阅读说明：本技术 一种电解用全氟离子交换膜的制备方法 (Preparation method of perfluorinated ion exchange membrane for electrolysis ) 是由 梁国富 于 2021-08-18 设计创作，主要内容包括：本发明公开了一种电解用全氟离子交换膜的制备方法,包括主体,所述主体的顶部中间位置设置有制备装置,所述制备装置的右侧外壁连通有进料斗,所述制备装置的顶部中间位置固定连接有驱动箱,所述制备装置的正面顶部右侧固定连接有控制面板,所述制备装置的正面顶部右侧设置有连通管道,本发明涉及离子交换膜技术领域。该电解用全氟离子交换膜的制备方法,有效的提高了装置传递的密封性,定位导向件与升降体的紧密贴合,使得辅助机构能够对其进行固定,从而增大了装置内部成型空间的控制,有效的保证了装置产出交换膜厚度的均匀性,便于内部进行间歇式的运动,防止生产机构工作时因大的杂质造成内部卡死的情况,有利于延长装置的使用寿命。(The invention discloses a preparation method of a perfluorinated ion exchange membrane for electrolysis, which comprises a main body, wherein a preparation device is arranged in the middle of the top of the main body, the outer wall of the right side of the preparation device is communicated with a feed hopper, the middle of the top of the preparation device is fixedly connected with a driving box, the right side of the top of the front of the preparation device is fixedly connected with a control panel, and the right side of the top of the front of the preparation device is provided with a communication pipeline. This preparation method of perfluor ion exchange membrane for electrolysis, the effectual leakproofness that has improved the device transmission, the inseparable laminating of location guide and the body that goes up and down for complementary unit can fix it, thereby has increased the control in device inside shaping space, and the effectual homogeneity that guarantees device output exchange membrane thickness, the motion of the intermittent type formula of being convenient for inside carries out, prevents to produce the dead condition of inside card because of big impurity causes of mechanism during operation, is favorable to the life of extension fixture.)

1. The preparation method of the perfluorinated ion exchange membrane for electrolysis comprises a main body (1), and is characterized in that: the top intermediate position of main part (1) is provided with preparation facilities (4), the right side outer wall intercommunication of preparation facilities (4) has feeder hopper (2), the top intermediate position fixedly connected with drive case (6) of preparation facilities (4), the positive top right side fixedly connected with control panel (3) of preparation facilities (4), the positive top right side of preparation facilities (4) is provided with intercommunication pipeline (5).

2. The method for preparing a perfluorinated ion exchange membrane for electrolysis according to claim 1, wherein the method comprises the following steps: preparation facilities (4) are including preparing case (41), the inner chamber bottom intermediate position of preparing case (41) is provided with location guide (42), the inner chamber bottom of preparing case (41) is located the both sides fixedly connected with complementary unit (44) of location guide (42), complementary unit (44) are close to one side top fixedly connected with the body (43) that goes up and down of location guide (42), the inner chamber top intermediate position of the body (43) that goes up and down is provided with production mechanism (45).

3. The method for preparing a perfluorinated ion exchange membrane for electrolysis according to claim 2, wherein the method comprises the following steps: the auxiliary mechanism (44) comprises a connecting block (441), a fastening column (442) is arranged at the middle position of the top of the connecting block (441), a middle fixing bracket (4444) is arranged at the middle position of the bottom of an inner cavity of the fastening column (442), a sealing column (445) is fixedly connected to the top of the fastening column (442), and auxiliary supporting plates (443) are fixedly connected to the two sides of the fastening column (442) at the bottom of the sealing column (445).

4. The method for preparing a perfluorinated ion exchange membrane for electrolysis according to claim 2, wherein the method comprises the following steps: the production mechanism (45) comprises a cleaning box (451), a screening frame (452) is fixedly connected to the middle portions of the inner walls of the two sides of the cleaning box (451), an installation part (453) is arranged in the middle of the top of the cleaning box (452), the bottom of the installation part (453) penetrates through the cleaning box (451) and extends to the inside of the cleaning box (451), a stabilizing seat (455) is fixedly connected to the bottom portions of the outer walls of the two sides of the cleaning box (451), and a communicating mechanism (454) is fixedly connected to the top portions of the stabilizing seat (455).

