Fire-resistant oil regeneration filter material and manufacturing process and using method thereof

文档序号:1495546 发布日期:2020-02-07 浏览:30次 中文

阅读说明:本技术 一种抗燃油再生滤料及其制造工艺和使用方法 (Fire-resistant oil regeneration filter material and manufacturing process and using method thereof ) 是由 朱润定 于 2019-11-01 设计创作,主要内容包括:一种抗燃油再生滤料,包括如下重量份的组份:氧化铝3份、氧化硅3份、硅藻土1份、硅胶离子2份和木炭1份。一种抗燃油再生滤料的制造工艺,包括如下步骤:首先用超细粉碎机将氧化铝、氧化硅、硅藻土、硅胶离子和木炭分别加工成粉末;将氧化铝、氧化硅、硅藻土、硅胶离子、木炭按比例3:3:1:2:1进行彻底混合,形成合成粉料;将合成粉料用颗粒加工机加工成300目的微颗粒,得到抗燃油再生滤料。解决抗燃油(EH油)或抗燃油(EH油)系统在运行过程中出现的酸值高、电阻率低、氯离子升高、杂质超标、水分增高等问题。(The fire-resistant oil regeneration filter material comprises the following components in parts by weight: 3 parts of alumina, 3 parts of silicon oxide, 1 part of diatomite, 2 parts of silica gel ions and 1 part of charcoal. A manufacturing process of a fire-resistant oil regeneration filter material comprises the following steps: firstly, respectively processing alumina, silica, diatomite, silica gel ions and charcoal into powder by using an ultrafine grinder; mixing alumina, silica, diatomite, silica gel ions and charcoal according to a ratio of 3: 3: 1: 2: 1, thoroughly mixing to form synthetic powder; and processing the synthetic powder into micro-particles with 300 meshes by using a particle processing machine to obtain the fire-resistant oil regeneration filter material. The problems of high acid value, low resistivity, increased chloride ions, overproof impurities, increased moisture and the like in the operation process of the fire-resistant oil (EH oil) or the fire-resistant oil (EH oil) system are solved.)

1. The fire-resistant oil regeneration filter material is characterized by comprising the following components in parts by weight: 3 parts of alumina, 3 parts of silicon oxide, 1 part of diatomite, 2 parts of silica gel ions and 1 part of charcoal.

2. The manufacturing process of the fire-resistant oil regeneration filter material according to claim 1,

the method comprises the following steps:

firstly, respectively processing alumina, silica, diatomite, silica gel ions and charcoal into powder by using an ultrafine grinder;

mixing alumina, silica, diatomite, silica gel ions and charcoal according to a ratio of 3: 3: 1: 2: 1, thoroughly mixing to form synthetic powder;

and processing the synthetic powder into micro-particles with 300 meshes by using a particle processing machine to obtain the fire-resistant oil regeneration filter material.

3. The manufacturing process of the fire-resistant oil regeneration filter material according to claim 2, wherein the aluminum oxide, the silicon oxide, the diatomite, the silica gel ions and the charcoal are mixed according to a proportion of 3: 3: 1: 2: 1, when the materials are thoroughly mixed, adding and mixing the alumina, the silica, the kieselguhr, the silica gel ions and the charcoal in sequence.

4. The use method of the fire-resistant oil regeneration filter material according to claim 2, characterized by comprising the following steps: and calculating the weight of the filter material according to the volume of the fire-resistant oil, and then manufacturing the microparticles into a regenerative filter element.

5. The use method of the fire-resistant oil regeneration filter material according to claim 4, wherein the regeneration filter element is combined with a fire-resistant oil filter to carry out circulating filtration on fire-resistant oil.

6. The use method of the fire-resistant oil regeneration filter material according to claim 5, wherein the fire-resistant oil filter comprises an oil pump as a conveying power source, an oil pipeline for conveying the filter medium, a protective oil pump filter tank for installing a protective oil pump filter element, a heater for heating the filter medium, a regeneration filter tank for installing the regeneration filter element and a protective filter element tank for installing the protective filter element, which are connected in sequence, and the oil pipeline is provided with a plurality of control valves for controlling flow.

7. The use method of the fire-resistant oil regeneration filter material according to claim 6, wherein the fire-resistant oil filter machine further comprises a system detection probe for monitoring the temperature and the pressure of the filter medium, an instrument for observing the temperature and the pressure of the filter medium, an electrical control cabinet for controlling the normal operation of the oil filter machine and a machine body.

8. The use method of the fire-resistant oil regeneration filter material according to claim 6 is characterized in that the fire-resistant oil filter machine works in a way that an oil pump is started, and fire-resistant oil sequentially passes through an oil tank, a control valve, an oil conveying pipeline, a control valve, a protective oil pump filter tank, an oil pump, a pipeline, a heater, a regeneration filter tank, a protective filter element tank, a control valve, an oil conveying pipeline and an oil tank to form closed circulation.

