a bad place, namely the additives are too much, so that the sensitization factors of the product are more, the aim of repairing the skin cannot be achieved, and the skin is stimulated to cause the skin nourishing dependence. Therefore, a safe and effective repairing facial mask is urgently needed, and can repair various conditions caused by skin allergy or season change while nourishing the skin.

Disclosure of Invention

The invention aims to provide the multi-effect repairing facial mask liquid which is few in additive, safe and effective, and can repair and nourish the skin and repair various conditions caused by skin allergy or season change.

The invention also aims to provide a preparation method of the multi-effect repairing mask liquid.

The invention is realized by the following technical scheme: a multi-effect facial mask repairing solution comprises a composition prepared by compounding specific egg yolk antibody, ceramide and phosphatidylcholine as main ingredients.

The specific egg yolk antibody (IgY) utilized by the technical scheme reduces harmful bacteria (such as staphylococcus aureus, acne infection and the like) through the targeted combination with the harmful bacteria, and meanwhile, the specific egg yolk antibody is derived from egg yolk, so that the safety is undoubted, and the specific egg yolk antibody is macromolecular active moisturizing protein capable of protecting skin. Meanwhile, the lactobacillus fermentation extract is matched to provide factors for inhibiting harmful bacteria, so that the survival possibility of the harmful bacteria is reduced, and meanwhile, the beneficial skin protease and the like can be obtained through the lactobacillus enzyme. The strong combination of the specific chicken egg yolk antibody (IgY) and the lactobacillus fermentation extract strengthens the first barrier-microorganism layer of the skin. The ceramide can effectively agglomerate the keratinocytes, if the skin of people is compared with the urban wall for resisting external erosion, the keratinocytes are bricks of the urban wall, the ceramide corresponds to the mortar of people, if the mortar is lacked, the keratinocytes are not easy to agglomerate, the cohesion of the keratinocytes can be greatly reduced, and meanwhile, the ceramide has obvious effects on the aspects of moisture preservation, allergy resistance, aging resistance and the like. Phospholipid is a general name of substances, phosphate radical-containing lipid compounds are commonly present in protoplasm and biological membranes of animal and plant cells and have important regulation functions on biological activity of the biological membranes and normal metabolism of organisms, lecithin is only one component of the phospholipid, namely phosphatidylcholine is a main component of the phospholipid, and other forms of phospholipids such as cephalin, inositol phospholipid, phosphatidic acid and the like account for 35% -40% of the total phospholipid. The phospholipid has obvious effects on recombining, repairing and smoothing the skin, and can reduce the loss of water of the skin while enhancing the stratum corneum.

In order to better implement the invention, the invention further comprises other auxiliary components, specifically: chelating agent, humectant, thickener, stabilizer, oat kernel extract, and water.

Wherein the oat kernel extract contains avenanthramides as the main active ingredient, and is effective in relieving itching and skin inflammation.

To better implement the invention, further, the chelating agent is EDTA; the humectant is at least one of 1, 3-propylene glycol, 1, 2-pentanediol, butanediol, sodium hyaluronate and glycerol; the thickening agent is sodium acrylate copolymer; the stabilizer is at least one of propylene glycol and glycerol caprylate; the water is deionized water.

In order to better realize the invention, the egg yolk antibody is a compound specific chicken egg yolk antibody prepared by compounding an escherichia coli egg yolk antibody and a staphylococcus aureus egg yolk antibody according to the mass ratio of 1: 1-3.

