阅读说明：本技术 一种复配型修护冻干粉制剂制备方法及制备装置 (A kind of Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities ) 是由 谭晓阳 于 2019-09-24 设计创作，主要内容包括：本发明公开了一种复配型修护冻干粉制剂制备方法及制备装置,主要包括外框、密封盖、内框、制冷座和吸湿器,所述外框内侧右部固定安装有控制模块,所述外框前侧壁开设有与控制模块配合的装配口,所述外框内侧上部固定安装有内框,所述外框前侧上部外壁通过转销装配安装有与内框配合的密封盖,密封盖内部嵌设安装有透视窗。本发明设备在结构上设计合理,导热面积大,换热速度快,升华产生水蒸气的流通速度快,干燥效果好,纤连蛋白和蓝铜肽(三肽-1铜)复配加强受损细胞传输细胞代谢、生长、增殖所需的营养物质；能够调动吞噬系统---清除坏死的组织、细胞和外来异物,起到抑菌消炎的作用；深入表皮、真皮及皮下组织的受损及衰老细胞等。(The invention discloses a kind of Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities, it mainly include outline border, sealing cover, inside casing, refrigeration seat and dehydrating breather, right part is fixedly installed with control module on the inside of the outline border, the outline border front side wall offers the installation opening with control module cooperation, the outline border inside upper part is fixedly installed with inside casing, the outline border forward upper outer wall passes through assembly of shipping and reselling on another market and is equipped with the sealing cover cooperated with inside casing, is embedded inside sealing cover and is equipped with window.Present device designs rationally in structure, heat-conducting area is big, and heat transfer rate is fast, and the velocity of liquid assets that distillation generates vapor is fast, drying effect is good, and fibronectin and blue copper peptide (- 1 copper of tripeptides) compound nutriment needed for reinforcing the metabolism of damaged cell transfusion cell, growth, proliferation；Phagocytosis system can be transferred --- tissue, cell and the alien material for removing necrosis play the role of inhibiting bacteria and diminishing inflammation；That gos deep into epidermis, corium and subcutaneous tissue is undermined senile cell etc..)

1. a kind of preparation facilities of Compositional type maintenance freeze-dried powder preparation, mainly include outline border (1), sealing cover (2), inside casing (14), Freeze seat and dehydrating breather, which is characterized in that right part is fixedly installed with control module (5), the outline border on the inside of the outline border (1) (1) front side wall offers the installation opening with control module (5) cooperation, and outline border (1) inside upper part is fixedly installed with inside casing (14), outline border (1) the forward upper outer wall is equipped with the sealing cover (2) with inside casing (14) cooperation, sealing by assembly of shipping and reselling on another market It is embedded and is equipped with window (3) inside lid (2), sealing cover (2) lower front side is fixedly installed with sliding pin (6), in sliding pin (6) Portion is slidably fitted with card holder (4), and outline border (1) front side is fixedly installed with symmetrically arranged positioned at sealing cover (2) external wall beneath Deck (7)；Outer wall is embedded the assembly head (17) for being equipped with equidistant arrangement in the middle part of the inside casing (14), and assembly head (17) is located inside casing (14) external one end is fixedly installed with air-exhausting duct (13), and air-exhausting duct (13) rear end is fixedly installed with solenoid valve (16), institute It states inside casing (14) top inner wall and is fixedly installed with humidity sensor (36)；Inside casing (14) lower inside is fixedly installed with refrigeration Seat, refrigeration seat top are slidably fitted with sliding sash (19), and middle part is fixedly installed with knob (18), the sliding sash on front side of sliding sash (19) (19) it is fixedly installed at forward edge symmetrically arranged insert rack (12), offers on front side of the refrigeration seat and cooperate with insert rack (12) Slot；Through being equipped with heat exchanger tube (21), outline border (1) interior front is fixedly installed with anti-the refrigeration seat lower inside Protective case (22), protecting crust (22) inside are fixedly installed with radiator (35), and protecting crust (22) top right part is fixedly installed with Compressor (33), radiator (35) entrance and heat exchanger tube (21) fixed conducting, radiator (35) outlet and compressor (33) fixed conducting, compressor (33) top are fixedly installed with second solenoid valve (40), heat exchanger tube (21) bottom end with The fixed conducting of second solenoid valve (40), heat exchanger tube (21) left part, which runs through, to be equipped with expansion valve (41), the protecting crust (22) Right end, which is embedded, to be equipped with blower (9), and blower (9) right end, which is arranged, to be equipped with air inlet pipe (8), and protecting crust (22) left end is through peace Equipped with discharge pipe (34)；Outline border (1) inside back is fixedly installed with delivery pump (23), the fixed peace of the entrance of delivery pump (23) Equipped with reversal valve (29), the outlet of the delivery pump (23) is fixedly installed with bypass pipe (30)；Outline border (1) middle inside is solid Dingan County is equipped with symmetrically arranged dehydrating breather, and solenoid valve (16) rear end is fixedly installed with delivery pipe (37), delivery pipe (37) bottom End is through dehydrating breather is fixedly connected with, and through being equipped with drainpipe (27), drainpipe (27) left end is fixedly installed with for dehydrating breather bottom end Valve (39).

