阅读说明：本技术 一种医药中间体的过滤材料的制备装置及方法 (A kind of preparation facilities and method of the filtering material of medicine intermediate ) 是由 张会敏 于 2018-05-23 设计创作，主要内容包括：本发明公开了一种医药中间体的过滤材料的制备方法及装置,包括底座,所述底座的顶部从左至右依次固定连接有高温炉、冷却箱和支撑腿,所述高温炉的正面固定连接有显示屏,所述高温炉左侧的顶部连通有加料口,所述高温炉的右侧通过铰链铰接有操作门,所述操作门的右侧焊接有拉手,所述冷却箱的正面通过第二铰链铰接有冷却门,所述冷却门正面的左侧焊接有把手,所述底座顶部的右侧设置有焖烧炉,所述焖烧炉底部的两侧分别与两个支撑腿焊接,所述焖烧炉左侧的顶部连通有入口,所述焖烧炉右侧的底部连通有出口,所述冷却箱内腔的顶部设置有电机,所述电机的输出端套接有扇叶。本发明解决了现有的一体式制造机械效率低的问题。(The invention discloses a kind of preparation method of the filtering material of medicine intermediate and devices, including pedestal, the top of the pedestal is fixedly connected sequentially has high temperature furnace from left to right, cooler bin and supporting leg, the front of the high temperature furnace is fixedly connected with display screen, top on the left of the high temperature furnace is communicated with feed opening, the right side of the high temperature furnace is hinged with operation door by hinge, knob is welded on the right side of the operation door, the front of the cooler bin is hinged with cooling door by second hinge, the positive left side of the cooling door is welded with handle, smoldering furnace is provided on the right side of the base top, it is welded respectively with two supporting legs the two sides of the smoldering furnace bottom, top on the left of the smoldering furnace is communicated with entrance, bottom on the right side of the smoldering furnace is communicated with outlet, motor is provided at the top of the cooling box cavity, the motor Output end is socketed with flabellum.The present invention solves the problems, such as that existing integral type manufactures mechanical low efficiency.)

1. a kind of preparation facilities of the filtering material of medicine intermediate, including pedestal (1), it is characterised in that: the pedestal (1) Top is fixedly connected sequentially from left to right high temperature furnace (2), cooler bin (7) and supporting leg (13), the front of the high temperature furnace (2) It is fixedly connected with display screen (6), the top on the left of the high temperature furnace (2) is communicated with feed opening (3), the right side of the high temperature furnace (2) Side is hinged with operation door (4) by hinge, is welded with knob (5) on the right side of the operation door (4), the cooler bin (7) is just Face is hinged with cooling door (8) by second hinge, and described cooling door (8) positive left side is welded with handle (9), the pedestal (1) right side at the top of is provided with smoldering furnace (10), and the two sides of smoldering furnace (10) bottom are welded with two supporting legs (13) respectively It connects, the top on the left of the smoldering furnace (10) is communicated with entrance (11), and the bottom on the right side of the smoldering furnace (10) is communicated with outlet (12), it is provided with motor (14) at the top of cooler bin (7) inner cavity, the output end of the motor (14) is socketed with flabellum (15).

2. a kind of preparation facilities of the filtering material of medicine intermediate according to claim 1, it is characterised in that: the drawing The surface of hand (5) is socketed with Anti-slip cover, and the surface of Anti-slip cover offers anti-skid chequer.

3. a kind of preparation facilities of the filtering material of medicine intermediate according to claim 1, it is characterised in that: the electricity Locating piece is fixedly connected at the top of machine (14) two sides, the bottom of locating piece is provided with bolt, and the end of thread of bolt is through to The top of locating piece is connect with the inner thread of cooler bin (7).

