阅读说明：本技术 一种含有井冈霉素和腐植酸钠的药肥合剂 (Pesticide-fertilizer mixture containing validamycin and sodium humate ) 是由 夏桂平 于 2021-07-12 设计创作，主要内容包括：本发明属于新型生态复合肥料技术领域,具体的说是一种含有井冈霉素和腐植酸钠的药肥合剂,包括井冈霉素和腐植酸钠；本发明通过将井冈霉素和腐植酸钠按一定比例进行混合,运用一定的工艺技术将其稳定于复合体系中,进而形成新型生态复合肥料,因此混合后的药肥对农作物即具有营养的肥效,又具有抗病治病的药效,同时药肥对提高农作物的产量,提早农作物成熟时间也有一定的促进作用；药肥实现了将农药的植物保护和肥料的养分供给两个田间操作合二为一,节省劳力、降低生产成本；通过该工艺制取腐植酸钠,缩短了现有腐植酸钠制取的步骤,进而减少了设备的投入,节省了成本。(The invention belongs to the technical field of novel ecological compound fertilizers, and particularly relates to a pesticide-fertilizer mixture containing validamycin and sodium humate, which comprises validamycin and sodium humate; the validamycin and the sodium humate are mixed according to a certain proportion and are stabilized in a composite system by a certain process technology to form a novel ecological compound fertilizer, so that the mixed pesticide fertilizer has nutritional fertilizer effect on crops and disease-resistant drug effect, and meanwhile, the pesticide fertilizer has a certain promotion effect on improving the yield of the crops and advancing the maturation time of the crops; the pesticide fertilizer combines two field operations of plant protection of pesticide and nutrient supply of fertilizer, saves labor force and reduces production cost; the sodium humate is prepared by the process, so that the steps for preparing the existing sodium humate are shortened, the investment of equipment is reduced, and the cost is saved.)

1. A pesticide-fertilizer mixture containing validamycin and sodium humate is characterized in that: comprises validamycin and sodium humate; 63-84 parts of validamycin A; 13-18 parts of sodium humate;

the production process of the sodium humate comprises the following steps:

s1: putting raw material coal into a mixed reaction device (1); the mixed reaction equipment (1) is used for crushing, reacting and extracting and carrying out solid-liquid separation on the placed raw material coal, adding a mixture of water and NaOH in the process, and obtaining a clear water-soluble sodium humate solution after a period of time;

s2: introducing the sodium humate solution obtained in the S1 mixed reaction equipment (1) into evaporation equipment; the evaporation equipment is used for concentrating and evaporating the sodium humate solution;

s3: putting the sodium humate obtained by concentrating and evaporating the S2 into drying equipment; the drying equipment is used for drying the concentrated sodium humate to obtain a refined sodium humate product.

2. The insecticide-fertilizer mixture containing validamycin and sodium humate as claimed in claim 1, wherein: the mixing reaction equipment (1) comprises a barrel body (11), a supporting plate (12), a supporting rod (13), a filtering piece (14), a booster pump (15), a spray pipe (16) and an infusion ring (17); the filtering piece (14) is arranged in the middle of the barrel body (11); the filter element (14) is of a columnar structure; a gap is reserved between the filtering piece (14) and the inner wall of the barrel body (11); one end of the filter element (14) is fixedly connected in the barrel body (11) and is close to the feeding end of the barrel body (11); the other end of the filter element (14) is provided with the supporting disc (12); the support disc (12) is rotatably connected to the filter element (14); the middle part of the supporting disc (12) is fixedly connected with the upper end of the supporting rod (13); the lower end of the supporting rod (13) is rotatably connected to the bottom of the barrel body (11); a slag outlet (111) is formed in the side wall of the barrel body (11); the slag outlet (111) is close to the bottom of the barrel body (11); a liquid outlet (112) is formed in the side wall of the barrel body (11); the liquid outlet (112) is arranged far away from the slag outlet (111); a liquid pumping port (113) is formed in the side wall of the barrel body (11) and is positioned above the liquid outlet (112); the liquid extracting port (113) is higher than the liquid outlet (112); the liquid outlet (112) is higher than the slag outlet (111); the side wall of the barrel body (11) is fixedly connected with a mounting seat of the booster pump (15); the infusion ring (17) is sleeved on the side wall of the barrel body (11); the infusion ring (17) is fixedly connected to the barrel body (11); the liquid pumping port (113), the booster pump (15) and the infusion ring (17) are communicated through delivery pipes; the spray pipes (16) are uniformly arranged on the infusion ring (17) at intervals along the circumferential direction; one end of the spray pipe (16) is fixedly connected to the transfusion ring (17); the other end of the spray pipe (16) penetrates through the barrel body (11) and the filter element (14); the outlet of the spout (16) is arranged tangentially along the edge of the support disc (12).

3. The insecticide-fertilizer mixture containing validamycin and sodium humate as claimed in claim 2, wherein: a baffle disc (2) is arranged below the supporting disc (12); the baffle disc (2) is of a funnel-shaped structure; the outer wall of the baffle disc (2) is fixedly connected to the inner wall of the barrel body (11); a gap is reserved between the inner wall of the baffle disc (2) and the support rod (13); the side of the baffle disc (2) close to the supporting seat protrudes to the bottom of the barrel body (11).

4. The insecticide-fertilizer mixture containing validamycin and sodium humate as claimed in claim 3, wherein: a slag discharging disc (3) is arranged on the inner surface of the bottom of the barrel body (11); the middle part of the slag discharging disc (3) is fixedly connected to the supporting rod (13); the outer wall of the slag discharging disc (3) is in contact with the inner wall of the barrel body (11); the slag discharging disc (3) is of a conical structure; the bottom of the conical structure of the slag discharging disc (3) is close to the bottom of the barrel body (11).

5. The insecticide-fertilizer mixture containing validamycin and sodium humate as claimed in claim 4, wherein: a rotating ring (4) is arranged in the spray pipe (16) at a position close to the filter element (14); the rotating ring (4) is rotatably connected to the inner wall of the spray pipe (16); spoilers (41) are uniformly arranged in the rotating ring (4) at intervals along the circumferential direction; the spoiler (41) is helical.