5. The method for preparing a perfluorinated ion exchange membrane for electrolysis according to claim 4, wherein the method comprises the following steps: UNICOM mechanism (454) are including reposition of redundant personnel case (d1), the both sides inner wall middle part of reposition of redundant personnel case (d1) is provided with reposition of redundant personnel (d4), the inner chamber bottom fixedly connected with baffler (d5) of reposition of redundant personnel case (d1), the top of baffler (d5) is located the both sides fixedly connected with bracing piece (d2) of reposition of redundant personnel body (d4), bracing piece (d2) are close to one side top fixedly connected with arc curb plate (d3) of reposition of redundant personnel body (d 4).

6. The method for preparing a perfluorinated ion exchange membrane for electrolysis according to claim 5, wherein the method comprises the following steps: and a diversion hole is formed in the position, close to the diversion box (d1), of the diversion body (d 4).

7. The method for preparing a perfluorinated ion exchange membrane for electrolysis according to claim 3, wherein the method comprises the following steps: the bottom of the fastening column (442) penetrates through the connecting block (441) and extends to the inside of the connecting block (441).

8. The method for preparing a perfluorinated ion exchange membrane for electrolysis according to claim 2, wherein the method comprises the following steps: the middle position of the bottom of the lifting body (43) is fixedly connected with the positioning guide piece (42).

9. A using method for preparing a perfluorinated ion exchange membrane for electrolysis is characterized by comprising the following steps: the method comprises the following steps: the equipment is installed, the feed hopper (2) is communicated with the preparation device (4), and the preparation device (4) is communicated with the main body (1) by using a communication pipeline (5);

step two: the material enters the device to be in contact with the positioning guide piece (42), and the positioning guide piece (42) is connected with the auxiliary mechanism (44) by the lifting body (43), so that the moving range of the material is controlled, and the material conveyed to the inside of the production mechanism (45) is accurately positioned;

step three: the sealing column (445) and the fastening column (442) are connected by the auxiliary supporting plate (443), the inner part is hollow, the middle fixing bracket (444) supports the inner part, and the sealing column (445) can be fixed in the vertical direction by the diameter of the sealing column being larger than that of the fastening column (442);

step four: communicating the communicating mechanism (454) with the cleaning box (451), connecting the cleaning box (451) with the screening rack (452), and dropping the surface impurities through a vibration structure generated by the mounting part (453) and the screening rack (452);

step five: the shunt fluid (d4) is fixed through a limited space generated by a stabilizing seat (d5) and a support rod (d2), the clamping force of the shunt fluid (d4) is adjusted in a micro-adjusting mode along with different stress of an elastic arc plate (d3), and the support rod (d2) is connected with a shunt box (d 1);

step six: utilize opening and shutting of body (43) control location guide (42) to drive installed part (453) and sieve frame (452) along with drive case (6) and carry out the minicollision, and be difficult for influencing the transport of material, make partial forming part carry out the spaced transmission.

Technical Field

The invention relates to the technical field of ion exchange membranes, in particular to a preparation method of a perfluorinated ion exchange membrane for electrolysis.

Background

Fluorine-containing ion exchange membranes are excellent in heat resistance, chemical resistance and the like, Electrolysis (Electrolysis) is a process of causing an oxidation-reduction reaction on a cathode plate and an anode plate by passing current through an electrolyte solution or a molten electrolyte (also called an electrolyte), an electrochemical cell can perform an Electrolysis process when a direct current voltage is applied, but impurities are easily adhered after production, the produced exchange membranes are easily deviated or uneven in thickness, the production quality of the device is reduced, large impurities inside the device easily cause damage of the device, and the service life of the device is shortened.

In conclusion, impurities are easy to adhere after production, the produced exchange membrane is easy to deviate or has uneven thickness, the production quality of the device is reduced, the device is easy to damage due to large impurities inside the device, and the service life of the device is shortened.

Disclosure of Invention

Technical problem to be solved

Aiming at the defects of the prior art, the invention provides a preparation method of a perfluorinated ion exchange membrane for electrolysis, which solves the problems that impurities are easy to adhere after production, the produced exchange membrane is easy to deviate or has uneven thickness, the production quality of a device is reduced, the device is easy to damage due to large impurities in the interior, and the service life of the device is shortened.

(II) technical scheme

In order to achieve the purpose, the invention is realized by the following technical scheme: the preparation method of the perfluorinated ion exchange membrane for electrolysis comprises a main body, wherein a preparation device is arranged in the middle of the top of the main body, the outer wall of the right side of the preparation device is communicated with a feed hopper, the middle of the top of the preparation device is fixedly connected with a drive box, the right side of the front top of the preparation device is fixedly connected with a control panel, and the right side of the front top of the preparation device is provided with a communicated pipeline.

