阅读说明：本技术 一种环保型植物染料配方及调配方法 (Environment-friendly plant dye formula and blending method ) 是由 周佰康 于 2021-01-07 设计创作，主要内容包括：本发明公开了一种环保型植物染料配方及调配方法,具体调配方法步骤如下：步骤一：生产技术负责人编制环保型植物染料配方及调配方法的专项方案,并且编制针对性的应急预案,生产前对生产负责人和工作人员进行技术交底工作；步骤二：将称取的薰衣草花和凤仙花花瓣投入到超声波清洗机内,加入清水和碳酸钠溶液进行超声波清洗,在暖空气中快速吹干,去除基体表面的污垢杂质,并且置于柠檬酸溶液中浸泡4-6h；步骤三：烘干后然后研磨制粉,再通过超高温瞬时灭菌处理,后冷却至35-55℃得到粗料。本发明生产出来的染料环保性高,节能效果好、无毒无害等优点。在我国纺织节能应用领域具有极大的市场空间和发展前景。(The invention discloses an environment-friendly plant dye formula and a blending method, wherein the blending method comprises the following steps: the method comprises the following steps: the production technical responsible person compiles a special scheme of the environment-friendly plant dye formula and the blending method, compiles a specific emergency plan, and carries out technical interaction work on the production responsible person and workers before production; step two: putting the weighed lavender flower and balsamine flower petals into an ultrasonic cleaning machine, adding clear water and a sodium carbonate solution for ultrasonic cleaning, quickly drying in warm air to remove dirt and impurities on the surface of a substrate, and soaking in a citric acid solution for 4-6 h; step three: drying, grinding into powder, performing ultrahigh temperature instantaneous sterilization, and cooling to 35-55 deg.C to obtain coarse material. The dye produced by the invention has the advantages of high environmental protection, good energy-saving effect, no toxicity, no harm and the like. Has great market space and development prospect in the textile energy-saving application field of China.)

1. An environment-friendly plant dye formula and a blending method are characterized by comprising the following materials in parts by weight:

weighing 23.5-24.7 parts of clean water, 22-24.2 parts of accelerating agent, 2-5 parts of essential oil additive, 6.7-10.2 parts of aluminum sulfate octadecahydrate aqueous solution, 2.8-5.2 parts of methyl salicylate, 10-10.9 parts of n-hexanol, 5.4-7.6 parts of butyl methylbutyrate, 4.1-4.6 parts of leveling agent and 5.4-7.6 parts of modified graphene oxide;

the specific blending method comprises the following steps:

the method comprises the following steps: the production technical responsible person compiles a special scheme of the environment-friendly plant dye formula and the blending method, compiles a specific emergency plan, and carries out technical interaction work on the production responsible person and workers before production;

step two: putting the weighed lavender flower and balsamine flower petals into an ultrasonic cleaning machine, adding clear water and a sodium carbonate solution for ultrasonic cleaning, quickly drying in warm air to remove dirt and impurities on the surface of a substrate, and soaking in a citric acid solution for 4-6 h;

step three: drying, grinding into powder, performing ultrahigh temperature instantaneous sterilization, cooling to 35-55 deg.C to obtain coarse material, adding the coarse material and extractive solution into a reaction kettle, heating with an electric heater, stirring, condensing to obtain effective substances, and centrifuging with a centrifuge to obtain essential oil additive extracted from natural plants;

step four: weighing clean water, an accelerating agent, an essential oil additive, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate, a leveling agent and modified graphene oxide in corresponding parts by weight for later use;

step five: adding clean water, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate and modified graphene oxide into a reaction kettle together, and fully reacting to form a first mixed solution;

step six: continuously adding an accelerating agent, an essential oil additive and a leveling agent into the first mixed solution to fully react and form a second mixed solution;

step seven: and naturally cooling the second mixed solution to obtain the environment-friendly plant dye.

2. The formulation and blending method of claim 1, wherein the formulation comprises: the accelerating agent is glacial acetic acid, and the leveling agent comprises at least one of fatty alcohol, triethanolamine, toluene or octadecyl isocyanate.

