阅读说明：本技术 一种稀有金属碘化提纯装置 (Rare metal iodization purification device ) 是由 汪娟 于 2019-10-30 设计创作，主要内容包括：本发明公开了一种稀有金属碘化提纯装置,一种稀有金属碘化提纯装置,包括设备主体、碾碎装置、碘化剂入口、缓冲口装置、第一电机、转动杆、第一把手、热油入口、支撑脚、过滤层、出污口、冷凝管和观察窗,所述设备主体上端设置有物料入口,所述碾碎装置安装在物料入口内部,所述物料入口下端安装有筛网,所述碘化剂入口设置在设备主体上端。该稀有金属碘化提纯装置中设置有冷凝管和抽风装置,由于碘的不稳定性,容易在装置中升华变成挥发的气体,通过冷凝管对碘性气体进行冷凝,在通过抽风装置对碘进行吸收,将装置中汽化的碘重新收集到碘化剂入口,再次进入到反应内腔内发生反应,如此循环,提高了碘的利用率,避免了资源的浪费。(The invention discloses a rare metal iodination purification device which comprises an equipment main body, a crushing device, an iodizing agent inlet, a buffer port device, a first motor, a rotating rod, a first handle, a hot oil inlet, supporting legs, a filtering layer, a dirt outlet, a condensing pipe and an observation window. Be provided with condenser pipe and updraft ventilator among this rare metal iodine purification device, because the instability of iodine, easily sublime in the device and become volatile gas, condense iodine gas through the condenser pipe, absorb the iodine through updraft ventilator, with the iodine of vaporization in the device collect the iodinating agent entry again, reentrant reaction inner chamber takes place the reaction, so circulate, improved the utilization ratio of iodine, avoided the waste of resource.)

1. The utility model provides a rare metal iodination purification device, includes equipment main part (1), pulverizes device (3), iodizing agent entry (5), buffer port device (6), first motor (7), dwang (9), first handle (11), hot oil entry (16), supporting legs (19), filter layer (20), go out dirty mouthful (22), condenser pipe (24) and observation window (27), its characterized in that: the utility model discloses an iodizing agent grinding device, including equipment main body (1), grinding device (3), screen cloth (4) are installed to material entry (2) lower extreme, iodizing agent entry (5) set up in equipment main body (1) upper end, buffer port device (6) set up at iodizing agent entry (5) lower extreme, install between material entry (2) and iodizing agent entry (5) first motor (7), first motor (7) lower surface mounting has pivot (8), dwang (9) lower surface is installed at pivot (8), dwang (9) surface fixedly connected with brush (10), first in command (11) set up at first motor (7) side, first in command (11) lower surface fixedly connected with female silk (12), first in command (11) surface fixedly connected with first buckle (13), first buckle (13) side is provided with draw-in groove (14), and draw-in groove (14) install inside equipment main part (1), brush (10) side is provided with heat preservation (15), hot oil entry (16) alternate and connect inside heat preservation (15), hot oil entry (16) lower extreme is provided with heating pipe (17), heat preservation (15) lower surface alternates and is connected with hot oil export (18), install at equipment main part (1) lower surface supporting legs (19), filter layer (20) set up at dwang (9) lower extreme, solenoid valve device (21) is installed to filter layer (20) lower extreme, go out dirty mouthful (22) and install at solenoid valve device (21) lower surface, be close to go out dirty mouthful (22) solenoid valve device (21) lower surface mounting has iodine export (23), condenser pipe (24) set up at iodine export (23) end, updraft ventilator (25) are installed to condenser pipe (24) side, updraft ventilator (25) upper end is provided with second motor (26), install at equipment main part (1) surface mounting observation window (27), be close to observation window (27) equipment main part (1) surface is provided with temperature detector (28).

2. The apparatus for iodinating and purifying rare metals according to claim 1, wherein: the outer surface of the screen (4) is tangent to the inner surface of the material inlet (2), and a plurality of through holes are uniformly distributed on the screen (4).

3. The apparatus for iodinating and purifying rare metals according to claim 1, wherein: buffer (6) include funnel mouth (601), buffer layer (602) and export (603), funnel mouth (601) lower extreme fixedly connected with buffer layer (602), and buffer layer (602) inside evenly distributed have a plurality of triangle-shaped dogs, buffer layer (602) lower surface fixedly connected with export (603).

4. The apparatus for iodinating and purifying rare metals according to claim 1, wherein: the rotating shaft (8) and the rotating rod (9) form a rotating structure, and the rotating angle of the rotating rod (9) on the vertical plane is 0-360 degrees.

