阅读说明：本技术 一种含环丙氟虫胺的杀虫剂及其应用 (Insecticide containing cyflumetofen and application thereof ) 是由 洪湖 相君成 周同磊 周丽琪 汪忠良 关龙 于 2020-11-05 设计创作，主要内容包括：本发明提供一种含环丙氟虫胺的杀虫剂及其应用,所述杀虫剂的有效成分为环丙氟虫胺,所述杀虫剂重量份以100份计,其中有效成份环丙氟虫胺重量为0.001-99.9份。本发明所述的杀虫剂低毒高效,用量少,速效性好,持效期长,能够有效防控如鳞翅目、鞘翅目、半翅目、缨翅目、双翅目、蜚蠊目、线虫等有害生物；因环丙氟虫胺作用机制新颖,对抗性害虫有效,是害虫抗性管理的重要工具。(The invention provides a cyflumetofen-containing pesticide and application thereof, wherein the effective component of the pesticide is cyflumetofen, and the weight of the pesticide is calculated by 100 parts, wherein the weight of the effective component of the cyflumetofen is 0.001-99.9 parts. The pesticide disclosed by the invention is low in toxicity and high in efficiency, small in dosage, good in quick-acting property and long in lasting period, and can be used for effectively preventing and controlling pests such as lepidoptera, coleoptera, hemiptera, thysanoptera, diptera, blattaria, nematodes and the like; the cyflumetofen has novel action mechanism, is effective to resistant pests and is an important tool for pest resistance management.)

1. The insecticide containing the cyflumetofen is characterized in that the active ingredient of the insecticide is the cyflumetofen, and the total weight of the insecticide is calculated by 100 parts, wherein the weight of the active ingredient cyflumetofen is 0.001-99.9 parts.

2. The cyflumetofen-containing pesticide as claimed in claim 1, wherein the pesticide comprises the effective component cyflumetofen in an amount of 0.01 to 95 parts by weight, preferably 0.05 to 80 parts by weight, based on 100 parts by weight.

3. The cyflumetofen-containing pesticide as claimed in claim 1 or 2, wherein the pesticide further comprises auxiliary components, and the auxiliary components comprise one or a combination of at least two of water, wetting agent, dispersing agent, emulsifier, co-emulsifier, stabilizer, penetrant, film forming agent, thickener, organic solvent, cosolvent, binder, disintegrant, solid inert carrier, antifreezing agent, colorant, preservative, plant powder, combustion improver, attractant, defoamer, synergist, plant essential oil, lubricant, encapsulating material, oxidant, fuel, smoke agent and fire retardant.

4. The clothianidin-containing insecticide according to any one of claims 1 to 3, wherein the wetting agent is one or a combination of at least two selected from fatty alcohol-polyoxyethylene ether, fatty amine-polyoxyethylene ether, trisiloxane polyoxyethylene ether, calcium dodecylbenzene sulfonate, sodium dodecyl sulfate, phenol sulfonate, sodium diisobutylnaphthalenesulfonate and polyoxyethylene ether phosphate;

preferably, the dispersing agent is selected from one or a combination of at least two of alkyl naphthalene sulfonate formaldehyde condensate, sodium lignosulfonate, alkylphenol polyoxyethylene phosphate, phenethyl phenol polyoxyethylene ether phosphate, phenyl phosphate triethanolamine salt, fatty alcohol polyoxyethylene ether phosphate, fatty alcohol polyoxyethylene ether succinic acid monoester sulfonic acid disodium salt, polycarboxylate, fatty alcohol polyoxypropylene polyoxyethylene ether, polyoxyethylene polyoxypropylene block copolymer, polyvinyl alcohol, polyvinylpyrrolidone or hydroxystearate polyoxyethylene ether;

preferably, the emulsifier is selected from one or a combination of at least two of fatty alcohol-polyoxyethylene ether, fatty amine-polyoxyethylene ether, polyaryl benzene-polyoxyethylene ether formaldehyde condensation, polyoxyethylene fatty acid ester, sorbitan fatty acid ester, polyoxyethylene ether sorbitan fatty acid ester, calcium dodecyl benzene sulfonate, castor oil polyoxyethylene ether, fatty acid ester sulfonate, fatty alcohol ether phosphate, alkylphenol polyoxyethylene ether phosphate, sodium alkyl succinate sulfonate or alkyl glycoside;

preferably, the coemulsifier is selected from one or a combination of at least two of butanol, isobutanol, dodecanol-1, tetradecanol-1, octadecanol-1, nonadecanol-1 or eicosanol-1;

preferably, the stabilizer is selected from one or a combination of at least two of isopropanol, alkyl glycol ether, epoxidized vegetable oil, epoxidized fatty acid ester, butyl hydroxy anisole, dibutyl hydroxy toluene, acetic acid or triethanolamine;

preferably, the penetrant is selected from one or a combination of at least two of fatty alcohol-polyoxyethylene ether, alkylphenol ethoxylate phosphate, alkylphenol ethoxylate sulfate, azone, rapid penetrant T, sulfonated castor oil or organosilicon;

preferably, the film forming agent is selected from one or a combination of at least two of chitosan and derivatives thereof, cellulose derivatives, gelatin, gum arabic, polyethylene glycol, polyvinyl alcohol, polyvinylpyrrolidone or polyacrylamide;

preferably, the thickening agent is selected from one or a combination of at least two of xanthan gum, magnesium aluminum silicate, white carbon black, gelatin, arabic gum, polyvinyl alcohol, polyvinylpyrrolidone, cellulose derivatives, chitin, organic bentonite or sodium alginate;

preferably, the organic solvent is selected from one or a combination of at least two of acetone, cyclohexanone, methyl isobutyl ketone, diethyl ether, ethylene glycol monobutyl ether, ethylene glycol diethyl ether, methanol, ethanol, propanol, isopropanol, butanol, isobutanol, isoamyl alcohol, octanol, isooctanol, ethylene glycol, propylene glycol, glycerol, liquefied propane, liquefied butane, ethyl acetate, butyl acetate, sec-butyl acetate, N-methylpyrrolidone, isophorone, hexamethyl tertiary amine phosphate, N-dimethylformamide, decanoamide, paraffin oil, mineral spirits, linseed oil, peanut oil, corn oil, sesame oil, palm oil, soybean oil or methyl oleate;

preferably, the cosolvent is selected from one or a combination of at least two of ethylene glycol, propylene glycol, n-butanol, glycerol, cyclohexanol, hexanol, octanol or methyl diglycol;

preferably, the binder is selected from one or a combination of at least two of starch, pregelatinized starch, gelatin, gum arabic, polyvinylpyrrolidone, cellulose derivatives, polyethylene glycol, polyvinyl alcohol, sucrose, or glucose;

preferably, the disintegrating agent is selected from one or a combination of at least two of sodium carboxymethyl starch, cross-linked sodium carboxymethyl cellulose, modified starch, cross-linked polyvinylpyrrolidone, ammonium sulfate, sodium chloride, ammonium chloride, fumed silica, magnesium aluminum silicate, organic bentonite or montmorillonite;

preferably, the solid inert carrier is selected from one or a combination of at least two of diatomite, attapulgite, clay, kaolin, bentonite, sepiolite, zeolite, white carbon black, light calcium carbonate, starch, magnesium stearate, sodium stearate, talcum powder, micro silica gel, mannitol, compressible starch, hydroxypropyl starch, dextrin hydroxypropyl methyl cellulose or cross-linked povidone;

preferably, the antifreeze is selected from one or a combination of at least two of ethylene glycol, propylene glycol, glycerol, sodium chloride or urea;

preferably, the colorant is selected from one or a combination of at least two of permanent red, amaranth, carmine, brilliant blue, pigment red, permanent yellow, benzidine yellow or sunset yellow;

preferably, the preservative is selected from one or a combination of at least two of sorbic acid, sodium sorbate, potassium sorbate, benzoic acid, sodium benzoate, carbazone or benzisothiazolinone;

preferably, the plant powder is selected from one or a combination of at least two of pyrethrum residue powder, wood powder, coconut shell powder, fir wood powder, oat powder, corn flour or wheat flour;

preferably, the combustion improver is selected from potassium nitrate and/or p-nitrophenol;

preferably, the attractant is selected from one or a combination of at least two of a mixture of cis-9-carbene, trimethylamine, isovaleraldehyde, ethanol and its derivatives, furanone, anisaldehyde, linoleic acid, linolenic acid, turpentine oil or camphor oil;

preferably, the defoaming agent is selected from one or a combination of at least two of polyether defoaming agent and silicone defoaming agent;

preferably, the synergist is selected from one or a combination of at least two of piperonyl butoxide, synergistic amine, octachlorodipropyl ether or synergistic phosphorus;

preferably, the plant essential oil is selected from one or a combination of at least two of olive oil, lavender oil, wintergreen oil, cardamom oil, geranium oil, lemon oil, clove oil, peppermint oil, cinnamon oil or eucalyptus oil;

preferably, the lubricant is selected from one or a combination of at least two of sodium stearate, magnesium stearate, glycerin or talc;

preferably, the encapsulating material is divided into an oily monomer and a water-based monomer, wherein the oily monomer is selected from one or a combination of at least two of polyphenyl polyisocyanate and alkyl diisocyanate, and the water-based monomer is selected from one or a combination of at least two of diethylenetriamine, triethylenetetramine and tetraethylenepentamine;

preferably, the oxidant is one or a combination of at least two of potassium chlorate, potassium nitrate, ammonium nitrate, sodium nitrite, sodium chlorate, potassium perchlorate or potassium permanganate;

preferably, the fuel is one or a combination of at least two of wood powder, sawdust, white sugar, starch, sulfur, thiourea and urotropine;

preferably, the smoke agent is one or a combination of at least two of ammonium chloride, naphthalene, hexachloroethane or hexachlorobenzene;

preferably, the fire retardant is one or a combination of at least two of sodium carbonate, sodium bicarbonate, pottery clay, talcum powder, limestone or calcium sulfate.

5. The clothianidin-containing insecticide according to any one of claims 1 to 4, the insecticide is characterized in that the insecticide is in the form of any one of powder, granules, pellets, tablets, strips, oil dispersion powder, wettable powder, emulsion powder, water dispersion granules, emulsion granules, water dispersion tablets, film-spreading oil agents, soluble liquid agents, soluble gum agents, oil agents, missible oil, latex, dispersible liquid agents, paste agents, emulsion in water, oil emulsions, microemulsions, fat agents, suspending agents, microcapsule suspension-suspoemulsion agents, oil suspending agents, dispersible oil suspending agents, seed treatment dry powder agents, seed treatment dispersible granules, seed treatment liquid agents, seed treatment emulsion agents, seed treatment suspending agents, aerosol, smoke agents, mosquito-repellent incense, bait agents, concentrated bait agents, mosquito-repellent emulsion, mosquito-repellent liquid, mosquito-repellent toilet water, ultra-low-volume liquid agents or hot fogging agents.

6. The clothianidin-containing insecticide according to any one of claims 1 to 5, wherein the insecticide is in the form of powder, wherein the auxiliary ingredients comprise a dispersant, a lubricant and a solid inert carrier; preferably, the powder comprises 0.01-95 parts of cyflumetofen as an effective component, 0.1-25 parts of a dispersant, 0.1-25 parts of a lubricant and the balance of a solid inert carrier, wherein the total weight of the pesticide is 100 parts by weight;

preferably, the pesticide is in the form of granules, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a disintegrating agent, a lubricant and a solid inert carrier; preferably, the granule comprises the effective component of cyflumetofen 0.001-99.9 parts, the wetting agent 0.1-8 parts, the dispersant 0.1-8 parts, the lubricant 0.1-5 parts and the balance of solid inert carrier, wherein the total weight of the insecticide is 100 parts by weight;

preferably, the pesticide is in the form of a ball agent, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a lubricant and a solid inert carrier; preferably, the total weight of the spherical pesticide is 100 parts by weight, wherein the effective component of the cyflumetofen is 0.1-95 parts, the wetting agent is 0.1-10 parts, the dispersing agent is 0.1-30 parts, the binding agent is 0.1-20 parts, the lubricating agent is 0.1-15 parts, and the balance is a solid inert carrier;

preferably, the pesticide is in the form of tablets, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a lubricant, and a solid inert carrier; preferably, the total weight of the tablet insecticide is 100 parts by weight, wherein the effective component of the cyflumetofen is 0.1-80 parts, the wetting agent is 0.1-15 parts, the dispersing agent is 0.1-25 parts, the binding agent is 0.1-15 parts, the lubricating agent is 0.1-10 parts, and the balance is a solid inert carrier;

preferably, the pesticide is a strip agent, and the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a lubricant and a solid inert carrier; preferably, the strip agent is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-80 parts, the wetting agent is 0.1-20 parts, the dispersing agent is 0.1-35 parts, the binding agent is 0.1-15 parts, the lubricating agent is 0.1-25 parts, and the balance is a solid inert carrier;

preferably, the formulation of the pesticide is oil-dispersed powder, wherein the auxiliary ingredients comprise an emulsifier, a dispersant, a solid inert carrier; preferably, the total weight of the oil dispersible powder pesticide is 100 parts by weight, wherein the effective component of the cyflumetofen is 0.1-50 parts, the emulsifier is 0.1-30 parts, the dispersant is 0.1-15 parts, and the balance is a solid inert carrier;

preferably, the dosage form of the pesticide is wettable powder, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent and a solid inert carrier; preferably, the wettable powder comprises 0.1 to 80 parts of cyflumetofen as an effective component, 0.1 to 20 parts of a wetting agent, 0.1 to 20 parts of a dispersing agent and the balance of a solid inert carrier, wherein the total weight of the pesticide is 100 parts by weight;

preferably, the pesticide is in the form of milk powder, wherein the auxiliary ingredients comprise an emulsifier, a dispersant, a binder and a solid inert carrier; preferably, the emulsion powder comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-80 parts of the active ingredient cyflumetofen, 0.1-15 parts of an emulsifier, 0.1-25 parts of a dispersant, 0.1-10 parts of a binder and the balance of a solid inert carrier;

preferably, the pesticide is in the form of water dispersible granules, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a disintegrating agent and a solid inert carrier; preferably, the water dispersible granule is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-80 parts, the wetting agent is 0.1-15 parts, the dispersing agent is 0.1-20 parts, the binding agent is 0.1-25 parts, the disintegrating agent is 0.1-20 parts, and the rest components are solid inert carriers;

preferably, the pesticide is in the form of emulsion granules, wherein the auxiliary ingredients comprise an emulsifier, a dispersant, an organic solvent, a lubricant and a solid inert carrier; preferably, the emulsion granule comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-80 parts of the active ingredient of the cyflumetofen, 0.1-20 parts of the emulsifier, 0.1-8 parts of the dispersant, 0.1-50 parts of the organic solvent, 0.1-15 parts of the lubricant and the balance of the solid inert carrier;

preferably, the pesticide is in the form of water dispersible tablet, wherein the auxiliary ingredients comprise wetting agent, dispersant, binder, disintegrant, lubricant, and solid inert carrier; preferably, the water dispersible tablet is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-80 parts, the wetting agent is 0.1-10 parts, the dispersing agent is 0.1-30 parts, the binding agent is 0.1-20 parts, the disintegrating agent is 0.1-15 parts, the lubricating agent is 0.1-25 parts, and the balance is a solid inert carrier;

preferably, the pesticide is in the form of a film-spreading oil agent, wherein the auxiliary components comprise a cosolvent, a water surface expanding agent and an organic solvent; preferably, the film-spreading oil agent comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-65 parts of the active ingredient cyflumetofen, 0.1-10 parts of the cosolvent, 1-20 parts of the emulsifier, and the balance of the organic solvent.

