阅读说明：本技术 一种无毒鼠药硅酸盐水泥梗阻剂及制备方法 (Nontoxic rodenticide portland cement stemming agent and preparation method thereof ) 是由 单承仪 于 2021-08-27 设计创作，主要内容包括：一种无毒鼠药硅酸盐水泥梗阻剂及制备方法,无毒鼠药硅酸盐水泥梗阻剂由石蜡、硅酸盐水泥、水泥速凝剂、粘合剂、杨梅、大叶冬青、石榴、粮食、引诱剂、防腐剂组成,制备方法是,通过加热将石蜡制成蜡液,将杨梅、大叶冬青、石榴烘干粉碎,制成干粉,再将蜡液、硅酸盐水泥水泥、杨梅干粉、大叶冬青干粉、石榴干粉、水泥速凝剂、粘合剂、粮食、引诱剂、防腐剂按配方比例进行混合搅拌均匀后,装入成型设备压制成无毒鼠药硅酸盐水泥梗阻剂。该发明实现对生态环境的无危害性,杨梅、大叶冬青、石榴等成分为天然物质,在自然环境中易发霉变质,对人类、家禽家畜安全无害,且灭鼠效率高,效果明显,应用于鼠类药物防治技术领域中。(A non-toxic silicate cement inhibitor for mouse is prepared from paraffin wax, silicate cement, cement accelerator, adhesive, red bayberry, ilex latifolia thumb, pomegranate, grain, attractant and antiseptic through heating paraffin wax to obtain wax liquid, baking red bayberry, ilex latifolia thumb and pomegranate, pulverizing, drying, stirring, and die pressing. The invention realizes no harm to ecological environment, the components of waxberry, ilex latifolia, pomegranate and the like are natural substances, the waxberry, ilex latifolia and pomegranate are easy to go mouldy and deteriorate in natural environment, the raticide is safe and harmless to human beings, poultry and livestock, the deratization efficiency is high, the effect is obvious, and the raticide is applied to the technical field of rodent drug control.)

1. A nontoxic rodenticide portland cement stemming agent is characterized in that: the nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight: 350 parts of paraffin wax, 50-300 parts of Portland cement, 1-15 parts of cement accelerator, 50 parts of adhesive, 1-10 parts of waxberry, 1-10 parts of ilex latifolia, 1-10 parts of pomegranate, 650 parts of grain, 3 parts of attractant and 2 parts of preservative.

2. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 300 parts of paraffin, 235 parts of Portland cement, 5 parts of cement accelerator, 50 parts of adhesive, 5 parts of waxberry, 5 parts of ilex latifolia, 5 parts of pomegranate, 390 parts of grain, 3 parts of attractant and 2 parts of preservative.

3. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 250 parts of paraffin, 210 parts of Portland cement, 6 parts of cement accelerator, 50 parts of adhesive, 5 parts of waxberry, 5 parts of ilex latifolia, 4 parts of pomegranate, 465 parts of grain, 3 parts of attractant and 2 parts of preservative.

4. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 285 parts of paraffin, 150 parts of Portland cement, 7 parts of cement accelerator, 50 parts of adhesive, 4 parts of waxberry, 4 parts of ilex latifolia, 5 parts of pomegranate, 490 parts of grain, 3 parts of attractant and 2 parts of preservative.

5. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the adhesive is aquatic product adhesive, and plays a role in shaping under the combined action of the aquatic product adhesive and paraffin.

6. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the preservative is edible preservative calcium propionate, the dosage of the preservative is not more than 1.8g/kg of national standard grain dosage, and the preservative is safe and environment-friendly.

7. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the cement coagulant has the functions of shortening the cement setting time, accelerating the cement curing and enhancing the effect.

8. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the waxberry, the broadleaf holly and the pomegranate are all food materials, and are safe, non-toxic and pollution-free.

9. The method for preparing the non-toxic raticide portland cement stemming agent according to claim 1, is characterized in that: the preparation method of the nontoxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the ilex latifolia thumb and the pomegranates to prepare dry powder, mixing and stirring the wax liquid, the portland cement, the waxberry dry powder, the ilex latifolia dry powder, the pomegranate dry powder, the cement accelerator, the adhesive, the grain, the attractant and the preservative uniformly according to a formula ratio, and then filling the mixture into forming equipment to press the nontoxic rodenticide portland cement stem resistance agent.

10. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the non-toxic rodenticide portland cement stemming agent has the action mechanism that the non-toxic rodenticide portland cement stemming agent is a rodenticide which is developed specially aiming at the characteristics of rat intestinal tracts, and the rat intestinal tracts are characterized by small intestinal diameter, long intestinal tract and bent intestinal tract, so that the non-toxic rodenticide portland cement stemming agent is suitable for acting on drugs with obstruction, and obstruction can be formed even if small agglomerates are formed; in order to absorb food nutrition to the maximum extent in the long-term evolution of the rats, the intestinal tract proportion is higher in mammals, and long-term food in the intestinal tract is retained in the intestinal tract for a longer time, so that intestinal obstruction is favorably formed; the intestinal bending is also beneficial to the formation condition of obstruction; on the other hand, according to physiological anatomy observation, food in the rat intestinal tract starts to gather before the middle section to form a feces particle embryonic form, and gathering generated by pushing and extruding effects in the intestinal tract just conforms to the action mechanism of a silicate intestinal tract obstruction agent, so that the success rate of obstruction formation is enhanced, and the effect of intestinal tract obstruction is improved; the waxberry, the ilex latifolia and the pomegranate have astringent and astringent effects on the mouse intestinal tract, wherein the waxberry contains a large amount of organic acid components, so that the waxberry has a strong intestine astringing effect when eaten, can inhibit intestinal peristalsis and obstruct excretion, and portland cement is gathered, precipitated, coagulated and solidified in the mouse intestinal tract, is difficult to digest and absorb to form lumps to cause intestinal tract obstruction, so that metabolic disorders of various systems are generated due to intestinal obstruction, and the death is finally caused by organ failure; rats after intestinal obstruction are slow in action and reduced in activity before death, do not eat or eat a little, and have little or no defecation; intestinal obstruction suppressants, also known as econontoxic rodenticides, are physically responsible for death as distinguished from death due to poisoning caused by organic chemicals.

11. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the experimental method for indoor non-selective feeding of the non-toxic raticide, namely the portland cement stemming agent, is carried out under the laboratory condition, and silicate obstruction agents are used for feeding test rats for 7 days respectively; the test rats are divided into 3 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of silicate stemming agent (accurately measured) is placed on the opposite angle in a cage for the white mouse to take; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the average death time of the test mice is 6.4 days, the dead mice are dissected, and the death cause intestinal stalk blockage rate is 90 percent and the death rate is 100 percent.

12. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the experimental method for indoor non-selective ingestion of the non-toxic rodenticide portland cement blocking agent is characterized in that the silicate blocking agent is used for feeding a test rat for 5 days; the test rats are divided into 4 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic raticide portland cement stemming agent and a bait box containing 20-50 g of maintenance feed are respectively arranged at opposite corners in a cage for a white rat to eat, the amount of the residual bait (the bait and the maintenance feed) is accurately weighed every day, a new bait and the maintenance feed are replaced, and the positions of the bait box and the bait box are changed; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the average death time of the test mice is 6.6 days, the dead mice are dissected, and the death cause intestinal stalk blockage rate is found to be 90%, the average ingestion coefficient is 0.31, and the death rate is 90%.

13. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the non-toxic raticideThe experimental method of the Portland cement stem-drag agent field is that the experimental sites are arranged in the forest seed station in the northeast region, and the prevention and control objects are as follows: the forest culture medium comprises palm back flat, hypsizigus marmoreus, oriental voles and hypsizigus nigra, wherein crops are forests (secondary forests and artificial forests), and forest seeds are larch young forests, pinus sylvestris young forests, birch middle-aged forests and natural secondary forests; the silicate intestinal obstruction agent has the application dosage of 3kg/hm²、4kg/hm²The test adopts the mode of applying drugs with the pile pitch of 5 m and the line pitch of 15 m (5 m multiplied by 10 m), and the method of applying drugs to the whole environment of poison baits; the control effects of larch young forests and natural secondary forests with high concentration (4 kg) are both 100 percent; the control effects of the larch young forest and the natural secondary forest at low concentration (3 kg) are 84.98 percent and 79.64 percent respectively.

14. The non-toxic rodenticide portland cement blocking agent according to claim 1, characterized in that: the experimental method for the indoor drug effect comparison of the non-toxic rodenticide portland cement blocking agent is carried out under laboratory conditions, and the non-toxic rodenticide portland cement blocking agent and the ordinary calcium silicate non-toxic bait agent are respectively used for feeding a test rat for 7 days; the test rats are divided into 2 groups, each group comprises 20 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic rodenticide portland cement blocking agent (accurately measured) is placed on the opposite corners in a cage for the mice to eat; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the experimental result shows that the death time of the nontoxic rodenticide portland cement stemming agent group is 5-8 days, the average death time is 6 days, the dead mice are depalletized, the death factor intestinal stalk resistance rate is found to be 90%, and the death rate is 100%; the common calcium silicate non-toxic bait has the mortality rate of about 70 percent, the death time of 10 to 13 days and the average value of 11.4 days, the dead rats are removed, the obstruction rate is 40 percent, other dead rats show internal bleeding, and the effect is far less obvious than that of a non-toxic raticide, namely, a silicate cement stemming agent.