6. The insecticide-fertilizer mixture containing validamycin and sodium humate as claimed in claim 5, wherein: the filter piece (14) comprises a first connecting ring (141), a second connecting ring (142) and a connecting rod (143); the first connecting ring (141) is fixedly connected to the barrel body (11); the second connecting ring (142) is rotatably connected with the supporting disc (12); the connecting rod (143) is obliquely arranged between the first connecting ring (141) and the second connecting ring (142); the connecting rods (143) are uniformly arranged at intervals along the circumferential direction of the first connecting ring (141) or the second connecting ring (142); the inner layer and the outer layer of the connecting rod (143) are arranged in two layers, and the inclined directions of the connecting rods (143) on the inner layer and the outer layer are opposite; a reticular structure is formed between the inner layer of connecting rods (143) and the outer layer of connecting rods (143); welding points are formed at the junction between the connecting rods (143) of the inner layer and the outer layer through welding; the welding point is bulky and protrudes to the inner side.

7. The insecticide-fertilizer mixture containing validamycin and sodium humate as claimed in claim 6, wherein: a cover plate (5) is arranged at the feeding end of the barrel body (11); the middle part of the cover plate (5) is sunken downwards; a feed inlet is formed in the concave part; turning plates (51) are symmetrically arranged at the feed inlet; the ends, far away from each other, of the turning plates (51) are hinged to the cover plate (5); a torsion spring is arranged between the turning plate (51) and the cover plate (5).

8. The insecticide-fertilizer mixture containing validamycin and sodium humate as claimed in claim 7, wherein: the lower end of the supporting rod (13) penetrates through the bottom of the cylinder body; the lower end of the supporting rod (13) is fixedly connected with a clutch (6); a motor (7) is arranged below the clutch (6); a rotating shaft of the motor (7) is fixedly connected to the clutch (6); and the mounting seat of the motor (7) is fixedly connected to the supporting leg of the cylinder body.

Technical Field

The invention belongs to the technical field of novel ecological compound fertilizers, and particularly relates to a pesticide-fertilizer mixture containing validamycin and sodium humate.

Background

The drug and fertilizer mixture is popular, and the drug and fertilizer are integrated into a whole, namely drug and fertilizer integration. The pesticide-fertilizer mixture has one or more functions of killing and inhibiting crop diseases and pests or regulating crop growth, and can provide nutrients for crops or simultaneously provide nutrients and improve the utilization rate of fertilizers and pesticides. Balanced fertilization and complete nutrition; broad spectrum, high efficiency and one-time determination; the front control and the back control are promoted, and the stress resistance is enhanced; fertilizer and pesticide combination and interaction synergy; the operation is simple and convenient, and the use is safe; labor and cost are saved, and the yield and income are increased; the fertilizer is used for replacing the material, so that the fertilizer is safe and environment-friendly; the storage and transportation are convenient, and the low carbon and energy saving are realized; benefits multiple parties, benefits the nation and the people, and the like. The agricultural chemical integrates two most important agricultural chemicals, namely the agricultural chemical and the fertilizer, which are used in agriculture, considers the influence that respective effects of the agricultural chemical and the fertilizer are possibly decreased after the agricultural chemical and the fertilizer meet naturally, combines two field operations of plant protection of the agricultural chemical and nutrient supply of the fertilizer into a whole, saves labor and reduces production cost.

Validamycin is an antibiotic produced by actinomycetes, has strong systemic property, is easily absorbed by thallus cells and quickly conducts in the thallus cells, interferes and inhibits the growth and development of the thallus cells, and further has good prevention and treatment effects on various crops.

The sodium humate can reduce the loss of ammoniacal nitrogen by ammonium bicarbonate and improve the utilization rate of the nitrogen fertilizer; can inhibit urease activity and reduce urea volatilization; can inhibit the fixation of water-soluble phosphorus by soil and promote the absorption of phosphorus by root systems; meanwhile, sodium humate and insoluble trace elements are subjected to chelation reaction, so that the trace elements can be absorbed by root systems and leaf surfaces; the sodium humate contains various functional groups, the activated sodium humate becomes a high-efficiency bioactive substance, and has an stimulating effect on the growth and development of crops and the physiological metabolism in vivo, the characteristic is not possessed by common fertilizers, and the high-efficiency bioactive substance of the activated sodium humate has obvious stimulating effect on various crops by adopting the modes of seed soaking, root dipping, spraying, irrigating, base fertilizer making and the like according to a certain concentration; comprehensively shows the promotion of root system development and the good influence on the crop yield and quality factors.

Therefore, the validamycin and the sodium humate are prepared into the medical fertilizer which has nutrient fertilizer effect on crops and disease-resistant and disease-curing effect.

The existing process for preparing the sodium humate product firstly needs to crush, extract and separate solid and liquid from raw materials to obtain a solution, then the solution is evaporated and dried to prepare the sodium humate product, the existing process has various steps and more required equipment, so that the preparation time and cost are increased.

Disclosure of Invention

In order to make up the defects of the prior art, the invention provides a pesticide-fertilizer mixture containing validamycin and sodium humate. The method is mainly used for solving the problems of more equipment investment and high production time and cost due to multiple steps in the process of preparing the sodium humate product by the prior art.

The technical scheme adopted by the invention for solving the technical problems is as follows: the invention provides a pesticide-fertilizer mixture containing validamycin and sodium humate, which comprises validamycin and sodium humate; 63-84 parts of validamycin A; 13-18 parts of sodium humate;

the production process of the sodium humate comprises the following steps:

s1: putting raw material coal into a mixed reaction device; the mixed reaction equipment is used for crushing, reacting and extracting and carrying out solid-liquid separation on the placed raw material coal, a mixture of water and NaOH is added in the process, and a clear water-soluble sodium humate solution is obtained after a period of time;

s2: introducing the sodium humate solution obtained in the S1 mixed reaction equipment into evaporation equipment; the evaporation equipment is used for concentrating and evaporating the sodium humate solution;

s3: putting the sodium humate obtained by concentrating and evaporating the S2 into drying equipment; the drying equipment is used for drying the concentrated sodium humate to obtain a refined sodium humate product.