7. The clothianidin-containing insecticide according to any one of claims 1 to 6, wherein the insecticide is in a form of a soluble solution, wherein the auxiliary ingredients comprise an emulsifier, an organic solvent, water; preferably, the soluble solution comprises 0.1 to 55 parts of the effective component of the cyflumetofen, 0.1 to 40 parts of the emulsifier, 0.1 to 90 parts of the organic solvent and the balance of water, wherein the total weight of the pesticide is 100 parts by weight;

preferably, the pesticide is in the form of soluble gum, wherein the auxiliary components comprise a wetting agent, a penetrating agent, a cosolvent, an organic solvent and a thickening agent; preferably, the soluble gum agent is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the soluble gum agent is 0.1-75 parts of cyflumetofen, 0.1-10 parts of wetting agent, 0.1-10 parts of penetrating agent, 0.1-20 parts of cosolvent, 0.1-20 parts of organic solvent, and the balance of thickening agent;

preferably, the formulation of the pesticide is oil, wherein the auxiliary components comprise an emulsifier, a cosolvent and an organic solvent; preferably, the oil agent is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-80 parts, the emulsifier is 0.1-20 parts, the cosolvent is 0.1-15 parts, and the balance is an organic solvent;

preferably, the pesticide is in the form of emulsifiable concentrate, wherein the auxiliary components comprise an emulsifier, a cosolvent and an organic solvent; preferably, the missible oil is calculated by 100 parts by weight of the total pesticide, wherein the effective component of the cyflumetofen is 0.1-50 parts, the emulsifier is 0.1-40 parts, the cosolvent is 0.1-40 parts, and the balance is an organic solvent;

preferably, the pesticide is in the form of latex, wherein the auxiliary components comprise an emulsifier, a thickener, an organic solvent, a solid inert carrier and water; preferably, the emulsion comprises, by weight, 0.1-60 parts of cyflumetofen as an active ingredient, 0.1-25 parts of an emulsifier, 0.01-15 parts of a thickener, 0.1-60 parts of an organic solvent, 0.1-60 parts of a solid inert carrier and the balance of water, wherein the total weight of the insecticide is 100 parts;

preferably, the insecticide is in the form of a dispersible liquid, wherein the auxiliary ingredients comprise an emulsifier, an organic solvent; preferably, the dispersible agent comprises 0.1 to 70 parts of the effective component of the cyflumetofen, 0.1 to 35 parts of the emulsifier and the balance of the organic solvent, wherein the total weight of the pesticide is 100 parts by weight;

preferably, the pesticide is in the form of paste, wherein the auxiliary ingredients comprise an emulsifier, a thickener, an antifreeze and an organic solvent; preferably, the ointment comprises the effective components of 0.1-80 parts of cyflumetofen, 0.1-20 parts of emulsifier, 0.01-5 parts of thickener, 0.1-15 parts of antifreeze and the balance of water, wherein the total weight of the insecticide is 100 parts by weight;

preferably, the pesticide is in the form of an aqueous emulsion, wherein the auxiliary components comprise an emulsifier, a co-emulsifier, an antifreeze, a thickening agent, an organic solvent and water; preferably, the aqueous emulsion comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-50 parts of the active ingredient of the cyflumetofen, 0.1-30 parts of the emulsifier, 0.1-20 parts of the co-emulsifier, 0.1-20 parts of the antifreeze, 0.01-5 parts of the thickener, 0.1-50 parts of the organic solvent and the balance of water;

preferably, the formulation of the pesticide is oil emulsion, wherein the auxiliary components comprise emulsifier, co-emulsifier, antifreezing agent, thickener, water and organic solvent; preferably, the oil emulsion comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-50 parts of the active ingredient of the cyflumetofen, 0.1-35 parts of the emulsifier, 0.1-15 parts of the co-emulsifier, 0.1-20 parts of the antifreeze agent, 0.1-15 parts of the thickener, 0-50 parts of water and the balance of the organic solvent;

preferably, the pesticide is in the form of microemulsion, wherein the auxiliary components comprise emulsifier, co-emulsifier, antifreezing agent, organic solvent and water; preferably, the microemulsion is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-55 parts, the emulsifier is 0.1-30 parts, the co-emulsifier is 0.1-20 parts, the antifreezing agent is 0.1-10 parts, the organic solvent is 0.1-40 parts, and the balance is water;

preferably, the insecticide is in the form of a fatting agent, wherein the auxiliary ingredients comprise an emulsifier, a thickener and an organic solvent; preferably, the fat agent is calculated by 100 parts by weight of the total pesticide weight, wherein the effective component of the cyflumetofen is 1-50 parts, the emulsifier is 0.1-25 parts, the thickener is 0.01-10 parts, and the balance is vegetable oil;

preferably, the pesticide is in the form of a suspending agent, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a preservative, a thickening agent, an antifreezing agent and water; preferably, the suspending agent is calculated by the total weight of 100 parts of the pesticide, wherein the effective component of the suspending agent is 0.1-80 parts of cyflumetofen, 0.1-15 parts of wetting agent, 0.1-15 parts of dispersing agent, 0.01-5 parts of preservative, 0.01-5 parts of thickening agent, 0.1-15 parts of antifreezing agent and the balance of water;

preferably, the pesticide is in the form of microcapsule suspension, wherein the auxiliary ingredients comprise an oily encapsulating material, an aqueous encapsulating material, an organic solvent, a dispersing agent, a thickening agent and water; preferably, the microcapsule suspending agent comprises the effective component of 0.1-60 parts of cyflumetofen, 0.1-30 parts of oily encapsulating material, 0.1-30 parts of aqueous encapsulating material, 0.1-50 parts of organic solvent, 0.1-20 parts of dispersant, 0.01-5 parts of thickening agent and the balance of water, wherein the total weight of the pesticide is 100 parts by weight;

preferably, the pesticide is in the form of microcapsule suspension-suspoemulsion, wherein the auxiliary ingredients comprise oily capsule-forming materials, aqueous capsule-forming materials, organic solvents, emulsifiers, dispersants, thickeners, and water; preferably, the microcapsule suspension-suspoemulsion comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-60 parts of the active ingredient of the cyprocomiamide, 0.1-25 parts of the oily encapsulating material, 0.1-25 parts of the aqueous encapsulating material, 0.1-60 parts of the organic solvent, 0.1-20 parts of the emulsifier, 0.1-15 parts of the dispersant, 0.01-5 parts of the thickener, and the balance of water;

preferably, the pesticide is in the form of oil suspending agent, wherein the auxiliary components comprise emulsifier, dispersant, thickener and organic solvent; preferably, the oil suspending agent is calculated by 100 parts by weight of the total weight of the insecticide, wherein the effective component of the ciprofloxacin is 0.1-55 parts, the emulsifier is 0.1-25 parts, the dispersant is 0.1-10 parts, the thickening agent is 0.01-10 parts, and the balance is organic solvent;

preferably, the pesticide is in the form of dispersible oil suspending agent, wherein the auxiliary ingredients comprise emulsifier, dispersant, thickener and organic solvent; preferably, the dispersible oil suspending agent is calculated by 100 parts by weight of the total weight of the insecticide, wherein the effective component of the cyflumetofen is 0.1-65 parts, the emulsifier is 0.1-30 parts, the dispersant is 0.1-15 parts, the thickener is 0.01-10 parts, and the balance is organic solvent;

preferably, the pesticide is in a dosage form of dry powder for seed treatment, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a film forming agent, a lubricating agent, a coloring agent and a solid inert carrier; preferably, the seed treatment dry powder agent is calculated by the total weight of the pesticide as 100 parts by weight, wherein the effective component of the cyflumetofen is 0.1-80 parts, the wetting agent is 0.1-15 parts, the dispersing agent is 0.1-25 parts, the film forming agent is 0.1-10 parts, the lubricating agent is 0.1-20 parts, the coloring agent is 0.1-10 parts, and the balance is a solid inert carrier;

preferably, the pesticide is in the form of seed treatment dispersible granules, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a disintegrating agent, a film forming agent, a coloring agent and a solid inert carrier; preferably, the dispersible granule for seed treatment comprises the effective components of 0.1-80 parts of cyflumetofen, 0.1-10 parts of wetting agent, 0.1-20 parts of dispersing agent, 0.1-15 parts of binding agent, 0.1-15 parts of disintegrating agent, 0.1-15 parts of film forming agent, 0.1-15 parts of coloring agent and the balance of solid inert carrier, wherein the total weight of the insecticide is 100 parts by weight;

preferably, the pesticide is in the form of a seed treatment liquid, wherein the auxiliary components comprise an emulsifier, a film forming agent, a colorant, an organic solvent and water; preferably, the seed treatment liquid comprises, by weight, 0.1-70 parts of cyflumetofen, 0.1-45 parts of an emulsifier, 0.1-30 parts of a film-forming agent, 0.1-25 parts of a colorant, 0.1-50 parts of an organic solvent and the balance of water, based on 100 parts of the total weight of the pesticide;

preferably, the pesticide is in the form of a seed treatment emulsion, wherein the auxiliary ingredients comprise an organic solvent, an emulsifier, a dispersant, a film forming agent, a thickener, a colorant, an organic solvent and water; preferably, the seed treatment emulsion comprises the effective components of 0.1-60 parts of cyflumetofen, 0.1-35 parts of emulsifier, 0.1-15 parts of dispersant, 0.1-15 parts of film forming agent, 0.01-15 parts of thickening agent, 0.01-25 parts of colorant, 0.1-40 parts of organic solvent and the balance of water, wherein the total weight of the pesticide is 100 parts by weight;

preferably, the pesticide is in the form of a seed treatment suspending agent, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a film forming agent, a thickening agent, an antifreezing agent, a coloring agent and water; preferably, the seed treatment suspending agent is calculated by 100 parts of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-80 parts; 0.1-15 parts of wetting agent, 0.1-20 parts of dispersing agent, 0.01-15 parts of film forming agent, 0.01-5 parts of thickening agent, 0.1-15 parts of antifreezing agent, 0.01-15 parts of coloring agent and the balance of water;

preferably, the pesticide is in the form of aerosol, wherein the auxiliary ingredients comprise an emulsifier, a synergist, an organic solvent and water; preferably, the aerosol comprises, by weight, 100 parts of the total weight of the pesticide, 0.001-20 parts of the active ingredient cyflumetofen, 0.1-30 parts of an emulsifier, 0.1-18 parts of a synergist, 0.1-80 parts of an organic solvent, and the balance of water;

preferably, the pesticide is in the form of smoke agent, wherein the auxiliary components comprise an oxidant, a fuel, a smoke agent and a fire retardant; preferably, the smoke agent is calculated by 100 parts by weight of the total pesticide, wherein the effective component of the cyflumetofen is 0.1-60 parts, the oxidant is 0.1-55 parts, the fuel is 0.1-45 parts, the smoke agent is 0.1-65 parts, and the balance is fire retardant;

preferably, the pesticide is in the form of mosquito-repellent incense, wherein the auxiliary components comprise a binder, a preservative, a combustion improver and plant powder; preferably, the mosquito-repellent incense comprises the effective component of 0.001-10 parts of cyflumetofen, 0.1-40 parts of binder, 0.01-5 parts of preservative, 0.1-10 parts of combustion improver and the balance of plant powder, wherein the total weight of the pesticide is 100 parts by weight;

preferably, the pesticide is in the form of bait, wherein the auxiliary ingredients comprise a binder, an attractant, a synergist, a preservative, a lubricant, a colorant and water; preferably, the bait agent is calculated by 100 parts of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.001-50 parts; 0.1-5 parts of attractant, 0.1-20 parts of binder, 0.1-10 parts of synergist, 0.1-5 parts of preservative, 0.1-20 parts of lubricant, 0.1-10 parts of colorant, 0.1-20 parts of water and the balance of plant powder;

preferably, the pesticide is in the form of concentrated bait, wherein the auxiliary ingredients comprise a dispersing agent, an attractant, a synergist, a preservative, a colorant and water; preferably, the concentrated bait agent is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the concentrated bait agent is 0.001-55 parts of cyflumetofen, 0.1-25 parts of dispersant, 0.1-90 parts of attractant, 0.1-30 parts of synergist, 0.1-5 parts of preservative, 0.1-15 parts of colorant and the balance of water;

preferably, the formulation of the pesticide is mosquito repellent milk, wherein the auxiliary components comprise an emulsifier, an organic solvent, plant essential oil and water; preferably, the mosquito repellent emulsion is calculated by taking the total weight of the insecticide as 100 parts by weight, wherein the effective component of the cyflumetofen is 0.001-50 parts; 0.1-25 parts of emulsifier, 0.1-65 parts of organic solvent, 0.1-20 parts of vegetable essential oil and the balance of water;

preferably, the formulation of the pesticide is mosquito repellent liquid, wherein the auxiliary components comprise an organic solvent, plant essential oil and water; preferably, the mosquito repellent liquid is calculated by 100 parts by weight of the total weight of the insecticide, wherein the effective component of the cyflumetofen is 0.001-40 parts, the organic solvent is 0.1-50 parts, the vegetable essential oil is 0.1-25 parts, and the balance is water;

preferably, the formulation of the pesticide is mosquito repellent floral water, wherein the auxiliary components comprise an organic solvent, plant essential oil and water; preferably, the mosquito repellent floral water comprises, by weight, 100 parts of total pesticide weight, 0.001-40 parts of cyflumetofen as an effective ingredient, 0.1-20 parts of an organic solvent, 0.1-15 parts of plant essential oil and the balance of water;

preferably, the formulation of the pesticide is an ultra-low volume liquid formulation, wherein the auxiliary ingredients comprise a wetting agent, an osmotic agent, and an organic solvent; preferably, the ultra-low volume liquid comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-85 parts of the active ingredient ciprofloxacin, 0.1-25 parts of the wetting agent, 0.1-25 parts of the penetrating agent, and the balance of the organic solvent;

preferably, the formulation of the pesticide is a hot fogging concentrate, wherein the auxiliary components comprise an emulsifier, a synergist, a cosolvent and an organic solvent; preferably, the hot fogging concentrate comprises 0.1-50 parts of cyflumetofen, which is an effective component, by weight based on 100 parts of the total weight of the insecticide; 0.1-30 parts of emulsifier, 0.1-35 parts of synergist, 0.1-15 parts of cosolvent and the balance of organic solvent.