Technical Field

The invention relates to a non-toxic raticide portland cement stemming agent and a preparation method thereof, belonging to the technical field of rodent drug control.

Background

In the world, rat diseases have great negative influence on human production and life, so that the agricultural yield is reduced, a large amount of agricultural and sideline products are consumed, the ecological systems such as forestry, grassland and the like are seriously threatened, industrial and water conservancy facilities are damaged and consumed, diseases are infected, the environment is polluted, and the health and life safety of human beings are threatened, so that the control of the number of the rat populations is a long-term task required to face all over the world. However, the application of various raticides has many problems, the most popular raticides are the highly toxic raticides, the raticides have high toxicity, the problem of chemical three-waste emission exists in the production process, great pressure is caused to the environment and the ecology, and the reports of poisoning caused by mistaken eating of the raticides by people or animals and death of the mice are more rare. Aiming at the problems, the invention aims to develop a novel non-toxic raticide, which achieves the deratization effect without depending on a high-toxicity chemical raticide, and is more favorable for protecting the ecological environment and ensuring the safety of human beings.

The patent No. 202010184988.7 discloses a nontoxic deratization bait-V type and a preparation method thereof, the difference between the patent application and the patent is that the invention increases the intestine astringing effect of plants, and compared with the nontoxic deratization bait-V type and the preparation method, the invention increases the deratization effect.

However, in the prior art, various raticides have many problems in application, the mainstream raticide is mainly virulent, the raticide has high toxicity, the problem of discharge of three chemical wastes exists in the production process, great pressure is caused to the environment and the ecology, and the reports of poisoning caused by mistaken eating of the raticide by human beings or animals and death of the mice are more frequent. Therefore, the development of a nontoxic rodenticide portland cement retarder and a preparation method thereof are still new problems to be solved urgently.

Disclosure of Invention

The invention aims to provide a nontoxic rodenticide portland cement stemming agent and a preparation method thereof, wherein waxberry, ilex latifolia and pomegranate are used for producing intestine astringing and astringing effects on murine intestinal tracts, wherein the waxberry contains a large amount of organic acid components, has a strong intestine astringing effect when being eaten, inhibits the murine intestinal tract peristalsis and hinders excretion, portland cement is subjected to water absorption precipitation and solidification in the murine intestinal tracts, a cement accelerator can accelerate the coagulation speed of the portland cement, and formed solid particles fully fill the murine intestinal tracts to cause intestinal obstruction, so that rats can not eat food, substances in the intestinal tracts can not be discharged, and finally the death time is accelerated.

The purpose of the invention is realized as follows: the non-toxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight: 350 parts of paraffin wax, 50-300 parts of Portland cement, 1-15 parts of cement accelerator, 50 parts of adhesive, 1-10 parts of waxberry, 1-10 parts of ilex latifolia, 1-10 parts of pomegranate, 650 parts of grain, 3 parts of attractant and 2 parts of preservative;

the nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 300 parts of paraffin, 235 parts of Portland cement, 5 parts of cement accelerator, 50 parts of adhesive, 5 parts of waxberry, 5 parts of ilex latifolia, 5 parts of pomegranate, 390 parts of grain, 3 parts of attractant and 2 parts of preservative;

the nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 250 parts of paraffin, 210 parts of Portland cement, 6 parts of cement accelerator, 50 parts of adhesive, 5 parts of waxberry, 5 parts of ilex latifolia, 4 parts of pomegranate, 465 parts of grain, 3 parts of attractant and 2 parts of preservative;

the nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 285 parts of paraffin, 150 parts of Portland cement, 7 parts of cement accelerator, 50 parts of adhesive, 4 parts of waxberry, 4 parts of ilex latifolia, 5 parts of pomegranate, 490 parts of grain, 3 parts of attractant and 2 parts of preservative;

the adhesive is aquatic product adhesive, and plays a role in shaping under the combined action of the aquatic product adhesive and paraffin;

the preservative is edible preservative calcium propionate, the dosage of the preservative does not exceed 1.8g/kg of the dosage of national standard grain, and the preservative is safe and environment-friendly;

the cement coagulant has the effects of shortening the cement solidification time, accelerating the cement solidification and realizing synergism;

the waxberry, the broadleaf holly and the pomegranate are all food materials, and are safe, non-toxic and pollution-free;

the preparation method of the nontoxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the ilex latifolia thumb and the pomegranates to prepare dry powder, mixing and stirring the wax liquid, the portland cement, the waxberry dry powder, the ilex latifolia dry powder, the pomegranate dry powder, the cement accelerator, the adhesive, the grain, the attractant and the preservative uniformly according to a formula ratio, and then filling the mixture into forming equipment to press the nontoxic rodenticide portland cement stem resistance agent;