3. The formulation and blending method of claim 1, wherein the formulation comprises: and the concentration of the sodium carbonate solution in the second step is 0.1-0.5 g/ml.

4. The formulation and blending method of claim 1, wherein the formulation comprises: and uniformly mixing the materials in the fifth step and the sixth step by using an electric stirrer, wherein the stirring speed is 125-.

5. The formulation and blending method of claim 1, wherein the formulation comprises: in the fifth step and the sixth step, the mixed solution is heated in the mixing process, and the heating temperature is 70-85 ℃.

6. The formulation and blending method of claim 1, wherein the formulation comprises: in the first step, the data of the transaction should be signed by both parties and then recorded.

7. The formulation and blending method of claim 1, wherein the formulation comprises: the temperature of the ultrahigh temperature instant sterilization treatment in the third step is 135-155 ℃.

8. The formulation and blending method of claim 1, wherein the formulation comprises: the temperature of the drying warm air in the second step is 45-55 ℃.

Technical Field

The invention belongs to the technical field of dye preparation, and particularly relates to an environment-friendly plant dye formula and a blending method.

Background

The dye can improve the level dyeing property, the dyeing fastness and other dyeing properties of the dye by compounding. When dyes are compounded, dyes with similar structures are easy to compound, and dyes with far structures can be complemented, so that the compounding of the dyes needs to screen the dyes with similar structures according to the structural characteristics of the dyes, for example, the interaction between the dyes can be enhanced, particularly, the synergistic effect generated by the interaction on fibers can greatly improve the fixation rate of the dyes and achieve the effects of deepening and brightening, and the method is a clean and environment-friendly production technology and is suitable for the current market demands of low pollution and low cost. However, the existing dye formula and blending method are poor in environmental protection property and cannot achieve the effect of energy conservation, and the dye does not have plant fragrance and cannot achieve the effects of sunlight resistance and water washing resistance.

Disclosure of Invention

The invention aims to provide an environment-friendly plant dye formula and a blending method, and aims to solve the problems that the existing dye formula and blending method proposed in the background technology are poor in environment-friendliness and cannot achieve the energy-saving effect, and the dye does not have plant fragrance and cannot resist sunlight and water washing.

In order to achieve the purpose, the invention provides the following technical scheme: an environment-friendly plant dye formula and a blending method thereof comprise the following materials in parts by weight:

weighing 23.5-24.7 parts of clean water, 22-24.2 parts of accelerating agent, 2-5 parts of essential oil additive, 6.7-10.2 parts of aluminum sulfate octadecahydrate aqueous solution, 2.8-5.2 parts of methyl salicylate, 10-10.9 parts of n-hexanol, 5.4-7.6 parts of butyl methylbutyrate, 4.1-4.6 parts of leveling agent and 5.4-7.6 parts of modified graphene oxide;

the specific blending method comprises the following steps:

the method comprises the following steps: the production technical responsible person compiles a special scheme of the environment-friendly plant dye formula and the blending method, compiles a specific emergency plan, and carries out technical interaction work on the production responsible person and workers before production;

step two: putting the weighed lavender flower and balsamine flower petals into an ultrasonic cleaning machine, adding clear water and a sodium carbonate solution for ultrasonic cleaning, quickly drying in warm air to remove dirt and impurities on the surface of a substrate, and soaking in a citric acid solution for 4-6 h;

step three: drying, grinding into powder, performing ultrahigh temperature instantaneous sterilization, cooling to 35-55 deg.C to obtain coarse material, adding the coarse material and extractive solution into a reaction kettle, heating with an electric heater, stirring, condensing to obtain effective substances, and centrifuging with a centrifuge to obtain essential oil additive extracted from natural plants;

step four: weighing clean water, an accelerating agent, an essential oil additive, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate, a leveling agent and modified graphene oxide in corresponding parts by weight for later use;

step five: adding clean water, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate and modified graphene oxide into a reaction kettle together, and fully reacting to form a first mixed solution;

step six: continuously adding an accelerating agent, an essential oil additive and a leveling agent into the first mixed solution to fully react and form a second mixed solution;

step seven: and naturally cooling the second mixed solution to obtain the environment-friendly plant dye.

