阅读说明：本技术 一种电子烟乳化香精的生产配方及制备方法 (Production formula and preparation method of electronic cigarette emulsified essence ) 是由 刘家仁 范俊俊 翟文娟 于 2019-11-27 设计创作，主要内容包括：本发明公开了一种电子烟乳化香精的生产配方及制备方法,由以下组成：食用香精、抗氧化剂、乳化剂、变性淀粉、增稠剂、防腐剂和去离子水；其中食用香精为主料,抗氧化剂、乳化剂、变性淀粉为辅料,增稠剂、去离子水与防腐剂为基料；可大大提高乳状液的乳析稳定性,可提高乳状液的絮凝、聚结稳定性；同时具有良好的界面流变特性,可减少乳状液的奥氏熟化。多层乳化可有效减少外界因素对香精的影响；本发明在制备香精的过程中采用逐一搅拌的方式,增加了乳化香精整体的粘稠度,提高了整体的乳化能力,使获得香精不论在香味上还是口感上都更适合大众的口味。(The invention discloses a production formula and a preparation method of an electronic cigarette emulsified essence, which comprises the following components: edible essence, antioxidant, emulsifier, modified starch, thickener, preservative and deionized water; wherein the edible essence is taken as a main material, the antioxidant, the emulsifier and the modified starch are taken as auxiliary materials, and the thickener, the deionized water and the preservative are taken as base materials; the emulsion stability of the emulsion can be greatly improved, and the flocculation and coalescence stability of the emulsion can be improved; meanwhile, the emulsion has good interfacial rheological property, and can reduce the austenite curing of the emulsion. The influence of external factors on the essence can be effectively reduced by multilayer emulsification; the invention adopts a mode of stirring one by one in the process of preparing the essence, increases the overall viscosity of the emulsified essence, improves the overall emulsifying capacity, and ensures that the obtained essence is more suitable for the taste of the public in both aroma and taste.)

1. The electronic cigarette emulsified essence is characterized by comprising the following components in parts by weight: edible essence, antioxidant, emulsifier, modified starch, thickener, preservative and deionized water; the edible essence is a main material, the antioxidant, the emulsifier and the modified starch are auxiliary materials, and the thickener, the deionized water and the preservative are base materials;

the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 45-55 parts of edible essence, 5-8 parts of antioxidant, 10-15 parts of emulsifier, 2-5 parts of modified starch, 3-6 parts of thickener, 1-3 parts of preservative and 60-100 parts of deionized water.

2. The production formula and the preparation method of the emulsified essence for the electronic cigarette according to claim 1, wherein the emulsifier is sorbitan fatty acid ester and polyglycerol fatty acid ester in a mass ratio of 1: 1.5 of the mixed emulsion.

3. The production formula and the preparation method of the emulsified flavor for electronic cigarettes according to claim 1, wherein the thickener is one of acacia gum and pectin.

4. The production formula and the preparation method of the emulsified essence for the electronic cigarette according to claim 1 are characterized in that the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 45 parts of edible essence, 5 parts of antioxidant, 10 parts of emulsifier, 2 parts of modified starch, 3 parts of thickener, 1 part of preservative and 60 parts of deionized water.

5. The production formula and the preparation method of the emulsified essence for the electronic cigarette according to claim 1 are characterized in that the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 50 parts of edible essence, 6 parts of antioxidant, 12 parts of emulsifier, 3 parts of modified starch, 4 parts of thickener, 2 parts of preservative and 80 parts of deionized water.

6. The production formula and the preparation method of the emulsified essence for the electronic cigarette according to claim 1 are characterized in that the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 55 parts of edible essence, 8 parts of antioxidant, 15 parts of emulsifier, 5 parts of modified starch, 6 parts of thickener, 3 parts of preservative and 100 parts of deionized water.

