阅读说明：本技术 一种远红外、负离子整理剂的制备方法 (Preparation method of far infrared and negative ion finishing agent ) 是由 谢黎君 于 2021-08-23 设计创作，主要内容包括：本发明适用于纺织品整理剂制备技术领域,提供了一种远红外、负离子整理剂的制备方法,包括以下步骤：称取纳米远红外负离子粉进行超微粉碎处理；将超微纳米远红外负离子粉加入搅拌桶内；称取薄荷粉4-9份、金盏花粉10-15份、香樟粉25-28份、甘油5-8份和水32-42份合并；称取淀粉20-30份、苛性钠粉2.5-3.5份、硼砂粉2-2.5份和水70-80份合并；将防蛀处理液、粘合剂和增稠剂投入超微纳米远红外负离子液中,混合；超微粉碎的纳米远红外负离子粉能够提高整理后的纺织品的远红外发射率和负离子释放率,制备防蛀处理液能够有效提高整理后的纺织品的防蛀性能,有效解决了长时间使用后的远红外、负离子纺织品逐渐不具备释放远红外、负离子功效以及易出现虫蛀现象的问题。(The invention is applicable to the technical field of textile finishing agent preparation, and provides a preparation method of a far infrared and negative ion finishing agent, which comprises the following steps: weighing nano far infrared anion powder and carrying out superfine grinding treatment; adding the ultramicro nano far infrared anion powder into a stirring barrel; weighing 4-9 parts of mint powder, 10-15 parts of calendula powder, 25-28 parts of camphor powder, 5-8 parts of glycerol and 32-42 parts of water, and mixing; weighing 20-30 parts of starch, 2.5-3.5 parts of caustic soda powder, 2-2.5 parts of borax powder and 70-80 parts of water, and mixing; adding the mothproof treatment liquid, the adhesive and the thickening agent into the ultramicro nano far infrared anion liquid, and mixing; the superfine crushed nano far infrared anion powder can improve the far infrared emissivity and the anion release rate of the finished textile, the prepared mothproof treatment liquid can effectively improve the mothproof performance of the finished textile, and the problems that the far infrared and anion textile does not have the far infrared and anion release efficacy gradually and is easy to have a mothproof phenomenon after being used for a long time are effectively solved.)

1. A preparation method of a far infrared and negative ion finishing agent is characterized by comprising the following steps:

weighing nanometer far infrared anion powder, putting the nanometer far infrared anion powder into a grinding ultrafine pulverizer to perform ultrafine grinding treatment, and controlling the discharge particle size to be 300-400 meshes to obtain ultrafine nanometer far infrared anion powder;

adding the ultramicro nanometer far-infrared anion powder into a stirring barrel, adding neutral water while stirring, wherein the total amount of the added water is 1-4 times of the ultramicro nanometer far-infrared anion powder, and obtaining ultramicro nanometer far-infrared anion liquid;

weighing the following raw materials in parts by weight: 4-9 parts of mint powder, 10-15 parts of calendula powder, 25-28 parts of camphor powder, 5-8 parts of glycerol and 32-42 parts of water, mixing, and stirring and mixing at 500rpm of 300 plus materials for 25-30min to obtain a mothproof treatment solution;

weighing the following raw materials in parts by weight: 20-30 parts of starch, 2.5-3.5 parts of caustic soda powder, 2-2.5 parts of borax powder and 70-80 parts of water, mixing, and stirring and mixing at 500rpm of 300 plus materials for 45-60min to obtain an adhesive;

adding the mothproof treatment liquid, the adhesive and the thickening agent into the ultramicro nanometer far infrared anion liquid, mixing for 20-45min in a high-speed mixer, and discharging.

2. The preparation method of the far infrared and anion finishing agent according to claim 1, wherein the nano far infrared anion powder in the step 1) comprises the following raw materials in parts by weight: 20-30 parts of micro-energy radiator, 50-65 parts of nano negative ion tourmaline powder, 4-6 parts of dispersoid and 1-3 parts of protective agent.