Further, the accelerating agent is glacial acetic acid, and the leveling agent comprises at least one of fatty alcohol, triethanolamine, toluene or octadecyl isocyanate.

Further, the concentration of the sodium carbonate solution in the second step is 0.1-0.5 g/ml.

Further, the step five and the step six are uniformly mixed by an electric stirrer, and the stirring speed is 125-135 r/min.

Further, the mixed solution is heated in the mixing process in the fifth step and the sixth step, and the heating temperature is 70-85 ℃.

Furthermore, the data of the transaction in the first step should be signed by both parties and then recorded and saved.

Further, the temperature of the ultrahigh temperature instant sterilization treatment in the third step is 135-.

Further, the temperature of the drying warm air in the second step is 45-55 ℃.

Compared with the prior art, the invention has the beneficial effects that:

1. according to the invention, the modified graphene oxide is added in the dye formula, so that the prepared fiber textile has a good antistatic effect. Secondly, because the spatial structure of the graphene oxide, the coloring agent in the ingredients can be effectively retained on the fiber cloth, the coloring capability of the cloth is enhanced, and the color of the textile is more gorgeous. Meanwhile, the dyeing process can be rapidly carried out by adding the leveling agent and the accelerating agent to enhance the halation performance and the dyeing rate of the dye, and the diffusivity of the dye is improved to a certain extent, so that the dye has the advantages of sunlight resistance and water washing resistance.

2. Technical personnel compile specific operation scheme and pay attention to the details, and carry out the technological conflict to the staff, make the deployment method go on smoothly, when running into the problem, be convenient for the pertinence solution, save manpower and materials, put lavender flower and impatiens balsamina petal of weighing into ultrasonic cleaner, avoid losing the active ingredient of plant when wasing, the protection effect is showing, and add sodium carbonate solution and carry out ultrasonic cleaning, decontamination effect is more thorough, shorten the cleaning time, add lavender flower, impatiens balsamina petal in the formulation and make the essential oil additive who makes distribute the pleasing fragrance of plant, make the dyestuff fragrance strong and lasting, make people's heart clear and fresh and comfortable, the mood is happy, added several noble and graceful.

3. The dye produced by the invention has the advantages of high environmental protection, good energy-saving effect, no toxicity, no harm and the like. Has great market space and development prospect in the textile energy-saving application field of China.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1

An environment-friendly plant dye formula and a blending method thereof comprise the following materials in parts by weight:

weighing 23.5 parts by weight of clean water, 22 parts by weight of an accelerating agent, 2 parts by weight of an essential oil additive, 6.7 parts by weight of an aluminum sulfate octadecahydrate aqueous solution, 2.8 parts by weight of methyl salicylate, 10 parts by weight of n-hexanol, 5.4 parts by weight of butyl methylbutyrate, 4.1 parts by weight of a leveling agent and 5.4 parts by weight of modified graphene oxide;

the specific blending method comprises the following steps:

the method comprises the following steps: the production technical responsible person compiles a special scheme of the environment-friendly plant dye formula and the blending method, compiles a specific emergency plan, and carries out technical interaction work on the production responsible person and workers before production;

step two: putting the weighed lavender flower and balsamine flower petals into an ultrasonic cleaning machine, adding clear water and a sodium carbonate solution for ultrasonic cleaning, quickly drying in warm air to remove dirt and impurities on the surface of a substrate, and soaking in a citric acid solution for 4-6 h;

step three: drying, grinding into powder, performing ultrahigh temperature instantaneous sterilization, cooling to 35-55 deg.C to obtain coarse material, adding the coarse material and extractive solution into a reaction kettle, heating with an electric heater, stirring, condensing to obtain effective substances, and centrifuging with a centrifuge to obtain essential oil additive extracted from natural plants;

step four: weighing clean water, an accelerating agent, an essential oil additive, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate, a leveling agent and modified graphene oxide in corresponding parts by weight for later use;

step five: adding clean water, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate and modified graphene oxide into a reaction kettle together, and fully reacting to form a first mixed solution;

step six: continuously adding an accelerating agent, an essential oil additive and a leveling agent into the first mixed solution to fully react and form a second mixed solution;

step seven: and naturally cooling the second mixed solution to obtain the environment-friendly plant dye.

