阅读说明：本技术 一种服饰消毒喷雾剂的制备方法 (Preparation method of clothing disinfection spray ) 是由 代培义 于 2019-10-18 设计创作，主要内容包括：本发明公开了一种服饰消毒喷雾剂的制备方法,涉及消毒剂技术领域,包括以下步骤：(1)金银花的利用；(2)苦楝花的利用；(3)薰衣草的利用；(4)消毒喷雾剂的制备。本发明以金银花、苦楝花和薰衣草作为杀菌抑菌药效成分的制备原料,通过对这三味中药所含药效成分进行提取,并协以表面活性剂制得适用于服饰的消毒喷雾剂；制得的消毒喷雾剂味道清香,使用方便,具有显著的杀菌抑菌效果,并且经其消毒后的服饰不会对皮肤产生任何刺激,使用安全性高。(The invention discloses a preparation method of a clothing disinfection spray, relating to the technical field of disinfectants and comprising the following steps: (1) utilization of honeysuckle; (2) utilization of the melia azedarach flower; (3) utilization of lavender; (4) and (4) preparing a disinfection spray. The honeysuckle flower, the chinaberry flower and the lavender are used as preparation raw materials of bactericidal and bacteriostatic active ingredients, the active ingredients contained in the three traditional Chinese medicines are extracted, and a surfactant is cooperated to prepare the disinfection spray applicable to clothes; the prepared disinfection spray has fragrant taste, is convenient to use, has obvious sterilization and bacteriostasis effects, does not generate any stimulation to skin after the clothing is disinfected, and has high use safety.)

1. A preparation method of a clothes disinfection spray is characterized by comprising the following steps: the method comprises the following steps:

(1) utilization of honeysuckle flower: adding water into honeysuckle, making into slurry by a slurry mill, adding citric acid into the slurry, heating to 70-80 ℃, keeping the temperature, stirring, filtering, and freeze-drying the obtained filtrate to obtain powder, namely honeysuckle extract;

(2) utilization of the melia azedarach flowers: adding flos Meliae into anhydrous ethanol, heating to reflux state, stirring, filtering when the temperature is reduced to below 50 deg.C, adding water into the filtrate, stirring, and collecting upper oil layer to obtain flos Meliae extract;

(3) utilization of lavender: adding Lavender into anhydrous alcohol, heating to reflux state, stirring, filtering when the temperature is reduced to below 50 deg.C, adding water into the filtrate, stirring, and collecting upper oil layer to obtain Lavender extract;

(4) preparing a disinfection spray: adding flos Lonicerae extract, flos Meliae extract, Lavender extract and surfactant into water, and mixing.

2. The preparation method according to claim 1, wherein the surfactant is selected from one or more of sodium dodecyl sulfate, α -olefin sulfonate, and dodecyl glucoside.

3. The method of claim 1, wherein: the mass ratio of the honeysuckle extract to the chinaberry flower extract to the lavender extract to the auxiliary materials is 0.5-5:0.5-5:0.5-5: 1-15.

The technical field is as follows:

the invention relates to the technical field of disinfectant processing, in particular to a preparation method of a clothing disinfection spray.

Background art:

clothes, a general term for articles for decorating human bodies, including clothes, shoes, hats, socks, gloves, scarves, ties, accessories, bags, umbrellas and the like. In daily life, clothes used by people can be contacted with various bacteria, and if some bacteria are not killed in time, the bacteria can cause harm to human health. The existing partial washing products have a sterilization effect, but have a limited sterilization effect and short action time, and cannot meet the sterilization requirements of people at all. In addition, although the washing products added with the chemical sterilization components have strong sterilization effect, the washing products have pungent taste and potential safety hazards in use.

Aiming at the problem, the invention provides a preparation method of a clothing disinfection spray, which utilizes plant components to exert sterilization and bacteriostasis effects, and has high use safety and remarkable sterilization and bacteriostasis effects.