4. a kind of preparation method of the filtering material of medicine intermediate, characterized by the following steps:

(1) it carbonizes: timber, sawdust lamp raw material being added in high temperature furnace first, it then will according to the prompt of temperature on display screen Temperature in high temperature furnace controls between 400-600 degree, so that raw material is adequately burnt, after raw material carbonizes completely, passes through The raw material after charing is taken out in the cooperation of knob and operation door；

(2) cooling: cooling door being opened by the cooperation of handle and second hinge, the raw material after charing is then placed on cooler bin It is interior, then start motor, so that motor is driven flabellum rotation, to increase the flowing velocity of the air of cooler bin, thus to activity Charcoal is cooled down；

(3) it activates: first by the raw material after charing and after zinc chloride mixed according to the ratio of 2:1, being put by entrance stewing It burns in furnace, then the raw material after charing is dried by smoldering furnace and controls the temperature in smoldering furnace in 600-750 degree Between；

(4) impurity elimination: manganese trioxide is added in smoldering furnace, impurity elimination is carried out to raw material, to obtain active carbon.

5. a kind of method according to claim 4, it is characterised in that: the diameter of the timber is not more than 10cm, and each Timber it is uniform in size.

6. a kind of method according to claim 4, it is characterised in that: the high-efficient temperature range of the carbonization of wood is Between 450-500 degree.

Technical field

The present invention relates to technical field of mechanical processing more particularly to a kind of preparation methods of the filtering material of medicine intermediate And device.

Background technique

So-called medicine intermediate, more actually for some industrial chemicals or chemical industry in drug synthesis process Product, this chemical products do not need the production licence of drug, can produce in common chemical plant, as long as reaching Rank, can be used to the synthesis of drug.

Medicine intermediate needs to use filtering material, such as active carbon in the fabrication process, and active carbon is in manufacturing process In need integral type manufacture mechanical, but existing integral type manufactures mechanical low efficiency, when being cooled down to the timber after charing, It is all to waste a large amount of time in cooling procedure, to have slowed down the progress of active carbon manufacture by natural cooling, improved The cost of active carbon manufacture, thus it is inconvenient to use, reduce the mechanical practicability of integral type manufacture.

Summary of the invention

Technical problems based on background technology, the invention proposes a kind of preparations of the filtering material of medicine intermediate Method and device has the characteristics that manufacture efficiency is high, solves the problems, such as that existing integral type manufactures mechanical low efficiency.

The invention provides the following technical scheme:

A kind of preparation facilities of the filtering material of medicine intermediate, including pedestal, the top of the pedestal are successively solid from left to right Surely it is connected with high temperature furnace, cooler bin and supporting leg, the front of the high temperature furnace is fixedly connected with display screen, the high temperature furnace left side Top be communicated with feed opening, the right side of the high temperature furnace is hinged with operation door, the right side welding of the operation door by hinge There is knob, the front of the cooler bin is hinged with cooling door by second hinge, and the positive left side of the cooling door is welded with handle Hand is provided with smoldering furnace on the right side of the base top, and the two sides of the smoldering furnace bottom are welded with two supporting legs respectively, institute It states the top on the left of smoldering furnace and is communicated with entrance, the bottom on the right side of the smoldering furnace is communicated with outlet, the cooling box cavity Top is provided with motor, and the output end of the motor is socketed with flabellum.

Preferably, the surface of the knob is socketed with Anti-slip cover, and the surface of Anti-slip cover offers anti-skid chequer.

Preferably, it is fixedly connected to locating piece at the top of the motor two sides, the bottom of locating piece is provided with bolt, spiral shell The end of thread of bolt is through to the top of locating piece and the inner thread of cooler bin connects.

A kind of preparation method of the filtering material of medicine intermediate, includes the following steps:

(1) it carbonizes: timber, sawdust lamp raw material being added in high temperature furnace first, it then will according to the prompt of temperature on display screen Temperature in high temperature furnace controls between 400-600 degree, so that raw material is adequately burnt, after raw material carbonizes completely, passes through The raw material after charing is taken out in the cooperation of knob and operation door；

(2) cooling: cooling door being opened by the cooperation of handle and second hinge, the raw material after charing is then placed on cooler bin It is interior, then start motor, so that motor is driven flabellum rotation, to increase the flowing velocity of the air of cooler bin, thus to activity Charcoal is cooled down；

(3) it activates: first by the raw material after charing and after zinc chloride mixed according to the ratio of 2:1, being put by entrance stewing It burns in furnace, then the raw material after charing is dried by smoldering furnace and controls the temperature in smoldering furnace in 600-750 degree Between；

(4) impurity elimination: manganese trioxide is added in smoldering furnace, impurity elimination is carried out to raw material, to obtain active carbon.