When the fertilizer works, validamycin and sodium humate are mixed according to a certain proportion and are stabilized in a compound system by a certain process technology, so that a novel ecological compound fertilizer (drug fertilizer for short) is formed, because validamycin is an antibiotic produced by actinomycetes, has strong systemic property, is easily absorbed by thallus cells and quickly conducts in the thallus cells, interferes and inhibits the growth and development of the thallus cells, further has good prevention and treatment effects on various crops, and because the sodium humate can reduce the loss of ammoniacal nitrogen by the ammonium bicarbonate, the utilization rate of a nitrogen fertilizer is improved; can inhibit urease activity and reduce urea volatilization; can inhibit the fixation of water-soluble phosphorus by soil and promote the absorption of phosphorus by root systems; meanwhile, sodium humate and insoluble trace elements are subjected to chelation reaction, so that the trace elements can be absorbed by root systems and leaf surfaces; the sodium humate contains various functional groups, the activated sodium humate becomes a high-efficiency bioactive substance, and has an stimulating effect on the growth and development of crops and the physiological metabolism in vivo, the characteristic is not possessed by common fertilizers, and the high-efficiency bioactive substance of the activated sodium humate has obvious stimulating effect on various crops by adopting the modes of seed soaking, root dipping, spraying, irrigating, base fertilizer making and the like according to a certain concentration; comprehensively shows the promotion of root system development and the good influence on the crop yield and quality factors; therefore, the mixed pesticide fertilizer has nutritional fertilizer effect on crops and disease-resistant efficacy, and simultaneously has certain promotion effect on improving the yield of the crops and advancing the maturity time of the crops; the pesticide fertilizer combines two field operations of plant protection of pesticide and nutrient supply of fertilizer, saves labor force and reduces production cost; the sodium humate is prepared by the process, so that the steps of preparing the existing sodium humate are shortened, the investment of equipment is reduced, and the cost is saved; on the other hand, the content of the active ingredients of the prepared sodium humate is higher, so that the sodium humate content of the mixed pesticide fertilizer is higher under the same volume or weight, and the promotion effect on crops is improved under the condition of the same fertilizing amount.

Preferably, the mixing reaction equipment comprises a barrel body, a supporting plate, a supporting rod, a filtering piece, a booster pump, a spray pipe and an infusion ring; the filtering piece is arranged in the middle of the barrel body; the filter piece is of a columnar structure; a gap is reserved between the filter element and the inner wall of the barrel body; one end of the filter element is fixedly connected in the barrel body and is close to the feed end of the barrel body; the other end of the filter element is provided with the supporting disc; the supporting disc is rotatably connected to the filter element; the middle part of the supporting disc is fixedly connected with the upper end of the supporting rod; the lower end of the supporting rod is rotatably connected to the bottom of the barrel body; a slag outlet is formed in the side wall of the barrel body; the slag outlet is close to the bottom of the barrel body; a liquid outlet is formed in the side wall of the barrel body; the liquid outlet is far away from the slag outlet; a liquid pumping port is formed in the side wall of the barrel body and positioned above the liquid outlet; the liquid pumping port is higher than the liquid outlet; the liquid outlet is higher than the slag outlet; the side wall of the barrel body is fixedly connected with a mounting seat of the booster pump; the infusion ring is sleeved on the side wall of the barrel body; the infusion ring is fixedly connected to the barrel body; the liquid pumping port, the booster pump and the infusion ring are communicated through conveying pipes; the spray pipes are uniformly arranged on the infusion ring at intervals along the circumferential direction; one end of the spray pipe is fixedly connected to the infusion ring; the other end of the spray pipe penetrates through the barrel body and the filter element; the outlet of the spray pipe is tangentially arranged along the edge of the support plate.

When the device works, firstly, raw coal materials are placed into a mixing reaction device, then a booster pump is started, and then the booster pump extracts mixed liquid of water and NaOH, and then the mixed liquid enters a liquid conveying ring through a pipeline and is sprayed out from a nozzle of a spray pipe to form high-pressure mixed liquid flow, the sprayed liquid impacts on the raw coal, and then the raw coal is cracked under the impact force of the high-pressure liquid, so that the raw coal is crushed; in the process, the mixed liquid flows into the bottom of the barrel body from the filtering piece and is deposited, when the mixed liquid in the barrel body reaches a certain amount, the booster pump starts to extract the liquid in the barrel body to provide continuous power for crushing raw coal, and then the raw coal in larger particles left by filtering the filtering piece is continuously crushed, and simultaneously the supporting disk is driven to rotate under the combined action of liquid impact and moving raw coal, so that the raw coal on the supporting disk is thrown to the filtering piece under the action of centrifugal force, the raw coal is impacted on the filtering piece, and then the raw coal is crushed again, and further the crushing degree of the raw coal is improved; meanwhile, the raw material coal is rubbed with the side wall of the filtering piece in the movement process of the raw material coal, so that the raw material coal is further crushed, the crushing degree of the raw material coal is further improved, the extraction of humic acid in the raw material coal is facilitated, and the content of humate in a mixed solution is further improved; because the power of crushing is the mixed liquid of water and NaOH, the humic acid is extracted in the crushing process, the time required by the reaction is shortened, and the preparation efficiency of the sodium humate is improved; because the position of drawing liquid mouth is higher, and then when the extraction disturbance to staving inner liquid lower floor is less, and then is favorable to mixing the subsidence of impurity in the liquid, and then realizes separating the solid impurity in the mixed liquid.

Preferably, a blocking disc is arranged below the supporting disc; the baffle disc is of a funnel-shaped structure; the outer wall of the baffle disc is fixedly connected to the inner wall of the barrel body; a gap is reserved between the inner wall of the baffle disc and the supporting rod; the side of the blocking disc close to the supporting seat protrudes towards the bottom of the barrel body.

