阅读说明：本技术 一种直接与间接制冷相结合的三氟化氮电解气超低温冷阱装置 (Direct and indirect refrigeration combined nitrogen trifluoride electrolysis gas ultralow temperature cold trap device ) 是由 林坤 马朝选 孟祥军 王少波 徐海云 于 2021-08-27 设计创作，主要内容包括：本发明提供了一种直接与间接制冷相结合的三氟化氮电解气超低温冷阱装置,包括保护箱,保护箱内设置有冷却箱,冷却箱内设有冷却桶,所述冷却桶内内壁上设置有蛇形输送管,蛇形输送管的一端连接有进气设备,冷却桶的外部设有冷却机构,蛇形输送管的一端连接有连接管路,连接管路的一端连接有冷却罐,冷却罐的上端连接有冷却液添加设备,冷却罐的下端连接有回流设备。本发明通过直接冷却和间接冷却的结合,极大地提升了三氟化氮电解气冷却的速度和效率,保证了三氟化氮电解气加工的质量,提高了三氟化氮电解气冷却的实用性和快速性,降低了三氟化氮电解气的冷却成本。(The invention provides a nitrogen trifluoride electrolysis gas ultralow temperature cold trap device directly combined with indirect refrigeration, which comprises a protection box, wherein a cooling box is arranged in the protection box, a cooling barrel is arranged in the cooling box, a snakelike conveying pipe is arranged on the inner wall of the cooling barrel, one end of the snakelike conveying pipe is connected with an air inlet device, a cooling mechanism is arranged outside the cooling barrel, one end of the snakelike conveying pipe is connected with a connecting pipeline, one end of the connecting pipeline is connected with a cooling tank, the upper end of the cooling tank is connected with a cooling liquid adding device, and the lower end of the cooling tank is connected with a backflow device. According to the invention, through the combination of direct cooling and indirect cooling, the cooling speed and efficiency of the nitrogen trifluoride electrolytic gas are greatly improved, the processing quality of the nitrogen trifluoride electrolytic gas is ensured, the practicability and rapidity of the cooling of the nitrogen trifluoride electrolytic gas are improved, and the cooling cost of the nitrogen trifluoride electrolytic gas is reduced.)

1. The utility model provides a nitrogen trifluoride electrolysis gas ultra-low temperature cold-trap device that direct and indirect refrigeration combined together, its characterized in that adds equipment (24) including fixed cooler bin (16), cooling tank (3) and condensing agent that set up in protection box (6), set up in cooler bin (16) cooling barrel (25), the outer wall week side of cooling barrel (25) sets up refrigeration coil (15), the inner wall week side of cooling barrel (25) is provided with gas transmission coil (21), the one end of gas transmission coil (21) is connected with the pipeline of current nitrogen trifluoride electrolysis gas, and the other end of gas transmission coil (21) passes through gas-supply pipe (8) and is connected with cooling tank (23), be provided with outlet duct (1) on cooling tank (3), condensing agent adds equipment (24) and is connected with cooling tank (3) and refrigeration coil (15) simultaneously, it still is provided with reflux unit to set up in protection box (6), the reflux device is simultaneously connected with the refrigeration coil (15), the cooling tank (3) and the condensing agent adding equipment (24).

2. The ultra-low temperature cold trap device for nitrogen trifluoride electrolysis gas directly combined with indirect refrigeration as claimed in claim 1, wherein the gas inlet end of the gas transmission coil (21) is connected with a fixed pipe (17) and a gas inlet pipe (14) in sequence, and the gas inlet pipe (14) is connected with the existing nitrogen trifluoride electrolysis gas transmission pipeline.

3. A nitrogen trifluoride electrolysis gas ultra-low temperature cold trap device directly combined with indirect refrigeration according to claim 1, characterized in that the refrigerant adding device (24) is communicated with a transverse pipe (5) through a refrigerant conveying pipe (22), the transverse pipe (5) is communicated with a cooling tank (3) through a first refrigerant adding pipe (4), and the transverse pipe (5) is communicated with a refrigeration coil (15) through a second refrigerant adding pipe (7).