The invention also provides a preparation method of the multi-effect repairing mask liquid, wherein the mask liquid comprises the following components in percentage by mass of the total mass of the composition:

50-90% of deionized water, 0.01-0.05% of chelating agent, 0.1-0.3% of humectant a, 0.1-2% of thickening agent, 0.78-5% of humectant b3, 0.2-0.7% of stabilizer, 0.1-5% of humectant c2, 0.1-2% of oat kernel extract, 0.1-2% of ceramide, 0.1-2% of phosphatidylcholine and 3-20% of specific egg yolk antibody;

the preparation process comprises the following steps:

(1) adding a chelating agent and a humectant a into deionized water, stirring, heating to 75-95 ℃, sterilizing for 30 minutes until the chelating agent and the humectant are completely dissolved, and preparing a mixed solution A for later use;

(2) uniformly mixing a thickening agent and a humectant B, adding the thickening agent and the humectant B into the mixed solution prepared in the step (1), and stirring until the liquid is uniform and has no particles to obtain a mixed solution B;

(3) uniformly mixing the stabilizer and the humectant C until the mixture is transparent and free of particles to obtain a mixed solution C;

(4) cooling the mixed solution B prepared in the step (2) to 60-65 ℃, adding the mixed solution C obtained in the step (3), and stirring uniformly to obtain a mixed solution D;

(5) and (3) cooling the mixed solution D to room temperature, sequentially adding the oat kernel extract, the ceramide, the phosphatidylcholine and the specific egg yolk antibody, uniformly stirring, and filtering to remove impurities to obtain a finished product.

In order to better prepare the facial mask liquid, the humectant a is sodium hyaluronate; the humectant b is at least one of 1, 3-propylene glycol, butanediol and 1, 2-pentanediol; the humectant c is glycerin.

In order to better prepare the above facial mask solution, further, the cooling method for cooling the mixed solution D to room temperature in the step (5) is as follows: and (5) placing the glass tube at room temperature, and cooling the glass tube when the glass tube is normally radiated.

In order to better prepare the facial mask solution, in the step (4), the chicken egg yolk antibody is obtained by the following steps: the method comprises the steps of injecting harmful flora antigens into directionally cultured chickens to enable the directionally cultured chickens to obtain effective and independent biological antibodies, carrying out linear transfer of the antibodies in the process of laying eggs of the chickens, enabling the eggs hatched by the directionally cultured chickens to carry protein products with anti-harmful flora, and extracting the components to obtain active biological antibodies.

Compared with the prior art, the invention has the following advantages and beneficial effects:

(1) the invention utilizes the targeted combination of the egg yolk antibody and harmful bacteria to eliminate the harmful bacteria (such as staphylococcus aureus, heat-resistant escherichia coli and the like) and provides efficient, timely and targeted contribution to the microbial flora balance of the skin; meanwhile, the targeted antibacterial effect of the egg yolk antibody is utilized, and the ecological nutrient solution is combined to provide suitable living conditions for the beneficial bacteria to promote the propagation of the beneficial bacteria, so that the microbial population balance on the surface of the skin is safely and effectively maintained for a long time, the skin is kept in a microbial balance state for a long time, various stimulation populations of the external environment to the skin are effectively blocked, and the skin is in a healthy and beneficial environment;

(2) according to the invention, by adding ceramide, the product has obvious antiallergic capability, can improve the tolerance of skin and reduce the possibility of skin allergy, and has extremely strong capability of associating water molecules, so that the thickness of the skin cutin layer can be increased, the water holding capacity of the skin can be improved, and skin wrinkles can be reduced;

(3) by adding the phosphatidylcholine, the multi-effect facial mask liquid disclosed by the invention can reduce the loss of skin moisture while enhancing the cuticle, and has obvious effects on recombination, repair and skin smoothing;

(4) according to the invention, the specific egg yolk antibody, the ceramide and the phosphatidylcholine are compounded, and three substances are not simply combined together, so that the three main components of the egg yolk antibody, the ceramide and the phosphatidylcholine play original functions independently, but can play complementary functions, the use of additive types is greatly reduced, the probability of occurrence of sensitization factors is reduced, the egg yolk antibody is safer and more effective, and various conditions caused by skin allergy or season change are repaired while the skin is nourished;

(5) the humectant used in the present invention is preferably a polyhydric alcohol humectant and hyaluronic acid, also known as hyaluronic acid, which itself is a polysaccharide structure composed of glucose and glucuronic acid. As one of the main matrix components of the epidermis and the dermis of human skin, the physiological function of the skin-care product is to enable water to enter the intercellular space and combine with protein to form protein gel, so that the cells are adhered together to play the role of normal cell metabolism, simultaneously maintain the water of the cells, protect the cells from being invaded by pathogenic bacteria, accelerate the recovery of skin tissues, improve the healing and regeneration capacity of wounds, enhance the immunity and the skin barrier function, and enable the product to better play the multi-effect repair function.