Preferably, the diameter of the timber is not more than 10cm, and each timber is uniform in size.

Preferably, the high-efficient temperature range of the carbonization of wood is between 450-500 degree.

The present invention provides a kind of preparation method of the filtering material of medicine intermediate and devices, pass through setting for display screen It sets, the temperature in high temperature furnace can be shown, the temperature of charing is controlled to facilitate, so that operation is facilitated, By the setting of cooler bin, the raw material after charing can be placed, the raw material after avoiding charing needs to waste the plenty of time The situation of collection increases the speed air flow in cooler bin by the setting of motor and flabellum, thus after accelerating charing The cooling speed of raw material, to improve the mechanical production efficiency of integral type manufacture.

Detailed description of the invention

Fig. 1 is schematic structural view of the invention；

Fig. 2 is structure of the invention cooler bin cross-sectional view.

In figure: 1 pedestal, 2 high temperature furnaces, 3 feed openings, 4 operation doors, 5 knobs, 6 display screens, 7 cooler bins, 8 cooling doors, 9 Hand, 10 smoldering furnaces, 11 entrances, 12 outlets, 13 supporting legs, 14 motors, 15 flabellums.

Specific embodiment

Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.

The present invention provides a kind of technical solution referring to FIG. 1-2:

A kind of preparation facilities of the filtering material of medicine intermediate, including pedestal 1, the top of pedestal 1 are successively fixed from left to right It is connected with high temperature furnace 2, cooler bin 7 and supporting leg 13, the front of high temperature furnace 2 is fixedly connected with display screen 6,2 left side of high temperature furnace Top is communicated with feed opening 3, and the right side of high temperature furnace 2 is hinged with operation door 4 by hinge, and the right side of operation door 4 is welded with knob 5,5 surface of shaking hands is socketed with Anti-slip cover, and the surface of Anti-slip cover offers anti-skid chequer, and the front of cooler bin 7 passes through the second hinge Chain is hinged with cooling door 8, and the cooling positive left side of door 8 is welded with handle 9, and the right side at 1 top of pedestal is provided with smoldering furnace 10, boils in a covered pot over a slow fire The two sides for burning 10 bottom of furnace are welded with two supporting legs 13 respectively, and the top in 10 left side of smoldering furnace is communicated with entrance 11, smoldering furnace The bottom on 10 right sides is communicated with outlet 12, and motor 14 is provided at the top of 7 inner cavity of cooler bin, and the top of 14 two sides of motor is fixed It is connected with locating piece, the bottom of locating piece is provided with bolt, and the end of thread of bolt is through to top and the cooler bin 7 of locating piece Inner thread connection, the output end of motor 14 are socketed with flabellum 15.

A kind of preparation method of the filtering material of medicine intermediate, includes the following steps:

(1) it carbonizes: timber, sawdust lamp raw material being added in high temperature furnace first, it then will according to the prompt of temperature on display screen Temperature in high temperature furnace controls between 400-600 degree, so that raw material is adequately burnt, after raw material carbonizes completely, passes through The raw material after charing is taken out in the cooperation of knob and operation door；

(2) cooling: cooling door being opened by the cooperation of handle and second hinge, the raw material after charing is then placed on cooler bin It is interior, then start motor, so that motor is driven flabellum rotation, to increase the flowing velocity of the air of cooler bin, thus to activity Charcoal is cooled down；

(3) it activates: first by the raw material after charing and after zinc chloride mixed according to the ratio of 2:1, being put by entrance stewing It burns in furnace, then the raw material after charing is dried by smoldering furnace and controls the temperature in smoldering furnace in 600-750 degree Between；

(4) impurity elimination: manganese trioxide is added in smoldering furnace, impurity elimination is carried out to raw material, to obtain active carbon.