Preferably, the preparation facilities is including preparing the case, the inner chamber bottom intermediate position of preparation case is provided with the location guide, the inner chamber bottom of preparation case is located the both sides fixedly connected with complementary unit of location guide, complementary unit is close to one side top fixedly connected with lift body of location guide, the inner chamber top intermediate position of the lift body is provided with production mechanism, through the inseparable laminating of location guide with the lift body for complementary unit can fix it, and the motion of the intermittent type formula of being convenient for is carried out to inside, prevents that production mechanism during operation from causing the dead condition of inside card because of big impurity.

Preferably, complementary unit includes the connecting block, the top intermediate position of connecting block is provided with the fastening post, the inner chamber bottom intermediate position of fastening post is provided with well solid support, the sealed post of top fixedly connected with of fastening post, the bottom of sealed post is located the supplementary fagging of both sides fixedly connected with of fastening post, has fine toughness can be to the device when fixed difficult direct contact to fastening post through supplementary fagging, and then has alleviateed the wearing and tearing of device long-term service time, and the cooperation of fastening post and connecting block is convenient for keep inside sufficient activity space.

Preferably, production mechanism includes the clean case, the both sides inner wall middle part fixedly connected with screening frame of clean case, the top intermediate position of clean case is provided with the installed part, the bottom of installed part runs through the clean case and extends to the inside of clean case, the stable seat of both sides outer wall bottom fixedly connected with of clean case, the top fixedly connected with UNICOM mechanism of stable seat, the impurity of scraping off through the screening frame is after the work is accomplished, and the installed part can descend and collide with the screening frame for impurity drops, thereby has guaranteed the inside cleanness, the effectual frictional force that alleviates the exchange membrane and remove the in-process.

Preferably, UNICOM's mechanism is including the reposition of redundant personnel case, the both sides inner wall middle part of reposition of redundant personnel case is provided with the reposition of redundant personnel, the inner chamber bottom fixedly connected with baffler of reposition of redundant personnel, the top of baffler is located the both sides fixedly connected with bracing piece of the reposition of redundant personnel, the bracing piece is close to one side top fixedly connected with arc curb plate of the reposition of redundant personnel, through the zonulae occludens of bracing piece and arc curb plate for some fluid fastening ranges in the impurity are convenient for carry out micro-adjustment, are favorable to carrying out the support of multi-angle to inside, and then have guaranteed inside stability.

Preferably, a diversion hole is formed in the position, close to the diversion box, of the diversion body.

Preferably, the bottom of the fastening column penetrates through the connecting block and extends to the inside of the connecting block.

Preferably, the middle position of the bottom of the lifting body is fixedly connected with the positioning guide piece.

A method for using a perfluorinated ion exchange membrane for electrolysis in preparation comprises the following steps: installing the equipment, communicating the feed hopper with the preparation device, and communicating the preparation device with the main body by using a communication pipeline;

step two: the material enters the device to contact with the positioning guide part, and the positioning guide part is connected with the auxiliary mechanism by using the lifting body, so that the moving range of the material is controlled, and the material conveyed to the interior of the production mechanism is accurately positioned;

step three: the sealing column and the fastening column are connected by using the auxiliary supporting plate, the inner part is hollow, the middle fixing support supports the inner part, and the sealing column can be fixed in the vertical direction by using the diameter of the sealing column larger than that of the fastening column;

step four: communicating the communicating mechanism with the cleaning box, connecting the cleaning box with the screening frame, and dropping surface impurities through a vibration structure generated by the mounting part and the screening frame;

step five: the fixing of the shunting body is carried out through a limiting space generated by the stabilizing seat and the supporting rod, the clamping force of the shunting body is adjusted in a micro-scale mode along with the different stress of the elastic arc plate, and the supporting rod is connected with the shunting box;

step six: utilize opening and shutting of body control location guide, along with the drive box drives the installed part and carries out the minicollision with the screening frame, and the difficult transport that influences the material makes partial formed part carry out the spaced transmission.