The invention content is as follows:

the technical problem to be solved by the invention is to provide a preparation method of the clothing disinfection spray, the prepared disinfection spray has faint scent and obvious sterilization and bacteriostasis effects, and the disinfected clothing does not generate any stimulation to the skin.

The technical problem to be solved by the invention is realized by adopting the following technical scheme:

a preparation method of a clothes sterilizing spray comprises the following steps:

(1) utilization of honeysuckle flower: adding water into honeysuckle, making into slurry by a slurry mill, adding citric acid into the slurry, heating to 70-80 ℃, keeping the temperature, stirring, filtering, and freeze-drying the obtained filtrate to obtain powder, namely honeysuckle extract;

(2) utilization of the melia azedarach flowers: adding flos Meliae into anhydrous ethanol, heating to reflux state, stirring, filtering when the temperature is reduced to below 50 deg.C, adding water into the filtrate, stirring, and collecting upper oil layer to obtain flos Meliae extract;

(3) utilization of lavender: adding Lavender into anhydrous alcohol, heating to reflux state, stirring, filtering when the temperature is reduced to below 50 deg.C, adding water into the filtrate, stirring, and collecting upper oil layer to obtain Lavender extract;

(4) preparing a disinfection spray: adding flos Lonicerae extract, flos Meliae extract, Lavender extract and surfactant into water, and mixing.

The surfactant is selected from one or more of sodium dodecyl sulfate, α -olefin sodium sulfonate and dodecyl glucoside.

The mass ratio of the honeysuckle extract to the chinaberry flower extract to the lavender extract to the auxiliary materials is 0.5-5:0.5-5:0.5-5: 1-15.

In order to improve the storage stability of the melia azedarach extract and the lavender extract and ensure the sterilization and bacteriostasis effects of the melia azedarach extract and the lavender extract, the invention also adds a stabilizer into the hand sanitizer, namely replacing the content in the step (4) with: adding honeysuckle extract, chinaberry flower extract, lavender extract, surfactant and stabilizer into water, and mixing uniformly.

The stabilizer is modified carbomer and is prepared by chemically modifying carbomer, and the preparation method comprises the following steps: adding carbomer 941 and polyetheramine D-230 into water, heating to 60-70 deg.C, stirring under constant temperature, adding condensing agent, heating to reflux state, stirring under constant temperature, naturally cooling to room temperature, standing at 0-5 deg.C, filtering, washing with water, oven drying, and making into powder.

The condensing agent is EDCI and HOBt.

The mass ratio of the surfactant to the stabilizer is 5: 0.5-5.

And (3) taking polyether amine as a modifier, and carrying out condensation reaction on amino groups contained in the polyether amine and carboxyl groups contained in carbomer to generate amide bonds. Carbomer does not have stability to the storage of the melia azedarach extract and the lavender extract, modified carbomer obtained after modification by polyether amine can play a stabilizing role in the extracts, and the volatile oil in the extracts is prevented from volatilizing by utilizing the clathration effect.

The invention has the beneficial effects that:

(1) the invention takes honeysuckle, chinaberry flower and lavender as preparation raw materials of bactericidal and bacteriostatic active ingredients, extracts the active ingredients contained in the three traditional Chinese medicines and prepares the disinfection spray suitable for clothes by cooperating with a surfactant.

(2) The traditional Chinese medicine formula comprises honeysuckle, chinaberry flower and lavender, is simple, cheap and easy to obtain, and is obviously different from the traditional Chinese medicine disinfectant spray which needs to be added with a plurality of traditional Chinese medicines to obtain the sterilizing and bacteriostatic effect meeting the use requirement and the problem that the chemical disinfectant spray has potential safety hazard to human bodies although the sterilizing and bacteriostatic effect is good.

(3) The prepared disinfection spray has fragrant taste, is convenient to use, has obvious sterilization and bacteriostasis effects, does not generate any stimulation to skin after the clothing is disinfected, and has high use safety.

The specific implementation mode is as follows:

in order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.

The following examples and comparative examples were prepared with honeysuckle, melia azedarach and lavender, respectively, from the same manufacturer.