During operation, through setting up the fender dish, and the fender dish becomes to leak hopper-shaped, and then mixed liquid assembles to bracing piece one side along the fender dish, flow into the staving afterwards, and then mixed liquid is close to the bracing piece in the staving and makes the solid particle in the mixed liquid can subside fast to the in-process that the staving lateral wall flows, and then the solid particle that contains in having reduced mixed liquid in the staving is close to staving lateral wall department solution, it flows into the staving from whole barrel lateral wall to have avoided mixed liquid simultaneously, and then avoid disturbing the internal upper strata of staving to mix liquid, further reduced near mixed liquid upper strata department solid particle that contains of staving lateral wall, and then reduced in mixed liquid solid particle gets into the booster pump, and then reduced the damage to the booster pump, and then improved the life of booster pump.

Preferably, a slag discharging disc is arranged on the inner surface of the bottom of the barrel body; the middle part of the slag discharging disc is fixedly connected to the supporting rod; the outer wall of the slag discharging disc is in contact with the inner wall of the barrel body; the slag discharging disc is of a conical structure; the bottom of the slag discharging disc circular cone-shaped structure is close to the bottom of the barrel body.

When the device works, the slag discharging disc is arranged at the bottom of the barrel body and is of a conical structure, and meanwhile, the slag discharging disc rotates along with the supporting rod, so that solid particles deposited near the rotating rod are pushed to the side wall of the barrel body by the slag discharging disc in the rotating process, the solid particles at the supporting rod are prevented from being deposited, the contact area of mixed liquid and raw material coal is increased, the extraction rate is increased, and the extraction time is shortened; meanwhile, the rotating slag discharging disc pushes residual solid impurities after the reaction is finished, so that slag discharging is facilitated.

Preferably, a rotating ring is arranged in the spray pipe at a position close to the filter element; the rotating ring is rotatably connected to the inner wall of the spray pipe; spoilers are uniformly arranged in the rotating ring at intervals along the circumferential direction; the spoiler is spiral.

The during operation, the spoiler of contact setting in the spray tube exit when the spray tube blowout is followed to high-pressure mixed liquid, because the spoiler is the heliciform, and then the spoiler rotates under the effect of mixed liquid stream, and then make the mixed liquid in spray tube exit become the heliciform blowout, and then when making mixed liquid impact on raw coal, the impact force that raw coal received becomes complicated various, and then be favorable to the smashing of raw coal, and then be favorable to the extraction of solution to the raw coal after smashing, and then be favorable to improving the content of sodium humate active ingredient, and then improved after mixing the fertilizer to prevent and control crops and promote the effect.

Preferably, the filter element comprises a first connecting ring, a second connecting ring and a connecting rod; the first connecting ring is fixedly connected to the barrel body; the second connecting ring is rotatably connected with the supporting disc; the connecting rod is obliquely arranged between the first connecting ring and the second connecting ring; the connecting rods are uniformly arranged at intervals along the circumferential direction of the first connecting ring or the second connecting ring; the inner layer and the outer layer of the connecting rod are arranged in two layers, and the inclination directions of the connecting rods of the inner layer and the outer layer are opposite; a net structure is formed between the inner layer connecting rod and the outer layer connecting rod; welding points are formed at the junction between the connecting rods of the inner layer and the outer layer through welding; the welding point is bulky and protrudes to the inner side.

When the device works, the high-pressure mixed liquid sprayed by the spray pipe impacts on the raw material coal, so that the raw material coal is in friction and collision with the side wall of a net-shaped structure formed by the connecting rods in the moving process, an auxiliary effect is provided for crushing the raw material coal, the time required for crushing the raw material coal is shortened, and the preparation efficiency of sodium humate is improved; make the ectonexine connecting rod junction link together through the welding, and then improved the intensity that forms network structure between the connecting rod, and then increased and filtered the life-span that uses, again because the bulky of welding point just to the inboard arch, and then make and filter a piece inner wall surface convex and concave not flat, and then increased and filtered friction and collision between piece and the raw materials coal, and then improved the crushing degree to the raw materials coal, and then increased the area of contact of raw materials coal contact water and NaOH mixture, and then increased the speed to the extraction of the humic acid in the raw materials coal and the generation of sodium humate.

Preferably, a cover plate is arranged at the feeding end of the barrel body; the middle part of the cover plate is sunken downwards; a feed inlet is formed in the concave part; turning plates are symmetrically arranged at the feed inlet; one ends of the turning plates, which are far away from each other, are hinged on the cover plate; and a torsion spring is arranged between the turning plate and the cover plate.

During operation, pour the depressed part of apron into the raw materials coal who prepares, and then make under the effect of raw materials coal self gravity turn over the board and rotate, and then raw materials coal falls into in the bucket, turns over the board and gets back to initial position under the torsion effect of torsional spring afterwards, and then makes feed inlet department sealed, and then prevents that spray tube spun high-pressure mixed liquid from leading to the fact liquid and raw materials coal to splash out of the bucket after the impact on raw materials coal, and then avoids causing the waste.

Preferably, the lower end of the support rod penetrates through the bottom of the cylinder body; the lower end of the supporting rod is fixedly connected with a clutch; a motor is arranged below the clutch; a rotating shaft of the motor is fixedly connected to the clutch; the mounting seat of the motor is fixedly connected to the supporting leg of the cylinder body.

When the device works, when the raw material coal on the supporting disc is less, the high-pressure water flow drives the supporting disc to rotate to generate centrifugal force which is not enough to throw the residual raw material coal in the middle area of the supporting disc to the filtering piece, so that the raw material coal cannot be completely crushed and enters mixed liquid below the barrel body to be reacted and extracted, the content of sodium humate in the mixed liquid is reduced, the motor and the clutch are arranged to provide rotating power for the supporting disc, the centrifugal force on the residual raw material coal on the rotating disc is increased, the raw material coal is completely crushed and reacts with the mixed liquid, the content of sodium humate in the mixed liquid is increased, the content of effective components in the refined sodium humate is increased, and the control and promotion effects of the pesticide fertilizer on crops are improved; meanwhile, the clutch avoids the obstruction of the rotation of the supporting disc caused by the motor before the centrifugal force generated by the rotation of the supporting disc driven by high-pressure water flow is insufficient to throw the residual raw coal in the middle area of the supporting disc to the filter piece; after raw materials coal is smashed completely, booster pump stop work, and then row's sediment dish stall, and then the unable motion to around of solid impurity in the staving, and then can't continue to arrange the sediment, drive the bracing piece through the motor and rotate, and then drive and arrange the rotation of sediment dish, and then make solid impurity in the staving can continue to be got rid of, and then avoid remaining solid impurity in the staving and the follow-up preparation of influence.