the non-toxic rodenticide portland cement stemming agent has the action mechanism that the non-toxic rodenticide portland cement stemming agent is a rodenticide which is developed specially aiming at the characteristics of rat intestinal tracts, and the rat intestinal tracts are characterized by small intestinal diameter, long intestinal tract and bent intestinal tract, so that the non-toxic rodenticide portland cement stemming agent is suitable for acting on drugs with obstruction, and obstruction can be formed even if small agglomerates are formed; in order to absorb food nutrition to the maximum extent in the long-term evolution of the rats, the intestinal tract proportion is higher in mammals, and long-term food in the intestinal tract is retained in the intestinal tract for a longer time, so that intestinal obstruction is favorably formed; the intestinal bending is also beneficial to the formation condition of obstruction; on the other hand, according to physiological anatomy observation, food in the rat intestinal tract starts to gather before the middle section to form a feces particle embryonic form, and gathering generated by pushing and extruding effects in the intestinal tract just conforms to the action mechanism of a silicate intestinal tract obstruction agent, so that the success rate of obstruction formation is enhanced, and the effect of intestinal tract obstruction is improved; the waxberry, the ilex latifolia and the pomegranate have astringent and astringent effects on the mouse intestinal tract, wherein the waxberry contains a large amount of organic acid components, so that the waxberry has a strong intestine astringing effect when eaten, can inhibit intestinal peristalsis and obstruct excretion, and portland cement is gathered, precipitated, coagulated and solidified in the mouse intestinal tract, is difficult to digest and absorb to form lumps to cause intestinal tract obstruction, so that metabolic disorders of various systems are generated due to intestinal obstruction, and the death is finally caused by organ failure; rats after intestinal obstruction are slow in action and reduced in activity before death, do not eat or eat a little, and have little or no defecation; the intestinal tract obstruction inhibitor is also called ecological non-toxic raticide, is death caused by physical action and is different from death caused by poisoning caused by organic chemical agents;

the experimental method for indoor non-selective feeding of the non-toxic raticide, namely the portland cement stemming agent, is carried out under the laboratory condition, and silicate obstruction agents are used for feeding test rats for 7 days respectively; the test rats are divided into 3 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of silicate stemming agent (accurately measured) is placed on the opposite angle in a cage for the white mouse to take; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the death time average of the test mouse is 6.4 days, the dead mouse is dissected, and the death factor intestinal stalk blockage rate is found to be 90 percent and the death rate is 100 percent;

the experimental method for indoor non-selective ingestion of the non-toxic rodenticide portland cement blocking agent is characterized in that the silicate blocking agent is used for feeding a test rat for 5 days; the test rats are divided into 4 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic raticide portland cement stemming agent and a bait box containing 20-50 g of maintenance feed are respectively arranged at opposite corners in a cage for a white rat to eat, the amount of the residual bait (the bait and the maintenance feed) is accurately weighed every day, a new bait and the maintenance feed are replaced, and the positions of the bait box and the bait box are changed; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the death time average of the test mouse is 6.6 days, the dead mouse is dissected, the intestinal stalk resistance of the cause of death is found to be 90 percent, the average ingestion coefficient is 0.31, and the death rate is 90 percent;

the field test method of the non-toxic raticide portland cement stemming agent is characterized in that a forest seed station is arranged in a test place in northeast region, and the control objects are as follows: the forest species include young forest of larch, young forest of pinus sylvestris, middle aged forest of birch and natural secondary forest. Silicate intestinal tractThe stemming agent has the application dosage of 3kg/hm²、4kg/hm²The test adopts the mode of applying drugs with the pile pitch of 5 m and the line pitch of 15 m (5 m multiplied by 10 m), and the method of applying drugs to the whole environment of poison baits; the control effects of larch young forests and natural secondary forests with high concentration (4 kg) are both 100 percent; the control effects of the larch young forest and the natural secondary forest at low concentration (3 kg) are 84.98 percent and 79.64 percent respectively;

the experimental method for the indoor drug effect comparison of the non-toxic rodenticide portland cement blocking agent is carried out under laboratory conditions, and the non-toxic rodenticide portland cement blocking agent and the ordinary calcium silicate non-toxic bait agent are respectively used for feeding a test rat for 7 days; the test rats are divided into 2 groups, each group comprises 20 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic rodenticide portland cement blocking agent (accurately measured) is placed on the opposite corners in a cage for the mice to eat; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the experimental result shows that the death time of the nontoxic rodenticide portland cement stemming agent group is 5-8 days, the average death time is 6 days, the dead mice are depalletized, the death factor intestinal stalk resistance rate is found to be 90%, and the death rate is 100%; the common calcium silicate non-toxic bait has the mortality rate of about 70 percent, the death time of 10 to 13 days and the average value of 11.4 days, the dead rats are removed, the obstruction rate is 40 percent, other dead rats show internal bleeding, and the effect is far less obvious than that of a non-toxic raticide, namely, a silicate cement stemming agent.