2. a kind of preparation facilities of Compositional type maintenance freeze-dried powder preparation according to claim 1, which is characterized in that the system Cold seat mainly includes cold of electricity (11), heating plate (15), temperature sensor (20), slide (24) and thermally conductive shell (26), the cunning Seat (24) middle inside is fixedly installed with thermally conductive shell (26), and thermally conductive shell (26) bottom end, which is embedded, is equipped with electric cold (11), described to lead Hot shell (26) bottom end left part is fixedly installed with heating plate (15), and thermally conductive shell (26) the bottom end right part is fixedly installed with temperature sensing Device (20), cold (11) bottom end of the electricity are fixedly installed with heat exchange seat (28), and heat exchange seat (28) lower part, which is run through, is equipped with heat exchanger tube (21)。

3. a kind of preparation facilities of Compositional type maintenance freeze-dried powder preparation according to claim 1, which is characterized in that the suction Wet device mainly includes shell (10), guide card (31), interior cold frame (32), attachment flaps (38) and attachment shell (42), the shell (10) Inside left part is fixedly installed with attachment shell (42), and attachment shell (42) outer wall is fixedly installed with attachment flaps (38), the attachment shell (42) inside is fixedly installed with interior cold frame (32), and interior cold frame (32) is connected by the way that pipeline and second solenoid valve (40) are fixed, described Shell (10) inside upper part is fixedly installed with the guide card (31) of equidistant arrangement, and the attachment shell (42) is close to shell (10) side wall one End offers water hole, and attachment shell (42) side wall is fixedly installed with second temperature sensor (43).

4. a kind of preparation facilities of Compositional type maintenance freeze-dried powder preparation according to claim 1, which is characterized in that the cunning Frame (19) bottom end is fixedly installed with the fin (25) of equidistant arrangement, and thermally conductive shell (26) top is offered to be cooperated with fin (25) Sliding slot mouth.

5. a kind of preparation facilities of Compositional type maintenance freeze-dried powder preparation according to claim 1, which is characterized in that described It is embedded on front side of form (3) and protective fence is installed.

A kind of preparation of Compositional type maintenance freeze-dried powder preparation, which comprises the following steps:

(1) after disinfecting utensils are good, mannitol 4-6%, trehalose 0.2-0.6%, tremella (TREMELLA are accurately weighed FUCIFORMIS) fruiting body extract 0.03%-0.05%, deionized water 70-80% are put into high-pressure sterilizing pot in container 120 DEG C keep the temperature 40 minutes, are subsequently cooled to 33 DEG C (base-materials)；

(2) blue copper victory peptide (- 1 copper of tripeptides) 0.1%-0.2%, fibronectin 6%-10%, palmityl tetrapeptide -75%- are weighed 7%, hydrolytic collagen 0.1%-0.2% is added in the base-material to have sterilized, is filled in bottle immediately after stirring evenly；