Drawings

Other features, objects and advantages of the invention will become more apparent upon reading of the detailed description of non-limiting embodiments with reference to the following drawings:

FIG. 1 is a comparison graph of the inhibition effect of the multi-effect facial mask solution on Escherichia coli according to the present invention;

FIG. 2 is a comparison graph of the inhibitory effect of the multi-effect facial mask liquid on staphylococcus aureus

Fig. 3 is a comparison graph of the use effect of a test subject wangzhi using the fullerene rejuvenation solution of the present invention;

FIG. 4 is a comparison graph of the effect of applying the fullerene rejuvenation solution according to the present invention to a subject;

fig. 5 is a graph comparing the effect of a fullerene rejuvenation lotion according to the present invention on a subject per day;

FIG. 6 is a comparison graph of the effect of a subject on the fullerene rejuvenation solution of the present invention;

fig. 7 is a graph comparing the effect of a fullerene rejuvenation solution of the present invention on Liu's body of a subject.

Detailed Description

The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto, and various substitutions and alterations can be made without departing from the technical idea of the present invention as described above, according to the common technical knowledge and the conventional means in the field.

The present invention will be described in further detail with reference to the following examples for the purpose of making clear the objects, process conditions and advantages of the present invention, which are given by way of illustration only and are not intended to be limiting of the present invention.

Unless otherwise specified, "impregnation" as used herein means that the whole of the bio-fiber membrane used for preparing the mask is uniformly impregnated with the cosmetic composition of the present application, in other words, the cosmetic composition is uniformly distributed on the bio-fiber membrane, and the liquid layer of the cosmetic composition on the surface of the bio-fiber membrane has a uniform thickness.

In addition, the term "cosmetic" as used herein is to be understood in a broad sense and includes both color cosmetic products and facial mask solutions, such as facial masks, facial cleansers, shower gels, and the like.

The information of manufacturers and goods numbers of part of raw materials in the multi-effect repair mask liquid in the embodiment of the invention is shown in the following table:

table-raw material information table

The invention provides a multi-effect facial mask repairing liquid, which mainly comprises a composition formed by compounding a specific egg yolk antibody, ceramide and phosphatidylcholine.

In order to prepare the mask liquid with complete functions, other auxiliary components are added, and the auxiliary components specifically comprise a chelating agent, a humectant, a thickening agent, a stabilizer, oat kernel extract and water.

The raw materials comprise the following components in percentage by mass of the total mass of the composition:

50-90% of deionized water, 0.01-0.05% of chelating agent, 0.1-0.3% of humectant a, 0.1-2% of thickening agent, 0.78-5% of humectant b3, 0.2-0.7% of stabilizer, 0.1-5% of humectant c2, 0.1-2% of oat kernel extract, 0.1-2% of ceramide, 0.1-2% of phosphatidylcholine and 3-20% of specific egg yolk antibody;

wherein preferably, the chelating agent is EDTA;

the humectant is at least one of 1, 3-propylene glycol, 1, 2-pentanediol, butanediol, sodium hyaluronate and glycerol;

the thickening agent is sodium acrylate copolymer;

the stabilizer is at least one of propylene glycol and glycerol caprylate;

the water is deionized water;

the specific chicken egg yolk antibody is a composite specific chicken egg yolk antibody prepared by compounding an escherichia coli egg yolk antibody and a staphylococcus aureus egg yolk antibody according to the mass ratio of 1: 1-3.

Because the skin state of each person is different, the mask liquid can play a moisturizing role for most people, so that various different types of moisturizing agents are used, and different moisturizing agents are used in different preparation processes in the preparation process.