8. Use of the cyflumetofen-containing pesticide as claimed in any one of claims 1 to 7 in the control of insect pests in crops.

9. Use of the clothianidin-containing insecticide according to any one of claims 1 to 7 for the control of sanitary pests in the environment.

10. Use of a cyflumetofen-containing insecticide as claimed in any one of claims 1 to 7 in the treatment and prevention and control of pests.

Technical Field

The invention belongs to the technical field of insecticides, and relates to an insecticide containing cyflumetofen and application thereof.

Background

The cyhalofop-butyl is a creative insecticide independently developed by Nantong Taihe chemical industry Co., Ltd, has a novel chemical structure and a unique action mechanism, has the effects of stomach toxicity, contact killing, systemic absorption and the like, has excellent insecticidal activity on target pests, has interactive resistance with common insecticides, is safe to crops, high in safety to users, good in environmental compatibility and high in safety to aquatic organisms such as beneficial insects, fishes and shrimps in a rice field.

The cyflumetofen has the advantages of wide insecticidal spectrum, good insecticidal effect and quick response, and has excellent performance in the aspects of preventing and controlling pests in the field of crop protection and preventing and controlling pests in the field of public health pests. Can be used for various crops such as rice, corn, wheat, potato, soybean, cotton, sugarcane, fruit trees, vegetables, flowers, woods, gardening and the like, and can prevent and treat insect pests, mites, nematodes and the like.

The ciprofloxacin is used for controlling pests such as chilo suppressalis, rice leaf roller, tryporyza incertulas, sesamia inferens, rice thrips, rice weevil, rice gall midge, corn borer, spodoptera frugiperda, armyworm, stinkbug, cotton bollworm, armyworm, sucking worm, cabbage caterpillar, pod borer, spodoptera exigua, prodenia litura, inchworm, weevil, flea beetle, scarab beetle, leaf miner, leafhopper, aphid, scale insect, plant hopper, bemisia tabaci, thrips, red spider, mole cricket, grub, cutworm, wireworm, root maggot, root knot nematode and the like, acarid, nematode and the like; also can be used for preventing and controlling public health pests such as mosquitoes, flies, ants, cockroaches and the like. The cyflumetofen has unique action mechanism and obvious control effect on resistant pests, and is an important tool for controlling the resistance of the pests.

The ciprofloxacin is safe to people and livestock, and the result of a hygropathy test shows that the acute oral administration, the acute transdermal administration and the acute inhalation are all in a micro-toxicity level, and the Ames test result is negative. The cyflumetofen is friendly to environmental organisms, and the result of environmental biological toxicology tests shows that the cyflumetofen has low risk to aquatic organisms.

The pests cause a great deal of economic loss every year, and the self drug resistance of the pests also tends to increase year by year. Therefore, the research and development of new insecticides with novel structure, high activity and high safety are particularly important.

Disclosure of Invention

Aiming at the defects of the prior art, the invention aims to provide a cyflumetofen-containing pesticide and application thereof.

In order to achieve the purpose, the invention adopts the following technical scheme:

in one aspect, the invention provides a cyflumetofen-containing pesticide, wherein the active ingredient of the pesticide is cyflumetofen, and the total weight of the pesticide is 100 parts, wherein the weight of the active ingredient cyflumetofen is 0.001-99.9 parts.

In the invention, the cyflumetofen is a low-toxicity, high-efficiency and low-residue pesticide with a molecular formula C₂₈H₁₇BrF₁₂N₂O₂Relative molecular weight 721.34, CAS number 2375110-88-4, as white solid powder in appearance; the structural formula is shown as formula I:

in the present invention, the insecticide may be composed of, based on 100 parts by weight, cyflumetofen as an active ingredient in an amount of 0.001 part, 0.003 part, 0.005 part, 0.01 part, 0.05 part, 0.1 part, 0.5 part, 1 part, 3 parts, 5 parts, 8 parts, 10 parts, 20 parts, 25 parts, 30 parts, 40 parts, 50 parts, 60 parts, 70 parts, 80 parts, 90 parts, 95 parts or 99.9 parts, preferably 0.01 to 95 parts, and more preferably 0.05 to 80 parts.

In the present invention, the insecticide further contains an auxiliary component in order to sufficiently exert the insecticidal effect of the insecticide. The auxiliary components of the invention are selected from different components and used in different dosage forms, but are within the scope of the accepted or legal requirements.

Preferably, the pesticide also contains auxiliary components, wherein the auxiliary components comprise one or a combination of at least two of water, a wetting agent, a dispersing agent, an emulsifier, a co-emulsifier, a stabilizer, a penetrating agent, a film forming agent, a thickening agent, an organic solvent, a cosolvent, a binder, a disintegrating agent, a solid inert carrier, an antifreezing agent, a coloring agent, a preservative, plant powder, a combustion improver, an attractant, an antifoaming agent, a synergist, plant essential oil, a lubricant, an encapsulating material, an oxidant, fuel, a smoke agent and a fire retardant.

The invention has no special requirement on auxiliary components, and proper components are selected according to the requirement. For example, the wetting agent may be preferably selected from one or a combination of at least two of fatty alcohol-polyoxyethylene ether, fatty amine-polyoxyethylene ether, trisiloxane-polyoxyethylene ether, calcium dodecylbenzene sulfonate, sodium dodecyl sulfate, phenol sulfonate, sodium diisobutylnaphthalene sulfonate, and polyoxyethylene ether phosphate.

Preferably, the dispersing agent can be selected from one or a combination of at least two of alkyl naphthalene sulfonate formaldehyde condensate, sodium lignosulfonate, alkylphenol polyoxyethylene phosphate, phenethyl phenol polyoxyethylene ether phosphate, phenyl phosphate triethanolamine salt, fatty alcohol polyoxyethylene ether phosphate, fatty alcohol polyoxyethylene ether succinic acid monoester sulfonic acid disodium salt, polycarboxylate, fatty alcohol polyoxypropylene polyoxyethylene ether, polyoxyethylene polyoxypropylene block copolymer, polyvinyl alcohol, polyvinyl pyrrolidone or hydroxystearate polyoxyethylene ether.

Preferably, the emulsifier can be selected from one or a combination of at least two of fatty alcohol polyoxyethylene ether, fatty amine polyoxyethylene ether, polyaryl benzene polyoxyethylene ether formaldehyde condensation, polyoxyethylene fatty acid ester, sorbitan fatty acid ester, polyoxyethylene ether sorbitan fatty acid ester, calcium dodecyl benzene sulfonate, castor oil polyoxyethylene ether, fatty acid ester sulfonate, fatty alcohol ether phosphate, alkylphenol polyoxyethylene ether phosphate, alkyl succinate sodium sulfonate or alkyl glycoside.

Preferably, the co-emulsifier may be selected from one or a combination of at least two of butanol, isobutanol, dodecanol-1, tetradecanol-1, octadecanol-1, nonadecanol-1 or eicosanol-1.

Preferably, the stabilizer may be selected from one or a combination of at least two of isopropyl alcohol, alkyl glycol ether, epoxidized vegetable oil, epoxidized fatty acid ester, butyl hydroxy anisole, dibutyl hydroxy toluene, acetic acid or triethanolamine.

Preferably, the penetrant can be selected from one or a combination of at least two of fatty alcohol-polyoxyethylene ether, alkylphenol ethoxylate phosphate, alkylphenol ethoxylate sulfate, azone, sodium diisooctyl succinate sulfonate, sulfonated castor oil or organic silicon.

Preferably, the film forming agent may be selected from one or a combination of at least two of chitosan and its derivatives, cellulose derivatives, gelatin, gum arabic, polyethylene glycol, polyvinyl alcohol, polyvinylpyrrolidone, or polyacrylamide.

Preferably, the thickener can be selected from one or a combination of at least two of xanthan gum, magnesium aluminum silicate, white carbon black, gelatin, arabic gum, polyvinyl alcohol, polyvinylpyrrolidone, cellulose derivatives, chitin, organic bentonite or sodium alginate.

Preferably, the organic solvent may be selected from one or a combination of at least two of acetone, cyclohexanone, methyl isobutyl ketone, diethyl ether, ethylene glycol monobutyl ether, ethylene glycol diethyl ether, methanol, ethanol, propanol, isopropanol, butanol, isobutanol, isoamyl alcohol, octanol, isooctanol, ethylene glycol, propylene glycol, glycerol, liquefied propane, liquefied butane, ethyl acetate, butyl acetate, sec-butyl acetate, N-methylpyrrolidone, isophorone, hexamethyl tertiary amine phosphate, N-dimethylformamide, decanoamide, paraffin oil, mineral spirits, linseed oil, peanut oil, corn oil, sesame oil, palm oil, soybean oil, or methyl oleate.

Preferably, the cosolvent may be selected from one or a combination of at least two of ethylene glycol, propylene glycol, n-butanol, glycerol, cyclohexanol, hexanol, octanol, or methyl diethylene glycol.

Preferably, the binder may be selected from one or a combination of at least two of starch, pregelatinized starch, gelatin, gum arabic, polyvinylpyrrolidone, cellulose derivatives, polyethylene glycol, polyvinyl alcohol, sucrose, or glucose.

Preferably, the disintegrant may be selected from one or a combination of at least two of sodium carboxymethyl starch, sodium cross-linked carboxymethyl cellulose, modified starch, cross-linked polyvinylpyrrolidone, ammonium sulfate, sodium chloride, ammonium chloride, fumed silica, magnesium aluminum silicate, organobentonite or montmorillonite.

Preferably, the solid inert carrier may be selected from one or a combination of at least two of diatomaceous earth, attapulgite, clay, kaolin, bentonite, sepiolite, zeolite, white carbon, precipitated calcium carbonate, starch, magnesium stearate, sodium stearate, talc, aerosil, mannitol, compressible starch, hydroxypropyl starch, dextrin hydroxypropyl methylcellulose, or crospovidone.

Preferably, the antifreeze agent can be selected from one or a combination of at least two of ethylene glycol, propylene glycol, glycerol, sodium chloride or urea.

Preferably, the colorant may be selected from one or a combination of at least two of permanent red, amaranth, carmine, brilliant blue, pigment red, permanent yellow, benzidine yellow or sunset yellow.

Preferably, the preservative may be selected from one or a combination of at least two of sorbic acid, sodium sorbate, potassium sorbate, benzoic acid, sodium benzoate, carbazone, or benzisothiazolinone.

Preferably, the plant powder may be selected from one or a combination of at least two of pyrethrum residue powder, wood powder, coconut shell powder, fir wood powder, oat powder, corn flour or wheat flour.

Preferably, the combustion improver can be selected from potassium nitrate and/or p-nitrophenol.

Preferably, the attractant may be selected from one or a combination of at least two of a mixture of cis-9-carbene, trimethylamine, isovaleraldehyde, ethanol and its derivatives, furanone, anisaldehyde, linoleic acid, linolenic acid, turpentine, or camphor oil.

Preferably, the defoaming agent may be selected from one of a polyether-based defoaming agent, a silicone-based defoaming agent, or a combination of at least two thereof.

Preferably, the synergist can be selected from one or a combination of at least two of piperonyl butoxide, synergist amine, octachlorodipropyl ether or synergist phosphorus.

Preferably, the plant essential oil can be selected from one or a combination of at least two of olive oil, lavender oil, wintergreen oil, cardamom oil, geranium oil, lemon oil, clove oil, peppermint oil, cinnamon oil or eucalyptus oil.

Preferably, the lubricant may be selected from one or a combination of at least two of sodium stearate, magnesium stearate, glycerol or talc.