The key point of the invention lies in the proportion of each component, the preparation method and the action mechanism of the nontoxic rodenticide portland cement stemming agent.

Compared with the prior art, the non-toxic rodenticide portland cement stalk resistance agent and the preparation method thereof have the advantages of no harm to the ecological environment, capability of ensuring that the appearance of the bait is not easily damaged when the bait is eroded by water due to the addition of paraffin and a bonding agent, easiness in mildew and deterioration in the natural environment due to the adoption of natural substances such as waxberries, ilex latifolia and pomegranate, no toxicity, low content of portland cement, no harm to non-target animals and natural enemies of rats, safety and no harm to human beings, poultry and livestock, low content of effective substances, high deratization efficiency, obvious effect and the like, and can be widely applied to the technical field of rat drug control.

Detailed Description

The non-toxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight: 350 parts of paraffin wax, 50-300 parts of Portland cement, 1-15 parts of cement accelerator, 50 parts of adhesive, 1-10 parts of waxberry, 1-10 parts of ilex latifolia, 1-10 parts of pomegranate, 650 parts of grain, 3 parts of attractant and 2 parts of preservative.

The nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 300 parts of paraffin, 235 parts of Portland cement, 5 parts of cement accelerator, 50 parts of adhesive, 5 parts of waxberry, 5 parts of ilex latifolia, 5 parts of pomegranate, 390 parts of grain, 3 parts of attractant and 2 parts of preservative.

The nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 250 parts of paraffin, 210 parts of Portland cement, 6 parts of cement accelerator, 50 parts of adhesive, 5 parts of waxberry, 5 parts of ilex latifolia, 4 parts of pomegranate, 465 parts of grain, 3 parts of attractant and 2 parts of preservative.

The nontoxic rodenticide portland cement blocking agent is prepared from the following components in parts by weight according to a preferred ratio: 285 parts of paraffin, 150 parts of Portland cement, 7 parts of cement accelerator, 50 parts of adhesive, 4 parts of waxberry, 4 parts of ilex latifolia, 5 parts of pomegranate, 490 parts of grain, 3 parts of attractant and 2 parts of preservative.

The adhesive is aquatic product adhesive, and plays a role in shaping under the combined action of the aquatic product adhesive and paraffin.

The preservative is edible preservative calcium propionate, the dosage of the preservative is not more than 1.8g/kg of national standard grain dosage, and the preservative is safe and environment-friendly.

The cement coagulant has the functions of shortening the cement setting time, accelerating the cement curing and enhancing the effect.

The waxberry, the broadleaf holly and the pomegranate are all food materials, and are safe, non-toxic and pollution-free.

The preparation method of the nontoxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the ilex latifolia thumb and the pomegranates to prepare dry powder, mixing and stirring the wax liquid, the portland cement, the waxberry dry powder, the ilex latifolia dry powder, the pomegranate dry powder, the cement accelerator, the adhesive, the grain, the attractant and the preservative uniformly according to a formula ratio, and then filling the mixture into forming equipment to press the nontoxic rodenticide portland cement stem resistance agent.

The non-toxic rodenticide portland cement stemming agent has the action mechanism that the non-toxic rodenticide portland cement stemming agent is a rodenticide which is developed specially aiming at the characteristics of rat intestinal tracts, and the rat intestinal tracts are characterized by small intestinal diameter, long intestinal tract and bent intestinal tract, so that the non-toxic rodenticide portland cement stemming agent is suitable for acting on drugs with obstruction, and obstruction can be formed even if small agglomerates are formed; in order to absorb food nutrition to the maximum extent in the long-term evolution of the rats, the intestinal tract proportion is higher in mammals, and long-term food in the intestinal tract is retained in the intestinal tract for a longer time, so that intestinal obstruction is favorably formed; the intestinal bending is also beneficial to the formation condition of obstruction; on the other hand, according to physiological anatomy observation, food in the rat intestinal tract starts to gather before the middle section to form a feces particle embryonic form, and gathering generated by pushing and extruding effects in the intestinal tract just conforms to the action mechanism of a silicate intestinal tract obstruction agent, so that the success rate of obstruction formation is enhanced, and the effect of intestinal tract obstruction is improved; the waxberry, the ilex latifolia and the pomegranate have astringent and astringent effects on the mouse intestinal tract, wherein the waxberry contains a large amount of organic acid components, so that the waxberry has a strong intestine astringing effect when eaten, can inhibit intestinal peristalsis and obstruct excretion, and portland cement is gathered, precipitated, coagulated and solidified in the mouse intestinal tract, is difficult to digest and absorb to form lumps to cause intestinal tract obstruction, so that metabolic disorders of various systems are generated due to intestinal obstruction, and the death is finally caused by organ failure; rats after intestinal obstruction are slow in action and reduced in activity before death, do not eat or eat a little, and have little or no defecation; intestinal obstruction suppressants, also known as econontoxic rodenticides, are physically responsible for death as distinguished from death due to poisoning caused by organic chemicals.