The accelerating agent is glacial acetic acid, and the leveling agent comprises at least one of fatty alcohol, triethanolamine, toluene or octadecyl isocyanate.

Wherein, the concentration of the sodium carbonate solution in the second step is 0.1-0.5 g/ml.

Wherein, the step five and the step six are uniformly mixed by an electric stirrer, and the stirring speed is 125-135 r/min.

Wherein, the mixed solution is heated in the mixing process in the fifth step and the sixth step, and the heating temperature is 70-85 ℃.

Wherein, the data of the first transaction should be signed by both parties and then recorded.

Wherein the temperature of the ultrahigh temperature instant sterilization treatment in the third step is 135-.

Wherein the temperature of the drying warm air in the second step is 45-55 ℃.

Example 2

An environment-friendly plant dye formula and a blending method thereof comprise the following materials in parts by weight:

weighing 24.7 parts by weight of clean water, 24.2 parts by weight of an accelerating agent, 5 parts by weight of an essential oil additive, 10.2 parts by weight of an aluminum sulfate octadecahydrate aqueous solution, 5.2 parts by weight of methyl salicylate, 10.9 parts by weight of n-hexanol, 7.6 parts by weight of butyl methylbutyrate, 4.6 parts by weight of a leveling agent and 7.6 parts by weight of modified graphene oxide;

the specific blending method comprises the following steps:

the method comprises the following steps: the production technical responsible person compiles a special scheme of the environment-friendly plant dye formula and the blending method, compiles a specific emergency plan, and carries out technical interaction work on the production responsible person and workers before production;

step two: putting the weighed lavender flower and balsamine flower petals into an ultrasonic cleaning machine, adding clear water and a sodium carbonate solution for ultrasonic cleaning, quickly drying in warm air to remove dirt and impurities on the surface of a substrate, and soaking in a citric acid solution for 4-6 h;

step three: drying, grinding into powder, performing ultrahigh temperature instantaneous sterilization, cooling to 35-55 deg.C to obtain coarse material, adding the coarse material and extractive solution into a reaction kettle, heating with an electric heater, stirring, condensing to obtain effective substances, and centrifuging with a centrifuge to obtain essential oil additive extracted from natural plants;

step four: weighing clean water, an accelerating agent, an essential oil additive, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate, a leveling agent and modified graphene oxide in corresponding parts by weight for later use;

step five: adding clean water, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate and modified graphene oxide into a reaction kettle together, and fully reacting to form a first mixed solution;

step six: continuously adding an accelerating agent, an essential oil additive and a leveling agent into the first mixed solution to fully react and form a second mixed solution;

step seven: and naturally cooling the second mixed solution to obtain the environment-friendly plant dye.

The accelerating agent is glacial acetic acid, and the leveling agent comprises at least one of fatty alcohol, triethanolamine, toluene or octadecyl isocyanate.

Wherein, the concentration of the sodium carbonate solution in the second step is 0.1-0.5 g/ml.

Wherein, the step five and the step six are uniformly mixed by an electric stirrer, and the stirring speed is 125-135 r/min.

Wherein, the mixed solution is heated in the mixing process in the fifth step and the sixth step, and the heating temperature is 70-85 ℃.

Wherein, the data of the first transaction should be signed by both parties and then recorded.

Wherein the temperature of the ultrahigh temperature instant sterilization treatment in the third step is 135-.

Wherein the temperature of the drying warm air in the second step is 45-55 ℃.