3. The method for preparing a far infrared, negative ion finishing agent according to claim 1, wherein the total stirring time in the step 2) is 30-50 min.

4. The method for preparing a far infrared, negative ion finishing agent according to claim 1, wherein the stirring and mixing in the step 3) are performed at a temperature of 15-50 ℃.

5. The method for preparing far infrared, negative ion finishing agent according to claim 1, wherein the stirring and mixing in the step 4) are under the temperature condition of 20-40 ℃.

6. The preparation method of the far infrared and negative ion finishing agent according to claim 1, characterized in that the raw materials in the step 5) are as follows: 8-12 parts of mothproof treatment liquid, 3-5 parts of adhesive, 1-2 parts of thickening agent and 75-85 parts of ultramicro nano far infrared anion liquid.

7. The method for preparing far infrared, negative ion finishing agent according to claim 1 or 6, characterized in that the mixing in the step 5) is under the temperature condition of 20-30 ℃.

8. The method for preparing a far infrared, negative ion finishing agent according to claim 1, wherein the thickener in step 5) is a polyacrylic thickener.

Technical Field

The invention belongs to the technical field of textile finishing agent preparation, and particularly relates to a preparation method of a far infrared and negative ion finishing agent.

Background

The negative ion far infrared textile is directly worn on the body and is in large-area contact with the skin of a person, the emission of negative ions is accelerated by utilizing the heat energy of the human body and the friction between the human body movement and the skin, a negative ion air layer is formed between the skin and clothes, various damages of oxygen free radicals to the health of the human body are eliminated, and the body fluid of the human body is alkalescent, so that cells are activated, the metabolism is promoted, the effects of purifying blood, removing wastes in the body, inhibiting cardiovascular diseases and the like are achieved, and a series of medical health care effects are achieved.

The far infrared textile can absorb far infrared rays radiated from nature or human bodies to raise the temperature of the far infrared textile, and can also emit the far infrared rays, so that the far infrared textile can keep warm, raise the temperature, improve the microcirculation system of the human bodies, and has the functions of eliminating fatigue, recovering physical strength and relieving pain; the anion textile can reduce the content of 5-light tryptamine in blood, enhance the nerve inhibition process, has the functions of calming, hypnotizing and reducing blood pressure, can improve basal metabolism, promote protein metabolism and strengthen the immune system.

The textile used for a long time does not have the effects of releasing far infrared rays and negative ions gradually, so that a far infrared and negative ion finishing agent is required to be provided, the textile can be padded to have the effects of releasing the far infrared and negative ions, the blood circulation of a human body can be promoted, the sustainable development of textile resources is promoted, and the idle far infrared and negative ion textile is easy to damage due to moth-eating.

Disclosure of Invention

The embodiment of the invention aims to provide a preparation method of a far infrared and anion finishing agent, and aims to solve the problems that after long-time use, far infrared and anion textiles gradually do not have the effects of releasing far infrared and anions and are easy to damage by worms.

The embodiment of the invention is realized in such a way that the preparation method of the far infrared and negative ion finishing agent comprises the following steps:

weighing nanometer far infrared anion powder, putting the nanometer far infrared anion powder into a grinding ultrafine pulverizer to perform ultrafine grinding treatment, and controlling the discharge particle size to be 300-400 meshes to obtain ultrafine nanometer far infrared anion powder;

adding the ultramicro nanometer far-infrared anion powder into a stirring barrel, adding neutral water while stirring, wherein the total amount of the added water is 1-4 times of the ultramicro nanometer far-infrared anion powder, and obtaining ultramicro nanometer far-infrared anion liquid;

weighing the following raw materials in parts by weight: 4-9 parts of mint powder, 10-15 parts of calendula powder, 25-28 parts of camphor powder, 5-8 parts of glycerol and 32-42 parts of water, mixing, and stirring and mixing at 500rpm of 300 plus materials for 25-30min to obtain a mothproof treatment solution;

weighing the following raw materials in parts by weight: 20-30 parts of starch, 2.5-3.5 parts of caustic soda powder, 2-2.5 parts of borax powder and 70-80 parts of water, mixing, and stirring and mixing at 500rpm of 300 plus materials for 45-60min to obtain an adhesive;

adding the mothproof treatment liquid, the adhesive and the thickening agent into the ultramicro nanometer far infrared anion liquid, mixing for 20-45min in a high-speed mixer, and discharging.