4. A nitrogen trifluoride electrolysis gas ultra-low temperature cold trap device directly combined with indirect refrigeration, according to claim 1, characterized in that the reflux device comprises a receiving pipe (11), a first reflux pipe (10) and a second reflux pipe (13), the first reflux pipe (10) is connected with the cooling tank (3), the second reflux pipe (13) is connected with the refrigeration coil (15), the first reflux pipe (10) and the second reflux pipe (13) are simultaneously connected with the receiving pipe (11), and the receiving pipe (11) is connected with the condensing agent adding device (24).

5. The ultra-low temperature cold trap device for nitrogen trifluoride electrolysis gas directly combined with indirect refrigeration as claimed in claim 1, wherein a sealing cover (18) is arranged on the protection box (6), the sealing cover (18) is installed on the protection box (6) through screws, and mounting holes (20) for connecting the screws in a threaded manner are opened on the protection box (6).

6. A nitrogen trifluoride electrolysis gas ultra-low temperature cold trap device directly combined with indirect refrigeration according to claim 1, characterized in that the cooling tank (3) is fixed on the inner bottom surface of the protection box (6) by a plurality of support columns (19), and the cooling box (16) is fixed on the inner bottom surface of the protection box (6) by a plurality of support blocks (12).

7. The ultra-low temperature cold trap device for nitrogen trifluoride electrolysis gas directly combined with indirect refrigeration as claimed in claim 3, wherein the first refrigerant adding pipe (4) and the second refrigerant adding pipe (7) are both provided with a first solenoid valve (2), the refrigerant conveying pipe (22) is provided with a third solenoid valve (23), the air outlet pipe (1) and the air inlet pipe (14) are both provided with valves, and the air conveying pipe (8) is provided with a second solenoid valve (9).

Technical Field

The invention relates to a nitrogen trifluoride electrolytic gas cooling device, in particular to a nitrogen trifluoride electrolytic gas ultralow temperature cold trap device which is directly combined with indirect refrigeration.

Background

At present, when nitrogen trifluoride electrolysis gas is processed, the cold trap is generally used for cooling, but the existing cold trap is low in efficiency when cooling, long in required time and incapable of cooling quickly, so that the production cost is increased and the quality of the electrolysis gas is reduced, and therefore a device for cooling the nitrogen trifluoride electrolysis gas quickly and efficiently needs to be designed.

Disclosure of Invention

The technical problem to be solved by the invention is to provide a nitrogen trifluoride electrolytic gas ultralow temperature cold trap device which is directly combined with indirect refrigeration aiming at the defects of the prior art, the device has scientific and reasonable structural design, combines a direct cooling mode with an indirect cooling mode, can quickly and efficiently cool the nitrogen trifluoride electrolytic gas, has good use effect and simple operation, can effectively improve the quality level of the nitrogen trifluoride electrolytic gas, and reduces the production cost.

In order to solve the technical problems, the invention adopts the technical scheme that: the utility model provides a nitrogen trifluoride electrolysis gas ultra-low temperature cold-trap device that direct and indirect refrigeration combined together, its characterized in that adds equipment including fixed cooler bin, cooling tank and the condensing agent that sets up in the guard box, set up the cooling barrel in the cooler bin, the outer wall week side of cooling barrel sets up the refrigeration coil pipe, the inner wall week side of cooling barrel is provided with the gas transmission coil pipe, the one end of gas transmission coil pipe is connected with the delivery line of current nitrogen trifluoride electrolysis gas, and the other end of gas transmission coil pipe passes through the gas-supply pipe and is connected with the cooling tank, be provided with the outlet duct on the cooling tank, the condensing agent adds equipment and is connected with cooling tank and refrigeration coil pipe simultaneously, the setting still is provided with reflux unit in the guard box, reflux unit adds equipment with refrigeration coil pipe, cooling tank and condensing agent simultaneously and is connected.