Preferably, the encapsulating material is divided into an oily monomer and a water-based monomer, wherein the oily monomer can be selected from one or a combination of at least two of polyphenyl polyisocyanate or alkyl diisocyanate, and the water-based monomer can be selected from one or a combination of at least two of diethylenetriamine, triethylene tetramine or tetraethylene pentamine;

preferably, the oxidant is one or a combination of at least two of potassium chlorate, potassium nitrate, ammonium nitrate, sodium nitrite, sodium chlorate, potassium perchlorate or potassium permanganate;

preferably, the fuel is one or a combination of at least two of wood powder, sawdust, white sugar, starch, sulfur, thiourea and urotropine;

preferably, the smoke agent is one or a combination of at least two of ammonium chloride, naphthalene, hexachloroethane or hexachlorobenzene;

preferably, the fire retardant is one or a combination of at least two of sodium carbonate, sodium bicarbonate, pottery clay, talcum powder, limestone or calcium sulfate;

preferably, the pesticide is in the form of any one of powder, granules, pellets, tablets, strips, oil dispersion powder, wettable powder, emulsion powder, water dispersion granules, emulsion granules, water dispersion tablets, film-spreading oil agents, soluble liquid agents, soluble gum agents, oil agents, missible oil, latex, dispersible liquid agents, paste agents, emulsion in water, oil emulsions, microemulsions, fatting agents, suspending agents, microcapsule suspension-suspoemulsion agents, oil suspending agents, dispersible oil suspending agents, seed treatment dry powder agents, seed treatment dispersible granules, seed treatment liquid agents, seed treatment emulsion agents, seed treatment suspension agents, aerosol, smoke agents, mosquito-repellent incense, bait agents, concentrated bait agents, mosquito-repellent milk, mosquito-repellent liquid, mosquito-repellent toilet water, ultra-low volume liquid agents or hot fogging agents.

Preferably, the formulation of the pesticide of the present invention is a powder, wherein the auxiliary ingredients comprise a dispersant, a lubricant and a solid inert carrier.

Preferably, the powder comprises 0.01-95 parts of cyflumetofen as an effective component, 0.1-25 parts of a dispersant, 0.1-25 parts of a lubricant and the balance of a solid inert carrier, wherein the total weight of the pesticide is 100 parts by weight.

Preferably, the dosage form of the pesticide of the invention is granules, wherein the auxiliary components comprise wetting agents, dispersing agents, binding agents, disintegrating agents, lubricating agents and solid inert carriers. Preferably, the granule comprises the effective component of cyflumetofen 0.001-99.9 parts, the wetting agent 0.1-8 parts, the dispersant 0.1-8 parts, the lubricant 0.1-5 parts and the balance of solid inert carrier, wherein the total weight of the pesticide is 100 parts by weight.

Preferably, the pesticide is in the form of a sphere, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a lubricant and a solid inert carrier. Preferably, the total weight of the spherical pesticide is 100 parts by weight, wherein the effective component of the cyflumetofen is 0.1-95 parts, the wetting agent is 0.1-10 parts, the dispersing agent is 0.1-30 parts, the binding agent is 0.1-20 parts, the lubricating agent is 0.1-15 parts, and the balance is a solid inert carrier.

Preferably, the formulation of the pesticide is a tablet, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a lubricant, and a solid inert carrier. Preferably, the total weight of the tablet insecticide is 100 parts by weight, wherein the effective component of the cyflumetofen is 0.1-80 parts, the wetting agent is 0.1-15 parts, the dispersing agent is 0.1-25 parts, the binding agent is 0.1-15 parts, the lubricating agent is 0.1-10 parts, and the balance is a solid inert carrier.

The pesticide of the invention can be prepared into a strip agent, and the auxiliary components can comprise a wetting agent, a dispersing agent, a binder, a lubricant and a solid inert carrier; preferably, the strip agent comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-80 parts of the active ingredient cyflumetofen, 0.1-20 parts of a wetting agent, 0.1-35 parts of a dispersing agent, 0.1-15 parts of a binding agent, 0.1-25 parts of a lubricating agent and the balance of a solid inert carrier.

Preferably, the formulation of the pesticide is oil-dispersed powder, wherein the auxiliary ingredients comprise an emulsifier, a dispersant, a solid inert carrier; preferably, the total weight of the oil dispersible powder pesticide is 100 parts by weight, wherein the effective component of the cyflumetofen is 0.1-50 parts, the emulsifier is 0.1-30 parts, the dispersant is 0.1-15 parts, and the balance is a solid inert carrier.

Preferably, the dosage form of the pesticide is wettable powder, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent and a solid inert carrier; preferably, the wettable powder comprises 0.1 to 80 parts of cyflumetofen as an effective component, 0.1 to 20 parts of a wetting agent, 0.1 to 20 parts of a dispersing agent and the balance of a solid inert carrier by taking the total weight of the pesticide as 100 parts by weight.

Preferably, the pesticide is in the form of milk powder, wherein the auxiliary ingredients comprise an emulsifier, a dispersant, a binder and a solid inert carrier; preferably, the emulsion powder comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-80 parts of the active ingredient cyflumetofen, 0.1-15 parts of an emulsifier, 0.1-25 parts of a dispersant, 0.1-10 parts of a binder and the balance of a solid inert carrier.

Preferably, the pesticide is in the form of water dispersible granules, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a disintegrating agent and a solid inert carrier; preferably, the water dispersible granule comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-80 parts of the active ingredient cyflumetofen, 0.1-15 parts of a wetting agent, 0.1-20 parts of a dispersing agent, 0.1-25 parts of a binder, 0.1-20 parts of a disintegrating agent and the balance of a solid inert carrier.

Preferably, the pesticide is in the form of emulsion granules, wherein the auxiliary ingredients comprise an emulsifier, a dispersant, an organic solvent, a lubricant and a solid inert carrier; preferably, the emulsion granule comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-80 parts of the active ingredient of the cyflumetofen, 0.1-20 parts of the emulsifier, 0.1-8 parts of the dispersant, 0.1-50 parts of the organic solvent, 0.1-15 parts of the lubricant and the balance of the solid inert carrier.

Preferably, the pesticide is in the form of water dispersible tablet, wherein the auxiliary ingredients comprise wetting agent, dispersant, binder, disintegrant, lubricant, and solid inert carrier; preferably, the water dispersible tablet comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-80 parts of the active ingredient of the cyflumetofen, 0.1-10 parts of a wetting agent, 0.1-30 parts of a dispersing agent, 0.1-20 parts of a binding agent, 0.1-15 parts of a disintegrating agent, 0.1-25 parts of a lubricating agent and the balance of a solid inert carrier.

Preferably, the pesticide is in the form of a film-spreading oil agent, wherein the auxiliary components comprise a cosolvent, a water surface expanding agent and an organic solvent; preferably, the film-spreading oil agent comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-65 parts of the active ingredient cyflumetofen, 0.1-10 parts of the cosolvent, 1-20 parts of the emulsifier, and the balance of the organic solvent.

Preferably, the pesticide is in the form of soluble liquid, wherein the auxiliary components comprise an emulsifier, an organic solvent and water; preferably, the soluble solution comprises 0.1 to 55 parts of the effective component of the cyflumetofen, 0.1 to 40 parts of the emulsifier, 0.1 to 90 parts of the organic solvent and the balance of water, wherein the total weight of the pesticide is 100 parts by weight.

Preferably, the pesticide is in the form of soluble gum, wherein the auxiliary components comprise a wetting agent, a penetrating agent, a cosolvent, an organic solvent and a thickening agent; preferably, the soluble gum agent comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-75 parts of the active ingredient of the cyflumetofen, 0.1-10 parts of the wetting agent, 0.1-10 parts of the penetrating agent, 0.1-20 parts of the cosolvent, 0.1-20 parts of the organic solvent and the balance of the thickening agent.

Preferably, the formulation of the pesticide is oil, wherein the auxiliary components comprise an emulsifier, a cosolvent and an organic solvent; preferably, the oil agent is calculated by 100 parts by weight of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-80 parts, the emulsifier is 0.1-20 parts, the cosolvent is 0.1-15 parts, and the balance is an organic solvent.

Preferably, the pesticide is in the form of emulsifiable concentrate, wherein the auxiliary components comprise an emulsifier, an auxiliary organic solvent and an organic solvent; preferably, the missible oil is calculated by 100 parts by weight of the total pesticide, wherein the effective component of the cyflumetofen is 0.1-50 parts, the emulsifier is 0.1-40 parts, the cosolvent is 0.1-40 parts, and the balance is an organic solvent.

Preferably, the pesticide is in the form of latex, wherein the auxiliary components comprise an emulsifier, a thickener, an organic solvent, a solid inert carrier and water; preferably, the emulsion comprises, by weight, 0.1-60 parts of cyflumetofen as an active ingredient, 0.1-25 parts of an emulsifier, 0.01-15 parts of a thickener, 0.1-60 parts of an organic solvent, 0.1-60 parts of a solid inert carrier and the balance of water, wherein the total weight of the insecticide is 100 parts.

Preferably, the insecticide is in the form of a dispersible liquid, wherein the auxiliary ingredients comprise an emulsifier, an organic solvent; preferably, the dispersible agent comprises 0.1-70 parts of cyflumetofen as an effective component, 0.1-35 parts of an emulsifier and the balance of an organic solvent by taking the total weight of the pesticide as 100 parts by weight.

Preferably, the pesticide is in the form of paste, wherein the auxiliary ingredients comprise an emulsifier, a thickener, an antifreeze and an organic solvent; preferably, the ointment comprises 0.1 to 80 parts of cyflumetofen, 0.1 to 20 parts of emulsifier, 0.01 to 5 parts of thickener, 0.1 to 15 parts of antifreeze and the balance of water, wherein the total weight of the insecticide is 100 parts by weight.

Preferably, the pesticide is in the form of an aqueous emulsion, wherein the auxiliary components comprise an emulsifier, a co-emulsifier, an antifreeze, a thickening agent, an organic solvent and water; preferably, the aqueous emulsion comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-50 parts of the active ingredient cyflumetofen, 0.1-30 parts of an emulsifier, 0.1-20 parts of a co-emulsifier, 0.1-20 parts of an antifreeze, 0.01-5 parts of a thickener, 0.1-50 parts of an organic solvent and the balance of water.

Preferably, the formulation of the pesticide is oil emulsion, wherein the auxiliary components comprise emulsifier, co-emulsifier, antifreezing agent, thickener, water and organic solvent; preferably, the oil emulsion comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-50 parts of the active ingredient cyflumetofen, 0.1-35 parts of an emulsifier, 0.1-15 parts of a co-emulsifier, 0.1-20 parts of an antifreeze agent, 0.1-15 parts of a thickener, 0-50 parts of water and the balance of an organic solvent.

Preferably, the pesticide is in the form of microemulsion, wherein the auxiliary components comprise emulsifier, co-emulsifier, antifreezing agent, organic solvent and water; preferably, the microemulsion comprises 0.1-55 parts of cyflumetofen as an effective component, 0.1-30 parts of an emulsifier, 0.1-20 parts of a co-emulsifier, 0.1-10 parts of an antifreeze agent, 0.1-40 parts of an organic solvent and the balance of water, wherein the total weight of the pesticide is 100 parts by weight.

Preferably, the insecticide is in the form of a fatting agent, wherein the auxiliary ingredients comprise an emulsifier, a thickener and an organic solvent; preferably, the fat liquor is calculated by 100 parts by weight of the total pesticide weight, wherein the effective component of the cyflumetofen is 1-50 parts, the emulsifier is 0.1-25 parts, the thickener is 0.01-10 parts, and the balance is vegetable oil.

Preferably, the pesticide is in the form of a suspending agent, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a preservative, a thickening agent, an antifreezing agent and water; preferably, the suspending agent comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-80 parts of the active ingredient cyflumetofen, 0.1-15 parts of a wetting agent, 0.1-15 parts of a dispersing agent, 0.01-5 parts of a preservative, 0.01-5 parts of a thickening agent, 0.1-15 parts of an antifreezing agent and the balance of water.

Preferably, the pesticide is in the form of microcapsule suspension, wherein the auxiliary ingredients comprise an oily encapsulating material, an aqueous encapsulating material, an organic solvent, a dispersing agent, a thickening agent and water; preferably, the microcapsule suspending agent comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-60 parts of the active ingredient of the cyprocolfluramid, 0.1-30 parts of an oily encapsulating material, 0.1-30 parts of an aqueous encapsulating material, 0.1-50 parts of an organic solvent, 0.1-20 parts of a dispersing agent, 0.01-5 parts of a thickening agent and the balance of water.

Preferably, the pesticide is in the form of microcapsule suspension-suspoemulsion, wherein the auxiliary ingredients comprise oily capsule-forming materials, aqueous capsule-forming materials, organic solvents, emulsifiers, dispersants, thickeners, and water; preferably, the microcapsule suspension-suspoemulsion comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-60 parts of the active ingredient of the cyprocomiamide, 0.1-25 parts of the oily encapsulating material, 0.1-25 parts of the aqueous encapsulating material, 0.1-60 parts of the organic solvent, 0.1-20 parts of the emulsifier, 0.1-15 parts of the dispersant, 0.01-5 parts of the thickener and the balance of water.

Preferably, the pesticide is in the form of oil suspending agent, wherein the auxiliary components comprise emulsifier, dispersant, thickener and organic solvent; preferably, the oil suspending agent comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-55 parts of the active ingredient cyflumetofen, 0.1-25 parts of an emulsifier, 0.1-10 parts of a dispersant, 0.01-10 parts of a thickener, and the balance of an organic solvent.

Preferably, the pesticide is in the form of dispersible oil suspending agent, wherein the auxiliary ingredients comprise emulsifier, dispersant, thickener and organic solvent; preferably, the dispersible oil suspending agent comprises, by weight, 100 parts of the total weight of the insecticide, 0.1-65 parts of the active ingredient cyflumetofen, 0.1-30 parts of the emulsifier, 0.1-15 parts of the dispersant, 0.01-10 parts of the thickener and the balance of the organic solvent.

Preferably, the pesticide is in a dosage form of dry powder for seed treatment, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a film forming agent, a lubricating agent, a coloring agent and a solid inert carrier; preferably, the seed treatment dry powder agent comprises, by weight, 0.1-80 parts of cyflumetofen as an active ingredient, 0.1-15 parts of a wetting agent, 0.1-25 parts of a dispersing agent, 0.1-10 parts of a film forming agent, 0.1-20 parts of a lubricating agent, 0.1-10 parts of a coloring agent and the balance of a solid inert carrier, based on 100 parts of the total weight of the insecticide.