(3) Material filled is put into sliding sash (19), is closed sealing cover (2)；

(4) seat that freezes in equipment is cooled to -40 DEG C -- and 45 DEG C；

(5) dehydrating breather is frozen to -45 DEG C, is evacuated to -23Pa ± 3Pa, maintained at this range 3 hours；

(6) refrigeration seat is warming up to -15 DEG C, and dehydrating breather freezes to -35 DEG C, keeps the temperature 3 hours；

(7) refrigeration seat is warming up to 5 DEG C again, and dehydrating breather freezes to -25 DEG C, keeps the temperature 3 hours；

(8) refrigeration seat is warming up to 0 DEG C again, and dehydrating breather freezes to -15 DEG C, keeps the temperature 3 hours；

(9) refrigeration seat is warming up to 30 DEG C again, and dehydrating breather freezes to -0 DEG C, keeps the temperature 2.5 hours, turns off and vacuumize, and keeps the temperature 0.5 hour；

(10) it takes out and is packed, form product after mounted box packaging, save under room temperature.

Technical field

The present invention relates to beauty product field, specifically a kind of Compositional type maintenance freeze-dried powder preparation preparation method and preparation dress It sets.

Background technique

Currently, various cosmetics are mainly based on chemical component, then be added to some plant extract elites elements or other The beauty product that deep-sea nutriment is prepared into, to skin play moisturizing, whitening and oil-control the effects of.Although these cosmetics contain Have some nutriments, but the problems such as because of its active constituent content and validity, in terms of also far from Foot.

Existing Preparation equipment structure is simple and crude, has a single function, and the using effect of finished product is poor after processing, the structure inside equipment It is arranged unreasonable, drying effect is poor, and dehumidifying effect is insufficient；Drying structure inside equipment, uneven with heat, heating speed is slow； It is inconvenient that product picks and places, and inner sealing is inconvenient；Chilling rate is slow, and temperature control is unstable, inefficiency.

Summary of the invention

The purpose of the present invention is to provide a kind of Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities, to solve The problems mentioned above in the background art.

To achieve the above object, the invention provides the following technical scheme:

A kind of preparation facilities of Compositional type maintenance freeze-dried powder preparation, mainly include outline border, sealing cover, inside casing, refrigeration seat and Dehydrating breather, outline border inside right part are fixedly installed with control module, and the outline border front side wall offers and control module cooperates Installation opening, the outline border inside upper part is fixedly installed with inside casing, and the outline border forward upper outer wall passes through assembly installation of shipping and reselling on another market There is the sealing cover with inside casing cooperation, is embedded inside sealing cover and window is installed, the sealing cover lower front side is fixedly installed with Sliding pin, sliding pin middle part are slidably fitted with card holder, are fixedly installed on front side of the outline border positioned at sealing cover external wall beneath arranged symmetrically Deck；Outer wall is embedded the assembly head for being equipped with equidistant arrangement in the middle part of the inside casing, and it is solid that assembly head is located at one end outside inside casing Dingan County is equipped with air-exhausting duct, and the air-exhausting duct rear end is fixedly installed with solenoid valve, and inside casing top inner wall is fixedly installed with humidity Sensor；The inside casing lower inside is fixedly installed with refrigeration seat, and refrigeration seat top is slidably fitted with sliding sash, middle part on front side of sliding sash It is fixedly installed with knob, symmetrically arranged insert rack is fixedly installed at the sliding sash forward edge, is opened up on front side of the refrigeration seat There is the slot with insert rack cooperation；Through heat exchanger tube is equipped with, the outline border interior front is fixed to pacify the refrigeration seat lower inside Equipped with protecting crust, it is fixedly installed with radiator on the inside of protecting crust, protecting crust top right part is fixedly installed with compressor, described Radiator inlet and the fixed conducting of heat exchanger tube, the radiator outlet and compressor are fixed and are connected, and the compressor tip is fixed Second solenoid valve, the heat exchanger tube bottom end and the fixed conducting of second solenoid valve are installed, the heat exchanger tube left part, which runs through, to be equipped with Expansion valve, the protecting crust right end, which is embedded, is equipped with blower, and blower right end, which is arranged, is equipped with air inlet pipe, and the protecting crust left end is passed through It wears and discharge pipe is installed；The outline border inside back is fixedly installed with delivery pump, and the entrance of delivery pump is fixedly installed with reversal valve, The outlet of the delivery pump is fixedly installed with bypass pipe；The outline border middle inside is fixedly installed with symmetrically arranged dehydrating breather, The solenoid valve rear end is fixedly installed with delivery pipe, and delivery pipe bottom end is through dehydrating breather is fixedly connected with, and dehydrating breather bottom end is through peace Equipped with drainpipe, drainpipe left end is fixedly installed with valve.