The invention has the following beneficial effects:

1. the validamycin and the sodium humate are mixed according to a certain proportion and are stabilized in a composite system by a certain process technology, so that a novel ecological compound fertilizer (drug fertilizer for short) is formed, because the validamycin is an antibiotic produced by actinomycetes, has strong systemic property, is easily absorbed by thallus cells and quickly conducted in the thallus cells, interferes and inhibits the growth and development of the thallus cells, further has good prevention and treatment effects on various crops, and because the sodium humate can reduce the loss of ammoniacal nitrogen by the ammonium bicarbonate, the utilization rate of a nitrogen fertilizer is improved; can inhibit urease activity and reduce urea volatilization; can inhibit the fixation of water-soluble phosphorus by soil and promote the absorption of phosphorus by root systems; meanwhile, sodium humate and insoluble trace elements are subjected to chelation reaction, so that the trace elements can be absorbed by root systems and leaf surfaces; the sodium humate contains various functional groups, the activated sodium humate becomes a high-efficiency bioactive substance, and has an stimulating effect on the growth and development of crops and the physiological metabolism in vivo, the characteristic is not possessed by common fertilizers, and the high-efficiency bioactive substance of the activated sodium humate has obvious stimulating effect on various crops by adopting the modes of seed soaking, root dipping, spraying, irrigating, base fertilizer making and the like according to a certain concentration; comprehensively shows the promotion of root system development and the good influence on the crop yield and quality factors; therefore, the mixed pesticide fertilizer has nutritional fertilizer effect on crops and disease-resistant efficacy, and simultaneously has certain promotion effect on improving the yield of the crops and advancing the maturity time of the crops; the pesticide fertilizer combines two field operations of plant protection of pesticide and nutrient supply of fertilizer, saves labor force and reduces production cost; the sodium humate is prepared by the process, so that the steps of preparing the existing sodium humate are shortened, the investment of equipment is reduced, and the cost is saved; on the other hand, the content of the active ingredients of the prepared sodium humate is higher, so that the sodium humate content of the mixed pesticide fertilizer is higher under the same volume or weight, and the promotion effect on crops is improved under the condition of the same fertilizing amount.

2. According to the invention, the raw coal is firstly put into a mixing reaction device, then a booster pump is started, and then the booster pump extracts a mixed liquid of water and NaOH, and then the mixed liquid enters a liquid conveying ring through a pipeline, and then is sprayed out from the orifice of a spray pipe to form a high-pressure mixed liquid flow, the sprayed liquid impacts on the raw coal, and then the raw coal is cracked under the impact force of the high-pressure liquid, so that the raw coal is crushed; in the process, the mixed liquid flows into the bottom of the barrel body from the filtering piece and is deposited, when the mixed liquid in the barrel body reaches a certain amount, the booster pump starts to extract the liquid in the barrel body to provide continuous power for crushing raw coal, and then the raw coal in larger particles left by filtering the filtering piece is continuously crushed, and simultaneously the supporting disk is driven to rotate under the combined action of liquid impact and moving raw coal, so that the raw coal on the supporting disk is thrown to the filtering piece under the action of centrifugal force, the raw coal is impacted on the filtering piece, and then the raw coal is crushed again, and further the crushing degree of the raw coal is improved; meanwhile, the raw material coal is rubbed with the side wall of the filtering piece in the movement process of the raw material coal, so that the raw material coal is further crushed, the crushing degree of the raw material coal is further improved, the extraction of humic acid in the raw material coal is facilitated, and the content of humate in a mixed solution is further improved; because the power of crushing is the mixed liquid of water and NaOH, the humic acid is extracted in the crushing process, the time required by the reaction is shortened, and the preparation efficiency of the sodium humate is improved; because the position of drawing liquid mouth is higher, and then when the extraction disturbance to staving inner liquid lower floor is less, and then is favorable to mixing the subsidence of impurity in the liquid, and then realizes separating the solid impurity in the mixed liquid.

3. According to the invention, the baffle disc is arranged and is funnel-shaped, so that the mixed liquid is converged towards one side of the supporting rod along the baffle disc and then flows into the barrel body, solid particles in the mixed liquid can be rapidly settled in the process that the mixed liquid flows from the position, close to the supporting rod, in the barrel body to the side wall of the barrel body, so that the solid particles contained in the solution at the position, close to the side wall of the barrel body, of the mixed liquid in the barrel body are reduced, meanwhile, the mixed liquid is prevented from flowing into the barrel body from the side wall of the whole barrel body, the upper-layer mixed liquid in the barrel body is prevented from being disturbed, the solid particles contained at the upper-layer position of the mixed liquid near the side wall of the barrel body are further reduced, the solid particles in the mixed liquid are further reduced from entering the booster pump, the damage to the booster pump is further reduced, and the service life of the booster pump is prolonged.

4. According to the invention, the slag discharging disc is arranged at the bottom of the barrel body and is of a conical structure, and the slag discharging disc rotates along with the supporting rod, so that solid particles deposited and accumulated near the rotating rod are pushed to the side wall of the barrel body by the slag discharging disc in the rotating process, and the solid particles at the supporting rod are prevented from being deposited, thereby increasing the contact area of the mixed liquid and the raw material coal, further improving the extraction rate, and further shortening the extraction time; meanwhile, the rotating slag discharging disc pushes residual solid impurities after the reaction is finished, so that slag discharging is facilitated.

5. According to the invention, when the high-pressure mixed liquid is sprayed out of the spray pipe, the high-pressure mixed liquid contacts the spoiler arranged at the outlet of the spray pipe, and the spoiler is in a spiral shape, so that the spoiler rotates under the action of the mixed liquid flow, the mixed liquid at the outlet of the spray pipe is sprayed in a spiral shape, and further, when the mixed liquid impacts on raw material coal, the impact force on the raw material coal is complicated and diversified, so that the raw material coal is favorably crushed, the extraction of the crushed raw material coal by the solution is favorably realized, the content of effective components of sodium humate is favorably improved, and the prevention and promotion effects of the mixed pesticide fertilizer on crops are further improved.