Example 3

An environment-friendly plant dye formula and a blending method thereof comprise the following materials in parts by weight:

weighing 24.1 parts by weight of clean water, 23.1 parts by weight of an accelerating agent, 3.5 parts by weight of an essential oil additive, 8.45 parts by weight of an aluminum sulfate octadecahydrate aqueous solution, 4 parts by weight of methyl salicylate, 10.45 parts by weight of n-hexanol, 6.5 parts by weight of butyl methylbutyrate, 4.35 parts by weight of a leveling agent and 6.5 parts by weight of modified graphene oxide;

the specific blending method comprises the following steps:

the method comprises the following steps: the production technical responsible person compiles a special scheme of the environment-friendly plant dye formula and the blending method, compiles a specific emergency plan, and carries out technical interaction work on the production responsible person and workers before production;

step two: putting the weighed lavender flower and balsamine flower petals into an ultrasonic cleaning machine, adding clear water and a sodium carbonate solution for ultrasonic cleaning, quickly drying in warm air to remove dirt and impurities on the surface of a substrate, and soaking in a citric acid solution for 4-6 h;

step three: drying, grinding into powder, performing ultrahigh temperature instantaneous sterilization, cooling to 35-55 deg.C to obtain coarse material, adding the coarse material and extractive solution into a reaction kettle, heating with an electric heater, stirring, condensing to obtain effective substances, and centrifuging with a centrifuge to obtain essential oil additive extracted from natural plants;

step four: weighing clean water, an accelerating agent, an essential oil additive, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate, a leveling agent and modified graphene oxide in corresponding parts by weight for later use;

step five: adding clean water, an aluminum sulfate octadecahydrate aqueous solution, methyl salicylate, n-hexanol, butyl methylbutyrate and modified graphene oxide into a reaction kettle together, and fully reacting to form a first mixed solution;

step six: continuously adding an accelerating agent, an essential oil additive and a leveling agent into the first mixed solution to fully react and form a second mixed solution;

step seven: and naturally cooling the second mixed solution to obtain the environment-friendly plant dye.

The accelerating agent is glacial acetic acid, and the leveling agent comprises at least one of fatty alcohol, triethanolamine, toluene or octadecyl isocyanate.

Wherein, the concentration of the sodium carbonate solution in the second step is 0.1-0.5 g/ml.

Wherein, the step five and the step six are uniformly mixed by an electric stirrer, and the stirring speed is 125-135 r/min.

Wherein, the mixed solution is heated in the mixing process in the fifth step and the sixth step, and the heating temperature is 70-85 ℃.

Wherein, the data of the first transaction should be signed by both parties and then recorded.

Wherein the temperature of the ultrahigh temperature instant sterilization treatment in the third step is 135-.

Wherein the temperature of the drying warm air in the second step is 45-55 ℃.

The working effect of the invention is as follows: the carbon fiber and the glass fiber are added into the formula, so that the compression strength and the crack resistance of the porous brick are improved, the production period is short, the large-scale industrial production is facilitated, the supporting plate is placed below the porous brick mould, the concrete brick mould is filled with the mixture, the pressing die is lowered, the porous brick mould is pressed, the production efficiency is high, the precision is high, and the product quality is improved. Shale powder and graded gravel are used as aggregates to play a role of skeleton support in the mixture, the strength of the brick body is improved, the foaming agent is azodicarbonamide and has a good foaming effect, the porosity is as high as 30%, the weight of the brick body is reduced, the sludge has certain viscosity and small granularity, part of kaolin clay is replaced by the sludge, the strength of the porous brick can be improved, meanwhile, spiral stirring is used in the stirring process, the viscosity of the blank is increased, the strength of the porous brick is also improved, and the sound insulation and heat insulation effects of the prepared porous brick are also better. The foamed brick produced by the invention has the advantages of excellent heat preservation and insulation properties, sound insulation effect, high strength, good impact resistance, difficult water absorption, light weight, pressure resistance, good weather resistance, environmental protection, energy conservation, no toxicity, no harm and the like. Has great market space and development prospect in the application field of building energy conservation in China.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.