Preferably, the pesticide is in the form of seed treatment dispersible granules, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a binder, a disintegrating agent, a film forming agent, a coloring agent and a solid inert carrier; preferably, the dispersible granule for seed treatment comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-80 parts of the active ingredient cyflumetofen, 0.1-10 parts of the wetting agent, 0.1-20 parts of the dispersing agent, 0.1-15 parts of the binder, 0.1-15 parts of the disintegrant, 0.1-15 parts of the film forming agent, 0.1-15 parts of the coloring agent and the balance of the solid inert carrier.

Preferably, the pesticide is in the form of a seed treatment liquid, wherein the auxiliary components comprise an emulsifier, a film forming agent, a colorant, an organic solvent and water; preferably, the seed treatment liquid comprises, by weight, 0.1-70 parts of cyflumetofen, 0.1-45 parts of an emulsifier, 0.1-30 parts of a film-forming agent, 0.1-25 parts of a colorant, 0.1-50 parts of an organic solvent and the balance of water, based on 100 parts of the total weight of the pesticide.

Preferably, the pesticide is in the form of a seed treatment emulsion, wherein the auxiliary ingredients comprise an organic solvent, an emulsifier, a dispersant, a film forming agent, a thickener, a colorant, an organic solvent and water; preferably, the seed treatment emulsion comprises, by weight, 0.1-60 parts of cyflumetofen as an active ingredient, 0.1-35 parts of an emulsifier, 0.1-15 parts of a dispersant, 0.1-15 parts of a film-forming agent, 0.01-15 parts of a thickener, 0.01-25 parts of a colorant, 0.1-40 parts of an organic solvent and the balance of water, based on 100 parts of the total weight of the pesticide.

Preferably, the pesticide is in the form of a seed treatment suspending agent, wherein the auxiliary ingredients comprise a wetting agent, a dispersing agent, a film forming agent, a thickening agent, an antifreezing agent, a coloring agent and water; preferably, the seed treatment suspending agent is calculated by 100 parts of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.1-80 parts; 0.1-15 parts of wetting agent, 0.1-20 parts of dispersing agent, 0.01-15 parts of film forming agent, 0.01-5 parts of thickening agent, 0.1-15 parts of antifreezing agent, 0.01-15 parts of coloring agent and the balance of water.

Preferably, the pesticide is in the form of aerosol, wherein the auxiliary ingredients comprise an emulsifier, a synergist, an organic solvent and water; preferably, the aerosol comprises, by weight, 100 parts of the total pesticide weight, 0.001-20 parts of the active ingredient cyflumetofen, 0.1-30 parts of the emulsifier, 0.1-18 parts of the synergist, 0.1-80 parts of the organic solvent and the balance of water.

Preferably, the pesticide is in the form of smoke agent, wherein the auxiliary components comprise an oxidant, a fuel, a smoke agent and a fire retardant; preferably, the smoke agent comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-60 parts of the active ingredient of the cyflumetofen, 0.1-55 parts of the oxidant, 0.1-45 parts of the fuel, 0.1-65 parts of the smoke agent and the balance of the fire retardant.

Preferably, the pesticide is in the form of mosquito-repellent incense, wherein the auxiliary components comprise a binder, a preservative, a combustion improver and plant powder; preferably, the mosquito-repellent incense comprises, by weight, 100 parts of the total weight of the insecticide, 0.001-10 parts of the active ingredient of the cyflumetofen, 0.1-40 parts of the binder, 0.01-5 parts of the preservative, 0.1-10 parts of the combustion improver and the balance of plant powder.

Preferably, the pesticide is in the form of bait, wherein the auxiliary ingredients comprise a binder, an attractant, a synergist, a preservative, a lubricant, a colorant and water; preferably, the bait agent is calculated by 100 parts of the total weight of the pesticide, wherein the effective component of the cyflumetofen is 0.001-50 parts; 0.1 to 5 portions of attractant, 0.1 to 20 portions of binder, 0.1 to 10 portions of synergist, 0.1 to 5 portions of preservative, 0.1 to 20 portions of lubricant, 0.1 to 10 portions of colorant, 0.1 to 20 portions of water and the balance of plant powder.

Preferably, the pesticide is in the form of concentrated bait, wherein the auxiliary ingredients comprise a dispersing agent, an attractant, a synergist, a preservative, a colorant and water; preferably, the concentrated bait agent comprises, by weight, 100 parts of the total weight of the pesticide, 0.001-55 parts of cyflumetofen as an effective ingredient, 0.1-25 parts of a dispersing agent, 0.1-90 parts of an attractant, 0.1-30 parts of a synergist, 0.1-5 parts of a preservative, 0.1-15 parts of a colorant and the balance of water.

Preferably, the formulation of the pesticide is mosquito repellent milk, wherein the auxiliary components comprise an emulsifier, an organic solvent, plant essential oil and water; preferably, the mosquito repellent emulsion is calculated by taking the total weight of the insecticide as 100 parts by weight, wherein the effective component of the cyflumetofen is 0.001-50 parts; 0.1-25 parts of emulsifier, 0.1-65 parts of organic solvent, 0.1-20 parts of vegetable essential oil and the balance of water.

Preferably, the formulation of the pesticide is mosquito repellent liquid, wherein the auxiliary components comprise an organic solvent, plant essential oil and water; preferably, the mosquito repellent liquid comprises, by weight, 100 parts of the total weight of the insecticide, 0.001-40 parts of the active ingredient cyflumetofen, 0.1-50 parts of an organic solvent, 0.1-25 parts of plant essential oil and the balance of water.

Preferably, the formulation of the pesticide is mosquito repellent floral water, wherein the auxiliary components comprise an organic solvent, plant essential oil and water; preferably, the mosquito repellent floral water comprises, by weight, 100 parts of total pesticide weight, 0.001-40 parts of cyflumetofen as an effective ingredient, 0.1-20 parts of an organic solvent, 0.1-15 parts of plant essential oil, and the balance of water.

Preferably, the formulation of the pesticide is an ultra-low volume liquid formulation, wherein the auxiliary ingredients comprise a wetting agent, an osmotic agent, and an organic solvent; preferably, the ultra-low volume liquid comprises, by weight, 100 parts of the total weight of the pesticide, 0.1-85 parts of the active ingredient ciprofloxacin, 0.1-25 parts of the wetting agent, 0.1-25 parts of the penetrating agent, and the balance of the organic solvent.

Preferably, the formulation of the pesticide is a hot fogging concentrate, wherein the auxiliary components comprise an emulsifier, a synergist, a cosolvent and an organic solvent; preferably, the hot fogging concentrate comprises 0.1-50 parts of cyflumetofen, which is an effective component, by weight based on 100 parts of the total weight of the insecticide; 0.1-30 parts of emulsifier, 0.1-35 parts of synergist, 0.1-15 parts of cosolvent and the balance of organic solvent.

In the various formulations of the insecticide of the present invention, the content of each component is in the range of any one of the given content ranges, as long as all the components are added to make the total weight 100 parts by weight, for example, in the case of powder, the active ingredient cyprocomiamide is 0.01 to 95 parts, which means that the content may be any part by weight included in the range of 0.01 to 95 parts, for example, 0.01 part, 0.05 part, 0.08 part, 1 part, 3 parts, 5 parts, 8 parts, 10 parts, 20 parts, 25 parts, 30 parts, 40 parts, 50 parts, 60 parts, 70 parts, 80 parts, 90 parts or 95 parts, etc., the dispersant is 0.1 to 25 parts, for example, 0.1 part, 0.5 part, 1 part, 2 parts, 5 parts, 8 parts, 10 parts, 12 parts, 15 parts, 18 parts, 20 parts, 22 parts or 25 parts, etc., and other values are not listed, the contents of other components have the same meaning by analogy, and are not described in detail herein.

The pesticide has various using methods, is time-saving and labor-saving, can effectively prevent and treat various pests, has low efficient consumption, and can effectively delay the development of the drug resistance of the pests. The pesticide is suitable for preventing and treating pests such as lepidoptera, coleoptera, hemiptera, thysanoptera, diptera, hymenoptera, blattaria, mites, nematodes and the like, can effectively replace varieties which have already generated resistance or higher risk, and plays an active role in realizing reduction and synergism of pesticides.

In another aspect, the invention provides the application of the cyflumetofen-containing pesticide in the prevention and control of the insect pests of crops.

In the invention, the crops are one or at least two of rice, corn, wheat, fruit trees, cotton and vegetables; the pesticide is particularly suitable for preventing and controlling one or at least two of rice leaf roller, chilo suppressalis, tryporyza incertulas, sesamiella inferens, rice gall midge, corn borer, cotton bollworm, armyworm, fasciola giganteus, cabbage caterpillar, pod moth, looper, weevil, flea beetle, chafer, leaf miner, leaf hopper, Chinese toon, aphid, scale insect, plant hopper, thrips and red spider.

In another aspect, the present invention provides the use of a cyflumetofen-containing pesticide as described above for the control of sanitary pests.

In the invention, the environmental sanitation pest control comprises sanitation control of families, gardens, buildings, ancient temples or public places. In the aspect of preventing and controlling environmental sanitation pests, the pesticide is particularly suitable for preventing and controlling one or at least two of termite, red imported fire ant, termite, cockroach, fly or mosquito.

In another aspect, the invention provides the use of a cyflumetofen-containing insecticide as described above in the treatment of prevention and control of pests.

In the present invention, the seeds include seeds of rice, wheat, corn, peanut, garlic, shallot or leek. The pesticide is especially suitable for preventing and treating one or at least two of thrips, aphids, grubs, mole cricket, wireworms or chive maggots in seeds.

Compared with the prior art, the invention has the following beneficial effects:

the insecticide containing the cyflufenamide has low toxicity, high efficiency, small using amount, good quick action and long lasting period, and can effectively prevent and control pests such as Lepidoptera, Coleoptera, Hemiptera, Thysanoptera, Diptera, Blattaria, nematodes and the like; the cyflumetofen has novel action mechanism, is effective to resistant pests and is an important tool for pest resistance management.

Detailed Description

The technical solution of the present invention is further explained by the following embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.

Dosage form examples

Example 1

0.01 percent of cyflumetofen powder

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 0.01 part by weight of cyflumetofen, 5 parts by weight of sodium lignosulfonate, 5 parts by weight of talcum powder, 4 parts by weight of magnesium stearate and diatomite are taken to complement to 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 0.01% cyflumetofen powder, is obtained after powder preparation process processing.

Example 2

0.5% cyflumetofen granules

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 0.5 part by weight of cyflumetofen, 2 parts by weight of sodium salt of a naphthalene sulfonic acid formaldehyde polymer, 2 parts by weight of polyvinyl alcohol, 2 parts by weight of starch and zeolite to complement to 100 parts by weight, and processing by a granule preparation process to obtain the single pesticide of the embodiment, namely the 0.5% cyflumetofen granule.

Example 3

94% cyflumetofen ball agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 94 parts by weight of cyflumetofen, 0.5 part by weight of sodium dodecyl sulfate, 2 parts by weight of phenyl phosphate triethanolamine salt, 2 parts by weight of cellulose derivative, 1 part by weight of glycerol and white carbon black to complement to 100 parts by weight, and processing by a ball agent preparation process to obtain the pesticide single agent of the embodiment, namely the 94% cyflumetofen ball agent.

Example 4

10% cyflumetofen tablet

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 10 parts by weight of cyflumetofen, 1 part by weight of phenolsulfonate, 3 parts by weight of sodium lignosulfonate, 5 parts by weight of starch, 5 parts by weight of magnesium stearate and kaolin to complement to 100 parts by weight, and processing by a tablet preparation process to obtain the single pesticide preparation of the embodiment, namely the 10% cyflumetofen tablet.

Example 5

8% cyflumetofen strip agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 8 parts by weight of cyflumetofen, 0.5 part by weight of sodium dodecyl sulfate, 2 parts by weight of alkyl naphthalene sulfonate formaldehyde condensate, 4 parts by weight of polyethylene glycol, 5 parts by weight of talcum powder, 30 parts by weight of light calcium carbonate and clay to complement to 100 parts by weight, and processing the components by a strip agent preparation process to obtain the single pesticide agent of the embodiment, namely the 8% cyflumetofen strip agent.

Example 6

20% cyflumetofen oil dispersible powder

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 20 parts by weight of cyflumetofen, 5 parts by weight of calcium dodecyl benzene sulfonate, 6 parts by weight of polyaryl benzene polyoxyethylene ether, 2 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 3 parts by weight of hydroxystearate polyoxyethylene ether and white carbon black are made up to 100 parts by weight, and the pesticide single agent of the embodiment is obtained after processing through a dispersible powder preparation process, namely the 20% cyflumetofen oil dispersible powder.

Example 7

20% cyflumetofen wettable powder

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 20 parts by weight of cyflumetofen, 2 parts by weight of diisobutyl naphthalene sulfonate, 8 parts by weight of sodium lignin sulfonate, 3 parts by weight of alkyl naphthalene sulfonate formaldehyde condensate and kaolin are complemented to 100 parts by weight, and the single pesticide of the embodiment, namely the 20% cyflumetofen wettable powder, is obtained after processing by a wettable powder preparation process.

Example 8

95% cyflumetofen wettable powder

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 95 parts by weight of cyflumetofen, 1 part by weight of sodium dodecyl sulfate, 2 parts by weight of phenol sulfonate and polycarboxylate are taken to complement to 100 parts by weight, and the single pesticide of the embodiment, namely the 95% cyflumetofen wettable powder, is obtained after processing by a wettable powder preparation process.

Example 9

50% cyflumetofen emulsion powder

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: and (2) supplementing 50 parts by weight of cyflumetofen, 5 parts by weight of fatty alcohol-polyoxyethylene ether, 8 parts by weight of sodium lignin sulfonate, 3 parts by weight of polyvinylpyrrolidone and white carbon black to 100 parts by weight, and processing by using a milk powder preparation process to obtain the single pesticide preparation, namely the 50% cyflumetofen milk powder.