Preferably, the inlet end of gas transmission coil pipe has connected gradually fixed pipe and intake pipe, the intake pipe is connected with current nitrogen trifluoride electrolysis gas conveying line, and the end of giving vent to anger of fixed pipe passes the cooling barrel and communicates with the inlet end of gas transmission coil pipe, and the inlet end of fixed pipe passes the end intercommunication of giving vent to anger of cooling tank and intake pipe, and the inlet end of intake pipe passes the delivery line connection of guard box and current nitrogen trifluoride electrolysis gas.

Preferably, a condensing agent outlet of the condensing agent adding equipment is communicated with the side wall of the transverse pipe through a condensing agent conveying pipe, one end of the transverse pipe is communicated with the top of the cooling tank through a first condensing agent adding pipe, and the other end of the transverse pipe is communicated with a liquid inlet of the refrigerating coil pipe through a second condensing agent adding pipe.

Preferably, the return means comprises a receiving pipe, a first return pipe and a second return pipe, the first return pipe being connected to the bottom of the cooling tank, the second return pipe is connected with the liquid outlet of the refrigeration coil pipe, the first return pipe and the second return pipe are simultaneously connected with the two ends of the accommodating pipe, the side wall of the containing pipe is connected with a condensing agent inlet of condensing agent adding equipment through a tail end return pipe, condensing agent delivery pumps are arranged on the tail end return pipe and the condensing agent delivery pipe, a double-channel circulating system of the condensing agent is formed by a condensing agent adding device, a condensing agent conveying pipe, a transverse pipe, a first condensing agent adding pipe, a cooling tank, a second condensing agent adding pipe, a refrigerating coil and a reflux device, carry out indirect cooling through cooling coil and gaseous indirect contact, carry out direct contact through the condensing agent in the cooling tank and gaseous and carry out direct cooling, two kinds of cooling methods combine effectively to improve cooling efficiency and effect.

Preferably, the guard box is the cuboid box, is provided with the closing cap on the terminal surface of guard box, the closing cap passes through the mounting screw on the guard box, four corner positions of guard box are offered and are used for threaded connection four mounting holes of screw, through the screw with closing cap movable mounting on the guard box convenient each device to the guard box in overhaul the maintenance.

Preferably, the cooling tank and the cooling barrel are cylindrical containers horizontally arranged in the protection box, the bottom of the cooling tank is fixed on the inner bottom surface of the protection box through four support columns, and the cooling box is fixed on the inner bottom surface of the protection box through four support blocks.

Preferably, all be provided with first solenoid valve on first condensing agent adds pipe and the second condensing agent adds the pipe, get into cooling tank and refrigeration coil through first solenoid valve control condensing agent, be provided with the third solenoid valve on the condensing agent conveyer pipe, in third solenoid valve control condensing agent gets into the cross pipe, all be provided with the valve in outlet duct and the intake pipe, through the business turn over of valve control nitrogen trifluoride electrolysis gas, be provided with the second solenoid valve on the gas-supply pipe, control gaseous from gas transmission coil pipe entering cooling tank through the second solenoid valve, all be provided with the fourth solenoid valve on first return pipe and the second return pipe, through the backward flow of fourth solenoid valve control condensing agent.

Compared with the prior art, the invention has the following advantages:

1. according to the invention, through the combination of direct cooling and indirect cooling, the cooling speed and efficiency of the nitrogen trifluoride electrolytic gas are greatly improved, the processing quality and progress of the nitrogen trifluoride electrolytic gas are ensured, the practicability and rapidity of the cooling of the nitrogen trifluoride electrolytic gas are effectively improved, and the cooling cost of the nitrogen trifluoride electrolytic gas is reduced.

2. The device has the advantages of scientific and reasonable structural design, simple operation, convenient installation, maintenance, good use effect, high economic value and popularization and use.

3. The invention designs two condensing agent circulating pipelines, one of the two condensing agent circulating pipelines indirectly cools the gas in the gas transmission coil pipe through the refrigerating coil pipe, the other one indirectly cools the gas through the direct contact of the condensing agent in the cooling tank and the gas, and the indirect cooling mode and the direct cooling mode are combined, so that the cooling efficiency is obviously improved, the cooling mode is flexible and variable, and the practicability is strong.