The experimental method for indoor non-selective feeding of the non-toxic raticide, namely the portland cement stemming agent, is carried out under the laboratory condition, and silicate obstruction agents are used for feeding test rats for 7 days respectively; the test rats are divided into 3 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of silicate stemming agent (accurately measured) is placed on the opposite angle in a cage for the white mouse to take; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the average death time of the test mice is 6.4 days, the dead mice are dissected, and the death cause intestinal stalk blockage rate is 90 percent and the death rate is 100 percent.

The experimental method for indoor non-selective ingestion of the non-toxic rodenticide portland cement blocking agent is characterized in that the silicate blocking agent is used for feeding a test rat for 5 days; the test rats are divided into 4 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic raticide portland cement stemming agent and a bait box containing 20-50 g of maintenance feed are respectively arranged at opposite corners in a cage for a white rat to eat, the amount of the residual bait (the bait and the maintenance feed) is accurately weighed every day, a new bait and the maintenance feed are replaced, and the positions of the bait box and the bait box are changed; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the average death time of the test mice is 6.6 days, the dead mice are dissected, and the death cause intestinal stalk blockage rate is found to be 90%, the average ingestion coefficient is 0.31, and the death rate is 90%.

The field test method of the non-toxic raticide portland cement stemming agent is characterized in that a forest seed station is arranged in a test place in northeast region, and the control objects are as follows: the forest culture medium comprises palm back flat, hypsizigus marmoreus, oriental voles and hypsizigus nigra, wherein crops are forests (secondary forests and artificial forests), and forest seeds are larch young forests, pinus sylvestris young forests, birch middle-aged forests and natural secondary forests; the silicate intestinal obstruction agent has the application dosage of 3kg/hm²、4kg/hm²The test adopts the mode of applying drugs with the pile pitch of 5 m and the line pitch of 15 m (5 m multiplied by 10 m), and the method of applying drugs to the whole environment of poison baits; the control effects of larch young forests and natural secondary forests with high concentration (4 kg) are both 100 percent; the control effects of the larch young forest and the natural secondary forest at low concentration (3 kg) are 84.98 percent and 79.64 percent respectively.

The experimental method for the indoor drug effect comparison of the non-toxic rodenticide portland cement blocking agent is carried out under laboratory conditions, and the non-toxic rodenticide portland cement blocking agent and the ordinary calcium silicate non-toxic bait agent are respectively used for feeding a test rat for 7 days; the test rats are divided into 2 groups, each group comprises 20 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic rodenticide portland cement blocking agent (accurately measured) is placed on the opposite corners in a cage for the mice to eat; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the experimental result shows that the death time of the nontoxic rodenticide portland cement stemming agent group is 5-8 days, the average death time is 6 days, the dead mice are depalletized, the death factor intestinal stalk resistance rate is found to be 90%, and the death rate is 100%; the common calcium silicate non-toxic bait has the mortality rate of about 70 percent, the death time of 10 to 13 days and the average value of 11.4 days, the dead rats are removed, the obstruction rate is 40 percent, other dead rats show internal bleeding, and the effect is far less obvious than that of a non-toxic raticide, namely, a silicate cement stemming agent.

Example one

The preparation method of the non-toxic rodenticide portland cement blocking agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates to prepare dry powder, mixing and stirring uniformly 300 g of the wax liquid, 235 g of portland cement, 5 g of a cement accelerator, 50 g of an adhesive, 5 g of waxberries dry powder, 5 g of broadleaf holly roots, 5 g of pomegranate dry powder, 390 g of grains, 3 g of an attractant and 2 g of a preservative, and then filling into a forming device to press the non-toxic rodenticide portland cement blocking agent.

Example two

The preparation method of the non-toxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates to prepare dry powder, mixing and stirring 250 g of the wax liquid, 210 g of portland cement, 6 g of a cement accelerator, 50 g of an adhesive, 5 g of the waxberries dry powder, 5 g of the broadleaf holly roots, 4 g of the pomegranate dry powder, 465 g of grains, 3 g of an attractant and 2 g of a preservative uniformly, and then putting the mixture into a forming device to press the non-toxic rodenticide portland cement stem resistance agent.