Technical Field

The invention relates to a fire-resistant oil (EH oil) or a fire-resistant oil (EH oil) system used fire-resistant oil regeneration filter material, a manufacturing process and a using method thereof.

Background

The fire-resistant oil (EH oil) is a synthetic oil and has the characteristics of flame retardancy, no precipitate, low volatility, good abrasion resistance, good stability, stable physical property and the like. The fire-resistant oil (EH oil) has a high self-ignition point (350 ℃ of the ignition point of common hydraulic oil and 539 ℃ of the ignition point of fire-resistant oil) and can not be combusted even if falling on the surface of a high-temperature pipeline, so the fire-resistant oil (EH oil) is mainly used in high-temperature regulating systems (such as a steam turbine control and regulation system, a nuclear turbine lubricating oil system, a steel mill high-temperature part control system and the like). However, after the fire-resistant oil (EH oil) is operated for a period of time, the oil often has problems of increased particle size, increased acid value, increased moisture, increased chloride ions, decreased resistivity, and the like due to the environment, operation, system, and the like. These changes in the index cause significant damage (corrosion of the regulating parts, jamming, viscosity reduction, etc.) to the fuel regulation system.

The density of the fire-resistant oil is high (generally: 1.11-1.17), and the kinematic viscosity is also higher than that of the lubricating oil (generally 25mm2/s-45mm 2/s). Due to the high density of the fire-resistant oil, pollutants in the pipeline can be suspended on the liquid level and circulate in the system, so that certain parts are blocked and abraded; the excessive granularity can cause the jamming of a servo valve and the aggravation of the abrasion of an oil engine, and the operation safety of the unit is directly influenced. The high acid value can accelerate the hydrolysis of the fire-resistant oil, thereby shortening the service life of the fire-resistant oil and causing the corrosion of system components; the smaller the acid value, the better. The water can not only cause hydrolytic degradation of the fire-resistant oil and increase of acid value, but also cause corrosion of system components and influence the lubricating property of oil; if the system is flooded, chloride ions can corrode components in the system (oil motors, servo valves, pipes, etc.) and can damage the sealing materials; the low resistivity accelerates the deterioration of the oil quality of the fire-resistant oil and shortens the life of the fire-resistant oil. Therefore, the normal index of the fire-resistant oil is ensured, and the key for prolonging the service life of the unit and ensuring the operation safety of the unit is provided.

At present, although the regenerated filter materials such as diatomite, resin, molecular sieve and the like used domestically and internationally can solve the index problems, the regenerated filter materials are unstable, and the effect of the regenerated filter materials is gradually reduced until the regenerated filter materials lose the effect after long-term use.

Disclosure of Invention

In view of the above situation, in order to solve the problems in the prior art, the invention provides a fire-resistant oil regeneration filter material, and a manufacturing process and a using method thereof, which solve the problems of high acid value, low resistivity, increased chloride ions, excessive impurities, increased moisture and the like in the running process of a fire-resistant oil (EH oil) or an EH oil system.

The fire-resistant oil regeneration filter material comprises the following components in parts by weight: 3 parts of alumina, 3 parts of silicon oxide, 1 part of diatomite, 2 parts of silica gel ions and 1 part of charcoal.

A manufacturing process of a fire-resistant oil regeneration filter material comprises the following steps:

firstly, respectively processing alumina, silica, diatomite, silica gel ions and charcoal into powder by using an ultrafine grinder;

mixing alumina, silica, diatomite, silica gel ions and charcoal according to a ratio of 3: 3: 1: 2: 1, thoroughly mixing to form synthetic powder;

and processing the synthetic powder into micro-particles with 300 meshes by using a particle processing machine to obtain the fire-resistant oil regeneration filter material.

Preferably, the alumina, the silica, the diatomite, the silica gel ions and the charcoal are mixed according to the proportion of 3: 3: 1: 2: 1, when the materials are thoroughly mixed, adding and mixing the alumina, the silica, the kieselguhr, the silica gel ions and the charcoal in sequence.

The use method of the fire-resistant oil regeneration filter material comprises the following steps:

and calculating the weight of the filter material according to the volume of the fire-resistant oil, and then manufacturing the microparticles into a regenerative filter element. According to different conditions, the regeneration filter element can be installed in a fire-resistant oil system for filtering.

Preferably, the microparticles are made into a regenerative filter element, and then the regenerative filter element or the regenerative filter element which is installed in the fire-resistant oil system for filtering is combined with the fire-resistant oil filter for carrying out circulating filtration on the fire-resistant oil.