Drawings

The invention will be further explained with reference to the drawings.

FIG. 1 is a schematic view of the overall structure of a hybrid reaction apparatus according to the present invention;

FIG. 2 is a schematic view of the internal structure of the mixing reaction apparatus of the present invention;

FIG. 3 is a front view of a mixing reaction apparatus according to the present invention;

FIG. 4 is a schematic view of the filter element of the present invention;

FIG. 5 is a schematic view of the structure of the nozzle of the present invention;

FIG. 6 is a schematic view of the connection of the nozzle of the present invention;

in the figure: the device comprises a mixing reaction device 1, a barrel body 11, a slag outlet 111, a liquid outlet 112, a liquid pumping outlet 113, a supporting plate 12, a supporting rod 13, a filtering piece 14, a first connecting ring 141, a second connecting ring 142, a connecting rod 143, a booster pump 15, a spray pipe 16, a transfusion ring 17, a baffle disc 2, a slag discharging disc 3, a rotating ring 4, a spoiler 41, a cover plate 5, a turning plate 51, a clutch 6 and a motor 7.

Detailed Description

In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.

A pesticide-fertilizer mixture containing validamycin and sodium humate comprises validamycin and sodium humate; 63-84 parts of validamycin A; 13-18 parts of sodium humate;

the production process of the sodium humate comprises the following steps:

s1: putting raw material coal into a mixed reaction device 1; the mixed reaction equipment 1 is used for crushing, reacting and extracting and carrying out solid-liquid separation on the placed raw material coal, a mixture of water and NaOH is added in the process, and a clear water-soluble sodium humate solution is obtained after a period of time;

s2: introducing the sodium humate solution obtained in the S1 mixed reaction equipment 1 into evaporation equipment; the evaporation equipment is used for concentrating and evaporating the sodium humate solution;

s3: putting the sodium humate obtained by concentrating and evaporating the S2 into drying equipment; the drying equipment is used for drying the concentrated sodium humate to obtain a refined sodium humate product.

When the fertilizer works, validamycin and sodium humate are mixed according to a certain proportion and are stabilized in a compound system by a certain process technology, so that a novel ecological compound fertilizer (drug fertilizer for short) is formed, because validamycin is an antibiotic produced by actinomycetes, has strong systemic property, is easily absorbed by thallus cells and quickly conducts in the thallus cells, interferes and inhibits the growth and development of the thallus cells, further has good prevention and treatment effects on various crops, and because the sodium humate can reduce the loss of ammoniacal nitrogen by the ammonium bicarbonate, the utilization rate of a nitrogen fertilizer is improved; can inhibit urease activity and reduce urea volatilization; can inhibit the fixation of water-soluble phosphorus by soil and promote the absorption of phosphorus by root systems; meanwhile, sodium humate and insoluble trace elements are subjected to chelation reaction, so that the trace elements can be absorbed by root systems and leaf surfaces; the sodium humate contains various functional groups, the activated sodium humate becomes a high-efficiency bioactive substance, and has an stimulating effect on the growth and development of crops and the physiological metabolism in vivo, the characteristic is not possessed by common fertilizers, and the high-efficiency bioactive substance of the activated sodium humate has obvious stimulating effect on various crops by adopting the modes of seed soaking, root dipping, spraying, irrigating, base fertilizer making and the like according to a certain concentration; comprehensively shows the promotion of root system development and the good influence on the crop yield and quality factors; therefore, the mixed pesticide fertilizer has nutritional fertilizer effect on crops and disease-resistant efficacy, and simultaneously has certain promotion effect on improving the yield of the crops and advancing the maturity time of the crops; the pesticide fertilizer combines two field operations of plant protection of pesticide and nutrient supply of fertilizer, saves labor force and reduces production cost; the sodium humate is prepared by the process, so that the steps of preparing the existing sodium humate are shortened, the investment of equipment is reduced, and the cost is saved; on the other hand, the content of the active ingredients of the prepared sodium humate is higher, so that the sodium humate content of the mixed pesticide fertilizer is higher under the same volume or weight, and the promotion effect on crops is improved under the condition of the same fertilizing amount.

As shown in fig. 1, 2, 3 and 6, the mixing reaction apparatus 1 includes a barrel 11, a support plate 12, a support rod 13, a filter member 14, a booster pump 15, a nozzle 16 and an infusion ring 17; the filtering piece 14 is arranged in the middle of the barrel body 11; the filter element 14 is of a cylindrical structure; a gap is reserved between the filtering piece 14 and the inner wall of the barrel body 11; (ii) a One end of the filtering member 14 is fixedly connected in the barrel body 11 and is close to the feeding end of the barrel body 11; the other end of the filter element 14 is provided with the support disc 12; the support disc 12 is rotatably connected to the filter element 14; the middle part of the supporting disc 12 is fixedly connected with the upper end of the supporting rod 13; the lower end of the support rod 13 is rotatably connected to the bottom of the barrel body 11; a slag outlet 111 is formed in the side wall of the barrel body 11; the slag outlet 111 is close to the bottom of the barrel body 11; a liquid outlet 112 is formed in the side wall of the barrel body 11; the liquid outlet 112 is arranged far away from the slag outlet 111; a liquid pumping port 113 is formed in the side wall of the barrel body 11 above the liquid outlet 112; the liquid pumping port 113 is higher than the liquid outlet 112; the liquid outlet 112 is higher than the slag outlet 111; the side wall of the barrel body 11 is fixedly connected with a mounting seat of the booster pump 15; the infusion ring 17 is sleeved on the side wall of the barrel body 11; the infusion ring 17 is fixedly connected to the barrel body 11; the liquid pumping port 113, the booster pump 15 and the infusion ring 17 are communicated through delivery pipes; the spray pipes 16 are uniformly arranged on the infusion ring 17 at intervals along the circumferential direction; one end of the spray pipe 16 is fixedly connected to the infusion ring 17; the other end of the spray pipe 16 penetrates through the barrel body 11 and the filter element 14; the outlet of the spout 16 is arranged tangentially to the edge of the support disc 12.