7. A preparation method of emulsified essence for electronic cigarettes is characterized by comprising the following steps:

weighing a group of edible essences according to a weight ratio; one part of antioxidant, emulsifier, modified starch, thickener, preservative and deionized water;

secondly, adding the weighed components into a stirring device for stirring, wherein the stirring time is 30min, the stirring speed is 500-700 rpm,

step three, firstly, adding edible essence and deionized water, stirring, adding the antioxidant, the emulsifier and the modified starch in sequence after uniformly mixing, stopping stirring after adding the antioxidant, the emulsifier and the modified starch each time, adding the thickening agent and the preservative in a weight ratio in sequence for three times, and then stirring;

step four, after stirring is finished, taking out the mixture to obtain an emulsion;

step five, homogenizing the first emulsion by a homogenizer at the homogenizing pressure of 10-20MPa to finally obtain a second emulsion;

step six, standing the second emulsified essence for 20-30min, filtering the second emulsified essence by using a funnel after standing, and filtering out impurities to obtain the emulsified essence;

and step seven, inspecting the emulsified essence.

8. The production formula and the preparation method of the emulsified essence for electronic cigarettes according to claim 7, wherein the inspection items comprise aroma, stock solution stability, particle size, diluent stability, arsenic content, heavy metal ratio and total number of bacteria.

Technical Field

The invention relates to the technical field of electronic cigarette production, in particular to a production formula and a preparation method of electronic cigarette emulsified essence.

Background

Electronic cigarette liquid (or called electronic cigarette atomized liquid) is a popular cigarette substitute product at present, and relates to the blending prescription and preparation process of the electronic cigarette liquid, and the electronic cigarette liquid is recovered to the aspects of health and the like. As more and more smokers begin to accept the use of electronic cigarettes instead of cigarettes, some deficiencies in the aerosolized liquid used in these electronic cigarettes are becoming more and more apparent.

Compared with cigarettes, electronic cigarettes have the senses of shape, hand feeling, smoke and the like similar to cigarettes, but have larger sense difference from cigarettes in the aspects of aroma, taste and the like, particularly products blended by various flavors and fragrances are difficult to accept or get used to the aroma and taste, and the emulsified essence can be added into the electronic cigarettes only by meeting the standards of aroma, stock solution stability, granularity, diluent stability, arsenic content, heavy metal proportion and total number of bacteria, and meanwhile, the emulsified essence is directly mixed with raw materials and then stirred, so that the taste, smoke color and throat degree are not fully stirred, and the quality of the essence is influenced.

Disclosure of Invention

The purpose of the invention can be realized by the following technical scheme: a production formula and a preparation method of electronic cigarette emulsified essence comprise the following components: edible essence, antioxidant, emulsifier, modified starch, thickener, preservative and deionized water; the edible essence is a main material, the antioxidant, the emulsifier and the modified starch are auxiliary materials, and the thickener, the deionized water and the preservative are base materials;

the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 45-55 parts of edible essence, 5-8 parts of antioxidant, 10-15 parts of emulsifier, 2-5 parts of modified starch, 3-6 parts of thickener, 1-3 parts of preservative and 60-100 parts of deionized water.

Preferably, the emulsifier is sorbitan fatty acid ester and polyglycerol fatty acid ester according to the mass ratio of 1: 1.5 of the mixed emulsion.

Preferably, the thickening agent is one of gum arabic or pectin.

Preferably, the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 45 parts of edible essence, 5 parts of antioxidant, 10 parts of emulsifier, 2 parts of modified starch, 3 parts of thickener, 1 part of preservative and 60 parts of deionized water.

Preferably, the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 50 parts of edible essence, 6 parts of antioxidant, 12 parts of emulsifier, 3 parts of modified starch, 4 parts of thickener, 2 parts of preservative and 80 parts of deionized water.

Preferably, the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 55 parts of edible essence, 8 parts of antioxidant, 15 parts of emulsifier, 5 parts of modified starch, 6 parts of thickener, 3 parts of preservative and 100 parts of deionized water.