As a further solution of the present invention: the refrigeration seat mainly includes electric cold, heating plate, temperature sensor, cunning Seat and thermally conductive shell, the slide middle inside are fixedly installed with thermally conductive shell, and thermally conductive shell bottom end, which is embedded, is equipped with cold of electricity, described to lead Hot shell bottom end left part is fixedly installed with heating plate, and the thermally conductive shell bottom end right part is fixedly installed with temperature sensor, and the electricity is cold Piece bottom end is fixedly installed with heat exchange seat, and heat exchange seat lower part, which is run through, is equipped with heat exchanger tube.

As the present invention further scheme: the dehydrating breather mainly include shell, guide card, interior cold frame, attachment flaps and Adhere to shell, left part is fixedly installed with attachment shell on the inside of the shell, and attachment shell outer wall is fixedly installed with attachment flaps, the attachment shell Inside is fixedly installed with interior cold frame, and interior cold frame is connected by the way that pipeline and second solenoid valve are fixed, and the shell inside upper part is fixed The guide card of equidistant arrangement is installed, the attachment shell offers water hole close to side wall of outer shell one end, and the attachment shell side wall is solid Dingan County is equipped with second temperature sensor.

As further scheme of the invention: the sliding sash bottom end is fixedly installed with the fin of equidistant arrangement, described to lead Hot shell top offers the sliding slot mouth with fin cooperation.

As further scheme of the invention: being embedded on front side of the window and is equipped with protective fence.

As further scheme of the invention: the control module electrically connect by harness and power inside device It connects.

A kind of preparation method of Compositional type maintenance freeze-dried powder preparation, comprising the following steps:

(1) after disinfecting utensils are good, mannitol 4-6%, trehalose 0.2-0.6%, tremella (TREMELLA are accurately weighed FUCIFORMIS) fruiting body extract 0.03%-0.05%, deionized water 70-80% are put into high-pressure sterilizing pot in container 120 DEG C keep the temperature 40 minutes, are subsequently cooled to 33 DEG C (base-materials)；

(2) blue copper victory peptide (- 1 copper of tripeptides) 0.1%-0.2%, fibronectin 6%-10%, palmityl tetrapeptide-are weighed 75%-7%, hydrolytic collagen 0.1%-0.2%, are added in the base-material to have sterilized, are filled in bottle immediately after stirring evenly；

(3) Material filled is put into sliding sash, closes sealing cover；

(4) seat that freezes in equipment is cooled to -40 DEG C -- and 45 DEG C；

(5) dehydrating breather is frozen to -45 DEG C, -23Pa ± 3Pa is evacuated to inside equipment, maintained at this range 3 hours；

(6) refrigeration seat is warming up to -15 DEG C, and dehydrating breather freezes to -35 DEG C, keeps the temperature 3 hours, distils；

(7) refrigeration seat is warming up to 5 DEG C again, and dehydrating breather freezes to -25 DEG C, keeps the temperature 3 hours, distils；

(8) refrigeration seat is warming up to 0 DEG C again, and dehydrating breather freezes to -15 DEG C, keeps the temperature 3 hours, distils；

(9) refrigeration seat is warming up to 30 DEG C again, and dehydrating breather freezes to -0 DEG C, keeps the temperature 2.5 hours, turns off and vacuumize, and heat preservation 0.5 is small When；

Taking-up is packed, and is formed product after mounted box packaging, is saved under room temperature.