5. The apparatus for iodinating and purifying rare metals according to claim 1, wherein: the number of the brushes (10) is two, and the tail ends of the brushes (10) are tangent to the end face of the reaction inner cavity of the equipment main body (1).

6. The apparatus for iodinating and purifying rare metals according to claim 1, wherein: the first buckle (13) and the clamping groove (14) form a clamping structure, and a layer of elastic rubber is wrapped on the surface of the first buckle (13).

7. The apparatus for iodinating and purifying rare metals according to claim 1, wherein: the filter layer (20) comprises a sieve pore (2001), a second handle (2002) and a second buckle (2003), the second handle (2002) is fixedly connected to the upper end of the sieve pore (2001), the second buckle (2003) is fixedly connected to the lower end of the sieve pore (2001), and a clamping groove which forms a clamping structure with the second buckle (2003) is arranged inside the device.

8. The apparatus for iodinating and purifying rare metals according to claim 1, wherein: electromagnetic control valve device (21) includes coil (2101), connecting rod (2102), dog (2103), spring (2104), connector (2105) and magnet (2106), coil (2101) outer fixed surface is connected with connecting rod (2102), connecting rod outer fixed surface is connected with dog (2103), and dog (2103) are provided with 2, connecting rod (2102) end fixed connection has spring (2104), connector (2105) set up at dog (2103) lower extreme, and the distance between dog (2103) is greater than the distance between lower extreme connector (2105), and the width of dog (2103) is greater than the width of connector (2105), coil (2101) both ends are provided with magnet (2106).

9. A rare metal iodination purification method is characterized in that: firstly, a simple understanding of the rare metal iodination purification device needs to be carried out, a user places the device at a designated position, the device is fixed through a supporting leg 19, purified metal enters a material inlet 2, is crushed through a crushing device 3, flows into the device from a screen 4, iodine enters from an iodination agent inlet 5, passes through a buffering port device 6, a plurality of triangular stop blocks are uniformly distributed inside a buffering layer 602 in the buffering port device 6, the iodine passes through the inside of the buffering layer 602, the transportation time of the iodine can be prolonged through the triangular stop blocks, the iodine and the purified metal react in the device, the iodine is volatile to be gas, iodine gas is condensed through a condensing pipe 24, the iodine is absorbed through an air draft device 25, the vaporized iodine in the device is collected to the iodination agent inlet 5 again, the process is circulated, and a first buckle 13 and a clamping groove 14 form a clamping structure, take out female silk 12 through first in command 11, when needs cleared up the device inside, first motor 7 work drives pivot 8 and rotates to make dwang 9 rotatory, make brush 10 wash along the device inner wall, coil 2101 circular telegram opens out dirty mouthful 22, and dog 2103 shelters from iodine outlet 23, the discharge dirt, this is exactly the device's work flow.

Technical Field

The invention relates to the technical field of purification, in particular to a rare metal iodination purification device.

Background

Rare metals are less in earth crust, difficult to extract from raw materials, not very high in purity, and often extracted by some chemical methods, and iodination purification is one of the rare metals.

In some chemical laboratories, rare metal iodination purification devices need to be utilized, and the purification devices are widely available on the market, but the utilization efficiency of iodine is low and resource waste is caused easily when the purification devices on the market are used, so that a technology capable of improving the structure of the rare metal iodination purification device is urgently needed on the market to perfect the equipment.

Disclosure of Invention

The invention aims to provide a rare metal iodination purification device, which solves the problems that the prior purification device on the market is easy to cause low iodine utilization efficiency and resource waste when in use.

In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a rare metal iodization purification device, includes equipment principal, milling device, iodizing agent entry, buffering mouth device, first motor, dwang, the first in command, hot oil entry, supporting legs, filter layer, dirt outlet, condenser pipe and observation window, equipment principal upper end is provided with material inlet, milling device installs inside material inlet, the screen cloth is installed to the material inlet lower extreme, the iodizing agent entry sets up in equipment principal upper end, buffering mouth device sets up at iodizing agent entry lower extreme, first motor is installed between material entry and iodizing agent entry, the lower surface mounting of first motor has the pivot, the dwang is installed at the pivot lower surface, dwang surface fixedly connected with brush, the first in command sets up at first motor side, the lower surface fixedly connected with female silk of the first in command, the outer surface of the first handle is fixedly connected with a first buckle, the side end of the first buckle is provided with a clamping groove, the clamping groove is arranged in the equipment main body, the side end of the brush is provided with a heat preservation layer, a hot oil inlet is connected in the heat preservation layer in an inserting manner, the lower end of the hot oil inlet is provided with a heating pipe, the lower surface of the heat preservation layer is connected with a hot oil outlet in an inserting manner, the supporting legs are arranged on the lower surface of the equipment main body, the filtering layer is arranged at the lower end of the rotating rod, the lower end of the filtering layer is provided with an electromagnetic adjusting valve device, the sewage outlet is arranged on the lower surface of the electromagnetic adjusting valve device, the lower surface of the electromagnetic adjusting valve device close to the sewage outlet is provided with an iodine outlet, and a temperature detector is arranged on the outer surface of the equipment main body close to the observation window.