The present invention will be described in further detail with reference to the accompanying drawings and examples.

Drawings

Fig. 1 is a schematic view of the internal structure of the protective case of the present invention.

FIG. 2 is a schematic view showing a connection structure between a condensing agent adding apparatus and a horizontal and accommodating pipe according to the present invention.

Fig. 3 is a schematic view of the structure of the inside of the cooling box of the present invention.

Fig. 4 is a schematic view of the structure of the cooling tank of the present invention.

Fig. 5 is an external structural view of the protective case of the present invention.

Description of reference numerals:

1-air outlet pipe; 2-a first solenoid valve; 3-cooling the tank;

4-first condensing agent adding pipe; 5, a transverse pipe; 6, a protection box;

7-second condensing agent adding pipe; 8, a gas conveying pipe; 9-a second solenoid valve;

10-a first return pipe; 11-a storage tube; 12-a support block;

13 — a second return conduit; 14-an air inlet pipe; 15-a refrigeration coil;

16-a cooling box; 17-a fixed tube; 18-sealing the cover;

19-a support column; 20-mounting holes; 21-gas transmission coil pipe;

22-coolant delivery pipe; 23-a third solenoid valve; 24-a condensing agent adding device;

25-cooling barrel.

Detailed Description

As shown in fig. 1 to 5, the invention includes a cooling box 16, a cooling tank 3 and a condensing agent adding device 24 fixedly arranged in a protection box 6, wherein a cooling barrel 25 is arranged in the cooling box 16, a refrigerating coil 15 is arranged on the periphery of the outer wall of the cooling barrel 25, a gas transmission coil 21 is arranged on the periphery of the inner wall of the cooling barrel 25, one end of the gas transmission coil 21 is connected with a conveying pipeline of the existing nitrogen trifluoride electrolysis gas, the other end of the gas transmission coil 21 is connected with the cooling tank 3 through a gas transmission pipe 8, a gas outlet pipe 1 is arranged on the cooling tank 3, the condensing agent adding device 24 is simultaneously connected with the cooling tank 3 and the refrigerating coil 15, and a reflux device is further arranged in the protection box 6 and is simultaneously connected with the refrigerating coil 15, the cooling tank 3 and the condensing agent adding device 24.

In this embodiment, the inlet end of gas transmission coil 21 is connected with fixed pipe 17 and intake pipe 14 in proper order, intake pipe 14 is connected with current nitrogen trifluoride electrolysis gas conveying line, and the end of giving vent to anger of fixed pipe 17 passes cooling barrel 25 and gas transmission coil 21's inlet end intercommunication, and the inlet end of fixed pipe 17 passes cooling tank 16 and the end intercommunication of giving vent to anger of intake pipe 14, and the inlet end of intake pipe 14 passes protection box 6 and is connected with current nitrogen trifluoride electrolysis gas conveying line.

In this embodiment, the refrigerant outlet of the refrigerant adding device 24 is communicated with the side wall of the transverse pipe 5 through a refrigerant conveying pipe 22, one end of the transverse pipe 5 is communicated with the top of the cooling tank 3 through a first refrigerant adding pipe 4, and the other end of the transverse pipe 5 is communicated with the liquid inlet of the refrigerating coil 15 through a second refrigerant adding pipe 7.

In this embodiment, the backflow device includes a receiving pipe 11, a first backflow pipe 10 and a second backflow pipe 13, the first backflow pipe 10 is connected to the bottom of the cooling tank 3, the second backflow pipe 13 is connected to the liquid outlet of the cooling coil 15, the first backflow pipe 10 and the second backflow pipe 13 are connected to both ends of the receiving pipe 11, the side wall of the receiving pipe 11 is connected to the condensing agent inlet of the condensing agent adding device 24 through the terminal backflow pipe, a condensing agent delivery pump is arranged on the terminal backflow pipe and the condensing agent delivery pipe 22, a dual-channel circulation system of the condensing agent is formed by the condensing agent adding device 24, the condensing agent delivery pipe 22, the horizontal pipe 5, the first condensing agent adding pipe 4, the cooling tank 3, the second condensing agent adding pipe 7, the cooling coil 15 and the backflow device, indirect cooling is performed through indirect contact between the cooling coil 15 and gas, direct cooling is performed through direct contact between the condensing agent in the cooling tank 3 and gas, the two cooling modes are combined to effectively improve the cooling efficiency and effect.