EXAMPLE III

The preparation method of the non-toxic rodenticide portland cement blocking agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates to prepare dry powder, mixing and stirring 285 g of the wax liquid, 150 g of portland cement, 7 g of cement accelerator, 50 g of adhesive, 4 g of waxberries dry powder, 4 g of broadleaf holly roots dry powder, 5 g of pomegranate dry powder, 490 g of grains, 3 g of attractant and 2 g of preservative uniformly, and then filling the mixture into forming equipment to press the non-toxic rodenticide portland cement blocking agent.

Example four

The preparation method of the non-toxic rodenticide portland cement blocking agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates to prepare dry powder, mixing and stirring 225 g of the wax liquid, 255 g of portland cement, 50 g of adhesive, 1 g of waxberry dry powder, 1 g of broadleaf holly root dry powder, 1 g of pomegranate dry powder, 5 g of cement accelerator, 457 g of grain, 3 g of attractant and 2 g of preservative uniformly, and then filling the mixture into forming equipment to press the non-toxic rodenticide portland cement blocking agent.

EXAMPLE five

The preparation method of the non-toxic rodenticide portland cement blocking agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates to prepare dry powder, mixing and stirring 235 g of the wax liquid, 135 g of portland cement, 50 g of an adhesive, 5 g of waxberry dry powder, 5 g of broadleaf holly roots, 5 g of pomegranate dry powder, 10 g of a cement accelerator, 550 g of grains, 3 g of an attractant and 2 g of a preservative uniformly, and then filling the mixture into forming equipment to press the non-toxic rodenticide portland cement blocking agent.

EXAMPLE six

The preparation method of the non-toxic rodenticide portland cement blocking agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the ilex latifolia thumb and the pomegranates to prepare dry powder, mixing 255 g of wax liquid paraffin, 150 g of portland cement, 50 g of adhesive, 10 g of waxberry dry powder, 10 g of ilex latifolia dry powder, 10 g of pomegranate dry powder, 6 g of cement accelerator, 504 g of grain, 3 g of attractant and 2 g of preservative, uniformly stirring, and filling into a forming device to press the non-toxic rodenticide portland cement blocking agent.

EXAMPLE seven

The preparation method of the non-toxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin wax into wax liquid by heating, drying and crushing the waxberries, the ilex latifolia thumb and the pomegranates into dry powder, mixing and stirring 245 g of the wax liquid paraffin wax, 121 g of portland cement, 50 g of an adhesive, 2 g of the waxberries dry powder, 2 g of the ilex latifolia thumb dry powder, 2 g of the pomegranate dry powder, 8g of a cement accelerator, 565 g of grain, 3 g of an attractant and 2 g of a preservative uniformly, and then filling the mixture into a forming device to press the non-toxic rodenticide portland cement stem resistance agent.

Example eight

The preparation method of the non-toxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates, mixing and stirring 200 g of the wax liquid, 230 g of portland cement, 50 g of an adhesive, 3 g of dried waxberry powder, 3 g of dried broadleaf holly root powder, 3 g of pomegranate powder, 12 g of a cement accelerator, 494 g of grains, 3 g of an attractant and 2 g of a preservative uniformly, and then filling the mixture into forming equipment to press the non-toxic rodenticide portland cement stem resistance agent.

Example nine

The preparation method of the non-toxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates, mixing and stirring 200 g of the wax liquid, 160 g of portland cement, 50 g of an adhesive, 6 g of dried waxberry powder, 6 g of dried broadleaf holly root powder, 6 g of pomegranate powder, 1 g of a cement accelerator, 566 g of grains, 3 g of an attractant and 2 g of a preservative uniformly, and then filling the mixture into forming equipment to press the non-toxic rodenticide portland cement stem resistance agent.

Example ten

The preparation method of the non-toxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates, mixing and stirring 275 g of the wax liquid, 107 g of portland cement, 50 g of an adhesive, 8g of dried waxberry powder, 8g of dried broadleaf holly roots, 8g of dried pomegranate powder, 4 g of a cement accelerator, 535 g of grains, 3 g of an attractant and 2 g of a preservative uniformly, and then filling the mixture into forming equipment to press the non-toxic rodenticide portland cement stem resistance agent.

EXAMPLE eleven

The preparation method of the non-toxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing waxberries, broadleaf holly roots and pomegranates, mixing and stirring uniformly 200 g of the wax liquid, 185 g of portland cement, 50 g of an adhesive, 9 g of dried waxberry powder, 9 g of broadleaf holly root dry powder, 9 g of pomegranate dry powder, 7 g of a cement accelerator, 522 g of grains, 3 g of an attractant and 2 g of a preservative, and then filling into a forming device to press the non-toxic rodenticide portland cement stem resistance agent.