Preferably, the outer surface of the screen is tangent to the inner surface of the material inlet, and a plurality of through holes are uniformly distributed on the screen.

Preferentially, buffer includes flare opening, buffer layer and export, flare opening lower extreme fixedly connected with buffer layer, and the inside evenly distributed of buffer layer has a plurality of triangle-shaped dogs, the buffer layer lower surface fixedly connected with export.

Preferentially, the rotating shaft and the rotating rod form a rotating structure, and the rotating angle of the rotating rod on the vertical plane is 0-360 degrees.

Preferentially, the number of the hairbrushes is two, and the tail ends of the hairbrushes are tangent to the end face of the reaction inner cavity of the equipment main body.

Preferably, the first buckle and the clamping groove form a clamping structure, and the surface of the first buckle is wrapped by a layer of elastic rubber.

Preferentially, the filter layer includes sieve mesh, second handle and second buckle, sieve mesh upper end fixedly connected with second handle, sieve mesh lower extreme fixedly connected with second buckle, and device inside is provided with the draw-in groove that constitutes the block structure with the second buckle.

Preferentially, the electromagnetic control valve device comprises a coil, a connecting rod, a stop block, a spring, a connector and a magnet, wherein the outer surface of the coil is fixedly connected with the connecting rod, the outer surface of the connecting rod is fixedly connected with the stop block, the stop block is provided with 2 connecting rods, the spring is fixedly connected with the tail end of the connecting rod, the connector is arranged at the lower end of the stop block, the distance between the stop blocks is greater than the distance between the connectors at the lower end, the width of the stop block is greater than the width of the connector.

Compared with the prior art, the invention has the beneficial effects that: this rare metal iodination purification device:

1. the device is internally provided with a condenser pipe and an air draft device, an iodizing agent reacts with metal in the reaction inner cavity, the iodizing agent is easy to sublimate in the device and becomes volatile gas due to the instability of iodine, the iodized gas is condensed through the condenser pipe, the iodine is absorbed through the air draft device, the iodine vaporized in the device is collected to the iodizing agent inlet again and enters the reaction inner cavity again for reaction, and the cycle is repeated, so that the utilization rate of the iodine is improved, and the waste of resources is avoided;

2. the rotating rod and the brush are arranged in the device, the tail end of the brush is tangent to the end face of the reaction inner cavity of the equipment main body, the rotating shaft is driven to rotate through the first motor, so that the rotating rod rotates, the rotating angle of the rotating rod on a vertical plane is 0-360 degrees, the brush is fixedly connected with the rotating rod, the inside of the device can be cleaned through the brush, the operation is facilitated, and the problem that the service life of the device is influenced due to the fact that the inside of the reaction inner cavity is not cleaned for a long time is;

3. be provided with milling device and screen cloth in the device, can pulverize into the clastic form by the metal of purification, get into the reaction inner chamber through the screen cloth, increased the reaction area by the metal of purification, be provided with the buffer mouth device in the device, inside evenly distributed has a plurality of triangle-shaped dogs, iodine is inside through the buffer layer, through the triangle-shaped dog, can prolong the transit time of iodine, and last even feed, carry out incessant iodine that adds, the time of reaction has been improved, the purification effect can improve.