In this embodiment, guard box 6 is the cuboid box, is provided with closing cap 18 on the terminal surface of guard box 6, closing cap 18 passes through the mounting screw on guard box 6, four corner positions of guard box 6 are offered and are used for threaded connection four mounting holes 20 of screw, and each device of convenient in to guard box 6 overhauls and maintains through the screw with closing cap 18 movable mounting on guard box 6.

In this embodiment, the cooling tank 3 and the cooling barrel 25 are cylindrical containers horizontally placed in the protection box 6, the bottom of the cooling tank 3 is fixed on the inner bottom surface of the protection box 6 through four support columns 19, and the cooling box 16 is fixed on the inner bottom surface of the protection box 6 through four support blocks 12.

In this embodiment, all be provided with first solenoid valve 2 on first condensing agent adds pipe 4 and the second condensing agent and adds pipe 7, get into cooling tank 3 and refrigeration coil 15 through 2 control condensing agents of first solenoid valve, be provided with third solenoid valve 23 on condensing agent conveyer pipe 22, through the entering of third solenoid valve 23 control condensing agent violently manage 5 in, all be provided with the valve on outlet duct 1 and the intake pipe 14, through the business turn over of valve control nitrogen trifluoride electrolysis gas, be provided with second solenoid valve 9 on the gas-supply pipe 8, through the gaseous cooling tank 3 that gets into from gas transmission coil 21 of second solenoid valve 9 control, all be provided with the fourth solenoid valve on first return pipe 10 and the second return pipe 13, through the backward flow of fourth solenoid valve control condensing agent.

In this embodiment, the condensing agent adding device 24 is any one of feeding devices capable of realizing a refrigerant adding function, and is an existing mature product.

When the nitrogen trifluoride electrolytic gas needs to be cooled, the nitrogen trifluoride electrolytic gas is conveyed into the fixed pipe 17 through the air inlet pipe 14 in advance, then the nitrogen trifluoride electrolytic gas is conveyed into the gas transmission coil 21 through the fixed pipe 17, the condensing agent adding equipment 24 conveys the condensing agent into the transverse pipe 5 through the condensing agent conveying pipe 22, the first electromagnetic valve 2 on the second condensing agent adding pipe 7 is opened to convey the condensing agent into the refrigerating coil 15, the gas transmission coil 21 is cooled through the cooling barrel 25, and the second electromagnetic valve 9 is opened after indirect cooling to convey the nitrogen trifluoride electrolytic gas in the gas transmission coil 21 into the cooling tank 3. And opening a first electromagnetic valve 2 on a first condensing agent adding pipe 4, conveying a part of condensate in a transverse pipe 5 to a cooling tank 3, directly contacting the condensing agent in the cooling tank 3 with the nitrogen trifluoride electrolytic gas subjected to indirect cooling to realize rapid cooling, and discharging the nitrogen trifluoride electrolytic gas cooled by the directly contacted condensing agent through an air outlet pipe 1. When the condensing agent in the cooling tank 3 needs to be replaced, the fourth electromagnetic valve on the first return pipe 10 is opened, the condensing agent is recovered and re-refrigerated by using the condensing agent adding device 24, and when the condensing agent in the refrigerating coil 15 needs to be circulated, the fourth electromagnetic valve on the second return pipe 13 is opened, the condensing agent is recovered and re-refrigerated by using the condensing agent adding device 24, so that the double-channel circulation of the condensing agent is completed.

The above description is only for the preferred embodiment of the present invention, and is not intended to limit the present invention in any way. Any simple modification, change and equivalent changes of the above embodiments according to the technical essence of the invention are still within the protection scope of the technical solution of the invention.