(III) advantageous effects

The invention provides a preparation method of a perfluorinated ion exchange membrane for electrolysis. The method has the following beneficial effects:

(I), this preparation method of perfluor ion exchange membrane for electrolysis, the feeder hopper has been set up, the intercommunication pipeline, the location guide, the body goes up and down, carrying out inside material and transporting fashioned in-process, the intercommunication pipeline communicates with production mechanism, the effectual leakproofness that improves the device transmission, the inseparable laminating of location guide and the body goes up and down, make complementary unit can fix it, thereby the control in device inside shaping space has been increased, the effectual homogeneity that has guaranteed device output exchange membrane thickness, the inside motion of carrying out the intermittent type formula of being convenient for, prevent that production mechanism during operation from causing the dead condition of inside card because of big impurity, be favorable to extension fixture's life.

(II), this preparation method of perfluor ion exchange membrane for electrolysis, through when carrying out impurity and dropping and clear up, the reposition of redundant personnel can guide the gas of reposition of redundant personnel incasement portion, the effectual inside clean scope that has increased, and the zonulae occludens of bracing piece and arc curb plate, make the partial fluid fastening scope in the impurity be convenient for carry out micro-regulation, be favorable to carrying out the support of multi-angle to inside, and then guaranteed the stability of inside, avoided inside to pile up too much impurity, it is convenient for the device to use.

(III), this preparation method of perfluor ion exchange membrane for electrolysis, through when exchanging the cleanness on membrane surface, a plurality of vertical spaces that the screening frame had are convenient for contact the volume of exchanging the membrane, the impurity that the screening frame was scraped off simultaneously is after work is accomplished, the installed part can descend and collide with the screening frame, make impurity drop, thereby guaranteed inside cleanness, the effectual frictional force that alleviates exchange membrane and remove the in-process, thereby the work efficiency of device has been increased when having improved the exchange membrane quality of output.

According to the preparation method of the perfluorinated ion exchange membrane for electrolysis, the shunt box is connected with the cleaning box, so that direct contact between a shunt body and the cleaning box can be avoided, impurities entering the shunt box are reduced, the collected impurities can be quickly cleaned, the constant temperature inside the device is effectively guaranteed, and continuous operation of the device is facilitated.

(five), this preparation method of perfluor ion exchange membrane for electrolysis, through carrying out the condition of device internal work at the material, well solid support and the inseparable laminating of fastening post, the effectual inside area of contact that has increased, the stability of device use has further been improved, supplementary fagging has fine toughness simultaneously and can be fixed the time difficult direct contact to the fastening post to the device, and then the wearing and tearing of device long-term during operation have been alleviateed, the cooperation of fastening post and connecting block can support inside, be convenient for keep inside sufficient activity space.

(VI) the preparation method of the perfluorinated ion exchange membrane for electrolysis can clear the interior within a range through the flow dividing box, thereby avoiding impurities from splashing and adhering to the surface of the fastening column, effectively reducing the condition that the efficiency of the electronic element is reduced as the impurities fall on the surface of the electronic element, avoiding the control of the working time of the device, and reducing the waiting time of workers

(VII) this preparation method of perfluor ion exchange membrane for electrolysis, through the cooperation of clean box and sealed post for the device is inside to carry out fine support, has avoided the loss of device during operation resource to appear, is favorable to guaranteeing the inside abundant contact of device, prevents simultaneously that impurity from appearing the phenomenon on adhesion exchange membrane surface again when just dropping, makes the device bottom have certain adsorptivity.

Drawings

FIG. 1 is a flow chart of a method for preparing a perfluorinated ion exchange membrane according to the present invention;

FIG. 2 is a schematic structural view of the present invention as a whole;

FIG. 3 is a schematic view of the structure of a manufacturing apparatus according to the present invention;

FIG. 4 is a schematic structural view of the auxiliary mechanism of the present invention;

FIG. 5 is a schematic structural view of a production mechanism of the present invention;

fig. 6 is a schematic structural view of a feed-through mechanism of the present invention.