Compared with prior art, the beneficial effects of the present invention are:

Present device designs rationally in structure, and heat-conducting area is big, and heat transfer rate is fast, and distillation generates the circulation of vapor Speed is fast, and drying effect is good, and fibronectin and blue copper peptide (- 1 copper of tripeptides) compound reinforcement damaged cell transfusion cell and be metabolized, be raw Nutriment needed for long, proliferation；Phagocytosis system can be transferred --- tissue, cell and the alien material for removing necrosis play suppression The effect of bacterium anti-inflammatory；That gos deep into epidermis, corium and subcutaneous tissue is undermined senile cell etc..

Detailed description of the invention

Fig. 1 is the structural schematic diagram of Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities.

Fig. 2 is the structural schematic diagram inside Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities.

Fig. 3 is in Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities between air-exhausting duct, solenoid valve and inside casing The structural schematic diagram of LOOK RIGHT degree.

Fig. 4 is outline border in Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities, inside casing, refrigeration seat, delivery pump With the structural schematic diagram of dehydrating breather.

Fig. 5 is heat exchanger tube, radiator, expansion valve and pressure in Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities Structural schematic diagram between contracting machine.

Fig. 6 is the structural representation of heat exchanger tube depression angle in Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities Figure.

Fig. 7 is the position view of interior of shell in Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities.

Fig. 8 is the assembling schematic diagram in Fig. 1 at A.

In figure: outline border 1, sealing cover 2, window 3, card holder 4, control module 5, sliding pin 6, deck 7, air inlet pipe 8, blower 9, Shell 10, electricity cold 11, insert rack 12, air-exhausting duct 13, inside casing 14, heating plate 15, solenoid valve 16, assembly head 17, knob 18, sliding sash 19, temperature sensor 20, heat exchanger tube 21, protecting crust 22, delivery pump 23, slide 24, fin 25, thermally conductive shell 26, drainpipe 27, change Hot seat 28, reversal valve 29, bypass pipe 30, guide card 31, interior cold frame 32, compressor 33, discharge pipe 34, radiator 35, humidity sensor Device 36, delivery pipe 37, attachment flaps 38, valve 39, second solenoid valve 40, expansion valve 41, attachment shell 42, second temperature sensor 43。

Specific embodiment

Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.

In the description of the present invention, it is to be understood that, term " center ", "upper", "lower", "front", "rear", " left side ", The orientation or positional relationship of the instructions such as " right side ", "vertical", "horizontal", "top", "bottom" "inner", "outside" is side based on the figure Position or positional relationship, are merely for convenience of description of the present invention and simplification of the description, rather than the device or member of indication or suggestion meaning Part must have a particular orientation, be constructed and operated in a specific orientation, therefore be not considered as limiting the invention.

In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " installation ", " phase Even ", " setting " shall be understood in a broad sense, for example, it may be being fixedly linked, being arranged, may be a detachable connection, is arranged or one It connects to body, be arranged.For the ordinary skill in the art, above-mentioned term can be understood in the present invention with concrete condition Concrete meaning.