Example twelve

The preparation method of the nontoxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates, mixing and stirring 239 g of the wax liquid, 100 g of portland cement, 50 g of adhesive, 3 g of waxberry dry powder, 3 g of broadleaf holly root dry powder, 3 g of pomegranate dry powder, 12 g of cement accelerator, 585 g of grain, 3 g of attractant and 2 g of preservative uniformly, and then filling the mixture into forming equipment to press the nontoxic rodenticide portland cement stem resistance agent.

EXAMPLE thirteen

The preparation method of the non-toxic rodenticide portland cement stem resistance agent comprises the steps of preparing paraffin into wax liquid by heating, drying and crushing the waxberries, the broadleaf holly roots and the pomegranates, mixing and stirring 289 g of the wax liquid, 120 g of portland cement, 50 g of an adhesive, 2 g of dried waxberry powder, 2 g of dried broadleaf holly roots, 2 g of pomegranate powder, 5 g of a cement accelerator, 525 g of grains, 3 g of an attractant and 2 g of a preservative uniformly, and then filling the mixture into forming equipment to press the non-toxic rodenticide portland cement stem resistance agent.

Animal experiment report one (indoor non-selective test)

The method for the indoor non-selective feeding test of the non-toxic rodenticide silicate cement blocking agent is carried out under the laboratory condition, and the silicate blocking agent is used for feeding test rats for 7 days respectively; the test rats are divided into 3 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of silicate stemming agent (accurately measured) is placed on the opposite angle in a cage for the white mouse to take; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the average death time of the test mice is 6.4 days, the dead mice are dissected, and the death cause intestinal stalk blockage rate is 90 percent and the death rate is 100 percent.

Animal experiment report two (indoor selectivity test)

The indoor selective feeding test method of the non-toxic rodenticide portland cement blocking agent comprises the steps of feeding a test rat with the silicate blocking agent for 5 days; the test rats are divided into 4 groups, each group comprises 10 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic raticide portland cement stemming agent and a bait box containing 20-50 g of maintenance feed are respectively arranged at opposite corners in a cage for a white rat to eat, the amount of the residual bait (the bait and the maintenance feed) is accurately weighed every day, a new bait and the maintenance feed are replaced, and the positions of the bait box and the bait box are changed; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the average death time of the test mice is 6.6 days, the dead mice are dissected, and the death cause intestinal stalk blockage rate is found to be 90%, the average ingestion coefficient is 0.31, and the death rate is 90%.

Animal experiment report three (field test)

The field test method of the nontoxic rodenticide portland cement stemming agent is characterized in that a forest seed station is arranged in a test place in northeast region, and the control objects are as follows: the forest species include young forest of larch, young forest of pinus sylvestris, middle aged forest of birch and natural secondary forest. The silicate intestinal obstruction agent has the application dosage of 3kg/hm²、4kg/hm²The test adopts the mode of applying drugs with the pile pitch of 5 m and the line pitch of 15 m (5 m multiplied by 10 m) and the method of applying drugs to the whole environment of poison baits. The control effects of larch young forests and natural secondary forests with high concentration (4 kg) are both 100 percent; the control effects of the larch young forest and the natural secondary forest at low concentration (3 kg) are 84.98 percent and 79.64 percent respectively.

Animal experiment report four (indoor efficacy contrast experiment, the invention and calcium silicate bait contrast experiment)

The method for the indoor efficacy contrast experiment of the non-toxic rodenticide portland cement blocking agent is carried out under laboratory conditions, and the non-toxic rodenticide portland cement blocking agent and the ordinary calcium silicate non-toxic bait agent are respectively used for feeding a test rat for 7 days; the test rats are divided into 2 groups, each group comprises 20 rats, and the rats are male and female; during feeding, a bait box containing 20-50 g of nontoxic rodenticide portland cement blocking agent (accurately measured) is placed on the opposite corners in a cage for the mice to eat; accurately weighing the residual bait amount every day and replacing new bait; after the feeding period is finished, normal feeding (single cage) is resumed, the mice are put in the feed for maintaining, and continuous observation is carried out for 10 days; the experimental result shows that the death time of the nontoxic rodenticide portland cement stemming agent group is 5-8 days, the average death time is 6 days, the dead mice are depalletized, the death factor intestinal stalk resistance rate is found to be 90%, and the death rate is 100%; the common calcium silicate non-toxic bait has the mortality rate of about 70 percent, the death time of 10 to 13 days and the average value of 11.4 days, the dead rats are removed, the obstruction rate is 40 percent, other dead rats show internal bleeding, and the effect is far less obvious than that of a non-toxic raticide, namely, a silicate cement stemming agent.