4. The device is provided with the observation window and the temperature detector, so that the purification reaction of the reaction inner cavity can be observed and recorded in real time, the internal temperature can be conveniently adjusted and adjusted in time, the use of the actual condition is facilitated, the heating pipe is arranged in the device, the interior of the heat-insulating layer can be heated, the temperature required by the rare metal iodination reaction is met, and the overall effect is good;

5. the device is internally provided with the electromagnetic regulating valve device, the coil is powered off, the iodine outlet is opened, the baffle blocks the iodine outlet, iodine in the device can be conveniently recycled, the coil is powered on, the iodine outlet is opened, the baffle blocks the iodine outlet, and then the dirt cleaned by the device is discharged, the function of the connecting port is clearly divided, and the overall practicability is improved;

6. be provided with the first in command in the device, and the first buckle of first in command surface fixed connection constitutes the block structure with the draw-in groove, because rare metal is attached to on the female silk that links to each other with the first in command after being purified, through the setting of block structure, can conveniently take out the rare metal after the purification, whole leakproofness is better.

Drawings

FIG. 1 is a schematic structural view of the present invention;

FIG. 2 is a view of the exterior surface of the present invention;

FIG. 3 is a view of the first handle structure of the present invention;

FIG. 4 is a diagram of a buffer port device according to the present invention;

FIG. 5 is a view showing the structure of a filter layer according to the present invention;

fig. 6 is a structural view of an electromagnetic regulating valve device of the present invention.

In the figure: 1. the device comprises a device main body, 2, a material inlet, 3, a crushing device, 4, a screen mesh, 5, an iodizing agent inlet, 6, a buffer port device, 601, a funnel port, 602, a buffer layer, 603, an outlet, 7, a first motor, 8, a rotating shaft, 9, a rotating rod, 10, a brush, 11, a first handle, 12, a female wire, 13, a first buckle, 14, a clamping groove, 15, a heat insulation layer, 16, a hot oil inlet, 17, a heating pipe, 18, a hot oil outlet, 19, a supporting leg, 20, a filter layer, 2001, a sieve mesh, 2002, a second handle, 2003, a second buckle, 21, an electromagnetic adjusting valve device, 2101, a coil, 2102, a connecting rod, 3, a stop block, 2104, a spring, 2105, a connecting port, 2106, a magnet, 22, a dirt outlet, 23, an iodine outlet, 24, a condensation pipe, 25, an air draft device, 26, a second motor, 27, an observation window, 28 and a.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Referring to fig. 1-6, the present invention provides a technical solution: a rare metal iodination purification device comprises an equipment main body 1, a material inlet 2, a crushing device 3, a screen 4, an iodination agent inlet 5, a buffer port device 6, a first motor 7, a rotating shaft 8, a rotating rod 9, a brush 10, a first handle 11, a female wire 12, a first buckle 13, a clamping groove 14, a heat preservation layer 15, a hot oil inlet 16, a heating pipe 17, a hot oil outlet 18, a supporting leg 19, a filtering layer 20, an electromagnetic regulating valve device 21, a dirt outlet 22, an iodine outlet 23, a condensing pipe 24, an air draft device 25, a second motor 26, an observation window 27 and a temperature detector 28, wherein the material inlet 2 is formed in the upper end of the equipment main body 1, the crushing device 3 is installed in the material inlet 2, the screen 4 is installed at the lower end of the material inlet 2, the iodination agent inlet 5 is formed in the upper end of the equipment main body 1, the buffer port device 6 is arranged at, the utility model discloses a heat preservation device, including a first motor 7, a first handle 11, a second handle 11, a heating pipe 17, a heat preservation layer 15, a first buckle 13, and a clamping groove 14, the first motor 7 is installed between material entry 2 and iodizing agent entry 5, surface mounting has pivot 8 under the first motor 7, dwang 9 is installed at pivot 8 lower surface, dwang 9 outer fixed surface is connected with brush 10, the first handle 11 sets up at first motor 7 side, surface fixed surface is connected with female silk 12 under the first handle 11, the first handle 11 outer fixed surface is connected with first buckle 13, first buckle 13 side is provided with draw-in groove 14, and draw-in groove 14 installs inside equipment main body 1, brush 10 side is provided with heat preservation layer 15, hot oil entry 16 alternates to be connected inside heat preservation layer 15, hot oil entry 16 lower extreme is provided, the lower end of the filter layer 20 is provided with an electromagnetic regulating valve device 21, the dirt outlet 22 is arranged on the lower surface of the electromagnetic regulating valve device 21, the lower surface of the electromagnetic regulating valve device 21 close to the dirt outlet 22 is provided with an iodine outlet 23, the condenser pipe 24 is arranged at the tail end of the iodine outlet 23, the side end of the condenser pipe 24 is provided with an air draft device 25, the upper end of the air draft device 25 is provided with a second motor 26, the observation window 27 is arranged on the outer surface of the equipment main body 1, the outer surface of the equipment main body 1 close to the observation window 27 is provided with a temperature detector 28, the outer surface of the screen 4 is tangent to the inner surface of the material inlet 2, and a plurality of through holes are uniformly distributed on the screen 4 to filter purified metal, and only crushed metal can pass; the buffer device 6 comprises a funnel opening 601, a buffer layer 602 and an outlet 603, the buffer layer 602 is fixedly connected to the lower end of the funnel opening 601, a plurality of triangular baffle blocks are uniformly distributed in the buffer layer 602, the outlet 603 is fixedly connected to the lower surface of the buffer layer 602, iodine passes through the buffer layer 602, the iodine can be transported for a long time through the triangular baffle blocks, the iodine can be continuously and uniformly fed, the iodine can be continuously added, and the reaction time is prolonged; the rotating shaft 8 and the rotating rod 9 form a rotating structure, the rotating angle of the rotating rod 9 on a vertical plane is 0-360 degrees, the rotating shaft 8 is driven to rotate through the first motor 7, and therefore the rotating rod 9 rotates, and conditions are provided for the interior of the cleaning device; the number of the brushes 10 is two, the tail ends of the brushes 10 are tangent to the end face of the reaction inner cavity of the equipment main body 1, and the brushes 10 are driven to rotate to clean the surface of the reaction inner cavity through rotation of the rotating rod 9, so that the operation is convenient; the first buckle 13 and the clamping groove 14 form a clamping structure, a layer of elastic rubber is wrapped on the surface of the first buckle 13, and the first buckle 13 and the clamping groove 14 form the clamping structure, so that the female wire 12 can be conveniently taken out from the first handle 11; the filtering layer 20 comprises a sieve pore 2001, a second handle 2002 and a second buckle 2003, the second handle 2002 is fixedly connected to the upper end of the sieve pore 2001, the second buckle 2003 is fixedly connected to the lower end of the sieve pore 2001, and a clamping groove which forms a clamping structure with the second buckle 2003 is arranged in the filtering layer, so that unrefined metal is prevented from flowing out and polluting the condensation pipe 24; the electromagnetic regulating valve device 21 comprises a coil 2101, a connecting rod 2102, a stop 2103, springs 2104, a connecting port 2105 and magnets 2106, the connecting rod 2102 is fixedly connected to the outer surface of the coil 2101, the stop 2103 is fixedly connected to the outer surface of the connecting rod, 2 stops 2103 are arranged, the springs 2104 are fixedly connected to the tail ends of the connecting rod 2102, the connecting port 2105 is arranged at the lower end of the stop 2103, the distance between the stops 2103 is larger than the distance between the lower end connecting ports 2105, the width of the stop 2103 is larger than the width of the connecting port 2105, the magnets 2106 are arranged at two ends of the coil 2101, the iodine outlet 23 is opened when the coil 2101 is powered off, the dirt outlet 22 is shielded by the stop 2103, iodine in the device can be conveniently recycled, the coil 2101 is powered on, the dirt outlet 22 is opened, the iodine outlet 23.