Example 10

20% cyflumetofen water dispersible granule

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: and (2) taking 20 parts by weight of cyflumetofen, 3 parts by weight of sodium dodecyl sulfate, 5 parts by weight of phenolsulfonate, 2 parts by weight of sodium lignosulfonate, 3 parts by weight of sucrose, 6 parts by weight of sodium sulfate and kaolin to complement to 100 parts by weight, and processing by a water dispersible granule preparation process to obtain the single pesticide preparation of the embodiment, namely the 20% cyflumetofen water dispersible granule.

Example 11

75% cyflumetofen water dispersible granule

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: and supplementing 75 parts by weight of cyflumetofen, 2 parts by weight of diisobutyl naphthalene sulfonate, 8 parts by weight of sodium naphthalene sulfonate formaldehyde polymer, 5 parts by weight of ammonium sulfate and kaolin to 100 parts by weight, and processing by a water dispersible granule preparation process to obtain the single pesticide preparation of the embodiment, namely the 75% cyflumetofen water dispersible granule.

Example 12

90% cyflumetofen water dispersible granule

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 90 parts by weight of cyflumetofen, 2 parts by weight of diisobutylnaphthalenesulfonate, 3 parts by weight of polycarboxylate, 2 parts by weight of polyoxyethylene polyoxypropylene block copolymer and ammonium sulfate are made up to 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 90% cyflumetofen water dispersible granule, is obtained after water dispersible granule preparation process processing.

Example 13

15% cyflumetofen emulsion granule

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 15 parts by weight of cyflumetofen, 5 parts by weight of polyarylphenyl polyoxyethylene ether phosphate, 4 parts by weight of calcium dodecylbenzene sulfonate, 2 parts by weight of polycarboxylate, 15 parts by weight of solvent oil, 5 parts by weight of glycerol, 30 parts by weight of white carbon black and light calcium carbonate to complement to 100 parts by weight, and processing by a preparation process of emulsion granules to obtain the single pesticide of the embodiment, namely the 15% cyflumetofen emulsion granules.

Example 14

45% cyflumetofen water dispersible tablet

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 45 parts by weight of cyflumetofen, 2 parts by weight of sodium dodecyl sulfate, 2 parts by weight of phenolsulfonate, 6 parts by weight of sodium lignosulfonate, 5 parts by weight of pregelatinized starch, 3 parts by weight of ammonium chloride, 2 parts by weight of sodium stearate, 2 parts by weight of talcum powder and diatomite to complement to 100 parts by weight, and processing by a water dispersion tablet preparation process to obtain the single pesticide preparation of the embodiment, namely the 45% cyflumetofen water dispersion tablet.

Example 15

5% cyflumetofen film-spreading oil agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: the preparation method comprises the following steps of taking 5 parts by weight of cyflumetofen, 5 parts by weight of calcium dodecyl benzene sulfonate, 3 parts by weight of castor oil polyoxyethylene ether, 5 parts by weight of sorbitan fatty acid ester, 15 parts by weight of solvent oil, 10 parts by weight of decanamide and soybean oil, supplementing the rest to 100 parts by weight, and processing the mixture by a preparation process of a film spreading oil agent to obtain the pesticide single agent of the embodiment, namely the 5% cyflumetofen film spreading oil agent.

Example 16

10% cyflumetofen soluble solution

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 30 parts by weight of cyflumetofen, 5 parts by weight of fatty alcohol-polyoxyethylene ether, 5 parts by weight of polyarylphenyl polyoxyethylene ether, 5 parts by weight of castor oil polyoxyethylene ether, 8 parts by weight of N, N-dimethylacetamide, 15 parts by weight of N-butanol, 5 parts by weight of methanol and water, and supplementing to 100 parts by weight, and processing by a soluble agent preparation process to obtain the single insecticide preparation of the embodiment, namely the 10% cyflumetofen soluble agent.

Example 17

25% cyflumetofen soluble solution

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 25 parts by weight of cyflumetofen, 5 parts by weight of fatty alcohol-polyoxyethylene ether, 10 parts by weight of sodium diisooctyl succinate sulfonate, 8 parts by weight of N, N-dimethylformamide, 5 parts by weight of cyclohexanone and ethanol, and supplementing to 100 parts by weight, and processing by a soluble agent preparation process to obtain the single pesticide of the embodiment, namely the 25% cyflumetofen soluble agent.

Example 18

15% cyflumetofen soluble gum agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 15 parts by weight of cyflumetofen, 3 parts by weight of fatty alcohol-polyoxyethylene ether, 2 parts by weight of alkylphenol polyoxyethylene, 5 parts by weight of isopropanol, 10 parts by weight of solvent oil and polyethylene glycol are taken to complement to 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 15% cyflumetofen soluble glue agent, is obtained after processing by a soluble glue agent preparation process.

Example 19

12% cyflumetofen oil solution

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: and (2) supplementing 12 parts by weight of cyflumetofen, 10 parts by weight of calcium dodecyl benzene sulfonate, 8 parts by weight of castor oil polyoxyethylene ether, 5 parts by weight of N, N-dimethylformamide and decanamide to 100 parts by weight, and processing by an oil preparation process to obtain the single pesticide preparation of the embodiment, namely the 12% cyflumetofen oil.

Example 20

15% cyflumetofen emulsifiable concentrate

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 15 parts of cyflumetofen, 5 parts of calcium dodecyl benzene sulfonate, 4 parts of polyaryl benzene polyoxyethylene ether, 1 part of fatty alcohol-polyoxyethylene ether, 10 parts of N, N-dimethylacetamide and solvent oil by weight are taken and added to make up to 100 parts by weight, and the pesticide single agent of the embodiment, namely the 15% cyflumetofen missible oil, is obtained after the missible oil preparation process.

Example 21

40% cyflumetofen emulsifiable concentrate

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 40 parts by weight of cyflumetofen, 5 parts by weight of calcium dodecyl benzene sulfonate, 5 parts by weight of castor oil polyoxyethylene ether, 3 parts by weight of polyoxyethylene ether fatty acid ester, 20 parts by weight of N-methyl pyrrolidone, 10 parts by weight of cyclohexanone and solvent oil are taken to complement to 100 parts by weight, and the pesticide single agent of the embodiment is obtained after processing by an emulsifiable concentrate preparation process, namely the 40% cyflumetofen emulsifiable concentrate.

Example 22

2% cyflumetofen latex

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 0.5 part by weight of cyflumetofen, 3 parts by weight of sorbitan fatty acid ester, 2 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 2 parts by weight of polyoxyethylene fatty acid ester, 3 parts by weight of xanthan gum, 2 parts by weight of polyethylene glycol, 5 parts by weight of isopropanol, 20% of hydroxypropyl starch, 35% of sodium stearate and water are made up to 100 parts by weight, and the single pesticide of the embodiment, namely the 2% cyflumetofen latex, is obtained after the emulsion preparation process.

Example 23

12.5% cyflumetofen dispersible agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 12.5 parts by weight of cyflumetofen, 5 parts by weight of calcium dodecyl benzene sulfonate, 7 parts by weight of castor oil polyoxyethylene ether, 2 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 10 parts by weight of decanamide, 5 parts by weight of isopropanol and methyl oleate, supplementing to 100 parts by weight, and processing by a dispersible agent preparation process to obtain the single pesticide of the embodiment, namely the 12.5% cyflumetofen dispersible agent.

Example 24

3.5% cyflumetofen ointment

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 3.5 parts by weight of cyflumetofen, 5 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 60 parts by weight of polyethylene glycol, 8 parts by weight of glycerol and soybean oil are taken to supplement 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 3.5% cyflumetofen ointment, is obtained after the ointment preparation process.

Example 25

10% cyflumetofen water emulsion

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 10 parts by weight of cyflumetofen, 4 parts by weight of calcium dodecyl benzene sulfonate, 5 parts by weight of polyaryl benzene polyoxyethylene ether, 2 parts by weight of castor oil polyoxyethylene ether, 2 parts by weight of isobutanol, 5 parts by weight of ethylene glycol, 0.15 part by weight of xanthan gum, 15 parts by weight of solvent oil and water to complement to 100 parts by weight, and processing the mixture by an emulsion in water preparation process to obtain the single pesticide of the embodiment, namely the 10% cyflumetofen emulsion in water.

Example 26

30% cyflumetofen water emulsion

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: the preparation method comprises the following steps of taking 30 parts by weight of cyflumetofen, 5 parts by weight of calcium dodecyl benzene sulfonate, 8 parts by weight of castor oil polyoxyethylene ether, 2 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 1 part by weight of butanol, 5 parts by weight of ethylene glycol, 0.12 part by weight of xanthan gum, 23 parts by weight of quinamide and water to complement to 100 parts by weight, and obtaining the single pesticide of the embodiment after processing through an emulsion in water preparation process, namely the 30% cyflumetofen emulsion in water.

Example 27

3.5% cyflumetofen oil emulsion

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: preparing 3.5 parts by weight of cyflumetofen, 1.5 parts by weight of calcium dodecyl benzene sulfonate, 2 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 3 parts by weight of N, N-dimethylformamide, 3 parts by weight of isopropanol and 10 parts by weight of water into a water phase; taking 6 parts by weight of castor oil polyoxyethylene ether and 71 parts by weight of soybean oil, preparing an oil phase, adding a water phase into the oil phase, and processing by an oil emulsion preparation process to obtain the single insecticide of the embodiment, namely the 3.5% cyhalothrin oil emulsion.

Example 28

5% cyflumetofen microemulsion

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 5 parts by weight of cyflumetofen, 7 parts by weight of calcium dodecyl benzene sulfonate, 2 parts by weight of sodium alkyl succinate sulfonate, 2 parts by weight of polyaryl benzene polyoxyethylene ether phosphate, 6 parts by weight of castor oil polyoxyethylene ether, 5 parts by weight of polyaryl benzene polyoxyethylene ether, 8 parts by weight of ethylene glycol, 6 parts by weight of N, N-dimethylacetamide, 5 parts by weight of ethanol and water to complement to 100 parts by weight, and processing by a microemulsion preparation process to obtain the single pesticide of the embodiment, namely the 5% cyflumetofen microemulsion.

Example 29

20% cyflumetofen microemulsion

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 20 parts by weight of cyflumetofen, 8 parts by weight of calcium dodecyl benzene sulfonate, 3 parts by weight of sodium alkyl succinate sulfonate, 5 parts by weight of castor oil polyoxyethylene ether, 5% polyaryl benzene polyoxyethylene ether, 2 parts by weight of polyaryl benzene polyoxyethylene ether formaldehyde condensate, 8 parts by weight of propylene glycol, 8 parts by weight of N, N-dimethylformamide, 8 parts by weight of cyclohexanone, 5 parts by weight of methanol and water are added to 100 parts by weight, and the single pesticide of the embodiment, namely the 20% cyflumetofen microemulsion, is obtained after the microemulsion is processed by a microemulsion preparation process.

Example 30

5% cyflumetofen fat liquor

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 5 parts by weight of cyflumetofen, 5 parts by weight of sorbitan fatty acid ester, 5 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 10% of polyamide and soybean oil to supplement the total weight to 100 parts by weight, and processing the mixture by a fat liquor preparation process to obtain the pesticide single agent of the embodiment, namely the 5% cyflumetofen fat liquor.

Example 31

5% Cyclopropanamide suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 25 parts by weight of cyflumetofen, 0.5 part by weight of fatty alcohol-polyoxyethylene ether phosphate, 3 parts by weight of phenyl phosphate triethanolamine salt, 2 parts by weight of polycarboxylate, 0.5 part by weight of cason, 0.5 part by weight of sodium benzoate, 0.2 part by weight of xanthan gum, 2 parts by weight of white carbon black, 0.3 part by weight of magnesium aluminum silicate, 5 parts by weight of glycerol and water are added to 100 parts by weight, and the pesticide single agent of the embodiment, namely the 5% cyflumetofen suspending agent, is obtained after processing by a suspending agent preparation process.

Example 32

20% cyflumetofen suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 20 parts by weight of cyflumetofen, 1 part by weight of fatty alcohol-polyoxyethylene ether phosphate, 2 parts by weight of polyoxyethylene polyoxypropylene block copolymer, 3 parts by weight of phenethyl phenol polyoxyethylene ether phosphate, 1 part by weight of polycarboxylate, 0.5 part by weight of karson, 0.15 part by weight of xanthan gum, 0.5 part by weight of magnesium aluminum silicate, 5 parts by weight of glycol and water are added to 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 20% cyflumetofen suspending agent, is obtained after the suspending agent preparation process.

Example 33

50% cyflumetofen suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 50 parts by weight of cyflumetofen, 2 parts by weight of alkyl naphthalene sulfonate formaldehyde condensate, 5 parts by weight of polyoxyethylene polyoxypropylene block copolymer, 1 part by weight of sodium lignosulfonate, 2 parts by weight of polycarboxylate, 0.5 part by weight of kason, 0.1 part by weight of xanthan gum, 0.5 part by weight of magnesium aluminum silicate, 5 parts by weight of propylene glycol and water to complement to 100 parts by weight, and processing the mixture by a suspending agent preparation process to obtain the single pesticide, namely the 50% cyflumetofen suspending agent.

Example 34

25% cyflumetofen microcapsule suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 25 parts by weight of cyflumetofen, 3 parts by weight of polyphenyl polyisocyanate, 2.5 parts by weight of diethylenetriamine, 15 parts by weight of solvent naphtha, 3 parts by weight of polycarboxylate, 2 parts by weight of sodium lignosulfonate, 0.3 part by weight of xanthan gum and the balance of water are taken and processed by a method for preparing microcapsules by an interfacial polymerization method to obtain the single pesticide of the embodiment, namely the 25% cyflumetofen microcapsule suspending agent.