Preferably, the nano far infrared anion powder in the step 1) comprises the following raw materials in parts by weight: 20-30 parts of micro-energy radiator, 50-65 parts of nano negative ion tourmaline powder, 4-6 parts of dispersoid and 1-3 parts of protective agent.

Preferably, the total stirring time in step 2) is 30-50 min.

Preferably, the stirring and mixing in the step 3) are carried out at a temperature of 15-50 ℃.

Preferably, the stirring and mixing in the step 4) are carried out at a temperature of 20-40 ℃.

Preferably, the raw materials in the step 5) are as follows by weight: 8-12 parts of mothproof treatment liquid, 3-5 parts of adhesive, 1-2 parts of thickening agent and 75-85 parts of ultramicro nano far infrared anion liquid.

Preferably, the mixing in step 5) is performed at a temperature of 20-30 ℃.

Preferably, the thickener in step 5) is a polyacrylic thickener.

According to the preparation method of the far infrared and anion finishing agent provided by the embodiment of the invention, the far infrared emissivity and the anion release rate of the finished textile can be effectively improved through the nano far infrared anion powder subjected to superfine grinding, the mothproof performance of the finished textile can be effectively improved through the prepared mothproof treatment solution, the problems that the far infrared and anion textile does not gradually release far infrared and anions and is easy to damage by worms after being used for a long time are effectively solved, the toxicity to a human body can be reduced through the herbal raw materials, and the requirements of people on the comfort and the durability of the textile are met.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.

Specific implementations of the present invention are described in detail below with reference to specific embodiments.

Example 1

The preparation method of the far infrared and negative ion finishing agent provided by one embodiment of the invention comprises the following steps:

1) weighing nano far infrared anion powder, putting the nano far infrared anion powder into a grinding ultrafine grinder to carry out ultrafine grinding treatment, and controlling the discharge granularity to be 300 meshes to obtain ultrafine nano far infrared anion powder, wherein the nano far infrared anion powder comprises the following raw materials in parts by weight: 20 parts of micro-energy radiator, 50 parts of nano negative ion tourmaline powder, 4 parts of dispersoid and 1 part of protective agent;

2) adding ultramicro nanometer far infrared anion powder into a stirring barrel, adding neutral water while stirring, wherein the total amount of the added water is 1 time of that of the ultramicro nanometer far infrared anion powder, and the total stirring time is 30min to obtain ultramicro nanometer far infrared anion liquid;

3) weighing the following raw materials in parts by weight: 4 parts of mint powder, 10 parts of calendula powder, 25 parts of camphor powder, 5 parts of glycerol and 32 parts of water, mixing, stirring and mixing at 300rpm for 25min, and stirring and mixing at the temperature of 15 ℃ to obtain a mothproof treatment solution;

4) weighing the following raw materials in parts by weight: 20 parts of starch, 2.5 parts of caustic soda powder, 2 parts of borax powder and 70 parts of water, mixing, stirring and mixing at 300rpm for 45min, and obtaining the adhesive under the temperature condition of 20 ℃;

5) adding 8 parts by weight of mothproof treatment liquid, 3 parts by weight of adhesive and 1 part by weight of thickener into 75 parts by weight of ultramicro nano far infrared anion liquid, mixing for 20min at the temperature of 20 ℃ in a high-speed mixer, and discharging to obtain the mothproof treatment liquid.