The working principle is as follows: when the rare metal iodination purification device is used, firstly, a user needs to simply know the rare metal iodination purification device, places the device at a designated position, fixes the device through the supporting legs 19, purified metal enters the material inlet 2, is crushed through the crushing device 3 and flows into the device from the screen 4, iodine enters from the iodination agent inlet 5, passes through the buffer port device 6, a plurality of triangular stop blocks are uniformly distributed inside the buffer layer 602 in the buffer port device 6, iodine passes through the inside of the buffer layer 602, the transportation time of the iodine can be prolonged through the triangular stop blocks, the iodine reacts with the purified metal in the device, the iodine is volatilized to form gas, iodine gas is condensed through the condensing pipe 24, the iodine is absorbed through the air draft device 25, the vaporized iodine in the device is collected to the iodination agent inlet 5 again, so circulate, first buckle 13 constitutes block structure with draw-in groove 14, take out female silk 12 through first handle 11, when needs clear up the device inside, first motor 7 work, drive pivot 8 and rotate to make dwang 9 rotatory, make brush 10 wash along the device inner wall, coil 2101 circular telegram, open out dirty mouthful 22, dog 2103 shelters from iodine outlet 23, the discharge dirt matter, this is the work flow of the device, the content that does not make detailed description in this description belongs to the prior art that skilled person in the art knows.

Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the invention can be made, and equivalents and modifications of some features of the invention can be made without departing from the spirit and scope of the invention.