Example 35

Suspension-suspoemulsion of 18% cyflumetofen microcapsule

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 18 parts by weight of cyflumetofen, 2.5 parts by weight of alkyl diisocyanate, 2.5 parts by weight of tetraethylenepentamine, 12 parts by weight of solvent oil, 5 parts by weight of polycarboxylate, 1 part by weight of polyphosphate, 0.25 part by weight of xanthan gum and the balance of water, processing by an interfacial polymerization method for preparing microcapsules to obtain a microcapsule suspending agent, adding 10 parts by weight of methyl oleate, 2.5 parts by weight of calcium dodecyl benzene sulfonate and 3 parts by weight of castor oil polyoxyethylene ether into the microcapsule suspending agent of the embodiment, and shearing to obtain the single pesticide of the embodiment, namely the 18% cyflumetofen microcapsule suspension-suspoemulsion.

Example 36

12% cyflumetofen oil suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 12 parts by weight of cyflumetofen, 4 parts by weight of calcium dodecyl benzene sulfonate, 2 parts by weight of polyoxyethylene polyoxypropylene block copolymer, 6 parts by weight of castor oil polyoxyethylene ether, 2 parts by weight of hydroxystearate polyoxyethylene ether, 0.5 part by weight of organobentonite, 2 parts by weight of white carbon black and soybean oil are taken to supplement 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 12% cyflumetofen oil suspending agent, is obtained after being processed by an oil suspending agent preparation process.

Example 37

35% cyflumetofen oil suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 35 parts by weight of cyflumetofen, 6 parts by weight of calcium dodecyl benzene sulfonate, 3 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 4 parts by weight of castor oil polyoxyethylene ether, 4 parts by weight of hydroxystearate polyoxyethylene ether, 0.6 part by weight of organobentonite, 2 parts by weight of white carbon black, 5 parts by weight of ethylene glycol and methyl oleate are added to 100 parts by weight, and the pesticide single agent of the embodiment is obtained after the oil suspending agent is processed by the preparation process, namely the 35% cyflumetofen oil suspending agent.

Example 38

Dispersible oil suspending agent containing 30% cyflumetofen

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 30 parts by weight of cyflumetofen, 5 parts by weight of calcium dodecyl benzene sulfonate, 8 parts by weight of castor oil polyoxyethylene ether, 2 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 2 parts by weight of hydroxystearate polyoxyethylene ether, 0.3 part by weight of organobentonite, 2 parts by weight of white carbon black and methyl oleate are taken to complement to 100 parts by weight, and the pesticide single agent of the embodiment is obtained after being processed by the preparation process of the dispersible oil suspending agent, namely the 30% cyflumetofen dispersible oil suspending agent.

Example 39

35% cyflumetofen seed treatment dry powder

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 35 parts by weight of cyflumetofen, 3 parts by weight of sodium dodecyl sulfate, 2 parts by weight of alkyl naphthalene sulfonate formaldehyde condensate, 3 parts by weight of sodium lignosulfonate, 2 parts by weight of polyvinyl alcohol, 5 parts by weight of sodium stearate, 2 parts by weight of permanent red and kaolin are complemented to 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 35% cyflumetofen seed treatment dry powder, is obtained after the seed treatment dry powder preparation process.

Example 40

50% cyflumetofen seed treatment dispersible granule

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: the preparation method comprises the steps of taking 50 parts by weight of cyflumetofen, 2 parts by weight of sodium dodecyl sulfate, 3 parts by weight of phenolsulfonate, 3 parts by weight of starch, 4 parts by weight of montmorillonite, 2 parts by weight of polyethylene glycol, 2 parts by weight of permanent red and white carbon black, supplementing to 100 parts by weight, and processing through a seed treatment dispersible granule preparation process to obtain the pesticide single agent of the embodiment, namely the 50% cyflumetofen seed treatment dispersible granule.

EXAMPLE 41

15% cyflumetofen seed treatment liquid agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 15 parts of cyflumetofen, 5 parts of fatty alcohol-polyoxyethylene ether, 1 part of sodium lignin sulfonate, 8 parts of decanamide, 5 parts of cyclohexanone, 3 parts of polyvinyl alcohol, 2 parts of permanent red and water by weight are taken and added to 100 parts by weight, and the single pesticide preparation is obtained after the seed treatment liquid preparation process, namely the 15% cyflumetofen seed treatment liquid.

Example 42

10% cyflumetofen seed treatment emulsion

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 10 parts by weight of cyflumetofen, 4 parts by weight of calcium dodecyl benzene sulfonate, 8 parts by weight of castor oil polyoxyethylene ether, 5 parts by weight of isopropanol, 5 parts by weight of glycerol, 0.12 part by weight of xanthan gum, 15 parts by weight of solvent oil, 2 parts by weight of brilliant blue and water to complement to 100 parts by weight, and processing the mixture by a preparation process of the seed treatment emulsion to obtain the pesticide single agent of the embodiment, namely the 10% cyflumetofen seed treatment emulsion.

Example 43

25% cyflumetofen seed treatment suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 25 parts by weight of cyflumetofen, 3 parts by weight of polycarboxylate, 2 parts by weight of polyoxyethylene polyoxypropylene block copolymer, 3 parts by weight of cellulose derivative, 0.28 part by weight of xanthan gum, 2 parts by weight of white carbon black, 0.5 part by weight of benzoic acid, 0.2 part by weight of kasong, 5 parts by weight of ethylene glycol, 2 parts by weight of permanent red and water to complement to 100 parts by weight, and processing the materials by a seed treatment suspending agent preparation process to obtain the pesticide single agent of the embodiment, namely the 25% cyflumetofen seed treatment suspending agent.

Example 44

50% cyflumetofen seed treatment suspending agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 50 parts by weight of cyflumetofen, 5 parts by weight of polycarboxylate, 2 parts by weight of polyoxyethylene polyoxypropylene block copolymer, 3 parts by weight of polyvinyl alcohol, 0.12 part by weight of xanthan gum, 2 parts by weight of white carbon black, 0.5 part by weight of kasong, 5 parts by weight of glycerol, 3 parts by weight of permanent red and water to complement to 100 parts by weight, and processing the mixture by a preparation process of a seed treatment suspending agent to obtain the single pesticide preparation of the embodiment, namely the 50% cyflumetofen seed treatment suspending agent.

Example 45

0.01% cyflumetofen aerosol

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 0.01 part by weight of cyflumetofen, 2 parts by weight of calcium dodecyl benzene sulfonate, 1 part by weight of piperonyl butoxide oxide, 15 parts by weight of isopropanol, 35 parts by weight of liquefied propane, 5 parts by weight of ethanol and water are taken to complement to 100 parts by weight, and the single pesticide preparation of the embodiment, namely the 0.01% cyflumetofen aerosol, is obtained after processing by an aerosol preparation process.

Example 46

10% cyflumetofen smoke agent

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 0.1-55 parts of oxidant, 0.1-45 parts of fuel, 0.1-65 parts of smoke agent and the balance of fire retardant.

Taking 10 parts by weight of cyflumetofen, 41 parts by weight of potassium nitrate, 15 parts by weight of charcoal, 7 parts by weight of sulfur, 5 parts by weight of ammonium chloride and sodium carbonate to complement to 100 parts by weight, and processing by a smoke agent preparation process to obtain the single pesticide preparation of the embodiment, namely the 10% cyflumetofen smoke agent.

Example 47

0.1% cyflumetofen mosquito-repellent incense

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 0.1 part by weight of cyflumetofen, 5 parts by weight of cross-linked sodium carboxymethylcellulose, 0.5 part by weight of kasong, 3 parts by weight of potassium nitrate and coconut shell powder to complement to 100 parts by weight, and processing by a mosquito incense preparation process to obtain the single pesticide of the embodiment, namely the 0.1% cyflumetofen mosquito-repellent incense.

Example 48

0.5% cyflumetofen bait

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 0.5 part by weight of cyflumetofen, 5 parts by weight of starch, 0.25 part by weight of anisaldehyde, 1 part by weight of piperonyl butoxide, 0.5 part by weight of sorbic acid, 4 parts by weight of glycerol, 2 parts by weight of benzidine yellow, 5 parts by weight of peanut oil, 10 parts by weight of water and oat flour to complement to 100 parts by weight, and processing the mixture by a bait preparation process to obtain the pesticide single agent of the embodiment, namely the 0.5% cyflumetofen bait.

Example 49

10% cyflumetofen concentrated bait

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 10 parts by weight of cyflumetofen, 10 parts by weight of glucose, 8 parts by weight of sesame oil, 0.1 part by weight of citric acid, 5 parts by weight of propylene glycol, 15 parts by weight of water and corn flour, and supplementing to 100 parts by weight, and processing by a bait concentrate preparation process to obtain the single pesticide preparation of the embodiment, namely the 10% cyflumetofen bait concentrate.

Example 50

0.25% cyflumetofen mosquito repellent emulsion

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 0.25 part by weight of cyflumetofen, 4 parts by weight of polyoxyethylene ether sorbitan fatty acid ester, 5 parts by weight of isopropanol, 10 parts by weight of polyvinylpyrrolidone, 2 parts by weight of leaf amine oil and water are taken to complement to 100 parts by weight, and the single insecticide preparation of the embodiment, namely the 0.25% cyflumetofen mosquito repellent emulsion, is obtained after the preparation process of the mosquito repellent emulsion.

Example 51

0.2% cyflumetofen mosquito repellent liquid

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 0.2 part by weight of cyflumetofen, 6 parts by weight of isopropanol, 1.5 parts by weight of lemon oil and water to complement to 100 parts by weight, and processing by a mosquito repellent preparation process to obtain the single insecticide of the embodiment, namely the 0.2% cyflumetofen mosquito repellent.

Example 52

Mosquito-repellent toilet water containing 0.12% of cyflumetofen

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 0.12 part by weight of cyflumetofen, 5 parts by weight of isopropanol, 1.5 parts by weight of lavender oil and water to complement to 100 parts by weight, and processing the mixture by a mosquito repellent toilet water preparation process to obtain the single pesticide of the embodiment, namely the 0.12% cyflumetofen mosquito repellent toilet water.

Example 53

12% ciprofloxacin ultralow volume liquid

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 12 parts by weight of cyflumetofen, 6 parts by weight of calcium dodecyl benzene sulfonate, 5 parts by weight of castor oil polyoxyethylene ether, 2 parts by weight of polyaryl benzene polyoxyethylene ether, 5 parts by weight of N, N-dimethylformamide, 10 parts by weight of isophorone and methyl oleate, supplementing to 100 parts by weight, and processing by an ultra-low volume liquid preparation process to obtain the single pesticide of the embodiment, namely the 12% cyflumetofen ultra-low volume liquid.

Example 54

Ultra-low volume liquid containing 40% cyflumetofen

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: 40 parts by weight of cyflumetofen, 5 parts by weight of calcium dodecyl benzene sulfonate, 6 parts by weight of castor oil polyoxyethylene ether, 2 parts by weight of polyoxyethylene sorbitan fatty acid ester, 6 parts by weight of dimethyl sulfoxide, 10 parts by weight of hexamethyl tertiary amine phosphate and methyl oleate are taken to complement to 100 parts by weight, and the pesticide single agent of the embodiment, namely the 40% cyflumetofen ultra-low volume liquid agent, is obtained after processing by an ultra-low volume liquid agent preparation process.

Example 55

14% cyflumetofen hot fogging concentrate

The pesticide comprises the following components in parts by weight based on 100 parts by weight of the total pesticide weight: taking 14 parts by weight of cyflumetofen, 6 parts by weight of calcium dodecyl benzene sulfonate, 6 parts by weight of castor oil polyoxyethylene ether, 3 parts by weight of synergistic amine, 15 parts by weight of N, N-dimethylformamide and methyl oleate to complement 100 parts by weight, and processing by a hot fogging concentrate preparation process to obtain the single insecticide preparation of the embodiment, namely the 14% cyflumetofen hot fogging concentrate.

Application examples

The invention adopts various preparations, takes various pests such as lepidoptera, coleoptera, thysanoptera, blattaria and the like as targets or control objects, carries out indoor activity research and field application tests, and shows excellent insecticidal activity and remarkable control effect compared with common medicaments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.

Application example 1: field test of different formulations for controlling pest grubs under peanut field

The soil treatment method is adopted by using samples prepared in preparation examples 1 and 2 to control grubs as pests under peanut fields, and the control agents are 15% chlorpyrifos granules and 5% carbofuran granules.

The method comprises the following steps: the number of the plants to be investigated was examined with reference to GB/T17980.72-2004. Mixing different agents with fine sand according to the treatment doses shown in the table 1, ditching and broadcasting the mixture in the seedling stage of the peanuts, investigating the number of damaged plants of the peanuts 30 days after pesticide application, and counting the seedling protection effect.

The test result shows that: compared with the common medicament chlorpyrifos or carbosulfan, the preparation example 1 (0.01% cyflumetofen powder) and the preparation example 2 (0.5% cyflumetofen granule) have the advantages of remarkable control effect on grubs of the soil insects in the peanut fields, small using amount of effective components, small average number of plants to be killed and good seedling protection effect.

TABLE 1 field Effect of different formulations on controlling pest grubs in peanut fields

Application example 2: indoor bioactivity test of different preparations for diamondback moth

The indoor insecticidal activity of the samples prepared in preparation examples 7, 11, 17, 21, 26, 31, 33, 34 and 36 and abamectin serving as a control medicament are tested by taking plutella xylostella as a bioassay target in a laboratory and adopting a leaf-dipping disc feeding method.

The method comprises the following steps: diamondback moth and leaf soaking feeding method. With reference to NY/1154.14-2008, the main operations are described as follows: soaking clean bracteatum leaf dishes in the liquid medicine for 10s, airing, placing in culture dishes with 4 dishes in each dish, and placing filter paper in the culture dishes for moisture preservation. Each dish was inoculated with 10 plutella xylostella test insects, and the procedure was repeated 3 times. Placing in a light incubator at 25 deg.C under 14hL:10hD for culture. And (5) investigating the dead number of diamondback moth 3 days after the pesticide is applied, and calculating the death rate.