When the device works, firstly, raw coal materials are placed into the mixing reaction equipment 1, then the booster pump 15 is started, then the booster pump 15 pumps mixed liquid of water and NaOH, then the mixed liquid enters the liquid conveying ring 17 through a pipeline, then the mixed liquid is sprayed out from the orifice of the spray pipe 16 to form high-pressure mixed liquid flow, the sprayed liquid impacts on the raw coal, and then the raw coal is cracked under the impact force of the high-pressure liquid, so that the raw coal is crushed; in the process, the mixed liquid flows into the bottom of the barrel body 11 from the filter piece 14 and is deposited, when the mixed liquid in the barrel body 11 reaches a certain amount, the booster pump 15 starts to extract the liquid in the barrel body 11 to provide continuous power for crushing raw material coal, so that the larger granular raw material coal left after being filtered by the filter piece 14 is continuously crushed, meanwhile, the supporting plate 12 is driven to rotate under the combined action of liquid impact and moving raw material coal, so that the raw material coal on the supporting plate 12 is thrown to the filter piece 14 under the action of centrifugal force, the raw material coal is impacted on the filter piece 14, and then the raw material coal is crushed again, so that the crushing degree of the raw material coal is improved; meanwhile, the raw material coal is rubbed with the side wall of the filtering piece 14 in the movement process of the raw material coal, so that the raw material coal is further crushed, the crushing degree of the raw material coal is further improved, the extraction of humic acid in the raw material coal is facilitated, and the content of humate in a mixed solution is further improved; because the power of crushing is the mixed liquid of water and NaOH, the humic acid is extracted in the crushing process, the time required by the reaction is shortened, and the preparation efficiency of the sodium humate is improved; because the position of drawing liquid mouth 113 is higher, and then the disturbance to liquid lower floor in the staving 11 is less when the extraction, and then is favorable to subsiding of impurity in the mixed liquid, and then realizes separating the solid impurity in the mixed liquid.

As shown in fig. 2 and 3, a baffle disc 2 is arranged below the supporting disc 12; the baffle disc 2 is of a funnel-shaped structure; the outer wall of the baffle disc 2 is fixedly connected to the inner wall of the barrel body 11; a gap is reserved between the inner wall of the baffle disc 2 and the support rod 13; the side of the baffle disc 2 close to the supporting seat protrudes towards the bottom of the barrel body 11.

During operation, through setting up fender dish 2, and fender dish 2 becomes to leak hopper-shaped, and then mixed liquid assembles to bracing piece 13 one side along fender dish 2, flow into staving 11 afterwards, and then mixed liquid is close to bracing piece 13 in the staving 11 and makes the solid particle in the mixed liquid can subside fast to the in-process that flows to staving 11 lateral wall from staving 11, and then the solid particle that contains in the mixed liquid is close to staving 11 lateral wall department solution in the staving 11 has been reduced to mixed liquid, the mixed liquid has been avoided flowing into staving 11 from whole barrel lateral wall simultaneously, and then avoid disturbing the mixed liquid of upper strata in the staving 11, the solid particle that near mixed liquid upper strata department of staving 11 lateral wall contained has further been reduced, and then the solid particle in the mixed liquid has been reduced and has got into booster pump 15, and then the damage to booster pump 15 has been reduced, and then the life of booster pump 15 has been improved.

As shown in fig. 2 and 3, a slag discharging disc 3 is arranged on the inner surface of the bottom of the barrel body 11; the middle part of the slag discharging disc 3 is fixedly connected to the support rod 13; the outer wall of the slag discharging disc 3 is in contact with the inner wall of the barrel body 11; the slag discharging disc 3 is of a conical structure; the bottom of the conical structure of the slag discharging disc 3 is close to the bottom of the barrel body 11.

When the device works, the slag discharging disc 3 is arranged at the bottom of the barrel body 11, the slag discharging disc 3 is of a conical structure, and meanwhile, the slag discharging disc 3 rotates along with the supporting rod 13, so that the slag discharging disc 3 pushes solid particles deposited near the rotating rod to the side wall of the barrel body 11 in the rotating process, the solid particles at the supporting rod 13 are prevented from being deposited, the contact area of mixed liquid and raw material coal is increased, the extraction rate is increased, and the extraction time is shortened; meanwhile, the rotating slag discharging disc 3 pushes residual solid impurities after the reaction is finished, so that slag discharging is facilitated.

As shown in fig. 5, a rotating ring 4 is disposed in the nozzle tube 16 at a position close to the filter element 14; the rotating ring 4 is rotatably connected to the inner wall of the spray pipe 16; spoilers 41 are uniformly arranged in the rotating ring 4 at intervals along the circumferential direction; the spoiler 41 has a spiral shape.

The during operation, the spoiler 41 of contact setting in spray tube 16 exit when the mixed liquid of high pressure is spout from spray tube 16, because the spoiler 41 is the heliciform, and then spoiler 41 rotates under the effect of mixed liquid stream, and then make the mixed liquid of spray tube 16 exit become the heliciform blowout, and then when making the mixed liquid impact on raw material coal, the impact force that raw material coal received becomes complicated various, and then be favorable to the smashing of raw material coal, and then be favorable to the extraction of solution to the raw material coal after smashing, and then be favorable to improving the content of sodium humate active ingredient, and then improved the mixed back medical fertilizer and prevented and promoted the effect to crops.

As shown in fig. 2 to 4, the filter member 14 includes a first connecting ring 141, a second connecting ring 142 and a connecting rod 143; the first connecting ring 141 is fixedly connected to the barrel body 11; the second connecting ring 142 is rotatably connected with the support disc 12; the connecting rod 143 is obliquely arranged between the first connecting ring 141 and the second connecting ring 142; the connecting rods 143 are uniformly spaced along the circumferential direction of the first connecting ring 141 or the second connecting ring 142; the inner layer and the outer layer of the connecting rod 143 are arranged in two layers, and the inclined directions of the connecting rods 143 on the inner layer and the outer layer are opposite; a net structure is formed between the inner layer of connecting rods 143 and the outer layer of connecting rods 143; the welding points are formed at the junctions between the connecting rods 143 of the inner and outer layers by welding; the welding point is bulky and protrudes to the inner side.