A preparation method of emulsified essence for electronic cigarettes comprises the following steps:

weighing a group of edible essences according to a weight ratio; one part of antioxidant, emulsifier, modified starch, thickener, preservative and deionized water;

secondly, adding the weighed components into a stirring device for stirring, wherein the stirring time is 30min, the stirring speed is 500-700 rpm,

step three, firstly, adding edible essence and deionized water, stirring, adding the antioxidant, the emulsifier and the modified starch in sequence after uniformly mixing, stopping stirring after adding the antioxidant, the emulsifier and the modified starch each time, adding the thickening agent and the preservative in a weight ratio in sequence for three times, and then stirring;

step four, after stirring is finished, taking out the mixture to obtain an emulsion;

step five, homogenizing the first emulsion by a homogenizer at the homogenizing pressure of 10-20MPa to finally obtain a second emulsion;

step six, standing the second emulsified essence for 20-30min, filtering the second emulsified essence by using a funnel after standing, and filtering out impurities to obtain the emulsified essence;

and step seven, inspecting the emulsified essence.

Preferably, the test items include aroma, stock solution stability, particle size, diluent stability, arsenic content, heavy metal ratio and total number of bacteria.

The invention has the beneficial effects that:

1. the emulsion stability of the emulsion can be greatly improved, and the flocculation and coalescence stability of the emulsion can be improved; meanwhile, the emulsion has good interfacial rheological property, and can reduce the austenite curing of the emulsion. The influence of external factors on the essence can be effectively reduced by multilayer emulsification;

2. the invention adopts a mode of stirring one by one in the process of preparing the essence, increases the overall viscosity of the emulsified essence, improves the overall emulsifying capacity, and ensures that the obtained essence is more suitable for the taste of the public in both aroma and taste.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention provides a technical scheme that: a production formula and a preparation method of electronic cigarette emulsified essence comprise the following components: edible essence, antioxidant, emulsifier, modified starch, thickener, preservative and deionized water; the edible essence is a main material, the antioxidant, the emulsifier and the modified starch are auxiliary materials, and the thickener, the deionized water and the preservative are base materials;

the main material, the auxiliary material and the base material are composed of the following components in parts by weight: 45-55 parts of edible essence, 5-8 parts of antioxidant, 10-15 parts of emulsifier, 2-5 parts of modified starch, 3-6 parts of thickener, 1-3 parts of preservative and 60-100 parts of deionized water.

The emulsifier is sorbitan fatty acid ester and polyglycerol fatty acid ester according to the mass ratio of 1: 1.5 of the mixed emulsion.

The thickening agent is one of Arabic gum or pectin.

The main material, the auxiliary material and the base material are composed of the following components in parts by weight: 45 parts of edible essence, 5 parts of antioxidant, 10 parts of emulsifier, 2 parts of modified starch, 3 parts of thickener, 1 part of preservative and 60 parts of deionized water.

The main material, the auxiliary material and the base material are composed of the following components in parts by weight: 50 parts of edible essence, 6 parts of antioxidant, 12 parts of emulsifier, 3 parts of modified starch, 4 parts of thickener, 2 parts of preservative and 80 parts of deionized water.

The main material, the auxiliary material and the base material are composed of the following components in parts by weight: 55 parts of edible essence, 8 parts of antioxidant, 15 parts of emulsifier, 5 parts of modified starch, 6 parts of thickener, 3 parts of preservative and 100 parts of deionized water.

A preparation method of emulsified essence for electronic cigarettes comprises the following steps:

weighing a group of edible essences according to a weight ratio; one part of antioxidant, emulsifier, modified starch, thickener, preservative and deionized water;

secondly, adding the weighed components into a stirring device for stirring, wherein the stirring time is 30min, the stirring speed is 500-700 rpm,

step three, firstly, adding edible essence and deionized water, stirring, adding the antioxidant, the emulsifier and the modified starch in sequence after uniformly mixing, stopping stirring after adding the antioxidant, the emulsifier and the modified starch each time, adding the thickening agent and the preservative in a weight ratio in sequence for three times, and then stirring;

step four, after stirring is finished, taking out the mixture to obtain an emulsion;

step five, homogenizing the first emulsion by a homogenizer at the homogenizing pressure of 10-20MPa to finally obtain a second emulsion;

step six, standing the second emulsified essence for 20-30min, filtering the second emulsified essence by using a funnel after standing, and filtering out impurities to obtain the emulsified essence;

and step seven, inspecting the emulsified essence.

The inspection items comprise aroma, stock solution stability, granularity, diluent stability, arsenic content, heavy metal ratio and total number of bacteria.