The fire-resistant oil filter comprises an oil pump serving as a conveying power source, an oil pipeline used for conveying a filter medium, a protective oil pump filter tank used for installing a protective oil pump filter element, a heater used for heating the filter medium, a regeneration filter tank used for installing a regeneration filter element and a protective filter element tank used for installing a protective filter element, wherein the oil pump, the oil pipeline and the protective oil pump filter tank are sequentially connected, and the oil pump is provided with a plurality of control valves used for controlling flow.

The fire resistant oil filter also comprises a system detection probe for monitoring the temperature and the pressure of the filter medium, an instrument for observing the temperature and the pressure of the filter medium, an electrical control cabinet for controlling the normal operation of the oil filter and a machine body.

The working method of the fire-resistant oil filter is that the oil pump is started, and fire-resistant oil sequentially passes through the oil tank, the control valve, the oil pipeline, the control valve, the protective oil pump filter tank, the oil pump, the pipeline, the heater, the regeneration filter tank, the protective filter element tank, the control valve, the oil pipeline and the oil tank to form closed circulation.

After the technology provided by the invention is adopted, the fire-resistant oil regeneration filter material and the manufacturing process and the using method thereof have the following beneficial effects.

1) The problems of high acid value, low resistivity, increased chloride ions, overproof impurities, increased moisture and the like in the operation process of the fire-resistant oil (EH oil) or the fire-resistant oil (EH oil) system can be solved. The environment-friendly fire-resistant oil filter material can effectively solve the problems of fire-resistant oil, reduce the acid value, improve the resistivity, reduce chloride ions (the content is not more than 200), remove impurities, remove oil sludge and the like, can resist the fire-resistant oil for long-term use, can be recovered and concentrated to be reduced for continuous use when the filter material is invalid, and is economical and environment-friendly.

2) The conventional filter material needs 40 kg/ton of fire-resistant oil for treating, and the manufacturing cost is 72000 yuan; the filter material of the application needs 10 kg/ton of fire-resistant oil, the manufacturing cost is 12000 yuan, and the benefit is 6 times of the original benefit.

3) The time for processing the fire-resistant oil by the filter material in the prior art is 600 hours/ton, the time for processing the fire-resistant oil by the filter material in the application is 120 hours/ton, and the efficiency is 5 times that of the prior art.

Detailed Description

Various preferred embodiments of the present invention will be described below. The following description is provided to facilitate understanding of example embodiments of the invention as defined by the claims and their equivalents. It includes various specific details to assist understanding, but they are to be construed as merely illustrative. Accordingly, those skilled in the art will recognize that various changes and modifications can be made to the embodiments described herein without departing from the scope and spirit of the present invention. Also, in order to make the description clearer and simpler, a detailed description of functions and configurations well known in the art will be omitted.

The fire-resistant oil regeneration filter material comprises the following components in parts by weight: 3 parts of alumina, 3 parts of silicon oxide, 1 part of diatomite, 2 parts of silica gel ions and 1 part of charcoal.

Further, the manufacturing process of the fire-resistant oil regeneration filter material comprises the following steps:

firstly, respectively processing alumina, silica, diatomite, silica gel ions and charcoal into powder by using an ultrafine grinder;

mixing alumina, silica, diatomite, silica gel ions and charcoal according to a ratio of 3: 3: 1: 2: 1, thoroughly mixing to form synthetic powder;

and processing the synthetic powder into micro-particles with 300 meshes by using a particle processing machine to obtain the fire-resistant oil regeneration filter material.

Further, the alumina, the silica, the diatomite, the silica gel ions and the charcoal are mixed according to the proportion of 3: 3: 1: 2: 1, when the materials are thoroughly mixed, adding and mixing the alumina, the silica, the kieselguhr, the silica gel ions and the charcoal in sequence.

Further, the use method of the fire-resistant oil regeneration filter material comprises the following steps: and calculating the weight of the filter material according to the volume of the fire-resistant oil, then manufacturing the microparticles into a regenerative filter element, and combining the regenerative filter element with a fire-resistant oil filter to perform circulating filtration on the fire-resistant oil.

The fire-resistant oil filter comprises an oil pump serving as a conveying power source, an oil pipeline used for conveying a filter medium, a protective oil pump filter tank used for installing a protective oil pump filter element, a heater used for heating the filter medium, a regeneration filter tank used for installing a regeneration filter element and a protective filter element tank used for installing a protective filter element, wherein the oil pump, the oil pipeline and the protective oil pump filter tank are sequentially connected, and the oil pump is provided with a plurality of control valves used for controlling flow.

The fire resistant oil filter also comprises a system detection probe for monitoring the temperature and the pressure of the filter medium, an instrument for observing the temperature and the pressure of the filter medium, an electrical control cabinet for controlling the normal operation of the oil filter and a machine body.

The working method of the fire-resistant oil filter is that the oil pump is started, and fire-resistant oil sequentially passes through the oil tank, the control valve, the oil pipeline, the control valve, the protective oil pump filter tank, the oil pump, the pipeline, the heater, the regeneration filter tank, the protective filter element tank, the control valve, the oil pipeline and the oil tank to form closed circulation.