In the figure: the device comprises a main body 1, a feed hopper 2, a control panel 3, a preparation device 4, a preparation box 41, a positioning guide 42, a lifting body 43, an auxiliary mechanism 44, a connecting block 441, a fastening column 442, an auxiliary supporting plate 443, a middle fixing bracket 444, a sealing column 445, a production mechanism 45, a clean box 451, a screening frame 452, a mounting part 453, a communication mechanism 454, a shunt box d1, a supporting rod d2, an elastic arc plate d3, a shunt body d4, a barrier plate d5, a stable seat 455, a communication pipeline 5 and a driving box 6.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The first embodiment is as follows:

referring to fig. 1-5, the present invention provides a technical solution: a preparation method of a perfluorinated ion exchange membrane for electrolysis comprises a main body 1, wherein a preparation device 4 is arranged at the middle position of the top of the main body 1, the outer wall of the right side of the preparation device 4 is communicated with a feed hopper 2, the middle position of the top of the preparation device 4 is fixedly connected with a driving box 6, the right side of the front top of the preparation device 4 is fixedly connected with a control panel 3, and the right side of the front top of the preparation device 4 is provided with a communicating pipeline 5.

Wherein, preparation facilities 4 is provided with location guide 42 including preparation case 41, the inner chamber bottom intermediate position of preparation case 41, and the inner chamber bottom of preparation case 41 is located the both sides fixedly connected with complementary unit 44 of location guide 42, and complementary unit 44 is close to one side top fixedly connected with elevating body 43 of location guide 42, and the inner chamber top intermediate position of elevating body 43 is provided with production mechanism 45.

The auxiliary mechanism 44 comprises a connecting block 441, a fastening column 442 is arranged at the middle position of the top of the connecting block 441, a middle fixing bracket (4444) is arranged at the middle position of the bottom of an inner cavity of the fastening column 442, a sealing column 445 is fixedly connected to the top of the fastening column 442, and auxiliary supporting plates 443 are fixedly connected to the bottom of the sealing column 445 at two sides of the fastening column 442.

Wherein, production mechanism 45 includes clean case 451, the both sides inner wall middle part fixedly connected with screening frame 452 of clean case 451, and the top intermediate position of clean case 452 is provided with installed part 453, and the bottom of installed part 453 runs through clean case 451 and extends to the inside of clean case 451, and the both sides outer wall bottom fixedly connected with of clean case 451 stabilizes seat 455, the top fixedly connected with UNICOM mechanism 454 of stabilizing seat 455.

Wherein, UNICOM mechanism 454 includes reposition of redundant personnel case d1, and the both sides inner wall middle part of reposition of redundant personnel case d1 is provided with reposition of redundant personnel d4, and the inner chamber bottom fixedly connected with baffler d5 of reposition of redundant personnel case d1, and baffler d 5's top is located the both sides fixedly connected with bracing piece d2 of reposition of redundant personnel d4, and bracing piece d2 is close to one side top fixedly connected with arc curb plate d3 of reposition of redundant personnel d 4.

Example two:

referring to fig. 1-5, on the basis of the first embodiment, the present invention provides a technical solution: a use method for preparing a perfluorinated ion exchange membrane for electrolysis comprises the following steps: the method comprises the following steps: the equipment is installed, the feed hopper 2 is communicated with the preparation device 4, and the preparation device 4 is communicated with the main body 1 by utilizing a communication pipeline 5;

step two: the materials enter the device to contact with the positioning guide piece 42, and the positioning guide piece 42 is connected with the auxiliary mechanism 44 by the lifting body 43, so that the moving range of the materials is controlled, and the materials conveyed to the inside of the production mechanism 45 are accurately positioned;

step three: the sealing column 445 and the fastening column 442 are connected by the auxiliary supporting plate 443, and the hollow of the inside is ensured, so that the inside is supported by the middle fixing bracket 444, and the sealing column 445 can be fixed in the vertical direction by the diameter of the sealing column 445 being larger than the diameter of the fastening column 442;

step four: the communicating mechanism 454 is communicated with the cleaning box 451, the cleaning box 451 is connected with the screening frame 452, and the impurities on the surface fall off through a vibration structure generated by the mounting part 453 and the screening frame 452;

step five: the shunting body d4 is fixed through a limited space generated by the stabilizing seat d5 and the supporting rod d2, the clamping force of the shunting body d4 is adjusted in a micro-adjustment mode along with different stress of the elastic arc plate d3, and the supporting rod d2 is connected with the shunting box d 1;

step six: utilize the body 43 that goes up and down to control opening and shutting of location guide 42, along with drive case 6 drives installed part 453 and sieve frame 452 and carries out the minicollision, and difficult influence the transport of material, make partial forming part carry out the spaced type transmission.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. The term "comprising", without further limitation, means that the element so defined is not excluded from the group consisting of additional identical elements in the process, method, article, or apparatus that comprises the element.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.