Example 2

The preparation method of the far infrared and negative ion finishing agent provided by one embodiment of the invention comprises the following steps:

1) weighing nano far infrared anion powder, putting the nano far infrared anion powder into a grinding ultrafine grinder for ultrafine grinding treatment, controlling the discharge granularity to be 400 meshes, and obtaining ultrafine nano far infrared anion powder, wherein the nano far infrared anion powder comprises the following raw materials in parts by weight: 30 parts of micro-energy radiator, 65 parts of nano negative ion tourmaline powder, 6 parts of dispersoid and 3 parts of protective agent;

2) adding ultramicro nanometer far infrared anion powder into a stirring barrel, adding neutral water while stirring, wherein the total amount of the added water is 4 times of that of the ultramicro nanometer far infrared anion powder, and the total stirring time is 50min to obtain ultramicro nanometer far infrared anion liquid;

3) weighing the following raw materials in parts by weight: 9 parts of mint powder, 15 parts of calendula powder, 28 parts of camphor powder, 8 parts of glycerol and 42 parts of water, mixing, stirring and mixing at 500rpm for 30min, and stirring and mixing at the temperature of 50 ℃ to obtain a mothproof treatment solution;

4) weighing the following raw materials in parts by weight: 30 parts of starch, 3.5 parts of caustic soda powder, 2.5 parts of borax powder and 80 parts of water, mixing, stirring and mixing at 500rpm for 60min, and obtaining the adhesive under the temperature condition of 40 ℃;

5) 12 parts of mothproof treatment liquid, 5 parts of adhesive and 2 parts of thickening agent are added into 85 parts of ultramicro nano far infrared anion liquid according to the parts by weight, mixed for 45min at the temperature of 30 ℃ in a high-speed mixer, and discharged, so that the mothproof treatment liquid is prepared, and the thickening agent is polyacrylic acid thickening agent.

Example 3

The preparation method of the far infrared and negative ion finishing agent provided by one embodiment of the invention comprises the following steps:

1) weighing nano far infrared anion powder, putting the nano far infrared anion powder into a grinding ultrafine grinder for ultrafine grinding treatment, and controlling the discharge granularity to be 350 meshes to obtain the ultrafine nano far infrared anion powder, wherein the nano far infrared anion powder comprises the following raw materials in parts by weight: 25 parts of micro-energy radiator, 57.5 parts of nano negative ion tourmaline powder, 5 parts of dispersoid and 2 parts of protective agent;

2) adding ultramicro nanometer far-infrared anion powder into a stirring barrel, adding neutral water while stirring, wherein the total amount of the added water is 2.5 times of that of the ultramicro nanometer far-infrared anion powder, and the total stirring time is 40min to obtain ultramicro nanometer far-infrared anion liquid;

3) weighing the following raw materials in parts by weight: 6.5 parts of mint powder, 12.5 parts of calendula powder, 26.5 parts of camphor powder, 6.5 parts of glycerol and 37 parts of water, mixing, stirring and mixing at 400rpm for 27.5min, and obtaining the mothproof treatment solution under the temperature condition of 32.5 ℃;

4) weighing the following raw materials in parts by weight: mixing 25 parts of starch, 3 parts of caustic soda powder, 2.2 parts of borax powder and 75 parts of water, stirring and mixing at 400rpm for 52.5min, and obtaining the adhesive under the temperature condition of 30 ℃;

5) 10 parts of mothproof treatment liquid, 4 parts of adhesive and 1.5 parts of thickening agent are added into 80 parts of ultramicro nanometer far infrared anion liquid according to the parts by weight, mixed for 32.5min at the temperature of 25 ℃ in a high-speed mixer, and discharged, thus obtaining the mothproof treatment liquid, the thickening agent is polyacrylic acid thickening agent.