According to the application, the anti-fuel oil regeneration filter material comprises the following components in the formula:

alumina (AI2O 3): deacidifying, improving resistivity, absorbing water and the like;

silicon oxide (SiO 2): water absorption, impurity removal and the like;

diatomite: deacidifying, removing impurities, improving resistivity and the like;

silica gel ion: dechlorination, deacidification, resistivity improvement and the like;

charcoal: dechlorination of ions, decolouring, removing peculiar smell, removing oil sludge and the like.

According to the fire-resistant oil regeneration filter material, the problems that an fire-resistant oil (EH oil) or an EH oil system is high in acid value, low in resistivity, high in chloride ion content, excessive in impurity content, high in water content and the like in the operation process can be solved. The environment-friendly fire-resistant oil filter material can effectively solve the problems of fire-resistant oil, reduce the acid value, improve the resistivity, reduce chloride ions (the content is not more than 200), remove impurities, remove oil sludge and the like, can resist the fire-resistant oil for long-term use, can be recovered and concentrated to be reduced for continuous use when the filter material is invalid, and is economical and environment-friendly.

The fire-resistant oil (EH oil) system is also called a high-pressure fire-resistant oil system and is mainly used for a speed regulating oil system (or a system with high-temperature and high-pressure control) of a steam turbine, the high-temperature fire-resistant oil (EH oil) is adopted, the high oil pressure is adopted to control position signals of each main valve and each speed regulating valve of the steam turbine (or the system with high-temperature and high-pressure control), the position signals are sent to a servo valve and an oil engine, the adjustment and the control are realized, and the safety function of closing each valve in emergency is realized through the fire-resistant oil system.

According to the application, the fire-resistant oil filter mainly structurally comprises an oil pump (conveying power source), a pipeline (conveying filter medium), a control valve (controlling flow), a heater (heating filter medium), a regeneration filter tank (installing a regeneration filter core), a protection filter core tank (installing a protection filter core), a protection oil pump filter tank (installing a protection oil pump filter core), a system detection probe (monitoring filter medium temperature and pressure), an instrument (observing filter medium temperature and pressure), an electric appliance control cabinet (controlling normal operation of the oil filter) and a machine body (fixing the oil filter device to form a whole).

The working principle is as follows: starting the oil pump, and enabling the fire-resistant oil to form closed circulation through the oil tank, the valve, the oil pipeline, the valve, the protective oil pump filter tank, the oil pump, the pipeline, the heater, the regenerative filter tank, the protective filter element tank, the valve, the oil pipeline and the oil tank. The fire-resistant oil is contacted with the regenerated filter material in the regeneration filter tank in a large area through the filter equipment, so that acid ions, chloride ions, negative ions, water ions and impurity particles in the oil are absorbed by the filter material, the purified fire-resistant oil returns to the oil tank through a pipeline and a protective filter element, and the fire-resistant oil continuously circulates between the oil filter and the oil tank until the fire-resistant oil is qualified.

According to the fire-resistant oil filter, fire-resistant oil indexes such as granularity, acid value, resistivity, chloride ions (less than 200), oil sludge, color and the like of the fire-resistant oil have good treatment effects, and the deteriorated and deteriorated fire-resistant oil performance indexes can be recovered to reach the new oil standard. The service life of the unit is prolonged, the operation safety of the unit is guaranteed, and the effects of reducing cost and protecting the environment can be achieved.

According to the fire-resistant oil regeneration filter material and the manufacturing process and the using method thereof, compared with the prior art, the fire-resistant oil regeneration filter material has the beneficial effects that:

the conventional filter material needs 40 kg/ton of fire-resistant oil for treating, and the manufacturing cost is 72000 yuan; the filter material of the application needs 10 kg/ton of fire-resistant oil, the manufacturing cost is 12000 yuan, and the benefit is 6 times of the original benefit.

The time for processing the fire-resistant oil by the filter material in the prior art is 600 hours/ton, the time for processing the fire-resistant oil by the filter material in the application is 120 hours/ton, and the efficiency is 5 times that of the prior art.

The present invention has been described in detail, and the principle and embodiments of the present invention are explained herein by using specific examples, which are only used to help understand the method and the core idea of the present invention; meanwhile, for a person skilled in the art, according to the idea of the present invention, there may be variations in the specific embodiments and the application scope, and in summary, the content of the present specification should not be construed as a limitation to the present invention.

From the above description of the embodiments, it will be apparent to those skilled in the art that the present invention may be practiced. Of course, the above listed cases are only examples, and the present invention is not limited thereto. It should be understood by those skilled in the art that other modifications or simplifications according to the technical solution of the present invention may be appropriately applied to the present invention and should be included in the scope of the present invention.

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