When the device works, the high-pressure mixed liquid sprayed by the spray pipe 16 impacts on the raw material coal, so that the raw material coal is in friction and collision with the side wall of the net-shaped structure formed by the connecting rods 143 in the moving process, an auxiliary effect is provided for crushing the raw material coal, the time required for crushing the raw material coal is shortened, and the preparation efficiency of sodium humate is improved; make the junction of ectonexine connecting rod 143 link together through the welding, and then improved the intensity that forms network structure between the connecting rod 143, and then increased and filtered the life-span that 14 used, again because the bulky of welding point just to the inboard arch, and then make and filter 14 inner wall surface convex-concave uneven, and then increased and filtered friction and collision between 14 and the raw materials coal, and then improved the crushing degree to the raw materials coal, and then increased the area of contact of raw materials coal contact water and NaOH mixture, and then increased the speed to the extraction of the humic acid in the raw materials coal and the production of sodium humate.

As shown in fig. 1 to 3, a cover plate 5 is provided at the feed end of the tub 11; the middle part of the cover plate 5 is sunken downwards; a feed inlet is formed in the concave part; turning plates 51 are symmetrically arranged at the feed inlet; the ends of the turning plates 51 far away from each other are hinged on the cover plate 5; a torsion spring is arranged between the turning plate 51 and the cover plate 5.

During operation, pour the raw materials coal who prepares into the depressed part of apron 5, and then make under the effect of raw materials coal self gravity turn over board 51 and rotate, and then raw materials coal falls into staving 11 in, turn over board 51 and get back to initial position under the torsion effect of torsional spring afterwards, and then make feed inlet department sealed, and then prevent that 16 spun high-pressure mixed liquid from assaulting on raw materials coal and causing liquid and raw materials coal to fly away outside staving 11, and then avoid causing the waste.

As shown in fig. 1 to 3, the lower end of the support rod 13 passes through the bottom of the cylinder; the lower end of the supporting rod 13 is fixedly connected with the clutch 6; a motor 7 is arranged below the clutch 6; a rotating shaft of the motor 7 is fixedly connected to the clutch 6; and the mounting seat of the motor 7 is fixedly connected to the supporting leg of the cylinder body.

When the device works, when the raw material coal on the supporting plate 12 is less, the high-pressure water flow drives the supporting plate 12 to rotate to generate centrifugal force which is not enough to throw the residual raw material coal in the middle area of the supporting plate 12 to the filtering piece 14, so that the raw material coal cannot be completely crushed and enters mixed liquid below the barrel body 11 to be reacted and extracted, the content of sodium humate in the mixed liquid is reduced, the motor 7 and the clutch 6 are arranged to provide rotating power for the supporting plate 12, the centrifugal force on the residual raw material coal on the rotating plate is increased, the raw material coal is completely crushed and is ensured to react with the mixed liquid, the content of sodium humate in the mixed liquid is increased, the content of effective components in the refined sodium humate is increased, and the control and promotion effects of the pesticide fertilizer on crops are improved; meanwhile, the clutch 6 prevents the motor 7 from blocking the rotation of the supporting disc 12 before the centrifugal force generated by the rotation of the supporting disc 12 driven by high-pressure water flow is insufficient to throw the residual raw coal in the middle area of the supporting disc 12 to the filter element 14; after raw materials coal is smashed completely, booster pump 15 stop work, and then 3 stall of row's cinder pan, and then the solid impurity in the staving 11 can't continue to move around, and then can't continue to arrange the sediment, drive bracing piece 13 through motor 7 and rotate, and then drive row's cinder pan 3 and rotate, and then make the solid impurity in the staving 11 can continue to be got rid of, and then avoid remaining solid impurity in the staving 11 and the follow-up preparation of influence.

When the novel ecological compound fertilizer is in work, the validamycin and the sodium humate are mixed according to a certain proportion, and are stabilized in a compound system by a certain process technology, so that the novel ecological compound fertilizer, called drug fertilizer for short, is formed, because the validamycin is an antibiotic produced by actinomycetes, has strong systemic property, is easily absorbed by thallus cells and quickly conducts in the thallus cells, interferes and inhibits the growth and development of the thallus cells, further has good prevention and treatment effects on various crops, and because the sodium humate can reduce the loss of ammoniacal nitrogen by the ammonium bicarbonate, the utilization rate of the nitrogen fertilizer is improved; can inhibit urease activity and reduce urea volatilization; can inhibit the fixation of water-soluble phosphorus by soil and promote the absorption of phosphorus by root systems; meanwhile, sodium humate and insoluble trace elements are subjected to chelation reaction, so that the trace elements can be absorbed by root systems and leaf surfaces; the sodium humate contains various functional groups, the activated sodium humate becomes a high-efficiency bioactive substance, and has an stimulating effect on the growth and development of crops and the physiological metabolism in vivo, the characteristic is not possessed by common fertilizers, and the high-efficiency bioactive substance of the activated sodium humate has obvious stimulating effect on various crops by adopting the modes of seed soaking, root dipping, spraying, irrigating, base fertilizer making and the like according to a certain concentration; comprehensively shows the promotion of root system development and the good influence on the crop yield and quality factors; therefore, the mixed pesticide fertilizer has nutritional fertilizer effect on crops and disease-resistant efficacy, and simultaneously has certain promotion effect on improving the yield of the crops and advancing the maturity time of the crops; the pesticide fertilizer combines two field operations of plant protection of pesticide and nutrient supply of fertilizer, saves labor force and reduces production cost; the sodium humate is prepared by the process, so that the steps of preparing the existing sodium humate are shortened, the investment of equipment is reduced, and the cost is saved; on the other hand, the content of the active ingredients of the prepared sodium humate is higher, so that the sodium humate content of the mixed pesticide fertilizer is higher under the same volume or weight, and the promotion effect on crops is improved under the condition of the same fertilizing amount.

While the present invention has been described with reference to the embodiments shown in the drawings, the present invention is not limited to the embodiments, which are illustrative and not restrictive, and it will be apparent to those skilled in the art that various changes and modifications can be made therein without departing from the spirit and scope of the invention as defined in the appended claims.