Example 4

The preparation method of the far infrared and negative ion finishing agent provided by one embodiment of the invention comprises the following steps:

1) weighing nano far infrared anion powder, putting the nano far infrared anion powder into a grinding ultrafine grinder for ultrafine grinding treatment, and controlling the discharge granularity to be 325 meshes to obtain ultrafine nano far infrared anion powder, wherein the nano far infrared anion powder comprises the following raw materials in parts by weight: 22.5 parts of micro-energy radiator, 53 parts of nano negative ion tourmaline powder, 4.5 parts of dispersoid and 1.5 parts of protective agent;

2) adding ultramicro nanometer far infrared anion powder into a stirring barrel, adding neutral water while stirring, wherein the total amount of the added water is 2 times of that of the ultramicro nanometer far infrared anion powder, and the total stirring time is 35min to obtain ultramicro nanometer far infrared anion liquid;

3) weighing the following raw materials in parts by weight: 5 parts of mint powder, 11 parts of calendula powder, 26 parts of camphor powder, 6 parts of glycerol and 34 parts of water, mixing, stirring and mixing at 350rpm for 26min, and stirring and mixing at the temperature of 23 ℃ to obtain a mothproof treatment solution;

4) weighing the following raw materials in parts by weight: 22.5 parts of starch, 2.7 parts of caustic soda powder, 2.1 parts of borax powder and 72.5 parts of water, mixing, stirring and mixing at 350rpm for 48min, and obtaining the adhesive under the temperature condition of 25 ℃;

5) 9 parts of mothproof treatment liquid, 3.5 parts of adhesive and 1.5 parts of thickening agent are added into 77 parts of ultramicro nano far infrared anion liquid according to the parts by weight, mixed for 26min at the temperature of 22 ℃ in a high-speed mixer, and discharged, thus obtaining the mothproof treatment liquid, the thickening agent is polyacrylic acid thickening agent.

Example 5

The preparation method of the far infrared and negative ion finishing agent provided by one embodiment of the invention comprises the following steps:

1) weighing nano far infrared anion powder, putting the nano far infrared anion powder into a grinding ultrafine grinder for ultrafine grinding treatment, and controlling the discharge granularity to be 375 meshes to obtain ultrafine nano far infrared anion powder, wherein the nano far infrared anion powder comprises the following raw materials in parts by weight: 27 parts of micro-energy radiator, 60 parts of nano negative ion tourmaline powder, 5.5 parts of dispersoid and 2.5 parts of protective agent;

2) adding ultramicro nanometer far infrared anion powder into a stirring barrel, adding neutral water while stirring, wherein the total amount of the added water is 3.5 times of that of the ultramicro nanometer far infrared anion powder, and the total stirring time is 45min to obtain ultramicro nanometer far infrared anion liquid;

3) weighing the following raw materials in parts by weight: 7 parts of mint powder, 13 parts of calendula powder, 27 parts of camphor powder, 7 parts of glycerol and 40 parts of water, mixing, stirring and mixing at 450rpm for 29min, and stirring and mixing at 42 ℃ to obtain a mothproof treatment solution;

4) weighing the following raw materials in parts by weight: 27 parts of starch, 3.2 parts of caustic soda powder, 2.3 parts of borax powder and 77 parts of water, mixing, stirring and mixing at 450rpm for 57min, and obtaining the adhesive under the temperature condition of 35 ℃;

5) adding 11 parts by weight of mothproof treatment liquid, 4.5 parts by weight of adhesive and 1.5 parts by weight of thickening agent into 83 parts by weight of ultramicro nano far infrared anion liquid, mixing for 40min at the temperature of 27 ℃ in a high-speed mixer, and discharging to obtain the mothproof treatment liquid, wherein the thickening agent is a polyacrylic acid thickening agent.

According to the preparation method of the far infrared and anion finishing agent provided by the embodiment of the invention, the far infrared emissivity and the anion release rate of the finished textile can be effectively improved through the nano far infrared anion powder subjected to superfine grinding, the mothproof performance of the finished textile can be effectively improved through the prepared mothproof treatment solution, the problems that the far infrared and anion textile does not gradually release far infrared and anions and is easy to damage by worms after being used for a long time are effectively solved, the toxicity to a human body can be reduced through the herbal raw materials, and the requirements of people on the comfort and the durability of the textile are met.

It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.

Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.