Please refer to Fig. 1~8, in the embodiment of the present invention, a kind of preparation facilities of Compositional type maintenance freeze-dried powder preparation is main to wrap It includes outline border 1, sealing cover 2, inside casing 14, refrigeration seat and dehydrating breather, the 1 inside right part of outline border and is fixedly installed with control module 5, institute It states 1 front side wall of outline border and offers the installation opening cooperated with control module 5,1 inside upper part of outline border is fixedly installed with inside casing 14, The 1 forward upper outer wall of outline border passes through assembly of shipping and reselling on another market and is equipped with the sealing cover 2 cooperated with inside casing 14, is embedded inside sealing cover 2 Window 3 is installed, 2 lower front side of sealing cover is fixedly installed with sliding pin 6, card holder 4, institute are slidably fitted in the middle part of sliding pin 6 It states and is fixedly installed with symmetrically arranged deck 7 positioned at 2 external wall beneath of sealing cover on front side of outline border 1；The 14 middle part outer wall of inside casing is embedding If being equipped with the assembly head 17 of equidistant arrangement, one end that assembly head 17 is located at outside inside casing 14 is fixedly installed with air-exhausting duct 13, institute It states 13 rear end of air-exhausting duct and is fixedly installed with solenoid valve 16, the 14 top inner wall of inside casing is fixedly installed with humidity sensor 36；Institute It states 14 lower inside of inside casing and is fixedly installed with refrigeration seat, refrigeration seat top is slidably fitted with sliding sash 19, and 19 front side middle part of sliding sash is solid Dingan County is equipped with knob 18, and symmetrically arranged insert rack 12, the refrigeration seat front side are fixedly installed at 19 forward edge of sliding sash Offer the slot cooperated with insert rack 12；The refrigeration seat lower inside, which runs through, is equipped with heat exchanger tube 21, before 1 inside of outline border Portion is fixedly installed with protecting crust 22, and radiator 35 is fixedly installed on the inside of protecting crust 22, and the 22 top right part of protecting crust is fixed Compressor 33,35 entrance of radiator and the fixed conducting of heat exchanger tube 21, the outlet of radiator 35 and compressor 33 are installed Fixed conducting, 33 top of compressor is fixedly installed with second solenoid valve 40,21 bottom end of heat exchanger tube and second solenoid valve 40 fixed conductings, for 21 left part of heat exchanger tube through expansion valve 41 is equipped with, 22 right end of protecting crust, which is embedded, is equipped with blower 9,9 right end of blower, which is arranged, is equipped with air inlet pipe 8, and 22 left end of protecting crust, which is run through, is equipped with discharge pipe 34；1 inside of outline border Rear portion is fixedly installed with delivery pump 23, and the entrance of delivery pump 23 is fixedly installed with reversal valve 29, and the outlet of the delivery pump 23 is solid Dingan County is equipped with bypass pipe 30；1 middle inside of outline border is fixedly installed with symmetrically arranged dehydrating breather, 16 rear end of solenoid valve It is fixedly installed with delivery pipe 37, for 37 bottom end of delivery pipe through dehydrating breather is fixedly connected with, dehydrating breather bottom end, which is run through, is equipped with drainpipe 27,27 left end of drainpipe is fixedly installed with valve 39.

The refrigeration seat mainly includes electricity cold 11, heating plate 15, temperature sensor 20, slide 24 and thermally conductive shell 26, institute It states 24 middle inside of slide and is fixedly installed with thermally conductive shell 26, thermally conductive 26 bottom end of shell, which is embedded, is equipped with electricity cold 11, the thermally conductive shell 26 bottom end left parts are fixedly installed with heating plate 15, and the thermally conductive 26 bottom end right part of shell is fixedly installed with temperature sensor 20, described Electric cold 11 bottom ends are fixedly installed with heat exchange seat 28, and heat exchange 28 lower part of seat, which is run through, is equipped with heat exchanger tube 21.

The dehydrating breather mainly includes shell 10, guide card 31, interior cold frame 32, attachment flaps 38 and attachment shell 42, the shell 10 inside left parts are fixedly installed with attachment shell 42, and attachment 42 outer wall of shell is fixedly installed with attachment flaps 38,42 inside of attachment shell It is fixedly installed with interior cold frame 32, interior cold frame 32 is connected by the way that pipeline and second solenoid valve 40 are fixed, 10 inside upper part of shell It is fixedly installed with the guide card 31 of equidistant arrangement, the attachment shell 42 offers water hole close to 10 side wall one end of shell, described attached 42 side wall of shell be fixedly installed with second temperature sensor 43.