And (3) test results: formulation examples 7, 11, 17, 21, 26, 31, 33, 34, 36 formulated samples all had 100% mortality on day 3 at a dose of 1 mg/L.

TABLE 2 biological Activity test results for Plutella xylostella in different formulations

Name of medicament	Dosage mg/L	3d mortality%
			Formulation example 7 (20% Cyclopropanflufenoxuron wettable powder)	1.0	100
Formulation example 11 (75% cyflumetofen water dispersible granules)	1.0	100
			Formulation example 17 (25% cyflumetofen solubles)	1.0	100
Formulation example 21(40 Cyclopropanfluben emulsifiable concentrate)	1.0	100
			Formulation example 26 (30% Cyclopropanflufenoxam aqueous emulsion)	1.0	100
Formulation example 31 (5% Cyclopropanflufenoxam suspension)	1.0	100
			Formulation example 33 (50% Cyclopropanflufenamide suspension)	1.0	100
Formulation example 34 (25% Cyclopropanflufenoxuron microcapsule suspension)	1.0	100
			Formulation example 36 (12% Cyclopropanifenprodia oil suspension)	1.0	100
5% avermectin emulsion (Hebei Weiyuan biochemical company Limited)	1.0	100

Application example 3: field test of different preparations for preventing and controlling rice leaf roller

The samples prepared in the preparation examples 10, 16, 20, 32 and 35 and abamectin and chlorantraniliprole as control medicaments were subjected to a field test for controlling rice leaf rollers in Hunan of 2019.

The method comprises the following steps: spraying method. Refer to GB/T19780.2-2000. Spraying different medicaments according to the treatment doses shown in the table 3 from the late incubation period to the low-age larva period of the cnaphalocrocis medinalis eggs, performing leaf rolling rate and live insect peeling check 18 days after the medicaments are applied, and counting leaf protection effect and insect control effect.

And (3) test results: the samples prepared in preparation examples 10, 16, 20, 32 and 35 have excellent control effect on rice leaf rollers, and the leaf protection effect and the insecticidal control effect (namely the death rate of pests) are both more than 90 percent under the dosage of 45 g of active ingredients per hectare, are equivalent to chlorantraniliprole, and are obviously superior to abamectin.

TABLE 3 field Effect of different formulations on controlling cnaphalocrocis medinalis

Application example 4: field test of different preparations for controlling corn field pest agrotis parvus

With the samples prepared in the preparation examples 39, 40 and 43 and the 50% chlorantraniliprole seed treatment suspension seed coating agent as a control agent, a field test for controlling the pest agrotis xiaohui under the corn field was carried out in south China of Jiangsu in 2019.

The method comprises the following steps: seed dressing method for seed treatment. Refer to GB/T19780.72-2004. The seed dressing treatment was carried out on different agents at the treatment doses shown in Table 4, 3 replicates per treatment dose and 66.7m per replicate²And investigating 2-3 leaf stages after seedling emergence, investigating 250 holes in each cell, recording the number of seedlings, counting the rate of emergence, and counting the seedling protection effect.

And (3) test results: the samples prepared in preparation examples 39, 40 and 43 have excellent control effect on the pest cutworm under the corn field, and the seedling protection effect is over 85 percent and slightly superior to that of chlorantraniliprole under the seed dressing dosage of 3 gai/kg.

TABLE 4 test results of different preparations for controlling agrotis ypsilon as underground pest in corn field

Application example 5: field test of 10% cyflumetofen soluble solution for controlling rice stem borers in resistant areas

In Changsha areas of Jiangxi Nanchang and Hunan, the rice stem borer has obvious resistance to chlorantraniliprole, and the pesticide is characterized in that the chlorantraniliprole is basically ineffective under the recommended application dosage, and the dosage of the abamectin is increased to 10gai/667m²(registered dosage 0.5-0.75gai/667m²) The time is substantially controlled.

A10% cyclopropylflufenoxuron soluble solution is used as a test medicament, 5% chlorantraniliprole SC produced by Shenzhen norphin company and 5% abamectin missible oil produced by Hebei Weiyuan company are used as control medicaments, and the test is carried out on Jiangxi Nanchang second-generation chilo suppressalis in 2019.

The method comprises the following steps: according to GB/T19780.1-2000, spraying the pesticide at the period from hatching of high bees to young larvae, investigating the withered rate 20 days after 45L of pesticide is applied to each mu of water, and counting the withered rate and the control effect.

And (3) test results: the 10% cyflumetofen soluble solution can prevent and control the rice stem borers, under the dosage of 30, 45 and 60 g of effective components per hectare, the dead center rates are respectively 1.05%, 0.82% and 0.52%, and the control effects are respectively 82.5%, 86.5% and 91.3%; the insecticidal composition is remarkably superior to the control effect of a control medicament 5 percent chlorantraniliprole SC in 30 grams of active ingredients per hectare and superior to the control effect of a control medicament 5 percent abamectin EC in 150 grams of active ingredients per hectare.

Table 510% cyflumetofen soluble solution for preventing and controlling field effect of rice stem borers in resistant areas

Application example 6: field test for controlling cabbage caterpillars by using 20% cyflumetofen suspending agent

A field efficacy test was carried out in shaoxing of zhejiang in 2019 with 5% of cyhalothrin suspension prepared in preparation example 31 as a test agent and 25g/L of high-efficiency cyhalothrin emulsifiable concentrate as a control agent.

The method comprises the following steps: spraying method. According to GB/T17980.13-2000, the pesticide is applied to young cabbage caterpillars by using water: 450 l/ha, applied once.

And (3) test results: the composition shows excellent control effect after being applied for 3 days and 7 days, and is superior to a control medicament.

Table 65% field effect of cyflumetofen granular suspending agent on cabbage caterpillar control

Application example 7: field control effect of 75% cyflumetofen water dispersible granules for controlling soybean thrips

A field test for controlling the thistle was carried out on soybeans in shanghai Qingpu test base in 2019 with the 75% cyclopropylfluben amine water dispersible granule prepared in preparation example 11 as a test medicament and the 50% dinotefuran water dispersible granule as a control medicament.

The method comprises the following steps: a stem and leaf spraying method is disclosed in NY/T1464.6-2007. The water consumption is 450 liters/ha, and the application is carried out for 1 time. In the investigation, 10 plants were fixed per cell, 3 leaves were fixed per plant, and the number of thrips on the leaves was investigated.

And (3) test results: the 75% ciprofloxacin water dispersible granule has the control effect on soybean thrips at the dosage of 112.5-450 g active ingredients per hectare of 84.6-94.2%, which is better than the control agent 40% dinotefuran soluble powder at the dosage of 20g per mu (80.3%).

TABLE 7 statistical table of investigation results of test agent on soybean milk thistle

Application example 8: 20% cyhalothrin wettable powder for field control of phyllotreta striolata

A field test for controlling phyllotreta striolata was carried out on pakchoi in 2019 in Shanghai New creek test base by using 20% cyhalofop-butyl wettable powder prepared in preparation example 7 as a test agent and 5% acetamiprid missible oil as a control agent.

The method comprises the following steps: spraying stem and leaf. Refer to GB/T17980.18-2000. The water consumption is 450 liters/ha, and the application is carried out for 1 time. In the investigation, 5 plants are investigated at each cell by a 5-point method, 25 plants are investigated in total, and the damage of the adult insects on the leaves is visually observed. Statistic leaf-protecting effect

And (3) test results: the 20% cyflumetofen wettable powder has higher leaf protection effect on pakchoi than the control medicament 5% acetamiprid emulsion at the dosage of 40 g/mu, and the leaf protection control effect of medium-low high dosage is equivalent to that of a control single agent. The 60% cyflufenamid wettable powder has better prevention and treatment effect on phyllotreta striolata imagoes.

TABLE 8 statistical table of the results of the test agent for Phyllotreta striolata (7 d after drug)

Application example 9: indoor activity of 10% cyflumetofen water emulsion on spodoptera frugiperda

The 10% cyflumetofen aqueous emulsion obtained in the preparation example 25 is used as a test medicament, and the 15% indoxacarb suspending agent is used as a control medicament to test the biological activity of spodoptera frugiperda raised in a laboratory, so as to evaluate the application value of the spodoptera frugiperda.

The method comprises the following steps: leaf soaking method. Reference to NY/T1154.14-2008, test targets: cutting corn seedlings into leaf sections, immersing the leaf sections into liquid medicine for 10s, airing, putting the leaf sections into 24-hole plates, inoculating 1 test insect into each hole, and processing 24 test insects every time. After the treatment, the mixture is placed in an illumination incubator at the temperature of 26 +/-1 ℃. The number of dead and live insects was investigated 3d after the administration.

And (3) test results: LC of 3d, 10% cyclopropamide aqueous emulsion after medicine₅₀LC of 0.033 mg/L15% indoxacarb suspension₅₀The value was 1.132 mg/L. The relative virulence index of cyflumetofen is 3430, calculated as the relative virulence index of indoxacarb being 100. Therefore, the 10% cyflumetofen aqueous emulsion has extremely high activity on spodoptera frugiperda and has obvious development and application values.

Application example 10: indoor activity of 5% cyflumetofen microemulsion on cotton bollworm

The 5% cyflumetofen microemulsion obtained in the preparation example 28 is used as a test medicament, and 25g/L of high-efficiency cyhalothrin emulsifiable concentrate is used as a control medicament to test the biological activity of the cotton bollworm bred in a laboratory, so as to evaluate the application value of the cotton bollworm.

The method comprises the following steps: and (4) an insect soaking method. Refer to NY/T1154.6-2006. The method comprises the steps of taking cotton bollworm 3-instar larvae bred in a laboratory as targets, immersing test insects in liquid medicine for 10s, taking out the test insects, placing the test insects on absorbent paper, and airing. A24-hole plate is adopted, fresh artificial feed is placed in each hole, and one end of each hole is soaked with the medicine to test insects. After the treatment, the mixture is placed in an illumination incubator at the temperature of 26 +/-1 ℃. The number of dead insects was investigated 3d after the administration.

And (3) test results: LC of 3d, 5% ciprofloxacin microemulsion after drug administration₅₀High-efficiency cyhalothrin emulsifiable concentrate LC with the value of 1.30mg/L and 25g/L₅₀The value was 9.71 mg/L). Relative toxicity of lambda-cyhalothrinThe relative virulence index of cyflumetofen is 747, counting 100.

Therefore, the 5% cyflumetofen microemulsion is considered to have extremely high activity to cotton bollworms and has obvious development and application values.

Application example 11: indoor Activity test of 0.5% bait against Blatta Seu Periplaneta

The biological activity of a laboratory-cultivated cockroach was measured using the 0.5% cyflumetofen bait obtained in formulation example 48 as a test chemical and the 0.5% dinotefuran bait as a control chemical, and the application value was evaluated.

The method comprises the following steps: a square box method. Reference is made to GB/T13917.7-2009. The experimental method comprises the steps of putting 20 test insects into each case of Periplaneta americana adults (1-2 months after eclosion) bred in a laboratory, continuously investigating for 20 days, counting the mortality rate, and counting the LT50 (median lethal time) value.

And (3) test results: 0.5% cyflumetofen bait LT₅₀0.66d, total lethal time of 4 d; 0.5% dinotefuran bait LT₅₀It was 1.38d and the total lethal time was 7 d. Therefore, the cyflumetofen bait with the concentration of 0.5 percent has excellent killing activity on the periplaneta americana and has obvious development and application values.

TABLE 9 indoor killing effect of the test agent on Periplaneta americana

Application example 12

The 10% cyclophane soluble solution prepared in the preparation example 16 is used as a test medicament, and 97% cyclophane technical grade is used as a control medicament, so that the indoor activity of the preparation and the technical grade on chilo suppressalis is tested.

The method comprises the following steps: soaking rice stem. The key links from insect testing, liquid medicine preparation, treatment mode, investigation and the like are described as follows. Testing insects: chilo suppressalis is collected from Changsha fields in Hunan in 8 months in 2018, and the test insects are F bred for indoor generations₉And 3, generation of 3-instar larvae. Preparing a liquid medicine: 10mg of the original drug (in hundred percent) is weighed and dissolved by 1mL of DMF to prepare 10000ppm mother liquor. Taking 1mL of mother liquor, adding 0.05% Tween80 to 100g of water to obtain 100ppm of liquid medicine. Weighing 100mg of the preparation and adding clear water to 100g to prepare 100ppm of liquid medicine of 10 percent cyflumetofen SL. Diluting in turn according to dosage design to obtain the required liquid medicine. Thirdly, the method for treating the test insects by the medicament comprises the following steps: pouring the liquid medicine into a culture dish (the liquid medicine amount is 40mL) for each treatment, soaking the rice stems into the liquid medicine for 10s, taking out, and placing in a shade for airing. The bottom of the glass finger-shaped pipe is provided with a moisturizing cotton ball, 7 treated rice stems are placed in each pipe, 10 larvae are connected, each treatment is repeated for 3 times, the pipe orifice is sealed by cotton black cloth, a rubber band is tightly tied, the pipe is placed in an illumination incubator for cultivation, the temperature in the illumination incubator is 26.9-27.5 ℃, the relative humidity is 69.0-100%, and the darkness lasts. Fourthly, investigating time and method: the reaction symptoms and the number of dead insects of chilo suppressalis were investigated 3 days after the drug administration. The death is judged by the incapability of coordinated movement of the polypide.

The results show that: indoor toxicity LC of 10% soluble solution of cyflumetofen to chilo suppressalis₅₀Indoor toxicity LC of 97% cyclopropanamide technical to Chilo suppressalis with value of 0.2619mg/L₅₀The value is 0.6855mg/L, and the relative virulence index of the preparation is 2.61 times that of the original drug.

The applicant states that the invention is illustrated by the above examples to the insecticide containing cyflumetofen and the application thereof, but the invention is not limited to the above examples, that is, the invention is not limited to the above examples. It should be understood by those skilled in the art that any modification of the present invention, equivalent substitutions of the raw materials of the product of the present invention, addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.