19 bottom end of sliding sash is fixedly installed with the fin 25 of equidistant arrangement, and thermally conductive 26 top of shell offers and fin The sliding slot mouth of 25 cooperations.

It is embedded on front side of the window 3 and protective fence is installed.

The control module 5 is electrically connected by harness and power inside device.

A kind of preparation method of Compositional type maintenance freeze-dried powder preparation, comprising the following steps:

(1) after disinfecting utensils are good, mannitol 4-6%, trehalose 0.2-0.6%, tremella (TREMELLA are accurately weighed FUCIFORMIS) fruiting body extract 0.03%-0.05%, deionized water 70-80% are put into high-pressure sterilizing pot in container 120 DEG C keep the temperature 40 minutes, are subsequently cooled to 33 DEG C (base-materials)；

(2) blue copper victory peptide (- 1 copper of tripeptides) 0.1%-0.2%, fibronectin 6%-10%, palmityl tetrapeptide-are weighed 75%-7%, hydrolytic collagen 0.1%-0.2%, are added in the base-material to have sterilized, are filled in bottle immediately after stirring evenly；

(3) Material filled is put into sliding sash 19, closes sealing cover 2；

(4) seat that freezes in equipment is cooled to -40 DEG C -- and 45 DEG C；

(5) dehydrating breather is frozen to -45 DEG C, is evacuated to -23Pa ± 3Pa, maintained at this range 3 hours；

(6) refrigeration seat is warming up to -15 DEG C, and dehydrating breather freezes to -35 DEG C, keeps the temperature 3 hours；

(7) refrigeration seat is warming up to 5 DEG C again, and dehydrating breather freezes to -25 DEG C, keeps the temperature 3 hours；

(8) refrigeration seat is warming up to 0 DEG C again, and dehydrating breather freezes to -15 DEG C, keeps the temperature 3 hours；

(9) refrigeration seat is warming up to 30 DEG C again, and dehydrating breather freezes to -0 DEG C, keeps the temperature 2.5 hours, turns off and vacuumize, and heat preservation 0.5 is small When；

(10) it takes out and is packed, form product after mounted box packaging, save under room temperature.

The working principle of the invention is:

The present invention relates to a kind of Compositional type maintenance freeze-dried powder preparation preparation method and preparation facilities, the present apparatus can be quick On push the door open, and can quickly be clamped sealing, it is easy to use；

When freezing seat refrigeration, the heat of sliding sash 19 is quickly oriented to thermally conductive shell 26 by fin 25, and contact area is big, matches It closes electricity cold 11 to carry by electric power, heat is quickly oriented to heat exchange seat 28, it is thermally conductive quick, by being filled inside heat exchanger tube 21 Entering thermal medium, control module 5 control the movement of second solenoid valve 40 and compressor 33 and heat exchanger tube 21 are connected, and cooperate compressor 33 It exchanges heat with radiator 35, heat is discharged blower 9, quickly carries out freezing quick-frozen, the temperature of refrigeration passes through temperature sensor 20 detections；

Delivery pump 23 plays a part of extracting permanent gas, and low pressure necessary to being distilled with maintenance, 1g vapor is normal Pressure is expanded to 10000 liters in 13.3Pa for 1.25L, and common delivery pump 23 extracts so a large amount of within the unit time Volume be it is impossible, so dehydrating breather effect be will distil gasification vapor capture, reduce because distil caused by Portion's air pressure change, continuing working for cooperation delivery pump 23, guarantees hypobaric maintenance, and attachment flaps 38 and attachment shell in dehydrating breather 42 is big with internal contact area, and guide card 31 extends the path that gas passes through, and two dehydrating breather synchronous workings improve absorption effect Fruit, and the movement of second solenoid valve 40 is connected with interior cold frame 32, when being adsorbed, compressor 33 and interior cold frame 32 can be led It is logical, heat transferring medium is inputted in interior cold frame 32 and is absorbed heat, second temperature sensor 43 carries out temperature detection, cooperates control module 5 temperature for carrying out attachment shell 42 maintain, and shell 10 is discharged by drainpipe 27 in the water of generation, and passes through after equipment stops working Valve 39 is discharged；

When the temperature of product is -25 DEG C, the temperature of condensation is -50 DEG C, the saturated vapor pressure difference of ice at two temperatures For 63.3Pa and 1.1Pa, thus a sizable pressure difference is just produced between distillation face and cryosurface, if being at this time Incoagulable gas partial pressure in system can be ignored, and the vapor that it will promote product to distil out is fixed with certain flow velocity Coagulator surface is arrived to ground and forms frost, and multiple assembly heads 17 cooperate more mouthfuls of air-exhausting duct 13, channel width, improve and pass through Speed improves the velocity of liquid assets that distillation generates vapor；

The heat of sublimation of ice is about 2822J/ grams, if sublimation process does not supply heat, that product only reduce in can mend The heat of sublimation is repaid, until distillation also just stopped after its temperature and coagulator equalized temperature, for the temperature for keeping distillation to come with condensation It is poor to spend, it is necessary to provide enough heats to product by heating plate 15, guarantee being normally carried out for distillation；

The temperature and humidity of equipment can by temperature sensor 20, second temperature sensor 43 and humidity sensor 36 into Row detection, will test signal and is sent to control module 5 and calculated, and control module 5 carries out electricity by harness and power inside device Property connection, control module 5 by signal progress temperature control and equipment action control；

When dry at low temperature, some volatile components in substance lose very little, in freeze-drying process, the life of microorganism Long and enzyme effect can not carry out, therefore be able to maintain original character, due to being dried in the state of freezing, volume It is almost unchanged, maintain original structure, concentration phenomena will not occur, due in material moisture after pre-freeze with the shape of ice crystal State exists, and originally inorganic salts soluble in water dissolve substance and are uniformly distributed among material, soluble in water when distillation Dissolution substance is just precipitated, and avoids in general drying means because of material internal moisture to inorganic salts entrained by surface migration in table Face be precipitated and the phenomenon that cause Surface hardened layer, it is dry after substance it is loose porous, in spongy, add dissolve after water it is rapid and complete Entirely, original character is almost recovered immediately, since drying carries out under vacuum, oxygen is few, therefore some oxidizable substances Protected, drying can exclude 95%~99% or more moisture, enable it is dry after product long-term preservation without mutagens matter, because Material is in frozen state, and temperature is very low, so the heat source temperature of heat supply is of less demanding, using the not high heating of room temperature or temperature Device can be met the requirements；

The present invention reasonably compounds fibronectin and blue ketone victory peptide components to inside freeze-dried powder using freeze drying technology, effectively The activity for maintaining fibronectin and blue ketone victory peptide, can it is anti-inflammatory, repair aging dermal tissue, accelerate the healing of wound.Fibre is even Albumen is to be present in tissue and a kind of intracellular multifunctional protein, is the glycoprotein of macromolecule, high activity: by two phases As subunit constitute, C-terminal by disulfide bond be connected, entire molecule is V-shaped, and molecular weight is in 440-450KDa.Fibronectin Each subunit there are six functional areas and a RGD sequence, can heparin-binding, collagen, fiber, cell and 11 kinds of integrins etc. it is more Kind of substance, wound repair, cancer diagnosis, in terms of play a significant role.The maximum characteristic of blue ketone victory peptide is exactly Compound indigo plant copper is formed with Cu ion and wins peptide, and reparation and regenerated function are played as compound with bivalent cupric ion.Human body There are many important enzymes to need Cu ion on interior and skin, these enzymes are in connective tissue formation, anti-oxidative defense, cellular respiration It plays a role.Cu ion also plays semiotic function simultaneously, can influence the behavior and metabolism of cell, and the two generates collaboration and promotes to make With.

It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.

In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiments being understood that.